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Search results for: bis-tetrazole
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Solar light driven degradation of norfloxacin using as-synthesized Bi 3+ and Fe 2+ co-doped ZnO with the addition of HSO 5 – : Toxicities and degradation pathways investigation
PublicationIn this study, solar light responsive Bi3+ and Fe2+ doped ZnO were synthesized and used for photocatalytic degradation of norfloxacin (NOR), an emerging water pollutant. Analysis with Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HRTEM), selected area electron...
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Decision making process using deep learning
PublicationEndüstri 4.0, dördüncü endüstri devrimi veya Endüstriyel Nesnelerin İnterneti (IIoT) olarak adlandırılan sanayi akımı, işletmelere, daha verimli, daha büyük bir esneklikle, daha güvenli ve daha çevre dostu bir şekilde üretim yapma imkanı sunmaktadır. Nesnelerin İnterneti ile bağlantılı yeni teknoloji ve hizmetler birçok endüstriyel uygulamada devrim niteliği taşımaktadır. Fabrikalardaki otomasyon, tahminleyici bakım (PdM – Predictive...
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Architekturführer Danzig: Gdansk Sopot Gdynia
PublicationIm Zweiten Weltkrieg bis auf die Grundmauern zerstört, wurde der historische Stadtkern der Hansestadt Danzig als polnisches Gdańsk wiederaufgebaut – ein Paradebeispiel für kritische Rekonstruktion in Polen und zugleich eine bis heute stark umstrittene Entscheidung. Zusammen mit dem mondänen Seebad Sopot und der modernen Hafenstadt Gdynia bildet die Bernsteinstadt eine Metropolregion an der polnischen Ostseeküste: die Dreistadt...
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Chalcogen bonding interactions in a series of aromatic selenocyanates
PublicationSelenium atoms in aromatic selenocyanates are characterized by the occurrence of two σ-holes, a stronger one in the prolongation of the NC–Se bond and a weaker one in the prolongation of the Ar–Se bond. The crystal structures of several bis(selenocyanato) derivatives, prepared by a method originally developed for ortho bis-substituted derivatives, illustrate very well this difference, with a short NC–Se⋯NC ChB interaction organizing...
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Elimination of dominated partial schedules in scheduling deteriorating jobs
Publicationw artykule rozważany jest problem szeregowania zadań uwarunkowanych czasowo, w notacji trójpolowej opisywany przez 1 | pi = a + bisi | ?ci. wprowadzona jest koncepcja zdominowanych częściowych harmonogramów oraz przedstawiony jest niewielomianowy algorytm dla problemu, który bazuje na eliminacji zdominowanych częściowych harmonogramów. przedstawione są wyniki eksperymentów obliczeniowych, porównujących zaprezentowany algorytm oraz...
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Nanosilver-loaded PMMA bone cement doped with different bioactive glasses – evaluation of cytocompatibility, antibacterial activity, and mechanical properties
PublicationNanosilver-loaded PMMA bone cement (BC-AgNp) is a novel cement developed as a replacement for conventional cements. Despite favorable properties and antibacterial activity, BC-AgNp still lacks biodegradability and bioactivity. Hence, we investigated the doping with bioactive glasses (BGs) to create a new bioactive BC characterized by time-varying porosity and gradual release of nanosilver. The BC Cemex was used as the base material...
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Numerical methods for the assessment of bridge safety barriers
PublicationThe paper presents a numerical study of the bus crash test for bridge safety barriers. The analysis is conducted with the use of explicit code LS-DYNA. The problem of hourglass effect in shell elements is discussed. The simulations of bus impact against the barrier show that the analyzed barrier withstands the impact forces and restrains the bus trajectory to the bridge road.
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Zastosowanie sztucznych sieci neuronowych w sterowaniu robotem do prac pod-wodnych. Visnik Nacional´ Univ. L´viv**2002 nr 467 s. 19-24, 6 rys. bib- liogr. 5 poz. Wisnik Nacionalnogo Uniwiersitetu Lwiwska Politechnika
PublicationPrzedstawiono zagadnienie lokalizacji i sterowania podwodnego robota przeznaczonego do zadań przy kadłubie statku, zwłaszcza do czyszczenia z rdzy i biologicznych porostów. Zbadano możliwość zastosowania sztucznych sieci neuronowych do sterowania podwodną głowicą roboczą. W wyniku przeprowadzonej analizy został zaproponowany układ sterowania adaptacyjnego przy założeniu, że znane są wszystkie parametry rozpatrywanego obiektu...
