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Search results for: BIS-TETRAZOLE
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Cooperativity of Halogen- and Chalcogen-Bonding Interactions in the Self-Assembly of 4‑Iodoethynyl- and 4,7-Bis(iodoethynyl)benzo-2,1,3-chalcogenadiazoles: Crystal Structures, Hirshfeld Surface Analyses, and Crystal Lattice Energy Calculations
PublicationSeveral new 4-iodoethynyl- and 4,7-bis- (iodoethynyl)benzo-2,1,3-chalcogenadiazoles were prepared, and a comprehensive analysis of the most prominent secondary bonding interactions responsible for the crystal self-assembly was performed using X-ray diffraction. The presence of both the iodoethynyl and chalcogenadiazole moieties allows an evaluation of the preference of these molecules to aggregate through either chalcogen- or halogen-bonding...
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Wydawnictwo Agade Bis Magdalena Kapełuś
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Big Beautiful Buildings: Eine Schönheit, viele Maßstäbe - urbane Landschaften der Nachkriegsmoderne in Europa / Big Beautiful Buildings: one beauty, many scales - urban landscapes of the post-war modernism across Europe
PublicationMassive urbanization in Europe is not a phenomenon that began only in the 20th century. The roots of this process can be traced back two centuries. With the end of the Second World War the specific conjunction of powerful forces together changed the landscape of European cities. Urbanization was undoubtedly one of them. Among other factors, Musterd and van Kempen (2005) correctly itemized not only objective processes that can be...
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Overproduction of CaMet15p native and His-tag versions.
Open Research DataEnzyme of fungal L-methionine biosynthetic pathway: O-acetylhomoserine sulfhydrylase (Met15p) could be exploited as molecular target for antifungal chemotherapy. The goal of the study was to obtain conditions optimal for protein production with the use of prokaryotic cells. The constructed expression plasmids, designed in three different versions: encoding...
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Overproduction of CaStr2p native and His-tag versions.
Open Research DataEnzyme of fungal L-methionine biosynthetic pathway: cystathionine-γ-synthase (CaStr2p) could be exploited as molecular target for antifungal chemotherapy. The goal of the study was to obtain conditions optimal for protein production with the use of prokaryotic cells. The constructed expression plasmids, designed in three different versions: encoding...
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Ultrastructure of the bovine testis in cattle (Bos Taurus)
Open Research DataThe data present research results being part of the OPUS-22 project entitled “In search of new markers of male fertility in cattle. Aquaporins expression in the reproductive organs and sperm of the bulls (Bos taurus)” obtained from the National Science Center in Poland (grant no. 2021/43/B/NZ9/00204).
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XRD patterns of TeOx-BaO-BiO powder
Open Research DataThe DataSet contains the XRD patterns of the TeOx-BaO-BiO powder. The material was obtained by the sol-gel method. The starting solution was prepared by mixing telluric acid (precursor), barium carbonate, and bismuth carbonate with thetraetylene glycol, water, ethanol, and acetic acid. (Samples molar concentration: 73TeO2-4BaO-3Bi2O3 and 73TeO2-3BaO-4Bi2O3)....
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Hydrogen-bonded one-dimensional networks in 1:1 complexes of N,N`-bis(2-pi-rydyl)aryldiamines with anilic acid. Acta Cryst. Sect. C Crystal Struct.Commun.**2002 vol. 58 s. o735-o738, 4 rys. 4 tab. bibliogr. 15 poz. Jednowymiarowe sieci krystaliczne tworzone w wyniku oddziaływań wodorowych pomiędzy N,N`-bis(2-pirydylo)aryloaminami a kwasem anilowym.
PublicationOtrzymano związki kompleksowe kwasu anilowego z N,N`-bis(2-pirydylo)-1,4-diaminobenzenem oraz N,N`-bis(2-pirydylo)-4,4`-diaminobifenylem o stechiometrii1:1, a następnie przeprowadzono analizę rentgenograficzną monokryształów. Wobu przypadkach cząsteczki, wchodzące w skład kompleksu są powiązane ze sobąkonwencjonalnymi oddziaływaniami wodorowymi. Tym samym tworzy się jednowy-miarowa sieć krystaliczna z dziewięcioczłonowym pierścieniowym...
