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Dynamiczna spektroskopia impedancyjna w mikroskopowej analizie powierzchni metalicznych
PublikacjaW pracy przedstawiono możliwość zastosowania dynamicznej spektroskopii impedancyjnej do pomiaru lokalnej impedancji z wykorzystaniem mikroskopu AFM. Kontakt sondy mikroskopu z próbką jest układem dynamicznym, który ulega ciągłym zmianom. Skanowanie powierzchni, zmiana docisku sondy, czy nawet dryft skanera piezoelektrycznego powodują zmianę geometrii kontaktu sonda-próbka. W związku z tym klasyczna odmiana pomiaru impedancji...
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Does offshoring affect industry employment? Evidence from a wide European panel countries
Publikacjais paper contributes to the literature on the possible impact of international outsourcing on domestic labour markets. We focus on off shoring-employment relationship. Th e analysis is performed for a wide European panel, composed of 27 EU countries and 13 manufacturing sectors, observed in the period 1995-2009. Th anks to the use of input-output tables from the WIOD project, we measure the intensity of off shoring in the sectors,...
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Wpływ stopowania laserowego z użyciem nanorurek węglowych stopu Ti13Nb13Zr do zastosowań biomedycznych na jego wybrane własności mechaniczne
PublikacjaDo eksperymentu użyto stopu tytanu Ti13Nb13Zr, który ze względu na swój skład chemiczny i właściwości mechaniczne stanowi materiał do zastosowań w inżynierii medycznej. Celem pracy była ocena wpływu stopowania laserowego stopu Ti13Nb13Zr z powłoką z wielościennych nanorurek węglowych na jego właściwości mechaniczne (chropowatość, nanotwardość, moduł Younga). Do wytworzenia powłoki węglowej wykorzystano metodę osadzania elektroforetycznego (EDP)....
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Carbon dioxide sequestration by industrial wastes through mineral carbonation: Current status and perspectives
PublikacjaMineral carbonation using natural minerals or industrial wastes is a safe and promising strategy for CO2 sequestration. Application of industrial wastes for this purpose has significant ecological and environmental value, which is one of the key green technologies in the global carbon mitigation. This review summarizes the current research status of CO2 mineralization by industrial wastes. This work surveys the mechanisms and capacities...
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A Noded Carbon Emission Tool (NCET) to Measure Embodied Carbon (EC) in Compositional Cementitious Materials
PublikacjaThe ever evolving modern construction industry is now producing the highest levels of carbon content adversely affecting the construction associated environment. Although, the impact of carbon induced emission is quite large, but still not enough measurable standards and tools to scale these emission are available. This study contributes to the body of knowledge by providing a Grasshopper based definition to calculate the embodied...
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Improvement of ships seakeeping performance by application of the full-scale cfd simulations
PublikacjaThe ship’s fuel economy is increasingly important. The paper presents the effect of redesigning a case study ship for increasing seakeeping performance. Selected wave parameters reflect very difficult operational conditions existing on the North Sea and the Baltic Sea. The analyzed variants of a case study ship represent the latest developments of modern hull forms. The concepts similar to V-shaped bulbous bow, X-bow, X-aft, B-bow...
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Multiscalar Control Based Airgap Flux Optimization of Induction Motor for Loss Minimization
PublikacjaBased on the induction motor model, considering the core loss resistance that accounts for magnetic characteristic saturation, a speed control approach is devised with an adaptive full-order (AFO) speed observer. The induction motor model analysis is done sincerely in a stationary reference frame. The control approach incorporates a flux reference generator designed to meet optimal operational circumstances and a nonlinear speed...
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In search of molecular precursors for cadmium sulfide-new complexes with a sulfur-rich kernel: cadmium(II) tri-tert-butoxysilanethiolates with additional diethyldithiocarbamato ligand
PublikacjaW ramach rozprawy opracowano metodę syntezy związków koordynacyjnych kadmu zawierających mieszane ligandy S-donorowe, które stanowią reszta tri-tert-butoksysilanotiolanowa oraz ditiokarbaminianowa. Zostały one poddane badaniom za pomocą analizy składu pierwiastkowego, metod spektroskopowych (FTIR, FIR, UV-Vis, NMR, MS) oraz termicznych. W celu osadzenia cienkich warstw wybranych związków posłużono się techniką nakładania obrotowego...