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Nowe poliuretany dla celów medycznych.**2003, 132 s. 54 rys. 31 tab. bib-liogr. 118 poz. maszyn. Rozprawa doktorska /08.10.2003/ P. Gdań. Wydz. Chem. Promotor: dr hab. inż. B. Masiulanis, prof. nadzw. PG.
Publication.
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Azo and azoxythiacrown ethers: synthesis and properties
PublicationA series of 16- and 18-membered azo- and azoxythiacrown ethers have been synthesized by reductive macrocyclization of the respective bis(nitrophenoxy)oxaalkanes. The aromatic residues located in the polyether region of the molecule were introduced to macrocyclic skeletons and their affinities toward different groups of metal cations in ion-selective electrodes were described. X-ray structures for one dinitropodand and one azoxybenzothiacrown...
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Literature update of analytical methods for biogenic amines determination in food and beverages
PublicationBiogenic amines (BAs) have been reported in a variety of foods, such as fish, meat, cheese, and wines. The formation of BAs in food by the microbial decarboxylation of amino acids can result in human allergic reactions, characterized by difficulty in breathing, rash, vomiting, and hypertension. Control measures to prevent biogenic amine formation in foods and/or reduce their levels should be considered. Therefore, monitoring of...
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Phytoremediation—From Environment Cleaning to Energy Generation—Current Status and Future Perspectives
Publication:Phytoremediationis a technology based on the use of green plants to remove, relocate, deactivate, or destroy harmful environmental pollutants such as heavy metals, radionuclides, hydrocarbons, and pharmaceuticals. Under the general term of phytoremediation, several processes with distinctively different mechanisms of action are hidden. In this paper, the most popular modes of phytoremediation are described and discussed. A broad...
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Occurrence and Levels of Biogenic Amines in Beers Produced by Different Methods
PublicationThe concentration of biogenic amines (BAs) in beer depends, among other factors, on the activity of microorganisms, in particular lactic acid bacteria. In this work an analytical method based on derivatization with tosyl chloride and high-performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was used to determine 17 BAs in samples of commercially available beers, and to monitor the changes in concentration of...
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Problematyka doboru zabezpieczeń dławików kompensacyjnych pracujących w sieciach najwyższych napięć
PublicationW artykule przedstawiono trudności, jakie napotyka się podczas projektowania systemu zabezpieczeń dla dławików przyłączanych bezpośrednio do sieci najwyższych napięć (NN). Bazując na przykładzie budowanej aktualnie stacji 400 kV Ełk Bis, pokazano, że możliwości zabezpieczenia dławika, oparte na układach EAZ wykorzystujących pomiary sygnałów elektrycznych z przekładników prądowych i napięciowych, mają swoje ograniczenia i w pewnych...
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Wybrane problemy doboru zabezpieczeń dławików kompensacyjnych pracujących w sieciach najwyższych napięć
PublicationW referacie przedstawiono trudności jakie napotyka się podczas projektowania systemu zabezpieczeń dla dławików przyłączanych bezpośrednio do sieci najwyższych napięć (NN). Referat, bazując na przykładzie budowanej aktualnie stacji 400 kV Ełk Bis, pokazuje, że możliwości zabezpieczenia dławika, oparte na układach EAZ wykorzystujących pomiary sygnałów elektrycznych z przekładników prądowych i napięciowych mają swoje ograniczenia...
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A General Synthesis of Diaryl Cyclic Diamidines
PublicationA convenient and general method has been developed for directly converting bis-nitriles, e.g., I, to cyclic diamidines, e.g., II, using reagents derived from diaminoalkanes, e.g., H2NCH2CH2NH2, satd. with hydrogen sulfide. A 1:1 mixt. of a diaminoalkane and Et alc. (or without) was effective in most cases (72-88%). The synthetic utility of this methodol. in the prepn. of tetrakis(cyclic amidino)pyrenes III (R = H, Me) from 1,3,6,8-tetracyanopyrene...
