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wyświetlamy 1000 najlepszych wyników Pomoc
Wyniki wyszukiwania dla: MEMORIAL SITES
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Memorial Viewpoint for Shulamith Schlick
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ОТТОКАР УЛЬ. IN MEMORIAM
PublikacjaОттокар Уль считается одним из самых влиятельных архитекторов Австрии второй половины ХХ века. Он внес значительный вклад в развитие партисипативных методов проектирования и пост-соборной реформы сакральной архитектуры. Статья освещает его биографию, идеи и проекты, а также и публикации. Кажется, что стоит, чтобы данный архитектор присутствовал в нашей памяти.
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In Memoriam Professor Jerzy KAPELEWSKI
PublikacjaProfessor Jerzy Kapelewski In Memoriam
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In memoriam dr Marek Baran
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Memorias
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Historical crane on the redesigned original trestle bridge as a memorial of Gdansk Shipyard
PublikacjaThe paper includes selected aspects of the study, whose goal is to hold the historical crane 642-24 in its current location after the modification of trestle bridge static scheme. The scope of the paper includes the assessment of current technical condition of the object, a presentation of FEM analyses, a description of the assumed load cases, results of the static calculations, checking the effort of construction elements, global...
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Conservation and Management of Archaeological Sites
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Spatial pattern of ASG-EUPOS sites
PublikacjaThe article presents the spatial pattern analysis of the ASG-EUPOS permanent GNSS stations in Poland. Using different methods and tools (nearest neighbour, Riplay’s K-function, morphology of Thiessen polygons) we proved that the station distribution model changes within scales. At short distances up to 65 km, which are typical lengths in the network, stations are irregularly dispersed. Increasing this distance to 130 km and over...
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COMMON FIRE CAUSES IN INDUSTRIAL SITES
PublikacjaChapter presents common causes of fires in industrial places
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Contemporary French & Francophone Studies: Sites
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Investigation on stability of mountainous EUPOS sites’ coordinates
PublikacjaThe paper concerns analysis of solutions obtained during common processing of data from GNSS permanent stations situated on mountainous terrain: the Western Carpathians, the Sudetes Mountains and adjacent areas. As the outcome daily and weekly solutions (ellipsoidal coordinates) of forty Polish, Czech, Slovak, Ukrainian and German sites were obtained. Weekly solutions were used to determine velocity field and vertical movements,...
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New Eu2 +sites in KMgF3:Eu2 +crystal
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Projekt IST-2001-33441-MEMORIAL: zestaw narzędziowy do tworzenia dokumentów cyfrowych z zapisów osobowych
PublikacjaKonsorcjum projektu MEMORIAL zakłada osiągnięcie w 2,5 roku czterech podstawowych celów: opracowania nowych metod i narzędzi do przetwarzania i rozpoznawania dokumentów papierowych wypełnianych na maszynie, opracowanie narzędzi do interaktywnej manipulacji i oceny jakości dokumentu cyfrowego w różnych fazach jego cyklu życia, określenie prawnych, społecznych, etycznych i politycznych uwarunkowań tworzenia bibliotek cyfrowych zawierających...
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Chemometric analysis of rainwater and throughfall at several sites in Poland.
PublikacjaPróbki pobrano w stacjach w różnych rejonach Polski. Stacje te były umieszczone na terenach specjalnie chronionych (Wielkopolski Park Narodowy i Ojcowski Park Narodowy) oraz na niechronionych formacjach leśnych (leśnictwo Stara Piła). Celem badań było porównanie parametrów występujących w opadach atmosferycznych pod względem podobieństwa charakterystyki miejsca a także podobieństw i różnic związanych z przejściem wody opadowej...
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Simplified AutoDock force field for hydrated binding sites
Publikacjahas been extracted from the Protein Data Bank and used to test and recalibrate AutoDock force field. Since for some binding sites water molecules are crucial for bridging the receptor-ligand interactions, they have to be included in the analysis. To simplify the process of incorporating water molecules into the binding sites and make it less ambiguous, new simple water model was created. After recalibration of the force field on...
