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Search results for: COUNTER-CURRENT CHROMATOGRAPHY
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Current issues of functional safety and cybersecurity analysis of the industrial and critical infrastructures
PublicationThis article addresses some functional safety assessment procedures with cybersecurity aspects in critical industrial installations with regard to the functional safety requirements specified in standards IEC 61508 and IEC 61511. The functional safety management includes hazard identification, risk analysis and assessment, specification of overall safety requirements and definition of safety functions. Based on the risk assessment...
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Effect of temperature on dark current characteristics of silicon solar cells and diodes
PublicationW artykule przedstawiono analizę wpływu zmian temperatury na ciemne charakterystyki prądowo-napięciowe ogniw fotowoltaicznych i diod z monokrystalicznego krzemu. Badania eksperymentalne przeprowadzono w zakresie temperatur od 295 do 373 K. W celu wyznaczenia wartości rezystancji szeregowej wyznaczono szereg ciemnych charakterystyk I-U. Stwierdzono, że rezystancja szeregowa rośnie wraz ze wzrostem temperatury 0,65% /K i dlatego...
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Natural sweeteners: Sources, extraction and current uses in foods and food industries
PublicationFood producers have leaned towards alternative natural and synthetic sweeteners in food formulations to satisfy market demands. Even so, several synthetic sweeteners (e.g., aspartame, saccharin, sucralose) are becoming less popular due to health-related concerns, lower nutritional values, and controversies around their safety. Conversely, natural sweeteners confer favourable customer perceptions due to their association to a healthier...
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Artificial-Hand Technology—Current State of Knowledge in Designing and Forecasting Changes
PublicationThe subject of human-hand versatility has been intensively investigated for many years. Emerging robotic constructions change continuously in order to mimic natural mechanisms as accurately as possible. Such an attitude is motivated by the demand for humanoid robots with sophisticated end effectors and highly biomimic prostheses. This paper provides wide analysis of more than 80 devices that have been created over the last 40 years....
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Application of ionic liquids in microextraction techniques: Current trends and future perspectives
PublicationIonic liquids (ILs) with their unique properties found so far numerous analytical applications. Among them ILs both in their liquid form and immobilized on the surface or within the pores of a solid support were successfully utilized in microextraction techniques. The scope of this review will cover a comprehensive summarizing of available literature data on selected properties of ILs playing a key role in analytical purposes,...
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Potential applications of crude glycerol in polymer technology–Current state and perspectives
PublicationThe increasing use of bio-based fuels and fuel additives, among them biodiesel, causes significant surplus of crude glycerol on the market which creates new challenges in terms of its sustainable utilization. A lot of ways for the incorporation of this by-product into different branches of industry requires purification by expensive and complicated processes. Therefore, researchers are seeking for applications of untreated crude...
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Calculations of Short-Circuit Current Flows in Earth Wires of HV Lines
PublicationThis paper presents a method which enables calculating flows of short-circuit currents in earth wires of high voltage transmission lines, and its implementation in the form of a computer programme. The algorithm enables performing calculations for a double-fed line and starconnected lines (three terminal lines). The developed programme enables verifying dimensioning of earth wires in the context of their short-circuit thermal withstand...
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Corporate Social Responsibility and Family Business: Current Debates and Future Prospects
PublicationThis paper aims at examining the main perspectives on corporate social responsibility (CSR) in family firms discussed in international literature. The topic of CSR has grown exponentially in the last two decades in both, business practice and as an area of interest among academics and researchers. Most studies focus on multinational corporations, some on small and medium enterprises (SMEs) and the smallest number on family business...
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On the current state of dovetail wall-corner joints in wooden Greek Catholic churches in Polish Subcarpathia with structural and sensitivity analyses
PublicationThis paper describes the current condition of some dovetail joints which form the wall corners of two Greek Catholic churches of wooden construction in Polish Subcarpathia. It also gives the historical background of the sacral architecture of that region. The two structures, which represent the same type of log corner joints are situated in Chotylub and Cewków. The buildings were examined e.g. for damage, wood moisture content,...
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IgG Avidity Test as a Tool for Discrimination between Recent and Distant Toxoplasma gondii Infection—Current Status of Studies
PublicationToxoplasma gondii, an obligate intracellular protozoan parasite, is the causative agent of one of the most prevalent zoonoses worldwide. T. gondii infection is extremely important from a medical point of view, especially for pregnant women, newborns with congenital infections, and immunocompromised individuals. Thus, an accurate and proper diagnosis of this infection is essential. Among the available diagnostic tests, serology...