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Superconductivity on a Bi Square Net in LiBi
PublicationWe present the crystallographic analysis, superconducting characterization and theoretical modeling of LiBi, that contains the lightest and the heaviest nonradioactive metal. The compound crystallizes in a tetragonal (CuAu-type) crystal structure with Bi square nets separated by Li planes (parameters a = 3.3636(1)Å and c = 4.2459(2) Å, c/a = 1.26). Superconducting state was studied in detail by magnetic susceptibility and heat...
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High-performance liquid chromatography of di- and trisubstituted aromatic positional isomers on 1,3-alternate 25,27-dipropoxy-26,28-bis-[3-propyloxy]-calix[4]arene-bonded silica gel stationary phase.
PublicationOtrzymano nową fazę stacjonarną na bazie dipropyloksy pochodnej kaliks[4]arenu w konformacji 1,3-naprzemianległej chemicznie związaną z żelem krzemionkowym. Przeprowadzono badanie selektywności i sprawności tej fazy w rozdzielaniu izomerów konstytucyjnych benzenu. Zaprezentowano wyniki badania wpływu warunków chromatograficznych (pH fazy ruchomej, temperatura, stężenie modyfikatora organicznego) na zdolność rodzielczą tej nowej...
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Experimental and computational study on the reactivity of 2,3-bis[(3-pyridylmethyl)amino]-2(Z)-butene-1,4-dinitrile, a key intermediate for the synthesis of tribenzoporphyrazine bearing peripheral methyl(3-pyridylmethyl)amino substituents
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Maritime awareness and emergency management real time system using remotely accessible GIS technology
PublicationPrzedstawiono koncepcję oraz prototyp morskiego GIS do zdalnego monitorowania w czasie rzeczywistym zanieczyszczeń środowiska morskiego. System pozwala na gromadzenie i integrowanie różnych typów danych dotyczących zanieczyszczeń, pozyskiwanych na bieżąco za pomocą wielorakiego rodzaju sensorów, w tym akustycznych (echosondy jednowiązkowe i wielowiązkowe). Zadaniem systemu jest wizualizacja oraz mapowanie zanieczyszczeń, takich...
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Toxicity of aqueous mixture of phenol and chlorophenols upon photosensitized oxidation initiated by sunlight or vis-lamp
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Development of New UV–vis Spectroscopic Microwave-Assisted Method for Determination of Glucose in Pharmaceutical Samples
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Some methods of diagnosis of analog circuit using mixed signal test bus IEEE 1149.4
PublicationW artykule przedstawiono wybrane metody testowania i diagnostyki analogowych układów elektronicznych zamontowanych na pakiecie pomiędzy układami scalonymi wyposażonymi w magistralę IEEE 1149.4. Prezentowane metody dobrano pod kątem stopnia skomplikowania układów testowanych oraz specyficznych właściwości metrologicznych magistrali, które ograniczają możliwości pomiarowe i aplikacyjność metod. Rozważono trzy typy układów testowanych:...
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What makes them dream big? Determinants of business growth aspirations among Polish students
PublicationThe objective of the article is to explore the concept of business growth aspirations and identify its determinants at an early stage of the entrepreneurial process. In this exploratory study, I focused on the underexplored approach to entrepreneurial process i.e. to study the growth aspirations and its determinants alongside entrepreneurial intentions. Studying growth aspirations and their determinants provides valuable insights...
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Identification of Substrates of Cytoplasmic Peptidyl-Prolyl Cis/Trans Isomerases and Their Collective Essentiality in Escherichia Coli
PublicationProtein folding often requires molecular chaperones and folding catalysts, such as peptidyl-prolyl cis/trans isomerases (PPIs). The Escherichia coli cytoplasm contains six well-known PPIs, although a requirement of their PPIase activity, the identity of their substrates and relative enzymatic contribution is unknown. Thus, strains lacking all periplasmic and one of the cytoplasmic PPIs were constructed. Measurement of their PPIase...
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Bio-mitigation of organic pollutants using horseradish peroxidase as a promising biocatalytic platform for environmental sustainability
PublicationA wide array of environmental pollutants is often generated and released into the ecosystem from industrial and human activities. Antibiotics, phenolic compounds, hydroquinone, industrial dyes, and Endocrine-Disrupting Chemicals (EDCs) are prevalent pollutants in water matrices. To promote environmental sustainability and minimize the impact of these pollutants, it is essential to eliminate such contaminants. Although there are...
