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Wyniki wyszukiwania dla: PULSACYJNY DETEKTOR PŁOMIENIOWO FOTOMETRYCZNY
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Methods of assaying volatile oxygenated organic compounds in effluent samples by gas chromatography—A review
PublikacjaThe paper is a review of the procedures for the determination of volatile and semivolatile oxygenated organic compounds (O-VOCs) in effluent samples by gas chromatography. Current trends and outlook for individual steps of the procedure for the determination of O-VOCs in effluents are discussed. The available sample preparation techniques and their limitations are described along with GC capillary columns used for O-VOCs separation...
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Oznaczanie niezmienionych form lotnych związków bromo- i chloroorganicznych w próbkach płynów biologicznych z wykorzystaniem opracowanej metodyki TLHS-DAI-GC-ECD
PublikacjaRozprawa doktorska dotyczyła opracowania nowej procedury analitycznej opartej na wykorzystaniu analizy fazy nadpowierzchniowej nad cienkim filmem cieczy z samoczynną generacją strumienia ciekłego sorbentu w połączeniu z chromatografem gazowym wyposażonym w detektor wychwytu elektronów (TLHS-DAI-GC-ECD). Skupiono się na :1. wykonaniu badań optymalizacyjnych poprzedzających walidację metodyki TLHS-DAI-GC-ECD (sprawdzenie trwałości...
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Experimental and theoretical studies on the photodegradation of 2-ethylhexyl 4-methoxycinnamate in the presence of reactive oxygen and chlorine species
Publikacja2-Ethylhexyl 4-methoxycinnamate (EHMC) is one of the most commonly used sunscreen ingredient. In this study we investigated photodegradation of EHMC in the presence of such common oxidizing and chlorinating systems as H2O2, H2O2/HCl, H2O2/UV, and H2O2/HCl/UV. Reaction products were detected by gas chromatography with a mass spectrometric detector (GC-MS). As a result of experimental studies chloro-substituted 4-methoxycinnamic...
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Simultaneous determination of individual isothiocyanates in plant samples by HPLC-DAD-MS following SPE and derivatization with N-acetyl-l-cysteine
PublikacjaThe procedure for the isothiocyanates (ITCs) determination that involves derivatization with N-acetyl-l-cysteine (NAC) and separation by HPLC was developed. Prior to derivatization, plant ITCs were isolated and purified using solid-phase extraction (SPE). The optimum conditions of derivatization are: 500 μL of isopropanolic eluate obtained by SPE combined with 500 μL of derivatizing reagent (0.2 M NAC and 0.2 M NaHCO3 in water)...
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Badania symulacyjne dynamicznej odporności na zakłóceniacyfrowych układów kombinacyjnych.
PublikacjaPrzedstawiono opracowaną przez autorów metodę pomiaru dynamicznej odporności na zakłócenia układów cyfrowych z zastosowaniem szerokopasmowego wzorcowego sygnału szumowego. Modyfikacja metody polega na dodatkowym ograniczeniu szerokości pasma sygnału stymulującego. Przeprowadzono badania symulacyjne dla kilku modeli badanych układów cyfrowych, w tym modelu detektora progowego oraz szybkiego komparatora z histerezą, mające na celu...
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Determination of SCFAs in water using GC-FID. Selection of the separation system
PublikacjaIn the present study, an analytical procedure was developed for the determination of short-chain fatty acids (SCFAs) in landfill leachate and municipal wastewater employing injection of aqueous samples to gas chromatograph with flame ionization detector (GC-FID). Chromatographic conditions such as a separation system, injection volume, oven temperature program were investigated and selected. With two columns, one with a polar (polyethylene...
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SURFACTANTS IN KLODNICA RIVER (KATOWICE, POLAND). PART II. QUATERNARY AMMONIUM COMPOUNDS
PublikacjaThe paper presents methods of determination of analytes of the cation group (alkyl benzyl dimethyl ammonium (BDDA-C12-C16), alkyl trimethyl ammonium (TMA), hexadecyl piridinium (HP)) in surface water and bottom sediment samples. In the sample preparation phase the solid phase extraction (SPE) or accelerated solvent extraction/ultrasound assisted extraction (ASE/UAE)-SPE technique was used and in the identification phase and quantitative...