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Rapid and Green Separation of Mono- and Diesters of Monochloropropanediols by Ultrahigh Performance Supercritical Fluid Chromatography–Mass Spectrometry Using Neat Carbon Dioxide as a Mobile Phase
PublicationThis study demonstrates the effect of column selectivity and density of supercritical carbon dioxide (SC-CO2) on the separation of monochloropropanediol (MCPD) esters, known as food toxicants, using SC-CO2 without addition of cosolvent in ultrahigh performance supercritical fluid chromatography–mass spectrometry (UHPSFC-MS). This study shows that over 20 2-monochloropropanediol (2-MCPD) and 3-monochloropropanediol (3-MCPD) mono-...
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Solid phase microextraction–comprehensive twodimensional gas chromatography–time-of-flight mass spectrometry: a new tool for determining PAHs in airport runoff water samples
Publicationfundamental aspect of airport operations is the pollution caused by airport runoff waters. Polycyclic aromatic hydrocarbons (PAHs) are one of the most important groups of xenobiotics which are commonly found in runoff water originating from airports. Only very limited data on the analysis of airport runoff water have been published until now. Therefore, a reliable and accurate analytical method based on headspace solid-phase microextraction...
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Dispersive liquid-liquid microextraction combined with gas chromatography–mass spectrometry for in situ determination of biogenic amines in meat: Estimation of meat's freshness
PublicationA dispersive liquid-liquid microextraction (DLLME) gas chromatography–mass spectrometry (GC–MS) technique was developed for the determination of selected biogenic amines (BAs) in samples of poultry, pork and beef. Prior to the extraction process, an appropriate volume of sodium hydroxide solution was added to each of the portioned samples. Next, samples were homogenized, centrifuged and finally sonicated at an increased temperature....
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Evaluation of Terpene Decomposition in Kaffir Lime Juice during Storage Using Gas Chromatography–Mass Spectrometry and Proton Transfer Reaction–Mass Spectrometry
PublicationKaffir lime juice, often treated as production waste, can be a good source of terpenes. These compounds undergo various decomposition processes under the influence of external factors, especially during transportation and storage. In this paper, it was possible to monitor changes in the terpene profile of kaffir lime juice under different storage conditions, namely, 4 ◦C, 20 ◦C, and 35 ◦C. The identification of key decomposition...
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Micellar liquid chromatography for lipophilicity determination of new biologically active 1,3‐purinodiones
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Multidimensional Gas Chromatography in Essential Oil Analysis. Part 1: Technical Developments
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Headspace liquid phase microextraction for quantitation of hexanal in potato crisps by gas chromatography
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Determination of aliphatic amines in water by gas chromatography using headspace solvent microextraction
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Combined gas chromatography—mass spectrometry for the analysis of central and peripheral biogenic amines
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High resolution liquid chromatography and time of flight mass spectrometry in perfume analysis
PublicationPerfumes consist of a wide range of natural and synthetic compounds that belongs to different chemical classes. Most of these compounds are generally determined by GC. However, in this study RP-HPLC-Q-TOF-MS and HILIC-Q-TOF-MS technique was applied for the determination of ingredients of original perfumes and their imitations. Antioxidants and compounds specific to fragrances of animal \origin were found in original...
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Determination of cyanide in urine and saliva samples by ion chromatography with pulsed amperometric detection
PublicationCommonly known as a highly toxic chemical, cyanide is also an essential reagent for many industrial processes. It naturally occurs in plant seeds as a cyanogenic glycosides. Another relatively common mode of cyanide exposure is inhalation of environmental tobacco smoke. This study concerns importance to determine cyanide ion in human biological samples. Urine and saliva samples were collected healthy volunteers exposed to tobacco...
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Determination of MDPBP in postmortem blood samples by gas chromatography coupled with mass spectrometry
PublicationMDPBP (1-(3,4-methylenedioxyphenyl)-2-(1-pyrrolidinyl)-1-butanone) is a new psychoactive substance sold on the black market. It has been a controlled drug of abuse in Poland and China since 2015 as some toxic and fatal cases connected with use of synthetic cathinone derivatives were observed. The fatal case outlined here concerns a 19 year-old man, who was found dead with an envelope containing white powder lying nearby the cadaver....
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Identification of aromatic compounds in odours mixture by gas chromatography and field olfactometry techniques
PublicationThis paper shows the results of investigation on identification aromatic compounds present in odorous mixture in atmospheric air samples collected in a vicinity of the oil refinery LOTOS S.A., located in Gdansk, during March and April period have be presented. The studies were conducted by the use of comprehensive two-dimensional gas chromatograph equipped with a cryogenic modulator and coupled with a time-of-flight mass spectrometer,...