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Structure-Property Relationship and Multiple Processing Studies of Novel Bio-Based Thermoplastic Polyurethane Elastomers
PublicationCurrently, the growing demand for polymeric materials has led to an increased need to develop effective recycling methods. This study focuses on the multiple processing of bio-based thermoplastic polyurethane elastomers (bio-TPUs) as a sustainable approach for polymeric waste management through mechanical recycling. The main objective is to investigate the influence of two reprocessing cycles on selected properties of bio-TPUs....
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Effect of bio-polyol molecular weight on the structure and properties of polyurethane-polyisocyanurate (PUR-PIR) foams
PublicationThe increasing interest in polyurethane materials has raised the question of the environmental impact of these materials. For this reason, the scientists aim to find an extremely difficult balance between new material technologies and sustainable development. This work attempts to validate the possibility of replacing petrochemical polyols with previously synthesized bio-polyols and their impact on the structure and properties...
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A Web-GIS tool for diagnosing spatial orientation of young adults: design and evaluation of Geo-Survey
PublicationSpatial orientation is the effectiveness with which one is able to assess the mutual location of objects relative to a point of reference or a system of coordinates. Traditionally, this ability has been evaluated through field navigation tests, which do not take into account the prevailing influence of free online maps and virtual walks on a person’s interpretation of space. In this context, this study presents a Web-GIS tool designed...
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Teoretyczne i praktyczne aspekty zastosowania modulatora sigma-delta w testerze wbudowanym BIST
PublicationPrzedstawiono teoretyczne i praktyczne aspekty zastosowania modulatora sigma-delta w testerze wbudowanym BIST, przeznaczonym do diagnostyki mieszanych sygnałowo pakietów elektronicznych. Omówiono podstawowe parametry modulatorów. Przeprowadzono dyskusję możliwych wariantów wyboru rodzaju, parametrów, architektury oraz technologii wykonania modulatora sigma-delta. Opracowano behawioralny model modulatora drugiego rzędu o własciwościach...
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Amber extract as a bio‐additive to poly(lactic acid) films: Multimethod analysis of crystallinity and stability
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High dimensional Bio medical images denoising using wavelet transform and modified bilateral filter
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The Use of Raman Spectroscopy to Monitor Changes in the Intensity of Ratio of Integral Unsaturated Bands in Bio-Greases
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Recurrent assessment of lymphocyte subsets in 32 patients with multisystem inflammatory syndrome in children (MIS‐C)
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System GIS do analizy i wizualizacji zanieczyszczeń oraz innych składników środowiska morskiego
PublicationW artykule przedstawiono koncepcję oraz prototyp morskiego systemu GIS do zdalnego monitorowania w czasie rzeczywistym zanieczyszczeń środowiska morskiego. System pozwala na gromadzenie i integrowanie danych z różnego rodzaju sensorów, takich jak echosondy jednowiązkowe, sonary boczne i echosondy wielowiązkowe.
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Voice Maps - portable, dedicated GIS for supporting street navigtion and self-dependent movement of the blind
PublicationThe concept and the prototype application of the system supporting the street navigation and independent, outdoor movement of the blind is presented. The system utilises the GIS database of geometric network of the pedestrian paths in the city and is capable of finding the route from the indicated source to destination. Subsequently, the system supports the movement of the blind along the found route. The information on the user's...
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Algorytmy analizy i przetwarzania danych z sonarów wielowiązkowych w rozproszonych systemach GIS
PublicationTelemonitoring morski oraz szeroko rozumiane badania morza są ważnym elementem aktywności człowieka w sferze badań, nauki oraz gospodarki. Prowadzenie działań związanych z tworzeniem map dna, inspekcją nadbrzeży, umocnień, badaniem fauny morskiej pozwala zrozumieć procesy zachodzące w środowisku morskim oraz przyczynia się do rozwoju wielu gałęzi gospodarki takich jak transport morski, bezpieczeństwo, ochrona portów i inne. W ramach...
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Quantum superadditivity in linear optics networks: Sending bits via multiple-access Gaussian channels
PublicationSuperadditivity effects of communication capacities are known in the case of discrete variable quantum channels. We describe the continuous variable analog of one of these effects in the framework of Gaussian multiple access channels (MACs). Classically, superadditivity-type effects are strongly restricted: For example, adding resources to one sender is never advantageous to other senders in sending their respective information...