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Copper containing protein sites - structure, properties and models
PublikacjaEnzymy organizmów żywych katalizują wiele reakcji stosowanych w przemyśle chemicznym. Przykładem potencjalnego zastosowania enzymu w produkcji jest synteza L-Dopy przy udziale tyrozynazy. Ze względu na możliwe praktyczne zastosowanie w katalizie, otrzymano i opisano wiele prostych modeli miejsc aktywnych enzymów. W artykule opisano niektóre modele białek zawierających miedź.
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Inhomogeneous broadening of the dominant Cr3+sites in LiTaO3 system
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A NEW WORK SAFETY MANAGEMENT SYSTEM IN CONSTRUCTION SITES
PublikacjaThe hazards on the list are assessed on two levels, namely as minor and serious, and the risk relating to work at the site at three levels: small, average and high, within the range from 1 to 10, where 1 is the lowest value meaning a small risk, and 10 the value meaning a high risk.
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Koncert "In memoriam"
WydarzeniaKoncert w Archikatedrze Oliwskiej wykonają: Polska Orkiestra Kameralna Sopot, Akademicki Chóru Politechniki Gdańskiej oraz uznani soliści. W repertuarze "Requiem" W.A. Mozarta.
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Historia y Memoria
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Memoria e Ricerca
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Patrimonio e Memoria
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THE CIRCUS SITE
PublikacjaThe location of project is a site of over 1,2 ha, situated on the southern fringes of Gdynia formerly used as an area to host a Circus. Here artists were performing for the public, newcomers were meeting the locals, the temporality of the event was enhancing the experience of exchange. Circus used to be the place where people live, work and create art. Currently the site stays empty but surely not for long. Its potential, attractive...
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Experience-based knowledge increases confidence in discriminating our memories
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In Memoriam Professors Marianna Sankiewicz-Budzyński and Gustaw K.E. Budzyński - Founders of the Polish Audio Engineering
PublikacjaBiography and scientific achievements of Professors Marianna Sankiewicz-Budzyński and Gustaw K.E. Budzyński - Founders of the Polish Audio Engineering.
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Environmental Role of Rime Chemistry at Selected Mountain Sites in Poland
PublikacjaThe results of field experiments on fog pollutantdeposition enhanced by local mountain climate, completed by thedendrochronological analysis of the forest response, are presentedin this paper. In spite of their low absolute altitude (1,000-1,600 ma.s.l), the Sudetes and the Silesian Beskid form a noticeable orographicbarrier for the airflow of the humid Atlantic air masses.This results in the increase of cloudiness and fog frequency...
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Luminescence properties of different Eu sites in LiMgPO4:Eu2+, Eu3+
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Architektura pomników poświęconych ofiarom ataków terrorystycznych jako kontynuacja realizacji komemoratywnych kształtowanych w postpamięci
Publikacjaarchitecture of Memorials Dedicated to the Victims of terrorist attacks as a continuation of commemorative Structures created within Post-memory Having the rich art of commemorating events of the Second World War as a key reference, this article will try to show how contemporary architectural interven- tions in public space make attempts to respond to the social need of dealing with traumatic events and formulating a new attitude...
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Low and high field sites of Cr3+ ions in calcium tetraborate glasses
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Gazeta Uniwersytecka. Czasopismo Społeczności Akademickiej Uniwersytetu Gdańskiego: wydanie specjalne: Zbigniew Żakiewicz. In memoriam (redakcja naukowa)
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Modified Ventral Femoral Head and Neck Ostectomy: A Canine Cadaver Study
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Functional Protein Composition in Femoral Glands of Sand Lizards (Lacerta agilis)
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Influence of the femoral offset on the muscles passive resistance in total hip arthroplasty
PublikacjaBackground Soft tissue tension is treated as a crucial factor influencing the post-THA dislocation. The femoral offset is regarded as one of the major parameters responsible for the stabilization of the prosthesis. It is unclear which soft tissue is mostly affected by the offset changes. Methods A finite element model of the hip was created. The model comprised muscles, bones, a stem, the acetabular component and a liner. The muscles...