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Understanding the early-stage release of volatile organic compounds from rapeseed oil during deep-frying of tubers by targeted and omics-inspired approaches using PTR-MS and gas chromatography
PublicationDuring deep-frying, a plethora of volatile products is emitted with the fumes. These compounds could act as oil quality indicators and change the indoor air composition leading to health risks for occupants. The presented experiments focus on deep-frying of different tubers in rapeseed oil at different frying temperatures. Here, two scenarios for real-time monitoring of volatile organic compounds (VOCs) using proton transfer reaction...
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Determination of eight artificial sweeteners and common Stevia rebaudiana glycosides in non-alcoholic and alcoholic beverages by reversed-phase liquid chromatography coupled with tandem mass spectrometry.
PublicationThe method for the determination of acesulfame-K, saccharine, cyclamate, aspartame, sucralose, alitame, neohesperidin dihydrochalcone, neotame and five common steviol glycosides (rebaudioside A, rebaudioside C, steviol, steviolbioside and stevioside) in soft and alcoholic beverages was developed using high-performance liquid chromatography and tandem mass spectrometry with electrospray ionisation (HPLC-ESI-MS/MS). To the best of...
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Determination of parent and methylated polycyclic aromatic hydrocarbons in water samples by dispersive liquid–liquid microextraction–two dimensional gas chromatography–time-of-flight mass spectrometry
PublicationPolycyclic aromatic hydrocarbons (PAHs) are contaminants frequently found in environmental waters. Owing to their toxic effects, it is important to develop analytical methodologies that allow their fast and reliable determination. Dispersive liquid–liquid microextraction (DLLME) allows a quick extraction of analytes with little organic solvent consumption. The best results regarding sample preparation are obtained when 40 mL of...
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Overview of current communication systems for security forces. Features, limitations and potential solutions
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Numerical Analysis of Magnetic Core Properties Influence on Residual Current Device Behaviour
PublicationW artykule przedstawiono analizę wpływu kształtu prądu w uzwojeniu pierwotnym transformatora prądowego na pracę przekładnika różnicowo-prądowego. Przeprowadzono obliczenia symulacyjne dla wymuszenia o kształcie sinusoidy i sinusoidy wyprostowanej dla częstotliwości 50 Hz. Wzięto pod uwagę dwa typy charakterystyki magnesowania transformatora: dla materiału magnetycznie miękkiego i materiału o prostokątnej pętli histerezy. Analiza...
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Open-transistor fault diagnostics in voltage-source inverters by analyzing the load current
PublicationPrzedstawiono nową metodę detekcji i lokalizacji uszkodzeń polegających na braku przewodzenia tranzystorów w falownikach napięcia zasilających silniki indukcyjne. Metoda jest rozszerzeniem, opracowanej wcześniej, metody wykorzystującej znormalizowane składowe stałe prądów obciążenia. Znormalizowane wartości średnie prądów powiązano z dodatkowymi wskaźnikami diagnostycznymi, które zawierają informacje o czasie trwania nieprzewodzenia...
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Structural Investigations and Determination of Current and Voltage Characteristics in Htsc 2G SF12050 Tapes
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Adsorption performance of graphitic carbon nitride-based materials: Current state of the art
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Scabies – still current medical and social problem. A retrospective analysis of 193 cases
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Trans-Z-source-like inverter with built-in DC current blocking capacitors
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Assessment of hardened layer thickness for 40HNMA steel using eddy current method
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Current epidemiological situation in the context of inclusion body hepatitis in poultry flocks in Poland
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LOCAL E-MARKETING AND PHARAMACY SELECTION PROCESS AMONG CURRENT AND PROSPECTIVE CONSUMERS
PublicationWORK OBJECTIVES: To examine whether and to what extent a company's presence in Google Search mobile results, and Google Maps service search results, affects pharmacies' acquisition of new consumers RESEARCH QUESTIONS: Does the presence of pharmacies in Google MyBusiness increase the number of their customers ? Is the increase in the...
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Diffuse axonal injury – an interdisciplinary problem. Current knowledge and two case reports
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Transcranial magnetic stimulation (TMS) in treatment of psychiatric disorders – review of current studies
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Comparison Study on Sonodirect and Sonoalternate Current Electrocoagulation Process for Domestic Wastewater Treatment
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Influence of circuit breaker operation upon transformeros residual flux and inrush current
PublicationPrzedstawiono model i wyniki obliczeń prądu i strumienia magnetycznego w układzie zawierającym transformator trójfazowy i wyłącznik. Opracowano obwodowy model łącznika z łukiem elektrycznym. Model łuku zbudowano w oparciu o jego statyczną charakterystykę prądowo-napięciową z uwzględnieniem uproszczonej charakterystyki dynamicznej. Przeprowadzone symulacje wykazały, że wartość maksymalna prądu włączania transformatora zależy zarówno...