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Direct-Ultrasonic Assisted Microextraction Coupled with RTL-GC-FID/GC-MS as a Future Standard Procedure for Monitoring 26 potentially Allergenic Fragrances in Water Samples
PublikacjaThis research topic grew up as a result of awareness of constant anthropogenic and natural input to the environment constituents of personal care products (PCPs) residues. This group of emerging pollutants encompasses a wide range of chemicals, including potentially allergenic fragrance compounds. The aim of the present study was to investigate presence of 26 fragrance allergens in water samples. Simple and rapid methodology based...
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Effect of alcohol consumption on the levels of volatile organohalogen compounds in blood and urine = Wpływ spożywania alkoholu na poziom lotnych związków chlorowcoorganicznych w krwi i moczu ludzkim
PublikacjaW pracy przedstawiono wyniki oznaczania lotnych związków chlorowcoorganicznych w próbkach moczu i krwi pochodzących od dawców w różny sposób narażonych na ekspozycje lotnych związków chlorowcoorgnicznych (styl życia: palenie papierosów, picie alkoholu, przyjmowanie lekarstw czy rodzaj wykonywanej pracy). Do izolacji i wzbogacania analitów z próbek moczu i krwi, wykorzystano technikę analizy fazy nadpowierzchniowej nad cienką warstwą...
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Volatile organohalogen compounds in human urine: the effect of environmental exposure
PublikacjaW pracy przedstawiono wyniki oznaczania lotnych związków chlorowcoorganicznych w próbkach moczu pochodzących m.in. od dawcow narazonych na kancerogeny w miejscu pracy i dawcow spozywajacych wode poddana procesowi uzdatniania przez chlorowanie. Do izolacji i wzbogacania analitów z moczu, posiadającego skomplikowaną matrycę, wykorzystano technikę analizy fazy nadpowierzchniowej nad cienką warstwą cieczy z samoczynną generacją ciekłego...
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Problems of PAH quantification by GC-MS method using isotope-labelled standards.
PublikacjaChromatografia gazowa w połączeniu ze spektromerią mas (GC-MS) jest obecnie rutynowo stosowaną metodą w analityce środowiskowej do oznaczania śladowych ilości zanieczyszczeń organicznych. Stosowanie detektora mas sprawia, że wygodnym wzorcem wewnętrznym są stabilne izotopowo analogi oznaczanych związków. Związki te są wykorzystywane do śledzenia i kompensacji strat analitów podczas wykonywania określonych operacji związanych z...
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Determination of cyanide in urine and saliva samples by ion chromatography with pulsed amperometric detection
PublikacjaCommonly known as a highly toxic chemical, cyanide is also an essential reagent for many industrial processes. It naturally occurs in plant seeds as a cyanogenic glycosides. Another relatively common mode of cyanide exposure is inhalation of environmental tobacco smoke. This study concerns importance to determine cyanide ion in human biological samples. Urine and saliva samples were collected healthy volunteers exposed to tobacco...
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OCENA JAKOŚCI DESTYLATÓW ROLNICZYCH WYKONANYCH ZA POMOCĄ PROTOTYPU ELEKTRONICZNEGO NOSA I FAST/FLASH GC
PublikacjaPrzedstawiono wyniki badań oceny jakości destylatów rolniczych przy pomocy prototypu elektronicznego nosa i komercyjnego elektronicznego nosa typu Fast/Flash GC - HERACLES II. Prototyp był wyposażony w zestaw sześciu półprzewodnikowych czujników firmy FIGARO. HERACLES II wyposażony był w dwie kolumny chromatograficzne z różną polarnością fazy stacjonarnej oraz dwa detektory FID. Frakcję lotną próbek destylatu rolniczego wytwarzano...
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Rozpoznawanie urządzeń i wykrywanie nieautoryzowanego poboru energii elektrycznej na podstawie pomiaru napięcia
PublikacjaW pracy rozpatrywany jest problem wykrywania nieautoryzowanego poboru energii z sieci elektrycznej przez identyfikację podłączonych urządzeń. Estymacja stanu sieci, rozumianej jako zbiór podpiętych układów, wraz z ustaloną listą urządzeń dopuszczonych, pozwala określić, czy w danej chwili ma miejsce pobór nieautoryzowany. W celu wykrywania urządzeń, proponuje się wykorzystać prostą metodę opartą na analizie wysokoczęstotliwościowego...
