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Studies on the solid-liquid equilibria and intermolecular interactions Urea binary mixtures with Sulfanilamide and Sulfacetamide
PublicationThe binary phase diagrams of Sulfanilamide-Urea (SN-U) and Sulfacetamide-Urea (SC-U) were measured using differential scanning calorimetry technique (DSC). Both examined mixtures were found to form simple binary eutectics. The limited miscibility in the solid state observed by DSC, proving inability of co-crystallization in new multi-molecular form, was also confirmed using PXRD and FTIR-ATR measurements of solid dispersions...
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Evaluation of the photoprotective effect of β-cyclodextrin on the emission of volatile degradation products of ranitidine
PublicationThe process of the photo-excitation of ranitidine hydrochloride (RAN) in a solid state makes visible changes to its colour and generates an unpleasant odour. The purpose of the present study was to observe the protective effects of ˇ-cyclodextrin (CD) complexation as well as the effect of the mixture of two stoichiometries 1:1 and 1:2 (RAN:CD, IC) on the photostability of samples in a solid state. Samples of inclusion complexes...
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Evaluation of the photoprotective effect of ˇ-cyclodextrin on the emission of volatile degradation products of ranitidine
PublicationThe process of the photo-excitation of ranitidine hydrochloride (RAN) in a solid state makes visible changes to its colour and generates an unpleasant odour. The purpose of the present study was to observe the protective effects of ˇ-cyclodextrin (CD) complexation as well as the effect of the mixture of two stoichiometries 1:1 and 1:2 (RAN:CD, IC) on the photostability of samples in a solid state. Sam- ples of inclusion complexes...
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GTR/Thermoplastics Blends: How Do Interfacial Interactions Govern Processing and Physico-Mechanical Properties?
PublicationIn this work, GTR/thermoplastics blends (in ratio 50/50 and 75/25 wt.%) were prepared by melt-compounding in an internal mixer. During research, trans-polyoctenamer rubber (TOR), ethylene-vinyl acetate copolymer (EVA), ethylene-octene copolymer (EOC), and linear low-density polyethylene (LLDPE), were used in their thermoplastic phase. Microstructure and processing-performance property interrelationships of the studied materials...
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In-Out Surface Modification of Halloysite Nanotubes (HNTs) for Excellent Cure of Epoxy: Chemistry and Kinetics Modeling
PublicationIn-out surface modification of halloysite nanotubes (HNTs) has been successfully performed by taking advantage of 8-hydroxyquinolines in the lumen of HNTs and precisely synthesized aniline oligomers (AO) of different lengths (tri- and pentamer) anchored on the external surface of the HNTs. Several analyses, including FTIR, H-NMR, TGA, UV-visible spectroscopy, and SEM, were used to establish the nature of the HNTs’ surface engineering....
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A novel approach for processing CaAlSiON glass-ceramics by spark plasma sintering: Mechanical and electrical properties
PublicationLithium containing glassy materials can be used as solid electrolytes or electrode materials for lithium-ion batteries due to their high energy density. Conventional melt-quenched Ca11Al14Si16O49N10 glass powder containing 24 e/o N, doped with Li-ions (1, 3, and 6 wt. %) and sintered by spark plasma sintering technique (SPS) was studied. The benefits of using SPS to produce glass-ceramics are rapid heating rates compared to conventional...
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Ground lemon and stevia leaves as renewable functional fillers with antioxidant activity for high-density polyethylene composites
PublicationThe development of new sustainable material solutions in the processing of thermoplastic polymers concerns both the application of biopolymers and the use of valorized plant derivatives as fillers and modifiers of petrochemical polymers. Herein, the possibility of using unprocessed raw parts of two commonly used in the food industry leaves, i.e., lemon (LL) and stevia (ST), as active and functional fillers for high-density polyethylene...
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Design Optimization of an Anisotropic Magnetoresistance Sensor for Detection of Magnetic Nanoparticles
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Różne subpopulacje komórek dendrytycznych oraz sposoby regulowania ich aktywności
PublicationOpisano komórki dendrytyczne (DC), stanowiące złożoną, heterogenną populację leukocytów wywierającą różnorodny efekt na funkcjonowanie systemu odpornościowego.