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Memoria-Investigaciones en Ingenieria
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Assessment of the potential for dredged material dispersal from dumping sites in the Gulf of Gdańsk
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Heavy-metal tolerance of photobiont in pioneer lichens inhabiting heavily polluted sites
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Cadmium tri-tert-butoxysilanethiolates. Structural and spectroscopic models of metal sites in proteins.
PublikacjaW publikacji opisano syntezy i struktury dla dwóch heteroleptycznych kompleksów kadmu z rdzeniem CdS2NO2 i CdS2N2. Bis(tri-tert-butoksysilanotiolato)(1-metyloimidazol)kadmu(II) oraz bis(tri-tert-butoksysilanotiolato)bis(1-metyloimidazol)kadmu(II) współistnieją w roztworze chloroformu przy różnych stężeniach Bis(tri-tert-butoksysilanotiolanu) kadmu(II) i 1 metyloimidazolu. Rotzwór ten został scharakteryzowany za pomocą analizy spektralnej...
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Comparative Analysis of CpG Sites and Islands Distributed in Mitochondrial DNA of Model Organisms
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Wisłoujście Fortress, site 12
PublikacjaThis introductory article provides a synopsis of the range of archaeological work carried out at Wisłoujście Fortress in Gdańsk in 2013 and 2014. An outline is given of the circumstances in which this work was undertaken, the fieldwork methodology used and the technical problems encountered during excavation.
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Comparison of usefulness of different diagnostic procedures in slipped capital femoral epiphysis in cats
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Accuracy of CAD/CAM and 3D printing in the treatment of feline femoral neck fracture
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Novel Potential Binding Sites for Selective Inhibitor Design of Human Soluble Epoxide Hydrolase
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Characterization of various Eu2+ sites in Ca2SiO4:Eu2+ and Ba2SiO4:Eu2+ by high-pressure spectroscopy
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Endophytic microbiota and ectomycorrhizal structure of Alnus glutinosa Gaertn. at saline and nonsaline forest sites
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Redox property switching in MOFs with open metal sites for improved catalytic hydrogenation performance
PublikacjaIn this study, a decompression-thermalization strategy was utilized for a Cu-containing metal-organic framework (MOF) to tune its redox and catalytic hydrogenation properties. Remarkably, at just 120 °C, open metal sites (OMSs) were successfully constructed by removing coordinated solvent molecules to generate the daughter MOF-120. The tailored redox property of MOF-120 is correlated with the presence of OMSs. Compared with the...
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On extremal sizes of locally k-tree graphs
PublikacjaA graph G is a locally k-tree graph if for any vertex v the subgraph induced by the neighbours of v is a k-tree, k>=0, where 0-tree is an edgeless graph, 1-tree is a tree. We characterize the minimum-size locally k-trees with n vertices. The minimum-size connected locally k-trees are simply (k + 1)-trees. For k >= 1, we construct locally k-trees which are maximal with respect to the spanning subgraph relation. Consequently, the...
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Autoimmunity and Cancer—Two Sides of the Same Coin
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Site-to-site distance distribution in flexible molecules: theoretical evaluation of the donor and/or acceptor fluorescence decay function
PublikacjaPrzedstawiono wyrażenie teoretyczne opisujące zależność funkcji zaniku fluorescencji od rozkładu odległości P(r) pomiędzy donorami i akceptorami w giętkich molekułach dwuchromoforowych. Wyrażenie uwzględnia wiekoeksponencjalny zanik izolowanych donorów i akceptorów, a także możliwość niekompletnego oznakowania molekuł akceptorami. Przyjęto, że względne zmiany odległości donorów i akceptorów w czasie życia fluorescencji donora mogą...