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Processing, Performance Properties, and Storage Stability of Ground Tire Rubber Modified by Dicumyl Peroxide and Ethylene-Vinyl Acetate Copolymers
PublikacjaIn this paper, ground tire rubber was modified with dicumyl peroxide and a variable content (in the range of 0–15 phr) of ethylene-vinyl acetate copolymers characterized by different vinyl acetate contents (in the range of 18–39 wt.%). Modification of ground tire rubber was performed via an auto-thermal extrusion process in which heat was generated during internal shearing of the material inside the extruder barrel. The processing,...
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Chemical Composition of Atmospheric Air in Nemoral Scots Pine Forests and Submountainous Beech Forests: The Potential Region for the Introduction of Forest Therapy
PublikacjaStudies show that forests are one of the main recreational destinations. This can be explained by their beneficial effects on the health of their visitors, which can be attributed to compounds from the terpene group. The aim of this research was to determine the chemical composition of air in the interiors of Nemoral Scots pine forests and submountainous beech forests, with the determination of compounds of the terpene group. Samples...
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Semi complex navigation with an active optical gesture sensor
PublikacjaThis paper presents the methods of diversified touchless interactions between a user and a mobile platform utilizing the optical gesture sensor. The sensor uses 8 photodiodes to measure the reflected light in the active mode (using embedded LEDs) or it measures shadows caused by fingers in the passive mode. Several algorithms were implemented: automatic mode switching, adaptive illumination level compensation, resolution improvements...
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Automatic analysis of the aggressive behavior of laboratory animals using thermal video processing
PublikacjaThe bite detection is very important but difficult element of the social interaction analysis. Standard observation methods like human observer or a camcorder of visible light frequencies fail in this case. However, it is possible to discern cooler spots on the rodent's body that appear after body contact with another individual, and vanish after short time. These spots are assumed to be a saliva trace left on fur after bite. In...
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Detection and localization of selected acoustic events in acoustic field for smart surveillance applications
PublikacjaA method for automatic determination of position of chosen sound events such as speech signals and impulse sounds in 3-dimensional space is presented. The evens are localized in the presence of sound reflections employing acoustic vector sensors. Human voice and impulsive sounds are detected using adaptive detectors based on modified peak-valley difference (PVD) parameter and sound pressure level. Localization based on signals...
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Audio-visual surveillance system for application in bank operating room
PublikacjaAn audio-visual surveillance system able to detect, classify and to localize acoustic events in a bank operating room is presented. Algorithms for detection and classification of abnormal acoustic events, such as screams or gunshots are introduced. Two types of detectors are employed to detect impulsive sounds and vocal activity. A Support Vector Machine (SVM) classifier is used to discern between the different classes of acoustic...
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Quality evaluation of agricultural distillates using different types of electronic noses
PublikacjaThe paper presents the results of investigation on quality evaluation of agricultural distillates using a prototype of electronic nose instrument and a commercial electronic nose of Fast/Flash GC type – HERACLES II. The prototype was equipped with TGS type semiconductor sensors. HERACLES II included two chromatographic columns with different polarity of stationary phase and two FID detectors. In case of the prototype volatile fraction...
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Processing of acoustical data in a multimodal bank operating room surveillance system
PublikacjaAn automatic surveillance system capable of detecting, classifying and localizing acoustic events in a bank operating room is presented. Algorithms for detection and classification of abnormal acoustic events, such as screams or gunshots are introduced. Two types of detectors are employed to detect impulsive sounds and vocal activity. A Support Vector Machine (SVM) classifier is used to discern between the different classes of...
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Nanostruktury metalicznego bizmutu w redukowanych szkłach bizmutowo-germanianowych i bizmutowo-krzemianowych: wytwarzanie, struktura i transport nośników ładunku.
PublikacjaW pracy przedstawiono rezultaty badań struktury i własności transportowych szkieł bizmutowo-germanianowych i bizmutowo-krzemianowych. Potwierdzono, że przewodnictwo elektryczne jest typu jonowego. Tymi jonami są jony tlenu. Opisano związek między kolorem szkieł, a koncentracją jonów tlenu. Zbadano wpływ wygrzewania w atmosferze wodoru na własności szkieł. Opisano w sposób jakościowy i ilościowy procesy tworzenia się w wyniku redukcji...
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Detection and localization of selected acoustic events in 3D acoustic field for smart surveillance applications
PublikacjaA method for automatic determination of position of chosen sound events such as speech signals and impulse sounds in 3-dimensional space is presented. The events are localized in the presence of sound reflections employing acoustic vector sensors. Human voice and impulsive sounds are detected using adaptive detectors based on modified peak-valley difference (PVD) parameter and sound pressure level. Localization based on signals...
