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Search results for: M-SPME
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Precipitation and Transformation of Vaterite Calcium Carbonate in the Presence of Some Organic Solvents
PublicationIn this paper, the production of CaCO3 particles via the carbonation route in the reaction of CaCl2 and CO2, using NH3 as a promoter of CO2 absorption, was studied. The solvents used as the reaction media for CaCO3 precipitation were aqueous solutions of methanol, isopropanol and dimethyl sulfoxide (DMSO), in a concentration range of 0–20% (v/v). It was found that the presence of an organic additive influenced the precipitation...
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Novel amides of mycophenolic acid and some heterocyclic derivatives as immunosuppressive agents
PublicationThe group of new amide derivatives of mycophenolic acid (MPA) and selected heterocyclic amines was synthesised as potential immunosuppressive agents functioning as inosine-5'-monophosphate dehydrogenase (IMPDH) uncompetitive inhibitors. The synthesis employed uronium-type activating system (TBTU/HOBt/DIPEA) while or phosphonic acid anhydride method (T3P/Py) facilitating amides to be obtained in moderate to excellent yields without...
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Some accelerationist remarks on Marcuse’s drives theory and his dialectics of civilization
PublicationMarcuse’s theory of civilization offers a promising Freud-Marx synthesis. His approach, best articulated in Eros and Civilization, aims at a thorough reformulation of the Freudian drive doctrine to render it more historical and concatenate it to the problem of structural violence and the institutionalized (and internalized) mechanism of repression. I claim that the said reformulation provides a cornerstone for Marcuse’s highly...
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E-Estonia as a role model? Some general considerations and applicability in France
PublicationEstonia has recently been widely recognised – in the policy circles, academia, as well as the media space – as one of the more advanced nation states when it comes to digital government (and governance) transformation (e.g. Margetts and Naumann, 2017; Heller, 2017). Ever greater attention Estonia attracted with the two most recent digital government initiatives, namely the e-Residency and the virtual data embassy, both first of...
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Key-Marker Volatile Compounds in Aromatic Rice (Oryza sativa) Grains: An HS-SPME Extraction Method Combined with GC×GC-TOFMS
PublicationThe aroma of rice essentially contributes to the quality of rice grains. For some varieties, their aroma properties really drive consumer preferences. In this paper, using a dynamic headspace solid-phase microextraction (HS-SPME) system coupled to a two-dimensional gas chromatography (GC×GC) using a time-of-flight mass spectrometric detector (TOFMS) and multivariate analysis, the volatile compounds of aromatic and non-aromatic...
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A heterotrimetallic synthetic approach in versatile functionalization of nanosized {MxCu13–xW7}3+ and {M1Cu8W6} (M = Co, Ni, Mn, Fe) metal–cyanide magnetic clusters
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Ekspertyza techniczna dotycząca drgań konstrukcji mostu w km 26,571/26,578 linii kolejowej nr 4 (CMK) w m. Huta Zawadzka
PublicationOpracowanie zawiera wyniki symulacji obliczeniowych, których celem bylo wyjaśnienie przyczyn nadmiernych drgań wieszaków wiaduktu kolejowego.
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Deposition and characterization of organic polymer thin films using a dielectric barrier discharge with different C2Hm/N2 (m = 2, 4, 6) gas mixtures
PublicationOrganic polymer thin films have been deposited on Si(100) and aluminum coated glass substrates by a dielectric barrier discharge (DBD) operated at medium pressure using different C2Hm/N2 (m = 2, 4, 6) gas mixtures. The deposited films were characterized by various spectroscopic techniques. Fourier transform infrared reflection absorption spectroscopy (FT-IRRAS) revealed the chemical functional groups present in the films. The surface...
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Induction of G2/M phase arrest and apoptosis of human pancreatic cancer BxPC-3 cells by potenet antitumor 1-nitroacridine derivative C-1748
PublicationPancreatic ductal adenocarcinoma (PDA) is among the most lethal human cancers, in part because it is insensitive to many chemotherapeutic drugs. Gemcitabine still remains the best chemotherapeutic agent available for the treatment of advanced pancreatic cancer. However, gemcitabine treatment results in only a marginal survival advantage. Thus, there is a strong need for the continuous development of novel therapeutic agents...