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MEMORIAS DO INSTITUTO OSWALDO CRUZ
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Ce-modified zeolite BEA catalysts for the trichloroethylene oxidation. The role of the different and necessary active sites
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Memoria Americana. Cuadernos de Etnohistoria
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OTHER AND ILL-DEFINED SITES, Intra-abdominal site, NOS - Female, 53 - Tissue image [7270729584625041]
Dane BadawczeThis is the histopathological image of OTHER AND ILL-DEFINED SITES tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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OTHER AND ILL-DEFINED SITES, Intra-abdominal site, NOS - Female, 53 - Tissue image [3300730069476321]
Dane BadawczeThis is the histopathological image of OTHER AND ILL-DEFINED SITES tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Formation of bubbles from a single nucleation site.
PublikacjaPrzedstawiono wyniki systematycznych badań eksperymentalnych wrzenia wody destylowanej i metanolu z pojedynczego, sztucznego centrum nukleacji. Jako centra nukleacji służyły otwory wywiercone na czołowej powierzchni miedzianego pręta. Średnice otworów wynosiły: 0.25 mm, 0.60 mm oraz 1.0 mm. Do pomiaru częstotliwości odrywania się pęcherzyków zastosowano układ laser diodowy-fotodioda. Sygnał z fotodiody był rejestrowany za...
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Digitalization of Building Site Management in the Construction Industry
PublikacjaWith Industry 4.0, a digital transformation has started in the construction industry. However, 4.0 technologies have difficulties in the integration of digital systems due to the diversity and complexity of the processes in the construction industry. Multidisciplinary work in architectural projects and the need for high productivity require digital renovation planning in the construction industry. The application of the technologies...
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The profit as in-company evaluation of the construction site effectiveness
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Site-selective magnetic order of neptunium inNp2Ni17
PublikacjaWe present the results obtained by superconducting quantum interference device (SQUID) magnetometry, specific heat, and Mossbauer spectroscopy measurements carried out on Np2Ni17 polycrystalline samples. We show that long-range magnetic order, with a moment mu((2b)) similar to 2.25 mu(B), occurs below T-N = 17.5 K on the Np (2b) sites. A nontrivial situation is observed in that the other Np sites (2d) do not take part to the order...
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Waste disposal sites as sources of mercury in the atmosphere in the coastal zone of the Gulf of Gdańsk (southern Baltic Sea)
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Highly efficient rutile TiO2 photocatalysts with single Cu(ii) and Fe(iii) surface catalytic sites
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Insights into the Effects of Cancer Associated Mutations at the UPF2 and ATP-Binding Sites of NMD Master Regulator: UPF1
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Application des essais au dilatometre Marchetti en sites maritime et fluvial en Pologne
PublikacjaPrzedstawiono wyniki i interpretację badań DMT zrealizowanych w strefie nadmorskiej i na wałach przeciwpowodziowych w delcie Wisły.Przedstawiono zastosowanie badania dylatometrycznego do kontroli zagęszczenia, opisu stanu i historii naprężenia w gruncie oraz do kontroli stanu, renowacji i wzmocnienia wałów przeciwpowodziowych.
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INTERLABORATORY COMPARISON OF THE ELECTROMAGNETIC EMISSION MEASUREMENTS USING FAR AND GTEM TEST SITES UP TO 1 GHz
PublikacjaElectromagnetic emission limiting is one of the basic requirements in the European Directive 2014/30/EU (EMC Directive). Manufacturers often use alternative methods of measurements to make preliminary verification of emission. This paper presents and analyzes problem with comparison between measurements in different test sites: FAR (Fully Anechoic Room) and GTEM (Gigahertz Transverse Electromagnetic cell). FAR is assumed as the...
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Mapping the Transglycosylation Relevant Sites of Cold-Adapted β-D-Galactosidase from Arthrobacter sp. 32cB
PublikacjaB-Galactosidase from Arthrobacter sp. 32cB (ArthbetaDG) is a cold-adapted enzyme able to catalyze hydrolysis of beta-D-galactosides and transglycosylation reaction, where galactosyl moiety is being transferred onto an acceptor larger than a water molecule. Mutants of ArthbetaDG D207A and E517Q were designed to determine the significance of specific residues and to enable formation of complexes with lactulose and sucrose and to...
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Generation of conformance test suites for parallel and distributed languages and APIS.