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Comparison of various speech time-scale modificartion methods
PublikacjaThe objective of this work is to investigate the influence of the different time-scale modification (TSM) methods on the quality of the speech stretched up using the designed non-uniform real-time speech time-scale modification algorithm (NU-RTSM). The algorithm provides a combination of the typical TSM algorithm with the vowels, consonants, stutter, transients and silence detectors. Based on the information about the content and...
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Investigations of the Methods of Time Delay Measurement of Stochastic Signals Using Cross-correlation with the Hilbert Transform
PublikacjaThe article presents the results of simulation studies of four methods of estimating time delay for random signals using cross-correlation with the Hilbert Transform. Selected models of mutually delayed stochastic signals were used in the simulations, corresponding to the signals obtained from scintillation detectors in radioisotope measurements of liquid-gas two-phase flow. Standard deviations of the values of the individual functions...
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Investigation of Liquid–Gas Flow in a Horizontal Pipeline Using Gamma-Ray Technique and Modified Cross-Correlation
PublikacjaThis article presents the application of the radioisotope absorption method in the study of two-phase water–air flow in a horizontal pipe. The measurement principle and the test stand are briefly described. The main part of the article presents the signal analysis methods applied to data obtained from scintillation detectors. Because these signals are mostly stochastic waveforms, they were analyzed statistically using the cross-correlation...
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Technology of an adhesive silicone film as drug carrier in transdermal therapy I. Analytical methods used for characterization and design of the universal elastomer layers
PublikacjaSilicone polymers possess unique properties, which make them suitable for many different applications, for example in the pharmaceutical and medical industry. To create an adhesive silicone film, the appropriate silicone components have to be chosen first. From these components two layers were made: an adhesive elastomer applied on the skin, and a non-adhesive elastomer on the other side of the film. The aim of this study was...
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Forced Degradation Studies of Ivabradine and In Silico Toxicology Predictions for Its New Designated Impurities
PublikacjaAll activities should aim to eliminate genotoxic impurities and/or protect the API against degradation. There is a necessity to monitor impurities from all classification groups, hence ivabradine forced degradation studies were performed. Ivabradine was proved to be quite durable active substance, but still new and with insufficient stability data. Increased temperature, acid, base, oxidation reagents and light were found to cause...
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The Thin-Layer Microchromatography (μTLC) and TLC–FID Technique as a New Methodology in the Study of Lubricating Oils
PublikacjaThis paper concerns the possibility of using TLC coupled with a flame ionization detector (FID) and micro-TLC (μTLC) as precursors for microfluidized devices of analytical techniques to identify and determine the presence and content of the petroleum/vegetable oil base in the lubricating oils applied in cutting devices (chainsaws). This research is related to the problem of ensuring, in compliance with the requirements of environmental...
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Clothes Detection and Classification Using Convolutional Neural Networks
PublikacjaIn this paper we describe development of a computer vision system for accurate detection and classification of clothes for e-commerce images. We present a set of experiments on well established architectures of convolutional neural networks, including Residual networks, SqueezeNet and Single Shot MultiBox Detector (SSD). The clothes detection network was trained and tested on DeepFashion dataset, which contains box annotations...
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Contour Analysis of Bleeding Regions in Endoscopic Images
PublikacjaThis paper investigates the problem of detecting bleeding regions in images acquired from endoscopic examinations of gastrointestinal tract. The purpose is to identify the characteristic features of bleeding areas' contours in order to develop an accurate method for discriminating between true bleeding regions and missed detections, which could lead to a significant reduction of the false alarm rate of existing blood-detection...
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Analysis of pesticide residue in fruits and vegetables using analytical analytical protocol based on application of QuEChERS technique and GC-ECD system
PublikacjaQuEChERS sample preparation method was used for the determination of 10 pesticides and their metabolites in fruits (apple, grape) and vegetables (tomato, paprika), coupled to gas chromatography with electron capture detector (GC-ECD). The experimental parameters including amount of the sample, types of solvents, extraction time and types of sorbent at the purification stage were optimized. The GC-ECD method was validated in terms...