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Synthesis and characterization of mechanically alloyed nanostructured ternary titanium based alloy for bio-medical applications
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Effect of bio-polyol molecular weight on the structure and properties of polyurethane-polyisocyanurate (PUR-PIR) foams
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Development of the Mobile PoC Graphene-Based Biosensing Device Using Electrochemical Impedance Spectroscopy (EIS)
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Small Urban Hacks - Big Impact! Tackling major urban challenges through acupunctural smallness
PublicationSmall urban hacks, acupunctural action and process-oriented planning approaches might appear to address quite a socio-romantic attitude towards our urban environments. In this chapter, our aim is to remedy such a biased view, demonstrating the impact and potential of smallness in the context of major urban challenges. Small urban hacks and their multi-faceted and creativity-driven approaches of small is beautiful are selected from...
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Novel Interpolation Method of Multi-DFT-Bins for Frequency Estimation of Signal with Parameter Step Change
PublicationThe IpDFT(Interpolation Discrete Fourier Trans-form) method is one of the most commonly used non-parametric methods. However, when a parameter (frequency, amplitude or phase) step changes in the DFT period, the DFT coefficients will be distorted seriously, resulting in the large estimation error of the IpDFT method. Hence, it is a key challenge to find an IpDFT method, which not only can eliminate the effect of the step-changed...
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Chemical structure, thermal and mechanical characterization of bio-based polyurethane composites filled with microcrystalline cellulose
PublicationOver the past several decades, the interest in replacing the synthetic components used in the production of polymers and composites with their natural counteparts has been growing. Biocomposites belong to the group of materials produced with the use of renewable raw materials. There has been a recent surge of interest in the industrial applications of composites containing natural fibres reinforced with biopolymers. Biopolymers...
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SafeCity – a GIS-based tool profiled for supporting decision making in urban development and infrastructure protection
PublicationThis paper presents a system for analysis of municipal Critical Infrastructures, which offers integrated tools for target analysis, hazard scenario simulations and spatial analysis within a remotely accessible Web-based Geographic Information System. The system has been applied to research conducted in the city of Gdansk with the aid of blast attack, chemical leakage and flood hazard scenarios, as well as a spatial density algorithm,...
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A spectroscopic study of the cis/trans-isomers of penta-2,4-dienoic acid attached to gold nanoclusters
PublicationIn this theoretical work, we present a spectroscopic analysis of the cis/trans-isomers of a molecular switch, penta-2,4-dienoic acid, attached to gold clusters of different size (1, 2 and 20 gold atoms). We have simulated 4 different spectroscopic techniques: Infrared spectroscopy, normal Raman scattering, absorption spectra and resonance Raman scattering. We discuss how the position and the conformation of the molecule determine...
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Rozważania nad intensywnością zabudowy w kontekście praktyki urbanistycznej oraz potencjału technologii GIS
PublicationCelem artykułu jest zasygnalizowanie konieczności wypracowania jednolitej definicji i sposobu obliczania intensywności zabudowy na potrzeby praktyki urbanistycznej. Punktem odniesienia jest definicja intensywności zabudowy, przyjęta w znowelizowanej ustawie o planowaniu i zagospodarowaniu przestrzennym na tle definicji zaczerpniętych z innych źródeł. Intensywność zabudowy jest parametrem o najdalej idących skutkach w przestrzeni....
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Structure-rheology relationship of fully bio-based linear polyester polyols for polyurethanes - Synthesis and investigation
PublicationThe synthesis of polyols from renewable substances as an alternative for petrochemical-based polyols play important matter in the polyurethane industry. In this work, the fully bio-based linear polyester polyols with different catalyst amounts were synthesized via two-step polycondensation method. The effect of various catalyst content on the structure and rheological behavior were established. Fourier Transform Infrared Spectroscopy,...
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Driving Performance Indicators of Electric Bus Driving Technique: Naturalistic Driving Data Multicriterial Analysis
PublicationThe issue of electric energy saving in public transport is becoming the key area of interest. By improving of driving techniques and the implementation of eco-driving, it is possible to save electric energy. Systems that help to decrease energy consumption and to reduce fuel emissions are becoming popular in vehicles powered by diesel engines. However, these methods have not yet gained popularity in electric vehicles. Therefore,...