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Au–Si plasmonic platforms: synthesis, structure and FDTD simulations
PublikacjaPlasmonic platforms based on Au nanostructures have been successfully synthesized by directional solidification of a eutectic from Au and the substrate. In order to determine homogeneous shape and space distribution, the influence of annealing conditions and the initial thickness of the Au film on the nanostructures was analyzed. For the surface morphology studies, SEM and AFM measurements were performed. The structure of platforms...
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Mechanical properties of polyvinyl chloride-coated fabric under cyclic tests
PublikacjaThe aim of the present paper is to propose a method of laboratory tests necessary for the identification of mechanical properties of the coated fabric. The material parameters of the coated fabric AF 9032 are specified on the basis of the uniaxial and biaxial tensile tests. For the identification process, the techniques based on the least squares methods are used. Additionally, the uniaxial and biaxial cyclic tests are performed...
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Meander anisotropic magnetoresistance bridge geomagnetic sensors
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A Probe into the Corrosion Behavior of a WE43B Magnesium Alloy in a Simulated Body Fluid using Dynamic Electrochemical Impedance Spectroscopy
PublikacjaWE43B is one of the newest Mg alloys with practical application in biomedical implant technology. This work attempts to scrutinize the corrosion characteristics of WE43B alloy in a simulated body fluid (SBF) at a typical body temperature. The dynamic-electrochemical impedance spectroscopy with the capacity to track changes on surfaces in a dynamic corrosive system is used in combination with other classical techniques namely, linear...
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Incorporation of nitrogen in diamond films – A new way of tuning parameters for optical passive elements
PublikacjaThis paper investigates the impact of nitrogen incorporation in diamond films for the construction of an interferometric sensor to measure displacement. Diamond films with different nitrogen levels (0–5%) were deposited on silicon substrates by microwave plasma enhanced chemical vapor deposition. The structural characteristics of these samples are characterized using scanning electron microscopy (SEM), atomic force microscopy (AFM), confocal...
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The operation mode of E/E/PE system and its influence on determining and verifying the safety integrity level = Rodzaj pracy systemu E/E/PE i jego wpływ na określanie i weryfikację poziomu nienaruszalności bezpieczeństwa
PublikacjaNorma PN-EN 61508 wprowadza kryteria probabilistyczne dla wyróżnionych rodzajów pracy systemów E/E/PE, które związane są z poziomami nienaruszalności bezpieczeństwa SIL. Dla systemów sterowania i zabezpieczeń, pracujących w trybie rzadkiego przywołania do działania, kryterium tym jest przeciętne prawdopodobieństwo niewypełnienia funkcji bezpieczeństwa na żądanie PFDavg. W przypadku systemów realizujących funkcje bezpieczeństwa...
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Improvement of ships seakeeping performance by application of the Full-scale CFD simulations – case study
PublikacjaThe ship’s fuel economy is increasingly important. The paper presents the effect of redesigning a case study ship for increasing seakeeping performance. Selected wave parameters reflects very difficult operational con-ditions existing on the North Sea and the Baltic Sea. The analyzed variants of a case study ship represent the latest developments of modern hull forms. The concepts similar to V-shaped bulbous bow, X-bow, X-aft,...
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The influence of amorphous macrodiol, diisocyanate type and l-ascorbic acid modifier on chemical structure, morphology and degradation behavior of polyurethanes for tissue scaffolds fabrication
PublikacjaStudies described in this work were related to the bulk synthesis and characterization of polyurethanes (PURs) obtained with the use of cyclic 4,4′-methylene bis(cyclohexyl isocyanate) (HMDI) or linear 1,6-hexamethylene diisocyanate (HDI), amorphous α,ω-dihydroxy(ethylene-butylene adipate) macrodiol (PEBA), 1,4-butandiol (BDO) chain extender and dibutyltin dilaurate (DBTDL) catalyst. Obtained PURs were modified with l-ascorbic...