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Raport z badań podczas próbnego obciążenia konstrukcji odciążającej typu mostowego w km 20,151 LK nr 353 w m. Pobiedziska
PublicationW pracy przedstawiono metodykę pomiarów i wyniki badań podczas próbnego konstrukcji odciążającej typu mostowego w km 20,151 LK nr 353 w m. Pobiedziska. Sformułowano wnioski i wydano pinie dotyczącą rzeczywistej pracy konstrukcji i warunków dalszej eksploatacji obiektu.
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Discussion on “Coupled effective stress analysis of insertion problems in geotechnics with the Particle Finite Element Method” by L. Monforte, M. Arroyo, J.M. Carbonell, and A. Gens
PublicationAddressed here is the Particle Finite Element Method (PFEM) modelling of undrained CPTu penetration with regard to a reference analytical solution based on the Spherical Cavity Expansion Method (SCEM). Also discussed is the choice of the soil model and its parameters. The effect of cone interface friction on CPTu simulation is analyzed in a series of penetration tests using Arbitrary Lagrangian-Eulerian (ALE) and Updated Lagrangian...
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EFFECTS OF DOPING ON STRUCTURE AND PHASE TRANSITION OF HIGH TEMPERATURE PROTON CONDUCTOR LaNb1-xMxO4-σ (M=As, Sb, V, Ta AND X=0,05 TO 0,3)
PublicationIn this work synthesis of lanthanum orthoniobate has been done. Doping by arsenic, antimony, vanadium or tantalum in 5% to 30% have been introduced. The relationship between doping type and percentage and structural properties of the material have been investigated.
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Down-regulation of DNA topoisomerase IIalpha leads to prolonged cell cycle transit in G2 and early M phases and increased survival to microtubule-interacting agents
PublicationInhibitory polimeryzacji mikrotubul wykazują preferencyjną toksyczność wobec komórek mitotycznych. W ramach tego projektu badaliśmy czy oporność komórek ludzkich białaczek na inhibitor mikrotubul, winkrystynę, prowadzi do zmian w regulacji progresji cyklu komórkowego. Nasze wyniki wskazują, że oporności na winkrystynę towarzyszą zmiany w długości fazy G2 i M w nieobecności i obecności inhibitora wrzeciona mitotycznego, nokodazolu....
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Multifrequency Nanoscale Impedance Microscopy (m-NIM): A novel approach towards detection of selective and subtle modifications on the surface of polycrystalline boron-doped diamond electrodes
PublicationIn this paper, we describe the modification of Nanoscale Impedance Microscopy (NIM), namely, a combination of contact-mode atomic force microscopy with local impedance measurements. The postulated approach is based on the application of multifrequency voltage perturbation instead of standard frequency-by-frequency analysis, which among others offers more time-efficient and accurate determination of the resultant impedance spectra...
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The SPM Scanner Head Based on Piezoelectric Unimorph Disc
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Assessment of risks connected with economic activity in the SME sector
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The Impact of Conflicts in Foreign Business Relationships on SME Performance
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Revolutionizing SME Management: The Digital Transformation of Financial Operations
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The dynamic Polish suburban landscape created by SME sector
PublicationWspółcześnie zaobserwować można dynamiczne przeobrażenia przestrzeni wokół miast polegające na przemieszczaniu się ludności i podmiotów gospodarczych z miasta centralnego do strefy podmiejskiej. Wydaje się, że charakterystycznym elementem krajobrazu polskich obszarów podmiejskich jest duża ilość działających w nich przedsiębiorstw sektora MSP.
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Stellungnahme zur Zuschrift von Hanf M. zu Cywiński Z.: Formänderungsgrößenverfahren mittig gedrückter dünnwandiger Stäbe mit einfach- und doppeltsymmetrischen offenen Querschnitten
PublicationPraca zawiera głos zamykający dyskusję nt. przedmiotowego artykułu autora.