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A prototype of electrochemical sensor for measurement of carbonyl compounds in air
PublicationThe paper presents the results of investigation on a prototype sensor for measurement of benzaldehyde and formaldehyde in air. Sensitivity, limit of quantification and coefficient of selectivity of the sensor have been determined as a function of membrane thickness and electrode type using square wave voltammetry (SWV) technique. The working and counter electrodes were made of platinum and gold. Ionic liquids 1-hexyl, 3-methylimidazolium...
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Local impedance spectroscopy of membranes
PublicationCelem niniejszej publikacji jest zaprezentowanie zastosowania techniki Lokalnej Elektrochemicznej Spektroskopii Impedancyjnej (LEIS) do uzyskania lokalnej charakterystyki membran. Membranę wykonaną z polichlorku winylu (PCV), plastyfikowaną sebacynianem bis(2etyloheksylu) i domieszkowaną boranem tetradodecyloamoniowym zbadano pod kątem równomiernego rozkładu przewodnictwa na powierzchni badanej próbki. Lokalne pomiary impedancyjne,...
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A new Thermus sp. class-IIS enzyme subfamily: isolation of a ''twin'' endo nuclease TspDTI with a novel specificity 5´-ATGAA(N11/9)-3´, related to TspGWI, Taqll and Tth111II. 5´-ATGAA(N11/9)-3´, spokrewnionej z TspGWI, TaqII i Tth111II.
PublicationOdkryto i scharakteryzowano nową subrodzinę enzymów klasy IIS z Thermus sp.
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Implementation of Hermite-Ritz method and Navier’s Technique for Vibration of Functionally Graded Porous Nanobeam Embedded in Winkler-Pasternak Elastic Foundation Using bi-Helmholtz type of nonlocal elasticity
PublicationPresent study is devoted to investigating the vibration characteristics of Functionally Graded (FG) porous nanobeam embedded in an elastic substrate of Winkler-Pasternak type. Classical beam theory (CBT) or Euler-Bernoulli beam theory (EBT) has been incorporated to address the displacement of the FG nanobeam. Bi-Helmholtz type of nonlocal elasticity is being used to capture the small scale effect of the FG nanobeam. Further, the...
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Non-linear static stability of bi-layer carbon nanosheets resting on an elastic matrix under various types of in-plane shearing loads in thermo-elasticity using nonlocal continuum
PublicationIn this research, the shear and thermal buckling of bi-layer rectangular orthotropic carbon nanosheets embedded on an elastic matrix using the nonlocal elasticity theory and non-linear strains of Von-Karman was studied. The bi-layer carbon sheets were modeled as a double-layered plate, and van der Waals forces between layers were considered. The governing equations and boundary conditions were obtained using the first order shear...
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Evaluation of the Impact of Storage Conditions on the Biogenic Amines Profile in Opened Wine Bottles
PublicationA survey of biogenic amine (BA) profiles in opened wine bottles has been established to monitor the level of biogenic amines (BAs) in opened bottles against time and other conditions. Bottles of red and white wine were submitted to different temperatures, stopper type (screw cap, cork), and use of vacuum devices. A total of six wines made from a variety of grapes were obtained from vineyards from regions across Poland. Dispersive...
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Synthesis, structure and properties of novel poly(hydroxyurethane)s obtained by non-isocyanate route
PublicationNon-isocyanate polyurethanes (NIPUs) can be synthesized by polyaddition of five-membered bis(cyclic carbonate)s and primary diamines. NIPUs are an alternative for the commonly used (in the form of foams, elastomers, coatings or fibers) in the industry polyurethanes obtained using toxic and moisture sensitive diisocyanates, polyols and low-molecular weight chain extenders. The main aim of this work was to synthesize non-isocyanate...