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Piezoresponse force microscopy and dielectric spectroscopy study of Ba0.6Sr0.4TiO3 thin films
PublikacjaResearch on synthesis, characterization and determination of processing – structure – property relationships of commercially important ferroelectric thin films has been performed. The sol-gel-type solution deposition technique was applied to produce good quality thin films of Ba0.6Sr0.4TiO3 (BST60/40) chemical composition on the stainless steel substrates. The thin films were characterized in terms of their microstructure, crystal...
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Assessment of the impact of bacteria Pseudomonas denitrificans, Pseudomonas fluorescens, Bacillus subtilis and yeast Yarrowia lipolytica on commercial poly(ether urethanes)
PublikacjaThe assessment of the impact of the bacteria Pseudomonas denitrificans, Pseudomonas fluorescens, Bacillus subtilis and yeast Yarrowia lipolytica on commercial poly(ether urethanes) Tecoflex® and Tecothane® is presented. The polyurethane samples were incubated with pure cultures of the microorganisms at 30 °C for five months. The changes in the chemical structure of the polymers were evaluated using loss of weight and contact angle...
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Organic semiconductor rubrene thin films deposited by pulsed laser evaporation of solidified solutions
PublikacjaOrganic semiconductor rubrene (C42H28) belongs to most preferred spintronic materials because of the high charge carrier mobility up to 40 cm2(V·s)-1. However, the fabrication of a defect-free, polycrystalline rubrene for spintronic applications represents a difficult task. We report preparation and properties of rubrene thin films deposited by pulsed laser evaporation of solidified solutions. Samples of rubrene dissolved in aromatic...
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MICROSEISMIC EVENT DETECTION USING DIFFERENT ALGORITHMS ON REAL DATA FROM PATCH ARRAY GEOPHONE GRID FROM EASTERN POMERANIA FRACTURING JOB
PublikacjaThe microseismic monitoring is a method of monitoring of fracture propagation during hydraulic fracturing process. Hydraulic fracturing is a method of reservoir stimulation used especially for unconventional gas recovery. A matrix of several thousand geophones is placed on the surface of earth to record every little tremor of ground induced by fracturing process. Afterwards, the signal is analysed and the place of tremor occurrence...
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Proton transfer and hydrogen bonds in supramolecular, self-assembled structures of imidazolium silanethiolates. X-ray, spectroscopic and theoretical studies
PublikacjaThe reaction of 1-methylimidazole, 2-ethyl-4-methylimidazole and 2-ethylimidazole with tris(2,6- diisopropylphenoxy)silanethiol (TDST) leads to the formation of three new salts, which have been characterized by elemental analyses, thermogravimetric analyses, FTIR spectroscopy, and their structures were determined by single-crystal X-ray diffraction. Structural analyses indicate that in all three compounds a proton transfer has...
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WYBRANE WŁAŚCIWOŚCI FIZYCZNO-CHEMICZNE MIKROSFER I MOŻLIWOŚĆ ICH WYKORZYSTANIA W KOMPOZYTACH CEMENTOWYCH : The selected physico-chemical properties of microspheres and possibility of their use in cement composites
PublikacjaMicrospheres are formed during the mineral transformation stage in coal combustion. Their content in fly ashes from the combustion of different types of coals varies over a rather wide range from 0.01 to 4.8 wt.%. The microspheres have three main elements, silicon, aluminum and iron, the oxides of which account for about 89.0 wt.% of the material. Mineralogical analysis using XRD shows that microspheres mainly contain mullite and...
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Wytwarzanie i modyfikacja powierzchni porowatych struktur tytanowych przeznaczonych na implanty
PublikacjaCelem pracy było wytworzenie stopu Ti-13Nb-13Zr z wykorzystaniem technologii selektywnego topienia laserowego (SLM) oraz jego biofunkcjonalizacja za pomocą utleniania mikrołukowego (MAO), a następnie określenie wpływu parametrów procesowych na właściwości otrzymanych materiałów pod kątem ich zastosowania na implanty. Oceniono wpływ napięcia, natężenia i czasu procesu MAO przeprowadzanego w elektrolicie zawierającym wapń i fosfor...