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The effect of thermal modification of ash wood on granularity and homogeneity of sawdust in the sawing process on a sash gang saw PRW 15-M in view of its technological usefulness
PublicationPrzedstawiono wyniki analiz granulometrycznych trocin, drewna jesionowego niemodyfikowanego (Fraxinus exelsior L.) i modyfikowanego termicznie, otrzymanych w procesie przecinania drewna na pilarce ramowej wielopiłowej PRW15-M. Przecinanie drewna prowadzono dla dwu prędkości posuwu 0,36 m·min-1 oraz 1,67 m·min-1. Ziarnistośćpowstających trocin dla drewna jesionowego modyfikowanego termicznie zawierała się w przedziale od 33,5 μm...
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Some of Challenges Faced by Eco-Neighbourhoods in Poland in Comparison with EcoQuartier Program in France
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Spectral and photophysical properties of some imidazo[1,2-a]purine derivatives related to acyclovir
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The Oxolane Ring Opening of Some Muramic Acid Derivatives Under Acidic Conditions
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Synthesis, spectroscopy and computational studies of some biologically important hydroxyhaloquinolines and their novel derivatives
PublicationA series crystalline compounds of methyl and phosphinyl derivatives of 2-methylquinolin-8-ol (1a) and related 5,7-dichloro-2-methylquinolin-8-ol (1b) were quantitatively prepared and characterized by microanalysis, IR, UV-vis and multinuclear NMR spectroscopy. Five of them have been characterized by single crystal X-ray diffraction method. The known compounds, 8-methoxy-2-methylquinoline (2a) and 8-methoxyquinoline (2d), were synthesised...
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Isolation and some properties of collagen from the backbone of Baltic cod(Gadus morhua)
PublicationOssein from Baltic cod backbone was obtained after extraction of non-collagenous protein with 0.1 M NaOH solution and demineralization with 1.0 M HCl solution. The extractions were performed at 4 C for24, 48 and 72 h using a solid/solution ratio from 1:4 to 1:8 (w/v). After 48 h of extraction in 0.5 M acetic acid only about 25% of collagen was dissolved. After 48 h of extraction at optimal concentration of pepsin(4 mg/g ossein)...
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Synthesis, spectroscopy and computational studies of some novelphosphorylated derivatives of quinoline-5,8-diones
PublicationThe neutral phosphorus nucleophiles such as R2P(=Y)M allowed the radical addition to 2-methyl-5,8-dioxo-5,8-dihydroquinoline-7-amine and N-(2-methyl-5,8-dioxo-5,8-dihydroquinolin-7-yl)acetamide giving exclusively O-phosphorylated products. All products were quantitatively prepared and characterized by microanalysis, and multinuclear NMR spectroscopy. Seven of them, have been characterized by single crystal X-ray diffraction method....
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Influence of the extraction mode on the yield of some furanocoumarins from Pastinaca sativa fruits
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Maritime transportation risk analysis: Review and analysis in light of some foundational issues
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Links between Faith and Some Strengths of Character: Religious Commitment Manifestations as a Moderators
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On the inappropriate fit of diffusion functions at thermal decomposition of some azomonoethers in liquid state
PublicationW celu analizy rozkładu termicznego tytułowych barwników azowych zastosowano mechanizmy D1, D2, D3 i D4. W wyniku przeprowadzonych badań stwierdzono, że rozkład zachodzi w fazie ciekłej, zaś w celu wyznaczenia parametrów aktywacji oraz wyznaczenia funkcji przemiany zastosowano koncepcje homo- i heterogeniczne.
