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Search results for: high-temperature oxidation
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Evaluation and start-up of an electro-Fenton-sequencing batch reactor for dairy wastewater treatment
PublicationThis study examined the performance of an integrated wastewater (WW) treatment system, namely an electro-Fenton (EF)-sequencing batch reactor (SBR), for dairy industry WW. The EF process was used as the first stage of the SBR. It degrades bio-refractory compounds via advanced oxidation processes, thereby resulting in the formation of simple biodegradable intermediates. Several factors, including the hydraulic retention time (HRT),...
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The interplay between dopant and a surface structure of the photocatalyst – The case study of Nb-doped faceted TiO2
PublicationAnatase nanoparticles, exposing the majority of the {0 0 1}, {1 0 0} and {1 0 1} facets were synthesized and doped with different niobium amount to investigate the self-trapping of the excess electrons and resulting photocatalytic activity. Photocatalyst structure and presence of excess electrons inside the obtained Nb-doped anatase samples was confirmed by the combination of structural and spectroscopic analyses. Only for the...
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Nanotubular oxide layers and hydroxyapatite coatings on porous titanium alloy Ti13Nb13Zr
PublicationThe surface condition of an implant has a significant impact on response occurring at the implant-biosystem border. The knowledge of physical-chemical and biological processes allows for targeted modification of biomaterials to induce a specified response of a tissue. The present research was aimed at development of technology composing of obtaining the nanotube oxide layers on a porous titanium alloy Ti13Nb13Zr, followed by the...
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Influence of Two-Stage Anodization on Properties of the Oxide Coatings on the Ti–13Nb–13Zr Alloy
PublicationThe increasing demand for titanium and its alloys used for implants results in need of such innovative surface treatment that may jointly increase corrosion resistance and biocompatibility, and demonstrate antibacterial protection at no cytotoxicity. The purpose of this research was to characterize the effect of two-stage anodization, performed for 30 min in phosphoric acid, at the presence of hydrofluoric acid in the second stage....
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Mono- and bimetallic (Pt/Cu) titanium(IV) oxide photocatalysts. Physicochemical and photocatalytic data of magnetic nanocomposites’ shell
PublicationSurface modification of titania with noble and semi-noble metals resulted in significant enhancement of photocatalytic activity. Presented data, showing the photocatalytic properties of TiO2-M (where M is Pt and/or Cu) photocatalysts were further used as Fe3O4@SiO2/TiO2-M magnetic nanocomposites shells in "Mono- and bimetallic (Pt/Cu) titanium(IV) oxide core-shell photocatalysts with Vis light activity and magnetic separability"...
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Laser induced formation of copper species over TiO2 nanotubes towards enhanced water splitting performance
PublicationWe proposed fast and scalable route where the ordered TiO2 nanotubes coated with thin copper layers were annealed by the laser beam of 355 nm wavelength at different fluencies in the range of 15–120 mJ/cm2. As a result, copper species are integrated with the titania substrate and the formed material exhibits unique optical absorption bands in the visible range. Moreover, X-ray photoelectron spectroscopy analysis reveals the formation...
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In-situ monitoring of electropolymerization processes at boron-doped diamond electrodes by Mach-Zehnder interferometer
PublicationIn this work, the Mach-Zehnder interferometer was designed to monitor the electrochemical processes conducted at boron-doped diamond electrode surface. The diamond electrodes were synthesized via Microwave Plasma-Assisted Chemical Vapor Deposition on optical grade quartz glass. The achieved transmittance in working are of diamond electrodes reached 55 %. A cage system-based Mach-Zehnder interferometer was used which allowed the...
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Method for the determination of carboxylic acids in industrial effluents using dispersive liquid-liquid microextraction with injection port derivatization gas chromatography–mass spectrometry
PublicationThe paper presents a new method for the determination of 15 carboxylic acids in samples of postoxidative effluents from the production of petroleum bitumens using ion-pair dispersive liquid-liquid microextraction and gas chromatography coupled to mass spectrometry with injection port derivatization. Several parameters related to the extraction and derivatization efficiency were optimized. Under optimized experimental conditions,the...