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Monitoring ramanowski wzrostu cienkich warstw węglowych-studium
PublicationPrzedstawiono zagadnienia monitorowania in-situ prózniowego procesu wzrostu cienkich warstw węglowych, a w szczególności diamentowych i diamentopodobnych DLC. Zastosowanie pomiarów ramanowskich umożliwia zbadanie struktury warstwy na poziomie molekularnych (zawartości faz węglowych sp2 i sp3, a także defektów wodorowych). Użycie spektroskopii in-situ podczas procesu syntezy pozwala monotorować poprawność przebiegu procesu i opracować...
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Kinetics and mechanism of the chemically modified starches during gelatinization.
PublicationNative starch was silicated by means of microwave-assisted reactions with varying doses of reagents. Resulting products were characterized by DSC and HMR-relaxation methods. It was observed that the hydratation of the silicated starches during gelatinization decreases when compared to that of the native potato starch. The amount of unfrozen water for ungelitinizated silicated starches are less than in control samples. At the same...
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Assessment of copper surface coverage with corrosion inhibitor using AFM-based local electrical measurements
PublicationThe paper presents a new method of assessment of metal surface coverage with corrosion inhibitor and thus of inhibitor protective performance. It is based on the atomic force microscopy measurement performed in a contact mode. Apart from topography images the proposed approach allows acquisition of local DC maps and local electrical impedance spectra via application of DC bias voltage or AC perturbation signal between the conductive...
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Impedance Studies of Phosphate-iron Glasses Containing Niobium and Titanium
PublicationThe ac and dc conductivity in phosphate-iron-niobate glasses with addition of titanium oxide was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD), scanning electron microscopy (SEM), and confocal microscopy methods. The obtained results show that all samples are amorphous but they...
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Collagen Type II—Chitosan Interactions as Dependent on Hydroxylation and Acetylation Inferred from Molecular Dynamics Simulations
PublicationChitosan–collagen blends have been widely applied in tissue engineering, joints diseases treatment, and many other biomedical fields. Understanding the affinity between chitosan and collagen type II is particularly relevant in the context of mechanical properties modulation, which is closely associated with designing biomaterials suitable for cartilage and synovial fluid regeneration. However, many structural features influence...
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A novel hierarchically-porous diamondized polyacrylonitrile sponge-like electrodes for acetaminophen electrochemical detection
PublicationA novel composite electrode material consisting of tangled fibrous polyacrylonitrile-based hierarchically-struc- tured nanocomposites has been produced by wet-spinning, carbonized and decorated with a carbon nano- architecture by microwave plasma-enhanced chemical vapor deposition and investigated as a metal-free electrode for the enhanced electrochemical detection of acetaminophen. Surprisingly, the hierarchical fiber ar- chitecture...
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Is the Fatty Acids Profile in Blood a Good Predictor of Liver Changes? Correlation of Fatty Acids Profile with Fatty Acids Content in the Liver
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Meander anisotropic magnetoresistance bridge geomagnetic sensors
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Structural studies and melting of bismuth nanocrystals in reduced bismuthgermanate and bismuth silicate glasses.
PublicationOtrzymano nanostruktury krystalicznego bizmutu w matrycy XO2 (X=Si,Ge) oraz warstwę nanostruktur krystalicznego bizmutu na powierzchni redukowanych w atmosferze wodoru szkieł Bi0.33Ge0.67O1.84 i Bi0.57Si0.43O1.72. Kompozyt Bi-szkło badano metodą DSC, XRD oraz AFM. Zaobserwowano zmniejszenie temperatury topnienia nanokrystalicznego bizmutu znajdującego się w matrycy szkła z 544 K do 387 K oraz do 502 K w przypadku powierzchniowej...
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Decentralized control of a different rated parallel UPS systems
PublicationThe paper presents the single phase uninterruptible power supply (UPS) system with galvanic separated DC-AC-DC-AC converters operating in parallel. The CAN physical layer based system of communication between converters has been developed and applied, which allow to utilize a decentralized master-slave control providing high availability factor of the whole UPS system. The control system of particular converters has been developed...
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Power electronic transformer based on cascaded H-bridge converter
PublicationIn this paper the control strategy of power electronic transformer (PET) is proposed. The analyzed structure of PET uses two seven-level cascaded H-bridge (CHB) rectifiers. The electrical power of PET is transferred between DC-links of CHB converters using dual-active-bridges (DABs) and low voltage high frequency transformers. The roposed solution allows for controlling the active and reactive power with a low level of harmonic...
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Microstructure and Dielectric Properties of Barium-vanadate Glasses
PublicationThe ac and dc conductivity in barium-vanadate glasses was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD) and scanning electron microscopy (SEM) methods. The XRD results show that all samples are amorphous but microscopy investigation reveals that glasses with greater amount of V2O5...