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Postępy w rozwoju standardu IEEE 802.11 i jego zastosowań Część II: Nowe obszary zastosowań i nowe koncepcje pracy sieci WiFi
PublikacjaArtykuł stanowi kontynuację rozważań, podjętych w zeszycie nr 11 z 2016 r. PTiWT [1], na temat rozwoju standardu łEEE 802.11 , ukierunkowanego na zwiększanie szybkości przekazu i przekraczanie gigabitowej granicy przepływności łącza. Wskazano tam na modyfikacje i nowe mechanizmy implementowane w warstwie fizycznej i podwarstwie MAC standardów IEEE 802.11 n, IEEE 802.11 ac oraz IEEE 802.11 ad, mające istotny wpływ zarówno na wzrost...
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Tunneling in Systems of Coupled Dopant-Atoms in Silicon Nano-devices
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Incorporation of nitrogen in diamond films - A new way of tuning parameters for optical passive elements
PublikacjaThis paper investigates the impact of nitrogen incorporation in diamond films for the construction of an interferometric sensor to measure displacement. Diamond films with different nitrogen levels (0–5%) were deposited on silicon substrates by microwave plasma enhanced chemical vapor deposition. The structural characteristics of these samples are characterized using scanning electron microscopy (SEM), atomic force microscopy...
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Nanostructure and dielectric behavior of vanadate glasses containing BaTiO3
PublikacjaThe ac and dc electrical conductivity of barium titanate doped bismuth-vanadate as-quenched and heat-treated materials was measured in the frequency range from 1 mHz to 1 MHz and in the temperature range from 153 K to 423 K with the impedance spectroscopy method. The microstructure was investigated by means of XRD, scanning electron microscopy (SEM), atomic force microscopy (AFM) and confocal microscopy. The obtained results showed...
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Photovoltaic-Installation Performance in Central Europe on the Example of Poland
PublikacjaThe amount of the electric energy obtained from a photovoltaic (PV) installation depends on the energy of the radiation. Weather conditions differ strongly between various years even in the same season. Depending on the climatic conditions of a given location, fixed PV solar plants as well as one-axis and dual-axis tracking PV solar plants are being installed worldwide. The aim of this work is to analyse the sunlight intensity...
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Postępy w badaniach struktur nadcząsteczkowych poliuretanów segmentowych
PublikacjaW pracy opisano postępy w badaniach struktur nadcząsteczkowych poliuretanów segmentowych. Stwierdzono, że jest on złożona. Należy ją analizować zarówno w skali mikrometrycznej jak i nanometrycznej, co wskazuje na niezwykłą ostrożność interpretacji danych uzyskanych z metod badawczych, w których otrzymujemy dane uśrednione. Dzięki wykorzystaniu nowych metod badawczych takich jak AFM i m-Raman poznano naturę globul oraz ustalono...
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Thermal Instability of Gold Thin Films
PublikacjaThe disintegration of a continuous metallic thin film leads to the formation of isolated islands, which can be used for the preparation of plasmonic structures. The transformation mechanism is driven by a thermally accelerated diffusion that leads to the minimalization of surface free energy in the system. In this paper, we report the results of our study on the disintegration of gold thin film and the formation of nanoislands...
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Cyclic behavior of FeCoCrNiMn high entropy alloy coatings produced through cold spray
PublikacjaeCoCrNiMn high entropy alloy powders were employed to produce coatings on carbon steel through high pressure cold spray (at 1100 °C and 7 MPa in temperature and pressure respectively). X-ray diffraction of the sprayed material revealed a dense coating with the retention of the original crystallographic structure. Once splatted, particles revealed high flattening ratio with consequent excellent adhesion of the coating to the substrate....
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Elementary analysis and energetic potential of the municipal sewage sludges from the Gdańsk and Kościerzyna WWTPs
PublikacjaThis paper aims to present municipal sewage sludge (MSS) elementary analysis and energetic potential based on measurement of heat of combustion (higher heating value HHV) and calculation of calorific values (lower heating value LHV). The analysis takes into the consideration water content in sewage sludge, at different utilization stages, in wastewater treatment plants in Gdańsk Wschód and Kościerzyna – Pomeranian Voivodeship....
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Exhaled breath gas sensing using pristine and functionalized WO3 nanowire sensors enhanced by UV-light irradiation
PublikacjaThe development of advanced metal-oxide-semiconductor sensing technologies for the detection of Volatile Organic Compounds (VOCs) present in exhaled breath is of great importance for non-invasive, cheap and fast medical diagnostics. Our experimental studies investigate the effects of operating temperature selection and UV-light irradiation on improving the response of WO3 nanowire sensors towards exhaled breath exposure. Herein,...