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Current Trends in the Development of Microwave Reactors for the Synthesis of Nanomaterials in Laboratories and Industries: A Review
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Urinary tract infection in children: Diagnosis, treatment, imaging – Comparison of current guidelines
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Temperature effect on the current-voltage characteristic fill factor for the silicon solar cells
PublicationW pracy przedstawiono badania wpływu temperatury pracy krzemowych ogniw fotowoltaicznych na wartość współczynnika wypełnienia charakterystyki prądowo- napięciowej (FF). Efekty dyfuzyjne w obszarze złącza oraz rekombinacja nośników ładunku ograniczają wartość współczynnika wypełnienia charakterystyki. Spadek tej wartości wynika głównie ze wzrostu wartości rezystancji szeregowej rs. Na rezystancję szeregową składają się: opór emitera...
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Current commutation process in a ultra-fast fuse-IGBT hybrid circuit breaker.
PublicationUkład hybrydowy bezpiecznika topikowego i tranzystora IGBT umożliwia bardzo szybkie włączenie do obwodu zwarciowego impedancji ograniczającej wartość prądu. Po eksplozji krótkiego topika bezpiecznika wywołanej narastającym prądem zwarciowym wywołuje w czasie poniżej 2 ms wzrost napięcia na topiku do wartości ok.20 - 25V, po czym prąd jest komutowany do gałęzi z przyrządem półprzewodnikowym typu GTO lub IGBT. Ostateczne wyłączenie...
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Musical Metadata Retrieval with Flow Graphs, in Rough Sets and Current Trends in Computing.
PublicationW pracy opisano metody wyszukiwania muzyki w Internecie w oparciu o opis semantyczny. W eksperymentach wykorzystano opis muzyczny stosowany w bazie CDDB. Zaprezentowano metodę grafów przepływowych zaproponowaną przez Pawlaka.
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Single chamber solid oxide fuel cell - current stage of development and prospects
PublicationOgniwa paliwowe należą do jednego z najbardziej wydatnych żródeł energii. W konwencjonalnych ogniwach paliwo i powietrze są dostarczane do ogniwa oddzielnie. Jednokomorowych ogniwo dziala zasilane mieszanina paliwa i powietrza. W pracy przedstawiono obecny stan i perspektywy dlaszego rozwoju jednokomorowych tlenkowych ogniw paliwowych.
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Computer simulation of current voltage response of elektrocatalytic sensor.Optoelectronic and Electronic Sensors V.
PublicationW pracy przedstawiono wyniki symulacji komputerowej działania czujnika elektrokatalitycznego. Do badań wykorzystano program D. Gossera opierający się na metodzie różnic skończonych.
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Influence of ci rcuit parameters on the procces of current transfer in thehybrid circuit breaker.
PublicationW artykule przedstawiono działanie hybrydowego bezstykowego ogranicznika prądów zwarciowych w oparciu o symulację komputerową oraz porównanie eksperymentu z symulacją komputerową przy pomocy programu MATLAB i PSPICE. Przedstawiono również wady i zalety obliczeń numerycznych przeprowadzonych z zastosowaniem komercyjnych programów na analizę działania łącznika hybrydowego.W analizie uwzględniono model hybrydowego ogranicznika...
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Assessment of the Current Potential of Hydropower for Water Damming in Poland in the Context of Energy Transformation
PublicationThe present paper indicates that hydropower, including small hydropower plants (SHPs), may play a very important role in Poland’s energy transformation in the near future. The development of SHPs may also increase water resources in the steppe Poland. Additionally, the aim of the present research is to conduct the PEST analysis of SHPs in Poland, taking into account the SHP potential. For the first time, maps showing the power...
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Phytoremediation—From Environment Cleaning to Energy Generation—Current Status and Future Perspectives
Publication:Phytoremediationis a technology based on the use of green plants to remove, relocate, deactivate, or destroy harmful environmental pollutants such as heavy metals, radionuclides, hydrocarbons, and pharmaceuticals. Under the general term of phytoremediation, several processes with distinctively different mechanisms of action are hidden. In this paper, the most popular modes of phytoremediation are described and discussed. A broad...