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TBAF Promoted Formation of Symmetrical Trisulfides
PublicationWe have developed a new method for the synthesis of functionalized symmetrical trisulfides based on (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives prepared from readily available 5,5-dimethyl-2-sul-fanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical trisulfides can be obtained from aliphatic and aromatic thiols andL-cysteine derivatives...
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Electrochemical sensor for measurement of volatile organic compounds employing square wave perturbation voltage
PublicationThe paper presents the results of investigation on a prototype sensor for measurement of benzaldehyde in air. Sensitivity and limit of quantification of the sensor were determined for different internal electrolyte using the square wave voltammetry (SWV) as a detection technique. The working and counter electrodes were made of platinum. Ionic liquids 1-hexyl, 3-methylimidazolium chloride,1-hexyl, 3-methylimidazolium bis (trifluoromethanesulfonyl)...
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Novel and Efficient Methods for the Synthesis of Symmetrical Trisulfides
PublicationWe have developed a convenient methods for the synthesis of symmetrical trisulfides under mild conditions in very good yields. The described methods are based on the straightforward preparation of 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinane-2-disulfanyl derivatives from readily available 5,5-dimethyl-2-sulfanyl-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The symmetrical...
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Ionogel sorbent coatings for determining organophosphorus and pyrethroid insecticides in water and fresh juice samples by headspace-solid phase microextraction
PublicationThe sol–gel method yielded three different ionogel sorbent coatings that were obtained based on a silica material containing ionic liquids (ILs) immobilized in its pores. Two ILs, triethylsulfonium bis(trifluoromethylsulfonyl) imide [Set3][TFSI] and 1-butyl-1-methylpiperidinium bis(trifluoromethylsulfonyl)imide [C4C1Pip][TFSI], as well as their equimolar mixture [Set3/C4C1Pip], were used to obtain ionogel fibers. The developed...
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Tuning the extraction properties of ionogel-coated Solid-phase microextraction fibers based on the solvation properties of the ionic liquids
PublicationA silica-based network was used to immobilize ionic liquid-based ionogels and applied as a fiber coating forsolid-phase microextraction (SPME). The ionogels were prepared by a sol–gel process, using two ionic liquids,triethylsulfonium bis(trifluoromethylsulfonyl)imide ([Set3][TFSI]) and 1-butyl-1-methylpiperidinium bis(tri-fluoromethylsulfonyl)imide ([C4C1Pip][TFSI]), as well as their equimolar mixture. Methyltrimethoxysilane wasused...
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Sustainability of Cluster Organizations as Open Innovation Intermediaries
PublicationThe purpose of the paper is to identify the most important open innovation practices used by cluster organizations (COs). To reflect these practices, the paper uses the concept of the trajectory of relationship development in COs, applied in the Interizon cluster organization. Additionally, this paper introduces the potential sustainability-related implications of open innovation adoption in cluster organizations. An in-depth direct...
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Sustainability objectives and collaboration lifecycle in cluster organizations
PublicationIn our paper, we combine two issues, collaboration in cluster organizations and sustainability, aiming to answer the question: Does complex governance structure of cluster organizations support members in formulating and reaching sustainability objectives? Based on four case studies of cluster organizations and a still novel abductive approach, we present the ways in which sustainability was executed in their functioning. Our study...
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Structure and properties comparison of poly(ether-urethane)s based on nonpetrochemical and petrochemical polyols obtained by solvent free two-step method
PublicationThe application of thermoplastic polyurethanes (TPU) is becoming more and more extensive, and the decreasing of used petrochemical monomers and reduction of energy for the polymerization and processing processes is getting increasingly important. In this paper, we confirmed the positive influence of high bio-based monomers contents (by replacing petrochemical polyol and glycol by bio-based counterparts) on processing and properties...
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Fault detection in electronic circuits using test buses
PublicationA survey of test buses designed for diagnostics of digital and analog electronic circuits is presented: the IEEE 1149.1 bus for digital circuits, the IEEE 1149.4 bus for mixed-signal and the IEEE 1149.6 bus for AC coupled complex digital circuits. Each bus is presented with its structure, solution of key elements, particularly boundary registers and a set of test instructions. Diagnosis with the use of the described buses is...