PublikacjaArtykuł zarysowuje nową metodologię systematycznego tworzenia Zestawów Testów Zgodności. Testowanie zgodności ma na celu sprawdzenie, czy implementacja jest zgodna ze swoją specyfikacją, co jest szczególnie ważne w środowiskach równoległych i rozproszonych, gdzie musi ze sobą współpracować wiele różnych pakietów. Autor rozpoczął swoje badania w dziedzinie testowania zgodności dla języka równoległego sterowanego danymi Athapascan,...
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Bulletin de la Commission royale des Monuments et Sites
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Relationship of ground-level aerosol concentration and atmospheric electric field at three observation sites in the Arctic, Antarctic and Europe
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Distribution of gaseous and particle-bound Hg concentrations at the sites representative for urban and non-urban zones of Silesia Province
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New Pr3+ site in β-SiAlON red phosphor
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Monument / Las Szpęgawski
PublikacjaWspółczesne monumenty często projektowane są tak, aby angażować uwagę odwiedzających miejsce pamięci nie tylko pod względem wizualnym. Zapraszają one do wejścia w swoją przestrzeń, nawet do dotknięcia powierzchni, a tym samym tworzą bliższe i bogatsze więzi ze zwiedzającymi. Tekst przedstawia Monument Pamięci w Lesie Szpęgawskim autorstwa Katarzyny Ephraim jako współczesne miejsce pamięci.
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Investigation of MIEX® resin sedimentation in the aspect of particle sizes remaining in the supernatant
PublikacjaThe aim of the study was to evaluate the effectiveness of the MIEX® resin sedimentation process, both new and repeatedly used in hybrid water treatment MIEX®DOC + microfiltration (MF) or ultrafiltration (UF) processes (repeatedly regenerated). The tests consisted of performing 1 h sedimentation of the suspension resin in nonflow conditions and analysis of supernatant water at different process durations. The suspension weight analysis...
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Objects classification based on their physical sizes for detection of events in camera images
PublikacjaIn the paper, a method of estimation of the physical sizes of the objects tracked in the video surveillance system, and a simple module for object classification based on the estimated physical sizes, are presented. The results of object classification are then used for automatic detection of various types of events in the camera image.
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Tensile strength of a weave tendon suture using tendons of different sizes
PublikacjaThis study compared the maximum load, stress, elongation at failure and the mode of failure of three kinds of tendons most frequently used for tendon grafting and tendon transfers, using the Pulvertaftweave suture.
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Middle Eastern Christian Spaces in Europe: Multi-sited and Super-diverse
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High quality speech codec employing sines+noise+transients model
PublikacjaA method of high quality wideband speech signal representation employing sines+transients+noise model is presented. The need for a wideband speech coding approach as well as various methods for analysis and synthesis of sines, residual and transient states of speech signal is discussed. The perceptual criterion is applied in the proposed approach during encoding of sines amplitudes in order to reduce bandwidth requirements and...
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Sizes of iron hydroxide particles formed during ferric coagulation processes
PublikacjaThe aim of the study was to apply laser granulometer for measuring sizes of particles formed in iron-based coagulation process in water, which did not contain significant amounts of organic compounds. The research was conducted using tap water, obtained from underground sources. Iron sulfate in doses of 2.0–10.0 mgFe L–1 was added to water. During initial stage of flocculation, iron hydroxide particles reached dimensions between...
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The role of tungsten in formation of active sites for no SCR on the V-W-O catalyst surface — quantum chemical modeling (DFT)
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Tuning of eg electron occupancy of MnCo2O4 spinel for oxygen evolution reaction by partial substitution of Co by Fe at octahedral sites
PublikacjaTo study the effect of partial Co substitution by Fe in the B site of MnCo2O4 spinel on its physicochemical and electrochemical properties, a series of MnCo2-xFexO4 powders (x=0.125; 0.250; 0.500; 0.750; 1.000) were synthesized by means of the sol-gel method. The produced powders were characterized by powder X ray diffraction (pXRD), scanning and transmission electron microscopy (SEM & TEM) coupled with energy dispersive spectroscopy...