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Activity evaluation of some psychoactive drugs with the application of QSAR/QSPR modeling methods
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Studies of the complex formation between some proton sponges and Cu(II) cations
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Effect of pH and high pressure at sub-zero temperature on the viability of some bacteria
PublicationCelem badań było określenie przeżywalności Escherichia coli i Staphylococcus aureus zawieszonych w soku jabłkowym (pH 3,8) po działaniu ciśnienia 193MPa w temperaturze -20°C. Stwierdzono, że bezpośrednio po działaniu ciśnienia przeżywalność badanych szczepów bakterii nie zmieniała się znacząco. Jednakże liczba komórek zmniejszała się z czasem przechowywania ciśnieniowanych prób. Żywe komórki mikroorganizmów nie były wykrywane w...
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Acoustic streaming caused by some types of aperiodic sound. Buildup of acoustic streaming
PublicationThe analysis of streaming caused by aperiodic sound of different types (switched on at transducer sound or sound determined by initial conditions) is undertaken. The analysis bases on analytical governing equation for streaming Eulerian velocity, which is a result of decomposition of the hydrodynamic equations into acoustic and non-acoustic parts. Its driving force (of acoustic nature) represents a sum of two terms; one is the...
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Efficient three-dimensional fluorescence measurements for characterization of binding properties in some plants
PublicationThe main aim of this research was to characterize some plants and to determine their similarities and differences, using spectroscopic methods. The interactions of soluble polyphenols of different plants with human serum albumin (HSA) were investigated by 3D-fluorescence. The obtained fluorescence results allow to classify the investigated plants according to their binding properties. The HSA-binding capacities of these plants...
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Modelling of some stealth features for a small navy ship at the concept design stage.
PublicationIn this paper the basic research problems associated with modelling the basic stealth features for a small navy ship at the concept design stage are introduced. Amongst the major stealth features considered are: the modification of the immersed ship hull form by a rapid change of the ship loading condition, and modification of the ship boundary layer by the hull skin cover. The other stealth features of the ship are not presented...
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Specificity of Infant Digestive Conditions: Some Clues for Developing Relevant In Vitro Models
PublicationDigestion of nutrients is an essential function of the newborn infant gut to allow growth and development and understanding infant digestive function is essential to optimize nutrition and oral drug delivery. Ethical considerations prohibit invasive in vivo trials and as a consequence in vitro assays are often conducted. However, the choice of in vitro model parameters are not supported by an exhaustive analysis of the literature...
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Hysteresis curves and loops for harmonic and impulse perturbations in some non-equilibrium gases
PublicationEvolution of sound in a relaxing gas whose properties vary in the course of wave propagation, is studied. A relaxing medium may reveal normal acoustic properties or be acoustically active. In the first case, losses in acoustic energy lead to an increase in internal energy of a gas similarly as it happens in Newtonian fluids. In the second case, acoustic energy increases in the course of sound propagation, and the internal energy...
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Cavitation erosion of some alloys manufactured on steel and iron surfaces by laser beam.
PublicationPrzedstawiono badania odporności kawitacyjnej stali węglowej 45 odpornej na korozję 2H13 i technicznego żelaza po ich obróbce laserowej. Warstwę wierzchnią wybranych stali wzbogacono w różne pierwiastki stopowe i badano odporność kawitacyjną na stanowisku z wirującą tarczą. Stwierdzono niską odporność kawitacyjną dla warstw o obniżonej zdolności do utwardzania pod wpływem obciążeń kawitacyjnych oraz silną zależność odporności...
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Some remarks about numerical stability in nonlinear dynamics on the basic of truss structures.
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Structural properties of water: Comparison of the SPC, SPCE, TIP4P and TIP5P models of water
PublicationDla czterech najpopularniejszych modeli wody obliczono wartości entropii absolutnej ciekłej wody w temperaturze 298 K, średnią liczbę wiązań wodorowych tworzonych przez cząsteczkę wody, średni czas życia wiązania wodorowego, średni czas życia cząsteczki wody w stanie związanym (gdy tworzy ona co najmniej jedno wiązanie wodorowe) oraz średnią energię wiązania wodorowego. Otrzymane rezultaty porównano z eksperymentem. Uzyskane wyniki...