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Synergy between AgInS2 quantum dots and ZnO nanopyramids for photocatalytic hydrogen evolution and phenol degradation
PublicationDespite the unique properties of single semiconductor nanomaterials and quantum dots, poor photocatalytic activity has characterized them and the fabrication of nanocomposites has become necessary to enhance their photocatalytic performance. Thus, AgInS2 quantum dots (AIS QDs, 4.0±1.6 nm), have been successfully prepared and loaded onto ZnO nanopyramids (ZnO NPy). The effect of the nominal amount of AIS QDs decorating ZnO NPy on...
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Characteristic of Morpholinium Ionic Liquids as Gas Chromatography Stationary Phases with McReynolds Constants and Activity Coefficients at Infinite Dilution
PublicationIn this work, four ionic liquids based on N-alkyl-N-methylmorpholinium cation ([Mor1,R] where R= 2, 4, 8, 10) and bis(trifluoromethanesulfonyl)imide anion [TFSI] were synthesized. Using gas-liquid chromatography a number of parameters describing the sorption properties of the investigated ionic liquids were determined. The values of Kovats indices, McReynolds constants, and activity coefficients at infinite dilution were the basis...
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Electrochemical sensor for measurement of volatile organic compounds = Elektrochemiczny czujnik do oznaczania lotnych związków organicznych
PublicationPrzedstawiono rezultaty badań prototypowego czujnika do oznaczania benzaldehydu i formaldehydu w powietrzu. Określono czułość wskazań czujnika i jego granice oznaczalności wykorzystując jako technikę detekcyjną woltamperometrię fali prostokątnej (SWV). Elektrodę roboczą i przeciwelektrodę stanowiły elektrody z Pt. Elektrolitem wewnętrznym były ciecze jonowe: chlorek 1-heksylo,3- metyloimidazolinowy i bis(trifluorometylosulfonylo)imidek...
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A versatile and convenient preparation of unsymmetrical diaryl disulfides
PublicationWe have developed a convenient method for the synthesis of unsymmetrical diaryl disulfides under mild conditions in excellent yields. The described method is based on the straightforward preparation of 5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinane-2-sulfenyl bromide from readily available 5,5-dimethyl-2-thiolo-2-thioxo-1,3,2-dioxaphosphorinane or bis(5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorinan-2-yl) disulfide. The unsymmetrical...
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Zanieczyszczenie obecne w próbkach śniegu pobranego z warstw jako źródło informacji o stanie środowiska w dużej aglomeracji miejskiej = Pollutants present in snow samples collected from various layers of snow cover as a source of information about the state of environment in a big urban agglomeration
PublicationPróbki śniegu pobierano przez okres około miesiąca z 12 miejsc zlokalizowanych na terenie Trójmiasta. Sześć z nich znajdowało się w pobliżu dróg komunikacyjnych o różnym natężeniu ruchu. Każde z nich miało swój punkt odniesienia oddalony od niego o około 200 m. W próbkach śniegu oznaczano pH, przewodność, zawartość wybranych anionów i kationów. Wartości pH wyznaczono przy użyciu elektrody szklanej połączonej z pH/tlenomierzem mikrokomputerowym,...
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Discrepancies in determination of biogenic amines in beer samples by reversed phase and hydrophilic interaction liquid chromatography coupled with tandem mass spectrometry
PublicationBiogenic amines (BAs) are nitrogenous organic bases occurring mainly in fermented food and beverages as a result of free amino acids bacterial decarboxylation. The reversed phase liquid chromatography (RPLC) and hydrophilic interaction liquid chromatography (HILIC) based methods were compared in terms of usefulness for determination of BAs in beer samples. Analysis of BAs with the use of RPLC method were carried out after their...
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Exposure to Bisphenol A Analogs and the Thyroid Function and Volume in Women of Reproductive Age—Cross-Sectional Study
PublicationBisphenols (BPs) are commonly known plastifiers that are widely used in industry. The knowledge about the impact of BPs on thyroid function is scarce. Proper thyroid functioning is especially important for women of reproductive age, as hypothyroidism affects fertility, pregnancy outcomes and the offspring. There are no studies analyzing the influence of BPs on thyroid function and volume in non-pregnant young women. The aim of...