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Accurate Computation of IGBT Junction Temperature in PLECS
PublicationIn the article, a new method to improve the accuracy of the insulated-gate bipolar transistor (IGBT) junction temperature computations in the piecewise linear electrical circuit simulation (PLECS) software is proposed and described in detail. This method allows computing the IGBT junction temperature using a nonlinear compact thermal model of this device in PLECS. In the method, a nonlinear compact thermal model of the IGBT is...
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Speed dependency of temperature effects on road traffic noise
PublicationRecently, a new literature review on the influence of temperature on tire/road noise became available, based on a compilation of large amounts of data from empirical research. This review showed that the effect of temperature is roughly double of that previously assumed and taken account of in international standards. This makes temperature one of the main sources of error in measurement results. Furthermore, it suggested that...
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Temperature influence on tyre/road noise of selected tyres
PublicationAir and road temperatures substantially affect road vehicle noise emission. The temperature influence on tyre/road noise depends mainly on tyre-road combination. It is different for dense and porous pavements, for bituminous and cement ones. It differs also depending on tyres. The correction procedures for temperature effect are still under consideration and preparation. Tyre/road noise measurements using CPX method were performed...
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FEM and experimental investigations of concrete temperature field in the massive stemwall of the bridge abutment
PublicationThe paper deals with the prediction of early-age concrete temperature of cast-in-place stemwall of the bridge abutment. The considered object is an arch bridge located in Gda´nsk. In the case of massive structures, it is particularly important to not exceed the temperature difference between the core and the concrete surface. Too high temperature gradient generates an increase in thermal stresses, what could be the reason of exceeding...
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Temperature Sensors Based on Polymer Fiber Optic Interferometer
PublicationTemperature measurements are of great importance in many fields of human activities, including industry, technology, and science. For example, obtaining a certain temperature value or a sudden change in it can be the primary control marker of a chemical process. Fiber optic sensors have remarkable properties giving a broad range of applications. They enable continuous real-time temperature control in difficult-to-reach areas, in...
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Temperature influence on tyre/road noise frequency spectra
PublicationThe correction for temperature effect on measured tyre/road noise is very important as it may be one of the main sources of errors in measurement results due to substantial influence of this parameter on obtained values. The latest version of the Technical Specification ISO/CD TS 13471-1 about Temperature Corrections contains a proposal of correction procedure for normalizing measured noise levels to a reference air temperature...
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Influence of operation temperature instability on gas sensor performance
PublicationGas sensors based on the semiconducting metal-oxides, such as SnO2, have been found to be very useful for detecting a wide range of gases. The reversible interactions of the gas with the surface of the sensing layer made of semiconducting metal-oxides are responsible for changes of sensor resistance which is usually used as a measure of sensor response. Semiconductor gas sensors are commercially available and applied in numerous...
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Non-Contact Temperature Measurements Dataset
PublicationThe dataset titled The influence of the distance of the pyrometer from the surface of the radiating object on the accuracy of measurements contains temperature measurements using a selection of four commercially available pyrometers (CHY 314P, TM-F03B, TFA 31.1125 and AB-8855) as a function of the measuring distance. The dataset allows a comparison of the accuracy and measuring precision of the devices, which are very important...
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Modular high precision high current source for special applications — Simulation and verification
PublicationThis paper presents selected issues concerning realization of high precision high current source for special applications, where high demands of output parameters of such device are required. A new 80 kW prototype of modular high precision high current source is presented, where output current accuracy reaches 5x10-5. This paper presents also results of operation of the simulation model and of the prototype converter. In order...