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Historia y Memoria de la Educacion
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Nuestro Sur-Historia Memoria y Patrimonio
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Memoria y Civilizacion-Anuario de Historia
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A tool for integrating Web Site services over User Interface
PublikacjaCompanies and organizations are building information systems by integrating previously independent applications, together with new developments. This integration process has to deal with existing applications, which can only be used through their specific interfaces, and often cannot be modified. Integration of web applications running remotely and controlled by separate organizations becomes even more complicated, as their user...
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Integrating web site services into application through user interface
PublikacjaThe issue of integrating applications which are only accessible through visual user interface is not thoroughly researched. Integration of web applications running remotely and controlled by separate organizations becomes even more complicated, as their user interface can display differently in different browsers or change without prior notification as a result of application maintenance. While possible, it is generally not common...
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Ce site dilution effects in the antiferromagnetic heavy fermion CeIn3
PublikacjaLa-doped intermetallic single crystals of Ce1−xLaxIn3 were synthesized via an In self-flux method throughout the entire range (x = 0–1). The prototypical heavy-fermion compound CeIn3 shows an antiferromagnetic phase transition at 10.1 K and becomes superconducting near a critical pressure where TN is completely suppressed. As the La concentration increases, Ce moments are diluted, and the lattice constant increases linearly, satisfying Vegard’s...
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Consumer social network brand identification and personal branding. How do social network users choose among brand sites?
PublikacjaBrands’ social networking sites (fan pages) are increasingly attracting the attention of scientists and managers intrigued by their potential application for brand value creation. The aim of this research is to understand better how users choose among social networking sites as an act of brand identification. The study presents a new model whose structure of identification drivers for social networking brand sites varies for customer...
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Promotion of MXene (Ti3C2Tx) as a robust electrocatalyst for oxygen evolution reaction via active sites of ZIF-67 - In situ mechanism investigations
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Generating reliable conformance test suites for parallel and distributed languages, libraries, and APIs.
PublikacjaArtykuł nakreśla nową metodykę dla tworzenia Zestawów Testów Zgodności (ZTG) dla języków, bibliotek i API programowania równoległego i rozproszonego. Autor rozpoczął swoje badania w zakresie testowania zgodności dla języka równoległego sterowanego danymi Athapascan, opracował metodykę dla projektowania i analizowania ZTG nazwaną Metodą Kolejnych Zawężeń (ang. Consecutive Confinements Methods - CoCoM), stworzył narzędzie CTS Designer,...
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Vipera berus Bites in the Region of Southwest Poland—A Clinical Analysis of 26 Cases
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Site environment type – The main factor of urban road dust toxicity?
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Sensitivity analysis of the contractor’s financial effects achieved on a single building site
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Some remarks on problem of site characterisation - a subjective experience on theory and practice
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The Baltic Sea as a dumping site of chemical munitions and chemical warfare agents
PublikacjaW pracy przedstawiono problem składowania w Morzu Bałtyckim aminucji chemicznej i bojowych środków trujących. Przedstawiono typy oraz charakterystykę BST składowanych na dnie Morza Bałtyckiego. Omówiono potencjalne zagrożenia dla środowiska abiotytcznego oraz dla organizmów żywych związanych z tego typu składowiskami. Przedstawiono również podstawowe informacje o procedurach analitycznych, które mogą być wykorzystane do wykrywania...
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Effect of Ion and Binding Site on the Conformation of Chosen Glycosaminoglycans at the Albumin Surface
PublikacjaAlbumin is one of the major components of synovial fluid. Due to its negative surface charge, it plays an essential role in many physiological processes, including the ability to form molecular complexes. In addition, glycosaminoglycans such as hyaluronic acid and chondroitin sulfate are crucial components of synovial fluid involved in the boundary lubrication regime. This study presents the influence of Na+, Mg2+ and Ca2+ ions...