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Mechanical properties for preliminary design of structures made from PVC coated fabric
PublikacjaIn this paper, laboratory tests necessary for the identification of non-linear elastic immediate properties of the PVC coated polyester fabric (like AF 9032) are described. The material parameters are specified on the basis of the uniaxial tensile tests in the warp and weft directions as well as on the base of the biaxial tensile tests. For the identification process techniques based on the least squares method are used. The authors...
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Soil and groundwater contamination as a result of sewage sludge land application
PublikacjaThe leaching of chemical compounds (N-NO3, N-NH4, Norg, P-PO4, Ptot) and trace elements (Cd, Cu, Cr, Ni, Zn, and Pb) from sewage sludge and their migration through the soil profile was the subject of the study. The column experiments were carried out under atmospheric conditions corresponding to naturally occurring storm events - sewage sludge amended soil was irrigated with high rates of water. The column filter media used in...
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Ferromagnetic nanocrystallites in the SiO2 - PbO - Fe2O3 glass system
PublikacjaThe structure of 50% SiO2 - 35% PbO - 15% Fe2O3, 50% SiO2 - 30% PbO - 20% Fe2O3 and 50% SiO2 - 25% PbO - 25% Fe2O3 (in mol%) glass was investigated by the means of AFM microscopy and X-ray diffraction. Observation by the atomic force microscopy shows that each of prepared iron oxide glass doesn't have homogeneous structure and some nanocrystallites were detected. Next, test with neodymium magnet found out strong magnetic properties...
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Experimental and Numerical Investigations of the Effect of Curing Conditions on the Temperature Rise of Concrete
PublikacjaThis paper presents experimental and numerical studies investigating the impact of three curing conditions on temperature evolution in concrete cubes. The tests were performed on samples of the same volume (3.375 dm3) under different curing conditions: room temperature, insulation boxes, and adiabatic calorimeter. Various cements (Portland cement, Portland composite cement, and blast furnace slag cement) and aggregates (gravel...
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Application of the Chimney Cap as a Method of Improving the Effectiveness of Natural Ventilation in Buildings
PublikacjaAdequately designed natural ventilation is the cheapest and easiest way to effectively remove indoor pollutants and keep the air inside a building fresh. A prediction of the performance and effectiveness of ventilation in order to determine the design of a ventilation system can provide real and long-term cost savings. The worst time in terms of the efficiency of natural ventilation is the spring-autumn transition period [7]. In...
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Thermal utilization of meat-and-bone meal using the rotary kiln pyrolyzer and the fluidized bed boiler – The performance of pilot-scale installation
PublikacjaThermal utilization of meat-and-bone meal (MBM) is subject to stringent regulations that are meant to provide elimination of any potential pathogens. Incineration as well as other possible routes for thermal conversion of MBM are still at the research state. The universal technology was developed that allows to combust various types of waste organic materials, including animal waste, municipal solid waste and sludge, mixed at any...
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FTIR spectroscopic and thermogravimetric characterization of ground tyre rubber devulcanized by microwave treatment
PublikacjaIn this work, the phenomena involved in the microwave devulcanization of ground tyre rubber (GTR) were investigated. Three types of GTR with different content of organic compounds (elastomers, plasticizers, etc.), carbon black and ash have been studied. The chemical structure of GTR before and after a microwave devulcanization process was analyzed by Fourier transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA)...
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The Physicochemical and Antibacterial Properties of Chitosan-Based Materials Modified with Phenolic Acids Irradiated by UVC Light
PublikacjaThis paper concerns the physicochemical properties of chitosan/phenolic acid thin films irradiated by ultraviolet radiation with wavelengths between 200 and 290 nm (UVC) light. We investigated the preparation and characterization of thin films based on chitosan (CTS) with tannic (TA), caffeic (CA) and ferulic acid (FA) addition as potential food‐packaging materials. Such materials were then exposed to the UVC light (254 nm) for...