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High Ability Studies
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High Technology Letters
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HIGH PRESSURE RESEARCH
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HIGH ENERGY CHEMISTRY
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High-Confidence Computing
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MATERIALS AT HIGH TEMPERATURES
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Temperature Fiber-Optic Sensor with ZnO ALD Coating
PublicationThis study presents a microsphere-based fiber-optic sensor with a ZnO Atomic Layer Deposition (ALD) coating thickness of 100 nm for temperature measurements. Metrological properties of the sensor were investigated over the temperature range of 100 °C to 300 °C, with a 10 °C step. An interferometric signal is used to control whether the microstructure is whole. Spectrum shift of a reflected signal is used to ascertain changes in...
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Measurement of temperature at sliding polymer surface by grindable thermocouples
PublicationThis paper is devoted to experimental study of capabilities and limitations of grindable thermocouples as applied to polymer materials sliding on metal. Chromel–alumel and chromel–copel grindable thermocouples have been developed and tested for wide ranges of contact pressure and sliding velocity. The background temperature of the sliding surface can be determined as the lower envelope of the signal from the grindable thermocouple....
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Ordered TiO2 nanotubes: the effect of preparation parameters on the photocatalytic activity in air purification process
PublicationVertically ordered TiO2 nanotube arrays were synthesized by anodic oxidation of titanium foil in glycerol, ethylene glycol and water-based electrolytes. The effect of electrolyte composition, anodization voltage, ultrasonic treatment and calcination time on the morphology of the resulting thin films, as well as on their photocatalytic activity in toluene removal, used as a model volatile organic compound, was investigated. Toluene,...
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Towards spectroscopic monitoring of photoelectrodes: In-situ Raman photoelectrochemistry of a TiO2/prussian blue photoanode
PublicationHere, novel in-situ Raman photoelectrochemical measurements are performed. The obtained results have proved that it is possible to track the progress of a photoelectrochemical reaction that takes place on a semiconducting electrode using the spectroscopic method. As an exemplary system, the Ti/TiO2/Prussian blue electrode is investigated. Since TiO2 is an n-type semiconductor, it cannot act as an efficient anode in dark conditions....
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Effectiveness of a dual surface modification of metallic interconnects for application in energy conversion devices
PublicationA dual surface modification of an SOFC metallic interconnect with a Gd2O3 layer and an MnCo2O4 coating was evaluated. The tested samples were oxidized for 7000 h in air at 1073 K. Oxidation products were characterized using XRD, SEM-EDS, and confocal Raman imaging, and ASR was measured. The effect of gadolinium segregation at grain boundaries in Cr2O3 was evaluated using S/TEM-EDS. Area specific-resistance was measured and fuel...
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Development of Strategies for AOB and NOB Competition Supported by Mathematical Modeling in Terms of Successful Deammonification Implementation for Energy-Efficient WWTPs
PublicationNovel technologies such as partial nitritation (PN) and partial denitritation (PDN) could be combined with the anammox-based process in order to alleviate energy input. The former combination, also noted as deammonification, has been intensively studied in a frame of lab and full-scale wastewater treatment in order to optimize operational costs and process efficiency. For the deammonification process, key functional microbes include...
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Electrocatalytic gas sensor with reference layer
PublicationIn recent years electrochemical gas sensors based on solid state electrolytes have been intensively developed. They are easy to obtain, use and relative durable. Nasicon is one of the most promising materials, which have been used in construction of gas sensors. Most of these devices work in potentiometric or amperometric mode. However, some works are dedicated to sensors working in electrocatalytic mode. Principle of operation...
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Randomly Functionalized Polyethylenes: In Quest of Avoiding Catalyst Deactivation
PublicationWell-defined randomly functionalized polyolefins produced by catalysis form an interesting class of polymers with great potential for various applications. One of the major challenges for the production of these materials forms the incompatibility of the commonly used electrophilic group 4 metal based catalysts and the desired nucleophilic, especially protic functionalities like hydroxyl and carboxylic acid groups. Although pacification...
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Hyaluronan-Chondroitin Sulfate Anomalous Crosslinking Due to Temperature Changes
PublicationGlycosaminoglycans are a wide class of biopolymers showing great lubricating properties due to their structure and high affinity to water. Two of them, hyaluronic acid and chondroitin sulfate, play an important role in articular cartilage lubrication. In this work, we present results of the all-atom molecular dynamics simulations of both molecules placed in water-based solution. To mimic changes of the physiological conditions,...