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Chemical Composition of Atmospheric Air in Nemoral Scots Pine Forests and Submountainous Beech Forests: The Potential Region for the Introduction of Forest Therapy
PublikacjaStudies show that forests are one of the main recreational destinations. This can be explained by their beneficial effects on the health of their visitors, which can be attributed to compounds from the terpene group. The aim of this research was to determine the chemical composition of air in the interiors of Nemoral Scots pine forests and submountainous beech forests, with the determination of compounds of the terpene group. Samples...
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Tanatoarchitektura [=] Thanatoarchitecture
PublikacjaApart from medicine and philosophy, deliberations about thanatology - the science of dying and death - are nowadays a subject of interest in psychol-ogy, pedagogy, anthropology, sociology or theology. It seems that there is also space for such deliberations in the field of architecture. This may con-cern the conditions and dignity of death (i.e. in a hospice) but also matters related to the design of the burial and memorial sites....
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Pasado y memoria: Revista de historia contemporánea
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Clepsidra. Revista Interdisciplinaria de Estudios sobre Memoria
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Effects of sewage sludge supplementation on heavy metal accumulation and the expression of ABC transporters in Sinapis alba L. during assisted phytoremediation of contaminated sites
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Extension of the force-matching method to coarse-grained models with axially symmetric sites to produce transferable force fields: Application to the UNRES model of proteins
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Synthesis and Structure of Novel Copper(II) Complexes with N,O- or N,N-Donors as Radical Scavengers and a Functional Model of the Active Sites in Metalloenzymes
PublikacjaToevaluatetheantioxidantactivityofpotentialsyntheticenzymemimetics,wepreparednewfivecopper(II)complexesviaaself‐assemblymethodandnamedthem[Cu(2‐(HOCH2)py)3](ClO4)2(1),[Cu(2‐(HOCH2)py)2(H2O)2]SiF6(2),[Cu2(2‐(HOCH2CH2)py)2(2‐(OCH2CH2)py)2](ClO4)2(3),[Cu(pyBIm)3](BF4)2∙1.5H2O(4)and[Cu(py2C(OH)2)2](ClO4)2(5).ThesyntheticprotocolinvolvedN,O‐ orN,N‐donors:2‐(hydroxymethyl)pyridine(2‐(HOCH2)py),2‐(hydroxyethyl)pyridine(2‐(HOCH2CH2)py),2‐(2‐pyridyl)benzimidazole(pyBIm),di(2‐pyridyl)ke‐tone(py2CO).TheobtainedCu(II)complexeswerefullycharacterisedbyelementalanalysis,FTIR,EPR,UV‐Vis,single‐crystalX‐raydiffractionandHirshfeldsurfaceanalysis.Crystallographicandspectroscopicanalysesconfirmedchromophoresofbothmonomeric({CuN3O3}(1),{CuN2O4}(2),{CuN6}(4),{CuN4O2}(5))anddimericcomplex({CuN2O3}(3)).Mostoftheobtainedspeciespos‐sessedadistortedoctahedralenvironment,exceptdimer3,whichconsistedoftwocoppercentreswithsquarepyramidalgeometries.Thewater‐solublecompounds(1,3and5)wereselectedforbiologicaltesting.Theresultsofthestudyrevealedthatcomplex1insolutionsdisplayedbetterradicalscavengingactivitythancomplexes3,5andfreeligands.Therefore,complex1hasbeenselectedforfurtherstudiestotestitsactivityasanenzymemimetic.Thechosencompoundwastestedontheerythrocytelysateoftwogroupsofpatientsafterundergoingchemotherapyandchemoradiotherapy.Theeffectofthetestedcompound(1)onenzymeactivitylevels(TAS,SODandCAT)suggeststhattheselectedcomplexcanbetreatedasafunctionalmimeticoftheenzymes.
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Reclamation of phosphogypsum deposition site Wiślinka near Gdańsk with municipal sewage sludge.
PublikacjaOmówiono zastosowanie osadów ściekowych do rekultywacji składowiska fosfogipsów w Wiślince k. Gdańska. Głównie pojawiają się problemy ze stabilizacją stoków oraz z sukcesją roślinności i zwalczaniem erozji wiatrowej.