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Przedsiębiorczość społeczna w społeczeństwie obywatelskim w Polsce
PublicationW artykule przedstawiono koncepcję i zakres zjawiska przedsiębiorczości społecznej w Polsce, w kontekście funkcjonowania społeczeństwa obywatelskiego. W tym celu autorka analizuje dominujące szkoły badań nad zjawiskiem przedsiębiorczości społecznej, identyfikuje i charakteryzuje podstawowe modele przedsiębiorstw społecznych w Polsce oraz wskazuje na wyzwania związane z badaniem tego typu organizacji. Autorka przedstawia i poddaje...
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Teleopieka domowa w systemie opieki nad osobami starszymi – doświadczenia gmin województwa pomorskiego
PublicationCelem opracowania jest przedstawienie istoty teleopieki domowej oraz dotychczasowych doświadczeń w zakresie jej wdrażania w gminach województwa pomorskiego. Autorka artykułu omówiła założenia idei gminnych powszechnych systemów teleopieki domowej oraz zidentyfikowała warunki konieczne do ich efektywnego funkcjonowania.
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Isolation and 3-dimensional Culture of Primary Murine Intestinal Epithelial Cells
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Induction of Epithelial-mesenchymal Transition in MDCK II Cells
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Global variation in anastomosis and end colostomy formation following left‐sided colorectal resection
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Global wealth disparities drive adherence to COVID-safe pathways in head and neck cancer surgery
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System wynagradzania nauczycieli w Polsce – skutki dla lokalnych budżetów
PublicationArtykuł podejmuje problematykę systemu wynagradzania nauczycieli w Polsce. W pierwszej części przedstawiono oświatę jako zadanie publiczne polskich gmin, powiatów i województw oraz miast na prawach powiatu, które wypełniają zadania zarówno gmin, jak i powiatów. W kolejnej części omówiono kryteria (zwłaszcza dotyczące nauczycieli) podziału części oświatowej subwencji ogólnej z budżetu państwa pomiędzy jednostki samorządu terytorialnego....
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Zadłużenie jednostek samorządu terytorialnego i jego determinanty
PublicationW artykule zbadano przesłanki i skutki zadłużania się jednostek samorządu terytorialnego w Polsce, a także zidentyfikowano determinanty ich zadłużenia w podziale na prawno-finansowe, polityczne, ekonomiczno-społeczne i organizacyjno-zarządcze. Przedstawiono również poziom zadłużenia tych jednostek w latach 2003-2020. Najbardziej zadłużone są miasta na prawach powiatu i gminy, co jest przede wszystkim związane z realizowanymi przez...
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The bile salt/phospholipid ratio determines the extent of in vitro intestinal lipolysis of triglycerides: Interfacial and emulsion studies
PublicationThis study focused on the protein-stabilised triglyceride (TG)/water interfaces and oil-in-water emulsions, and explored the influence of varying molar ratios of bile salts (BSs) and phospholipids (PLs) on the intestinal lipolysis of TGs. The presence of these two major groups of biosurfactants delivered with human bile to the physiological environment of intestinal digestion was replicated in our experiments by using mixtures...
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Analysis of investment stages along with a construction project management project for an investment task regarding the reconstruction and expansion of the locomotor system rehabilitation center Krzeszowice SPZOZ in Poland
PublicationAutorzy: Gwóźdź-Lasoń Monika, Tkocz Sebastian.
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Podaż technologii vs potrzeby w zakresie technologii: rola instytucji pośredniczących w transferze technologii na Pomorzu
PublicationNiniejszy rozdział poświęcony jest na omówienie roli instytucji pośredniczących w procesach transferu technologii. Autorka, na podstawie badań przeprowadzonych w trzech grupach podmiotów działających na Pomorzu, obejmujących: instytucje pomostowe (wsparte środkami z Regionalnego Programu Operacyjnego Województwa Pomorskiego na lata 2007-2013), klientów tych instytucji oraz losowo dobraną próbę przedsiębiorców przeanalizowała –...