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Current trends in analytical strategies for the determination of polybrominated diphenyl ethers (PBDEs) in samples with different matrix compositions – Part 2: New approaches to PBDEs determination
PublikacjaHerein, we review the latest technical solutions for polybrominated diphenyl ethers (PBDEs) determination in samples with different matrix compositions, largely focusing on gas chromatography but also presenting some liquid chromatography–based solutions. Moreover, we discuss the use of diverse sample injection techniques while considering the advantages and disadvantages of each injection system in the context of PBDEs analysis....
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Machine learning applied to acoustic-based road traffic monitoring
PublikacjaThe motivation behind this study lies in adapting acoustic noise monitoring systems for road traffic monitoring for driver’s safety. Such a system should recognize a vehicle type and weather-related pavement conditions based on the audio level measurement. The study presents the effectiveness of the selected machine learning algorithms in acoustic-based road traffic monitoring. Bases of the operation of the acoustic road traffic...
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Machine learning applied to acoustic-based road traffic monitoring
PublikacjaThe motivation behind this study lies in adapting acoustic noise monitoring systems for road traffic monitoring for driver’s safety. Such a system should recognize a vehicle type and weather-related pavement conditions based on the audio level measurement. The study presents the effectiveness of the selected machine learning algorithms in acoustic-based road traffic monitoring. Bases of the operation of the acoustic road traffic...
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Solvent residue determination in Uncaria Tomentosa Bark by HS-GC technique
PublikacjaPrzedstawiono wyniki oznaczeń pozostałości rozpuszczalników organicznych w preparacie uzyskanym z kory liany U. Tomentosa, wykorzystywanej do produkcji farmaceutyków i dodatków do żywności. 1,1,2-trichloroeten oraz dichlorometan są powszechnie stosowane do usunięcia z kory kilku grup alkaloidów o znanych właściwościach biologicznych, co umożliwia zbadanie pozostałych jej związków. Ilościowe oznaczanie tych rozpuszcalników jest...
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Detekcja uszkodzeń w analogowych układach w pełni różnicowych.
PublikacjaPrzedmiotem pracy jest detekcja uszkodzeń w analogowych układach elektronicznych o architekturze w pełni różnicowej, cechującej się strukturalną redundancją ułatwiającą testowanie i diagnostykę. W oparciu o model matematyczny układów w pełni różnicowych, usystematyzowano metody ich testowania. Wykazano, że dotychczas stosowane metody są kosztowne w odniesieniu do układów ze wzmacniaczami operacyjnymi, w których zastosowano sprzężenie...
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Analysis of arsenic species in environmental samples
PublikacjaMany analytical methods for determining arsenic in various forms in environmental samples have been developed in recent years. The main objective of this review article is the presentation and comparison of the three principal techniques for the determination arsenic compounds, namely: hydride generation (HG), voltammetry and chromatography (liquid chromatography including high-performance liquid chromatography (HPLC), and gas...
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Optical method supported by machine learning for dynamics of C‐reactive protein concentrations changes detection in biological matrix samples
PublikacjaIn this article we present the novel spectroscopy method supported with machine learning for real-time detection of infectious agents in wastewater. In the case of infectious diseases, wastewater monitoring can be used to detect the presence of inflammation biomarkers, such as the proposed C-reactive protein, for monitoring inflammatory conditions and mass screening during epidemics for early detection in communities of concern,...
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Signals features extraction in radioisotope liquid-gas flow measurements using wavelet analysis
PublikacjaKnowledge of the structure of a flow is significant for the proper conduct of a number of industrial processes. In this case, a description of a two-phase flow regimes is possible by use of the time-series analysis in time, frequency and state-space domain. In this article the Discrete Wavelet Transform (DWT) is applied for analysis of signals obtained for water-air flow using gamma ray absorption. The presented method was illustrated...
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Occurence volatile halogenoorganic compounds in precipitation in an urban area in Tricity (Gdańsk-Gdynia-Sopot). Występowanie lotnych związków fluorowcoorganicznych w opadach atmosferycznych na terenie miejskim.
PublikacjaSzczególne znaczenie wśród zanieczyszczeń występujących w wielkomiejskim powietrzu atmosferycznym, mają lotne związki chlorowcoorganiczne, ze względu na powszechność stosowania i trwałość (od 77 dni - CH2Cl2 do 67 lat - CCl4). Większość związków chlorowcoorganicznych stanowi zagrożenie dla życia ludzkiego przez swoje kancerogenne, mutagenne i teratogenne działanie. Związki chlorowcoorganiczne obecne w środowisku są w większości...