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Temperature distribution of supercapacitors prepared by various technologies
PublicationSupercapacitors, also known by different names such as electrostatic double-layer capacitors (EDLCs) or ultra-capacitors, are electrical storage devices still in development. These devices require fast and reliable methods of assessing their state-of-health. Thermographic imaging is a method which can be applied with this aim due to its popularity, and the high negative impact of overheating on a supercapacitor’s parameters. Moreover,...
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PROBLEMS OF THE STARTING AND OPERATING OF HYDRAULIC COMPONENTS AND SYSTEMS IN LOW AMBIENT TEMPERATURE (PART IV) MODELLING THE HEATING PROCESS AND DETERMINING THE SERVICEABILITY OF HYDRAULIC COMPONENTS DURING THE STARTING-UP IN LOW AMBIENT TEMPERATURE
PublicationDesigners of hydraulically driven machines and devices are obliged to ensure during design process their high service life with taking into account their operational conditions. Some of the machines may be started in low ambient temperature and even in thermal shock conditions (due to delivering hot working medium to cold components). In order to put such devices into operation appropriate investigations, including experimental...
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Multi-Channel Virtual Instrument for Measuring Temperature—A Case Study
PublicationThe article presents the hardware and software configuration of the developed multi-channel temperature measurement system as well as calibration procedures and measurement results verifying the properties of measurement channels. The system has been developed and dedicated primarily for measuring the temperature distribution in a laboratory model simulating underground power lines. With the adopted configuration of the analog...
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High-accuracy polarimetric studies on lead germanate single crystals
PublicationA high-accuracy polarimetric technique has been used for the characterization of a lead germanate ferroelectric single crystal. The measurement results of the linear and circular birefringence in the [010] direction at a wavelength of 633 nm under the influence of an electric field are presented. Gyration–electric field hysteresis loops at alternative crystal positions in the polarization system have been used to determine the...
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Charge Transport in High-Entropy Oxides
PublicationThis work presents the results of research on the transport properties of the high-entropy BaZr1/8Hf1/8Sn1/8Ti1/8Y1/8In1/8Sm1/8Yb1/8O3–x perovskite oxide with special focus on proton transport. The presented study is part of broader work in which we focus on multiple different chemical compositions with the cation number varying from 5 up to 12 (in B-sublattice). The presence of proton defects is analyzed with thermogravimetry,...
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Changes of Conformation in Albumin with Temperature by Molecular Dynamics Simulations
PublicationThis work presents the analysis of the conformation of albumin in the temperature range of 300K – 312K, i.e., in the physiological range. Using molecular dynamics simulations, we calculate values of the backbone and dihedral angles for this molecule. We analyze the global dynamic properties of albumin treated as a chain. In this range of temperature, we study parameters of the molecule and the conformational entropy derived from...
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Photovoltaic module temperature stabilization with the use of phase change materials
PublicationThe worldwide growth of photovoltaics (PVs) has formed an exponential curve for more than four decades. During this period of time, PVs have evolved from a pure niche market of small-scale applications towards becoming a mainstream electricity source. The influence of temperature on the electrical parameters of crystalline silicon solar cells and solar modules is well described in the literature. In order to diminish these effects,...
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FTIR Studies of the Surface of TiO2, Fe-TiO2 and Fe-C-TiO2 Photocatalysts in Phenol Oxidation Via the Photo-Fenton Process
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DETERMINING THE TIME CONSTANT USING TWO METHODS AND DEFINING THE THERMOCOUPLE RESPONSE TO SINE EXCITATION OF GAS TEMPERATURE
PublicationThis paper describes the two methods of determining the time constant of type K thermocouple, for two construction solutions: the exposed weld and the mantle fillet weld. This is an important parameter indicating the response time of the thermocouple on the recorded signal. The first method consists of determining the value of τ in the way of numerical simulation of heat exchange between the thermocouple and the current of gas...