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Modified SPWM Technique with Zero-Sequence Voltage Injection for a Five-Phase, Three-Level NPC Inverter
PublicationThis article presents a modified sinusoidal pulse-width modulation (SPWM) scheme for a five-phase, three-level neutral-point-clamped inverter. The modulation scheme deploys a modified min–max function to inject the zero-sequence components into the reference modulating signals; hence enabling the effective utilization of the DC-link voltage. Balanced split-input DC-link voltages were achieved through further incorporation of adjustable...
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The Influence of Fluorine on the Disturbances of Homeostasis in the Central Nervous System
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Fluoride as a factor initiating and potentiating inflammation in THP1 differentiated monocytes/macrophages
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Jednofazowy falownik napięcia z aktywnym obwodem odsprzęgającym
PublicationZnanym zagadnieniem w jednofazowych falownikach napięcia jest pobieranie ze źródła napięcia stałego składowej przemiennej o częstotliwości dwukrotnie większej od częstotliwości generowanej przez falownik. Jednym z rozwiązań problemu jest stosowanie dużej baterii kondensatorów elektrolitycznych, lecz lepszym sposobem z punktu widzenia niezawodności i gęstości mocy przekształtnika jest stosowanie aktywnych układów odsprzęgania mocy....
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Daily diet containing canned products significantly increases serum concentrations of endocrine disruptor bisphenol A in young women
PublicationNowadays, exposure to environmental factors is considered to be one of the possible causes of several lifestyle diseases, such as obesity, type 2 diabetes, cardiovascular disease, and cancer. Particularly noteworthy are endocrine‑disrupting chemicals (EDCs), which affect the metabolism of hormones and interact with their receptors, thus exerting adverse health effects. One of the most ubiquitous EDC in daily life is bisphenol A...
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Structural, magnetic and spectral properties of tetrahedral cobalt(II) silanethiolates: a variety of structures and manifestation of field-induced slow magnetic relaxation
PublicationBlue crystals of five heteroleptic cobalt(II) silanethiolates 1–5 have been obtained by the reaction of [Co{SSi (tBuO)3}2(NH3)]2 with aminopyridines and aminomethylpyridines at an appropriate molar ratio and their structural, spectral, thermal and magnetic properties have been established and described. All complexes 1–5 contain Co(II) ions in a tetrahedral CoN2S2 environment formed by (tBuO)3SiS− residues and pyridines and present...
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Computer-Aided Detection of Hypertensive Retinopathy Using Depth-Wise Separable CNN
PublicationHypertensive retinopathy (HR) is a retinal disorder, linked to high blood pressure. The incidence of HR-eye illness is directly related to the severity and duration of hypertension. It is critical to identify and analyze HR at an early stage to avoid blindness. There are presently only a few computer-aided systems (CADx) designed to recognize HR. Instead, those systems concentrated on collecting features from many retinopathy-related...
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Optoelektroniczny monitoring stanu wzbudzenia plazmy niskotemperaturowej w procesach syntezy optycznych warstw diamentopodobnych
PublicationZrealizowana praca jest jednym z głównych zadań wieloletniego projektu badawczego z zakresu syntezy warstw diamentopodobnych. Celem bezpośrednim pracy było określenie rozkładu wzbudzenia plazmy w komorze technologicznej stanowiska PA ECR CVD. Głównym celem było opracowanie optoelektronicznego systemu pomiarowego, na którego potrzeby zastosowano przestrzennie selektywną optyczną spektroskopię emisyjną dedykowaną do badania procesu...
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Organic carbon fluxes of a glacier surface: a case study of Foxfonna, a small Arctic glacier
PublicationArctic glaciers are rapidly responding to global warming by releasing organic carbon (OC) to downstream ecosystems. The glacier surface is arguably the most biologically active and biodiverse glacial habitat and therefore the site of important OC transformation and storage, although rates and magnitudes are poorly constrained. In this paper, we present measurements of OC fluxes associated with atmospheric deposition, ice melt,...
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Buck-Boost Inverters with Symmetrical Passive Four-terminal Networks
PublicationAlternating Voltage Inverters (Converters) supplied by low-voltage sources DC (ex. fuel cell, photovoltaic cell) are most frequently realized on the basis of the three fundamental topologies: a) PWM voltage inverter with boost-converter" system, b) PWM voltage inverter with transformed converter DC/DC in the ,,boost-converter" system, c) PWM current converter. However none of these solutions is claimed to be the best and dominant...