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Determination of volatile organohalogen compounds in urban precipitation in Tricity area (Gdańsk, Gdynia, Sopot).
PublikacjaPróbki opadów atmosferycznych pobierano w 4 punktach na terenie Gdańska i Sopotu, od listopada 2000 do maja 2001. Oznaczano chloro- i bromopochodne metanu, etanu i etenu. Lotne związki chlorowcoorganiczne oznaczane były metodą bezpośredniego nastrzyku próbki wody do kolumny kapilarnej z wykorzystaniem detektora wychwytu elektronów na etapie detekcji (DAI-GC-ECD). Najczęściej oznaczanymi związkami na wszystkich stacjach pobierania...
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A Surrogate-Assisted Measurement Correction Method for Accurate and Low-Cost Monitoring of Particulate Matter Pollutants
PublikacjaAir pollution involves multiple health and economic challenges. Its accurate and low-cost monitoring is important for developing services dedicated to reduce the exposure of living beings to the pollution. Particulate matter (PM) measurement sensors belong to the key components that support operation of these systems. In this work, a modular, mobile Internet of Things sensor for PM measurements has been proposed. Due to a limited...
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Chromatografia cienkowarstwowa i technika TLC-FID w badaniach składu grupowego, szczególnie, tłuszczów i produktów ich konwersji
PublikacjaPraca dotyczy zbadania celowości stosowania oraz określenia korzystnych warunków wykorzystania "klasycznej" chromatografii cienkowarstwowej w normalnych układach faz (NP-TLC) oraz techniki chromatografii cienkowarstwowej z detekcją płomieniowo - jonizacyjną (TLC-FID) na pręcikach kwarcowych, jako technik zapewniających oznaczanie składu grupowego, w badaniach nad: - ustaleniem optymalnych warunków rozdzielania grupowego tłuszczów...
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Diagnostyka cienkościennych żelbetowych sklepień kolebkowych w budynku zabytkowym. Część II
PublikacjaW artykule przedstawiono opis oraz wyniki oceny stanu technicznego konstrukcji przekrycia Hali Głównej Dworca Kolejowego Gdańsk Główny. Ze względu na prowadzone prace związane z remontem kapitalnym Dworca Głównego PKP w Gdań- sku zaistniała konieczność przeprowadzenia rewitalizacji poddasza Hali Głównej, obejmująca między innymi jego termomodernizację (ocieplenie wysklepek) oraz zabezpieczenie elementów wiązarów dachowych przed...
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Forced degradation studies of ivabradine and in silico toxicology predictions for its new designated impurities
PublikacjaAll activities should aim to eliminate genotoxic impurities and/or protect the API againstdegradation. There is a necessity to monitor impurities from all classification groups,hence ivabradine forced degradation studies were performed. Ivabradine was provedto be quite durable active substance, but still new and with insufficient stability data.Increased temperature, acid, base, oxidation reagents and...
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Improvement of glass break acoustic signal detection via application of wavelet packet decomposition
PublikacjaThe main subject of the authors' research are non-contact methods of glass break detection based on analysis of the acoustic signal generated during the event. This problem has essential meaning for modern cost- effective alarm systems, particularly those installed into big buildings. The main difficulties of the matter are: transient character of the signal, great number of similar sounds (false signals, mainly accidental glass...
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Interrelationship between total volatile organic compounds emissions, structure and properties of natural rubber/polycaprolactone bio-blends cross-linked with peroxides
PublikacjaNatural rubber/polycaprolactone (NR/PCL) bio-based blends with different organic peroxides were prepared using an internal batch mixer and subsequently cross-linked at 170°C. Two types of commonly used organic peroxides, dicumyl peroxide and di(tert-butylperoxyisopropyl)benzene peroxide, were applied as free-radical initiator. Cross-linking efficiency of NR/PCL blends were investigated using oscillating disc rheometer measurements,...
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Key-Marker Volatile Compounds in Aromatic Rice (Oryza sativa) Grains: An HS-SPME Extraction Method Combined with GC×GC-TOFMS
PublikacjaThe aroma of rice essentially contributes to the quality of rice grains. For some varieties, their aroma properties really drive consumer preferences. In this paper, using a dynamic headspace solid-phase microextraction (HS-SPME) system coupled to a two-dimensional gas chromatography (GC×GC) using a time-of-flight mass spectrometric detector (TOFMS) and multivariate analysis, the volatile compounds of aromatic and non-aromatic...