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Some integrals and series involving the Gegenbauer polynomials and the Legendre functions on the cut (-1,1)
PublicationZaprezentowano metode obliczenia dwóch całek oznaczonych zawierających wielomiany Gegenbauera. Wynik wykorzystano do znalezienia sum czterech szeregów o wyrazach zawierających wielomiany Gegenbauera oraz funkcje Legendre'a (pierwszego lub drugiego rodzaju) na odcinku (-1,1).
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Effect of high pressure and sub-zero temperature on some gram-negative bacteria.
PublicationCelem pracy było określenie przeżywalności wybranych gramujemnych bakterii na działanie wysokiego ciśnienia i ujemnej temperatury. Traktowanie komórek bakterii ciśnieniem 193 MPa w temperaturze -20C przez 24 godziny, powodowało całkowitą inaktywację bakterii E. coli, P. fluorescens i T. thermophilus. Po działaniu ciśnienia przez krótszy czas występowały różnice we wrażliwości między badanymi szczepami. Najmniej odporny na działanie...
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Investigation of some taste substances using a set of electrodes with lipid-modified membranes.
PublicationSkonstruowano 5-cio kanałaowy sensor smaku oparty na elektordach jonoselektywnych z membranami polimerowymi modyfikowanymi lipidem. Badano potencjał elektrod w roztworach kwaśnych zawierających różne stężenie kwasu cytrynowego, solnego i octowego. Sensor jest czuły na stężenia substancji kwaśnych z wyjątkiem kwasu octowego. Testowano nowy typ elektrod zawierających polimer przewodzący PEDT/PSS i kwas oleinowy. Stwierdzono, że...
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Cavitation erosion of some laser-produced iron-base corrosion-resistance alloys
PublicationW pracy przedstawiono badania kawitacyjne stali C45, X20Cr13 oraz X5CrNi18-10 po laserowym stopowaniu ich warstwy wierzchniej proszkami Mn, Cr, Ni, Si, Ti, Co, Al, Mo, B. Badania kawitacyjne prowadzono na stanowisku z wirującą tarczą. Zniszczenia powierzchni w okresie inkubacji oceniano metodą optyczną. Przedstawiono związek pomiędzy uzyskaną mikrostrukturą obrabianej warstwy i jej odpornością kawitacyjną.
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Some fundamental aspects of self-levitating sliding contact bearings and their practical implementations
PublicationIn this study, fundamental aspects and mechanisms of acoustic levitation together with governing equations are presented first. Then, the acoustic levitation phenomenon is considered as a new way to design air suspension systems capable of self-levitation. A particular emphasis is laid on journal bearings and their specific geometrical configuration. A practical feasibility of using acoustic levitation to separate contacting surfaces...
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Some Artificial Intelligence Driven Algorithms For Mobile Edge Computing in Smart City
PublicationSmart mobile devices can share computing workload with the computer cloud that is important when artificial intelligence tools support computer systems in a smart city. This concept brings computing on the edge of the cloud, closer to citizens and it can shorten latency. Edge computing removes a crucial drawback of the smart city computing because city services are usually far away from citizens, physically. Besides, we introduced...
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Study on some of the strength properties of soft clay stabilized with plastic waste strips
PublicationIt is well known that if plastic wastes are not well managed, it has a negative impact on the environment as well as on human health. In this study, recycling plastic waste in form of strips for stabilizing weak subgrade soil is proposed. For this purpose, a weak clay soil sample was mixed with 0.2%, 0.3%, and 0.4% of plastic strips by weight of soil, and the experimental results were compared to the control soil sample with 0%...
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Effect of Laser Treatment on Intrinsic Mechanical Stresses in Titanium and Some of Its Alloys
PublicationLaser surface treatment conducted at different power levels is an option to modify titanium bone implants to produce nano- and microtopography. However, such processing can lead to excess mechanical stress within the surface layer. This research aims to calculate the level of such residual stresses after the surface processing of Ti grade IV, Ti15Mo, and Ti6Al7Nb alloys with an Nd:YAG laser. Light and scanning electron microscopies...