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(Invited) Effect of Individual Dopants in Nano-SOI-MOSFETs and Nano-pn-Diodes
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Effective yttrium based coating for steel interconnects of solid oxide cells: Corrosion evaluation in steam-hydrogen atmosphere
PublikacjaThis work describes manufacture, analysis and test of a new well conducting corrosion-protection coating that can be applied on steel types with high chromium content. Electrolytic deposition of yttrium salts is used to form thin (<100 nm) coatings on both flat steel sheets (material: Crofer 22 APU) and its properties are proven on woven wire-meshes (materials from two different sources: SUS316 and SUS316L). The oxide scale on...
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Electrochemical methods for corrosion rate determination under cathodic polarisation conditions - a review. Part II - AC methods
PublikacjaPrzedstawiono krytyczny przegląd prac dotyczących wykorzystania metod elektrochemicznych zmiennoprądowych do wyznaczania prądu korozyjnego metali polaryzowanych katodowo. Przedyskutowano stosowanie klasycznej liniowej spektroskopii impedancyjnej (EIS) z użyciem sygnałów pobudzających niskoamplitudowych, a następnie techniki zmiennoprądowe bazujące na sygnałach wysokoamplitudowych, a więc w zakresie nieliniowej charakterystyki polaryzacyjnej...
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Transport of lead across polymer inclusion membrane with p-tert-butylkalix[4]arene derivative
PublikacjaOpisane zostały ułatwienia w transporcie jonów ołowiu (II) przez polimerową membranę inkluzyjną (PIMs),która składała się z trój octanu celulozy jako polimerowego suportu, eteru o-nitrofenylooktylu jako plastyfikatora i 25,26,27,28, tetra-(N-hydroksy-N-metylokarbonylo metoksy)-p-tert-butylokaliks[4]arenu jako nośnika jonów. Polimerowa membrana inkluzyjna została scharakteryzowana przy pomocy mikroskopu sił atomowych (AFM). Otrzymane...
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Enhancing electrical properties through in-situ controlled nanocrystallization of V2O5–TeO2 glass
PublikacjaV2O5–TeO2 glass–ceramics (VTGC) were prepared by controlled annealing of the V2O5–TeO2 glass (VTG), which illustrates a parent glass matrix with a single charge carrier. The annealing proceeded at six temperatures selected between the glass transition and the maximum of the frst crystallization process to obtain various nanocrystallite sizes. Heat treatment caused an increase in DC conductivity by 2.5–3.5 (250–285 °C) order of...
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Application of Artificial Neural Networks to Predict Insulation Properties of Lightweight Concrete
PublikacjaPredicting the properties of concrete before its design and application process allows for refining and optimizing its composition. However, the properties of lightweight concrete are much harder to predict than those of normal weight concrete, especially if the forecast concerns the insulating properties of concrete with artificial lightweight aggregate (LWA). It is possible to use porous aggregates and precisely modify the composition...
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Pilot installation for thermal utilization of meat-and-bone meal using the rotary kiln pyrolyzer and the fluidised bed boiler
PublikacjaThe technology of thermal utilization of meat-and-bone meal (MBM) is still at the research state. However, there are already a number of existing pilot-scale installations that provide the complete, effective and environmentally safe process conducting. The universal technology was developed that allows to combust various types of waste, including animal waste, municipal waste and sludge, mixed at any ratio with different types...
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Compatibility of Sustainable Mater-Bi/poly(ε-caprolactone)/cellulose Biocomposites as a Function of Filler Modification
PublikacjaDespite their popularity and multiplicity of applications, wood–polymer composites (WPCs) still have to overcome particular issues related to their processing and properties. The main aspect is the compatibility with plant-based materials which affects the overall performance of the material. It can be enhanced by strengthening the interfacial adhesion resulting from physical and/or chemical interactions between the matrix and...
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Characteristics of silver-dopped carbon nanotube coating destined for medical applications
PublikacjaCarbon nanotubes are materials demonstrating outstanding mechanical, chemical, and physical properties and are considered coatings of titanium implants. The present research is aimed to characterize the microstructure and properties of the multi-wall carbon nanotubes (MWCNTs) layer decorated with silver nanoparticles (Ag NPs) on the Ti13Nb13Zr alloy destined for long-term implants. The electrophoretic deposition of coatings...