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Methodology of estimating temperature measurement uncertainty in a system for endurance tests.
PublicationThe team consisting of the article authors developed a non-invasive method and a system for measuring temperature during an endurance test. A thermocouple which provided the required accuracy of changes in temperature dynamics measurements was used for the purpose of the required research. The paper presents the methodology for estimating uncertainty of temperature measurement done with the presented system, using a method based...
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IMPEDANCE MEASUREMENT MODULE FOR GAS SENSORS WITH TEMPERATURE CONDITIONING FEATURE
PublicationThe paper presents an impedance measurement module which is aimed for gas sensor. Sensor’s heater temperature conditioning and modulation feature is available in order to allow implementation of different techniques improving selectivity and sensitivity of gas sensors. The measurement module uses three-parameter sine-fitting technique for impedance measurement. To monitor sensor temperature, the resistance of the sensor’s heater...
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A novel sensor for measuring temperature profile during the thermoablation
PublicationAbstract — A novel approach for monitoring a temperature distribution inside a tissue during thermoablation is presented in the paper. A thermal profile is measured using a set of serially connected thermistors each bypassed by a capacitor. This technique allows a two-wire and simultaneous multi- point measurements using a multi-frequency measurement of electrical impedance. It is...
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Local properties of organic coatings close to glass transition temperature
PublicationAcrylic coating applied on copper substrate has been investigated at different temperatures starting from the ambient one up to the level above the glass transition temperature. Its local topographic and electric properties have been examined with the atomic force microscopy (AFM) based approach including dc current mapping and local impedance spectroscopy. The local findings have been compared with the information from global...
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Performance of acicular grindable thermocouples for temperature measurements at sliding contacts
PublicationThe present study investigates the performance of acicular grindable thermocouples based on a constantan wire / steel hollow cylinder construction. The experiments showed that the measuring junction electrical resistance, temperature–voltage characteristic, measuring junction rise time and signal noise standard deviation of the acicular thermocouples are comparable to those of conventional J-type thermocouples with bare wire diameter...
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Central heating temperature control algorithm for systems with condensing boilers
PublicationThe problem of control of a central heating system in a small residence is considered. It is assumed that the system is based on a condensing boiler. Since the boiler efficiency depends on a returning water temperature, the proposed control goal is to provide proper air temperature in the residence as well as the lowest possible water temperature. The proposed algorithm is applied to two buildings. Both of them have the same heating...
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Experimental and Numerical Investigations of the Effect of Curing Conditions on the Temperature Rise of Concrete
PublicationThis paper presents experimental and numerical studies investigating the impact of three curing conditions on temperature evolution in concrete cubes. The tests were performed on samples of the same volume (3.375 dm3) under different curing conditions: room temperature, insulation boxes, and adiabatic calorimeter. Various cements (Portland cement, Portland composite cement, and blast furnace slag cement) and aggregates (gravel...
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The Influence of Drying Temperature on Color Change of Hornbeam and Maple Wood Used as Surface and Inner Layers of Wood Composites
PublicationThe thermal treatment of wood changes its structure due to the degradation of wood polymers (cellulose, hemicellulose and lignin), so the physical properties of wood are either improved or degraded. Color changes apply not only to natural wood, but also to such wood composites for which some amount of glue is used in their construction (e.g., plywood, blockboard or laminboard). This article is focused on the analysis of hornbeam...
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Determination of Thermophysical Parameters Involved in The Numerical Model to Predict the Temperature Field of Cast-In-Place Concrete Bridge Deck
PublicationThe paper dealswith a concept of a practical computationmethod to simulate the temperature distribution in an extradosed bridge deck. The main goal of the study is to develop a feasible model of hardening of concrete consistent with in-situ measurement capabilities. The presented investigations include laboratory tests of high performance concrete, measurements of temperature evolution in the bridge deck and above all, numerical...