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Przegląd systemów ładowania elektrycznych osobowych pojazdów i koncepcja dwukierunkowej ładowarki pokładowej
PublicationAktualnie trwa intensywny rozwój pojazdów elektrycznych (EV) i hybrydowych typu plug-in (PHEV) z pokładowymi bateriami akumulatorów. Badania w tej dziedzinie skupiają się na maksymalizowaniu sprawności oraz minimalizowaniu masy i objętości systemów ładowania baterii. W artykule przedstawiono podział systemów ładowania osobowych pojazdów typu EV/PHEV. Opisano systemy ładowania przewodowego z podziałem na ładowarki pokładowe i zewnętrzne, systemy...
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Układ wspomagania sterowania maksimum mocy modułów fotowoltaicznych
PublicationW artykule przedstawiono układ wspomagania sterowania mocą pobieraną z modułu fotowoltaicznego. Na wstępie przedstawiono i omówiono model ogniwa fotowoltaicznego. Następnie, bazując na właściwościach modułów fotowoltaicznych zaproponowano układ wspomagający system mikrokontrolera w sterowaniu przetwornicą impulsową DC/DC. W części końcowej przedstawiono wstępne wyniki pomiarów wykonanego układu prototypowego. Badany układ prototypowy...
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Power Electronic Transformer For Smart Grid Application
PublicationIn this paper the control system of Power Electronic Transformer (PET) for the Smart Grid application is proposed. The structure of PET is based on two Cascaded H-bridge (CHB) converters. The electrical energy is transferred between converters using Dual-Active-Bridges (DAB) and high-frequency transformers. This type of coupling has been used to connect the DC-links of all H-bridges. The proposed control system for PET makes it...
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The QDMC Model Predictive Controller for the Nuclear Power Plant Steam Turbine Control
PublicationThere are typically two main control loops with PI con trollers operating at each turbo-generator set. In this paper a model predictive controller QDMC for the steam turbine is proposed - instead of a typical PI controller. The QDMC controller utilize a step-response model for the controlled system. This model parameters are determined, based on the simplified and linear model of turbo-generator set, which parameters are identified...
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Preparation, characterization and antimicrobial activity of polyvinyl alcohol/gum arabic/chitosan composite films incorporated with black pepper essential oil and ginger essential oil
PublicationIn this study, biocomposite films based on polyvinyl alcohol (PVA), gum arabic (GA) and chitosan (CS) incorporated with BPEO and GEO were fabricated by solvent casting method. FTIR, XRD, SEM and DSC were performed with mechanical and antimicrobial properties of PVA/GA/CS films with and without BPEO and GEO. The BPEO and GEO incorporated PVA/GA/CS films were significantly inhibited the growth of Bacillus cereus, Staphylococcus aureus,...
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A simple access to o-acyl bicyne
PublicationW publikacji przedstawiono prostą metodę otrzymywania o-acylowych pochodnych bicyny. Substratem do syntezy była n,n-bis(2-hydroksyetylo)glicyna - bicyna. Bicynę najpierw przeprowadzano w ester benzylowy w reakcji z alkoholem benzylowym i kwasem p-toluenosulfonowym w temp. 75 st. C. Tak otrzymany związek, acylowano kwasami organicznymi w obecności DCC ( dicyklokeksylokarbodiimid)i DMAP (dimetyloaminopirydyna), otrzymując o-acylowe...
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A novel dual-band rectifier circuit with enhanced bandwidth for RF energy harvesting applications
PublicationIn recent years, a rapid development of low-power sensor networks, enabling machine-to-machine communication in applications such as environmental monitoring, has been observed. Contemporary sensors are normally supplied by an external power source, typically in a form of a battery, which limits their lifespan and increases the maintenance costs. This problem can be addressed by harvesting and converting ambient RF energy into...
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Performance of the PEM fuel cell module. Part 2. Effect of excess ratio and stack temperature
PublicationThe paper describes a fuel cell based system performance under different thermal conditions. The system could be fed with bottled hydrogen or with very high purity hydrogen obtained from reforming of methanol. The system is based on two fuel cell units (1.2 kW each, produced by Ballard Power Systems Inc. and called Nexa), DC/DC converter, DC/AC inverter, microprocessor control unit, load unit, bottled hydrogen supply system and...