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Kinetics study of the fully bio-based poly(propylene succinate) synthesis. Functional group approach
PublicationCurrently, the increasing importance of the bio-based chemical compounds development is visible in the polymer chemistry, chemical engineering and materials science. It is well-known that the various purity level and different contaminants characterize petrochemical-based compounds compared to their biobased counterparts. Therefore, it is necessary to find out the contaminants impact on the bio-based monomers synthesis. One of...
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Diagnostyka obiektów przemysłowych z wykorzystaniem wspólnej magistrali usług DIAGNOSTIC SERVICE BUS DSB
PublicationKorzystając ze znanego pojęcia magistrali, w pracy przedstawia się sposób przystosowania i wykorzystania magistrali usług w systemie diagnostyki obiektów przemysłowych. Koncepcja takiego środka komunikacyjnego opiera się na architekturze SOA (z architekturą zorientowanej na usługi). Koncepcja ta stanowi metodę rozwiązania problemów wydajnościowych rozwijanego projektu pt. "Sieciowy Monitor Obiektu" (SMO). Wspólna szyna danych zwiększa...
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Discrimination of Apple Liqueurs (Nalewka) Using a Voltammetric Electronic Tongue, UV-Vis and Raman Spectroscopy
PublicationThe capability of a phthalocyanine-based voltammetric electronic tongue to analyze strong alcoholic beverages has been evaluated and compared with the performance of spectroscopic techniques coupled to chemometrics. Nalewka Polish liqueurs prepared from five apple varieties have been used as a model of strong liqueurs. Principal Component Analysis has demonstrated that the best discrimination between liqueurs prepared from different...
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A testing method of analog parts of mixed-signal electronic systems equipped with the IEEE1149.1 test bus
PublicationA new solution of the JTAG BIST for testing analog circuits in mixed-signal electronic microsystems controlled by microcontrollers and equipped with the IEEE1149.1 bus is presented. It is based on a new fault diagnosis method in which an analog circuit is stimulated by a buffered signal from the TMS line, and the time response of the circuit to this signal is sampled by the ADC equipped with the JTAG. The method can be used for...
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High-Speed Binary-to-Residue Converter Design Using 2-Bit Segmentation of the Input Word
PublicationIn this paper a new approach to the design of the high-speed binary-to-residue converter is proposed that allows the attaining of high pipelining rates by eliminating memories used in modulo m generators. The converter algorithm uses segmentation of the input binary word into 2-bit segments. The use and effects of the input word segmentation for the synthesis of converters for five-bit moduli are presented. For the number represented...
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Development and validation of an eco-compatible UV–Vis spectrophotometric method for the determination of Cu2+ in aqueous matrices
PublicationCu 2+ are ubiquitous ions in the ecosystem and are responsible of serious environmental pollution. Indeed, the development of sensitive methods for Cu 2+ detection is an urgent demand. In this work, we proposed a new spectrophotometric method for Cu 2+ determination in different water matrices (distilled water, drinking water, wastewater, and river water). The method employs a bio-based organic ligand namely tetrasodium iminodisuccinate...
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3D buckling analysis of a cylindrical metal bin composed of corrugated sheets strengthened by vertical stiffeners
PublicationW artykule pokazano obszerne wyniki analizy wyboczeniowej 3D przy zastosowaniu metody elementów skończonych dla silosu złożonego z blachy falistej i słupów rozmieszczonych równomiernie wokół obwodu. Obliczenia wykonano dla silosu bez i z imperfekcjami geometrycznymi i obciążeniowymi. Wyniki obliczeń porównano z Eurokodem.
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INTERNATIONAL JOURNAL OF UNIVERSAL PHARMACY AND BIO SCIENCES
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Zbigniew Czaja dr hab. inż.
PeopleZbigniew Czaja was born in Czluchow, Poland, in 1970. He graduated from Gdansk University of Technology, Faculty of Electronics, Telecommunications and Informatics in 1995. The Ph.D. degree in electronics was received in 2001 from the same university. He worked as assistant professor at this university from 2002 to 2013. In 2014, he qualified as an associate professor, and in 2017, as a professor. His research interests are in...