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Evaluation of organic coatings condition with AFM-based method
PublicationThe paper presents an atomic force microscopy (AFM)-based approach to evaluation of local protective properties of organic coatings. Apart from topography, it provides local ac and dc characteristics of examined coating. The method consists in application of ac voltage perturbation signal between conductive AFM tip and coated metal substrate. The resulting current is used to determine local impedance characteristics. Both impedance...
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Eicosanoids in Nonalcoholic Fatty Liver Disease (NAFLD) Progression. Do Serum Eicosanoids Profile Correspond with Liver Eicosanoids Content during NAFLD Development and Progression?
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Effect of the Yerba mate (Ilex paraguariensis) brewing method on the content of selected elements and antioxidant potential of infusions
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Thermoplastic polyurethane/(organically modified montmorillonite) nanocomposites produced by in situ polymerization
PublicationA series of polyurethane nanocomposites were synthesized from thermoplastic polyurethanes (with different hard segment ratios) and two types of organically modified montmorillonites (OMMT) - Cloisite® 10A and Cloisite® 20A. The thermal behavior was examined by non-isothermal thermogravimetry (TG, DTG), Differential Scanning Calorimetry (DSC) and Dynamic-Mechanical Thermal Analysis (DMTA). The results of X-ray analyses showed that...
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Considerations of Adaptive Digital Communications in Underwater Acoustic Channel
PublicationDown-link communication (DLC) and air transportable communication (ATAC) buoys as well as autonomous underwater vehicles (AUV) use acoustic links for gathering oceanographic data from underwater monitoring systems. The underwater channel propagation conditions are diverse in nature and require a special adaptive approach to the communication system design. The article presents a methodology for the communication systems design,...
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Kinetics of cross-linking processes of fast-curing polyurethane system
PublicationThis work focuses on the application of thermal analysis and kinetics investigations to analyze chemical processes during cross-linking of the complex fast-curing polyurethane system. Non-isothermal Differential Scanning Calorimetry (DSC) measurements were performed for both stoichiometric mixtures of polyol and isocyanate component and for mixture with large isocyanate excess. Isoconversional methods were used to calculate initial...
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Badanie wpływu temperatury i czasu wygrzewania na właściwości elastomerów uretanowych.
PublicationOpisano syntezę lanych elastomerów uretanowych metodą prepolimerową oraz wyniki pomiarów właściwości otrzymanych polimerów poddanych wygrzewaniu w krótkich czasach w jednej z trzech temperatur: 100, 110 i 120 st. C. Do oceny właściwości termicznych zastosowano metodę DSC i DMT. Stabilność termiczną zbadano za pomocą TGA. Właściwości mechaniczne oznaczono przy użyciu maszyny wytrzymałościowej. Ustalono, że za optymalny czas wygrzewania...
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Tam gdzie fikcja spotyka się z rzeczywistością
PublicationNa tyłach budynku A Wydziału Elektroniki, Telekomunikacji i Informatyki (tego z zerami i jedynkami na elewacji) mieści się laboratorium odmienne wyglądem od innych laboratoriów politechnicznych. Zajmuje ono sięgającą czwartego piętra czarną sześcienną kostkę dobudowaną 10 lat temu w bezpośrednim sąsiedztwie audytorium, któremu od dwóch lat patronuje doc. Marianna Sankiewicz, przysiadłszy na ławeczce przed jego wejściem. Wydaje...
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Implementation of constant component filter in measurements of random telegraph signal noise
PublicationNoise is generated in all semiconductor devices. The intensity of these fluctuations depends on used elements, manufacturing process, operating conditions and device type. The result noise is a superposition of different kinds of fluctuations like thermal noise, generation-recombination noise, 1/f noise, shot noise and Random Telegraph Signal (RTS) noise. The last one, RTS noise is observed as nonstationary impulse fluctuations....
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CM Voltage Compensators for Power Electronic Interfaces
PublicationThe experimental results presented in the paper have shown that the application of the PEIs might cause EMC related problems, especially in the case of the application of a group of connected converters. The most convenient way to reduce EMI currents and prevent aggregation of EMI currents introduced by a group of converters is through passive compensation of voltage interference sources inside of the single converters. In the...
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Design and experimental validation of a single-stage PV string inverter with optimal number of interleaved buck-boost cells.
PublicationIncreasing converter power density is a problem of topical interest. This paper discusses an interleaved approach of the efficiency increase in the buck-boost stage of an inverter with unfolding circuit in terms of losses in semiconductors, output voltage ripples and power density. Main trends in the power converter development are reviewed. A losses model was designed and used for the proposed solution to find an optimal number...