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Search results for: RAJ
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A facile approach to fabricate load-bearing porous polymer scaffolds for bone tissue engineering
PublicationBiodegradable porous scaffolds with oriented interconnected pores and high mechanical are load-bearing biomaterials for bone tissue engineering. Herein, we report a simple, non-toxic, and cost-effective method to fabricate high-strength porous biodegradable scaffolds, composed of a polymer matrix of polycaprolactone (PCL) and water-soluble poly (ethylene oxide) (PEO) as a sacrificial material by integrating annealing treatment,...
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Fabrication and photoactivity of ionic liquid–TiO2 structures for efficient visible-light-induced photocatalytic decomposition of organic pollutants in aqueous phase
PublicationTo investigate the effect of the ionic liquid (IL) chain length on the surface properties and photoactivity of TiO2, a series of TiO2 microspheres have been synthesized via a solvothermal method assisted by 1-methyl-3-octadecylimidazolium chloride ([ODMIM][Cl]) and 1-methyl-3-tetradecylimidazolium chloride ([TDMIM][Cl]). All as-prepared samples were characterized by X-ray powder diffraction (XRD), X-ray photoelectron spectroscopy...
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Effect of irradiation intensity and initial pollutant concentration on gas phase photocatalytic activity of TiO2 nanotube arrays
PublicationWell-organized TiO2 nanotube arrays were fabricated via one-step anodization process. The as-prepared TiO2 nanotubes were characterized by X-ray powder diffractometry (XRD), X-ray photoelectron spectroscopy (XPS), diffuse reflectance spectroscopy (DRS) and scanning electron microscopy (SEM). Photocatalytic activity of obtained photocatalyst was studied in reaction of toluene degradation in the gas phase using low powered and low...
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Comprehensive Evaluation of the Biological Properties of Surface-Modified Titanium Alloy Implants
PublicationAn increasing interest in the fabrication of implants made of titanium and its alloys results from their capacity to be integrated into the bone system. This integration is facilitated by different modifications of the implant surface. Here, we assessed the bioactivity of amorphous titania nanoporous and nanotubular coatings (TNTs), produced by electrochemical oxidation of Ti6Al4V orthopedic implants’ surface. The chemical composition...
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The Influence of the Depth of Cut in Single-Pass Grinding on the Microstructure and Properties of the C45 Steel Surface Layer
PublicationThe paper contains the results of a metallographic examination and nanoindentation test conducted for the medium carbon structural steel with low content of Mn, Si, Cu, Cr, and Ni after its grinding to a depth ranging from 2 μm to 20 μm, at constant cutting speed (peripheral speed) of vs = 25 ms−1 and constant feed rate of vft = 1 m/min. Applied grinding parameters did not cause the surface layer hardening, which could generate...
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Impact of Tetrazolium Ionic Liquid Thermal Decomposition in Solvothermal Reaction on the Remarkable Photocatalytic Properties of TiO2 Particles
PublicationIonic liquids (ILs) could serve as a structuring agent, a solvent, or a source of dopant during solvothermal synthesis of semiconductors particles. To understand the role of IL during formation of TiO2 particles, it is necessary to study the stability of this IL in solvothermal synthesis conditions, as well as studying the surface properties of formed TiO2 particles. In view of this, the effect of the 2,3,5-triphenyltetrazolium...
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Superconducting SrSnP with Strong Sn–P Antibonding Interaction: Is the Sn Atom Single or Mixed Valent?
PublicationThe large single crystals of SrSnP were prepared using Sn self-flux method. The superconductivity in the tetragonal SrSnP is observed with the critical temperature of ∼2.3 K. The results of a crystallographic analysis, superconducting characterization, and theoretical assessment of tetragonal SrSnP are presented. The SrSnP crystallizes in the CaGaN structure type with space group P4/nmm (S.G. 129, Pearson symbol tP6) according...
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Synthesis, structure, DNA binding and anticancer activity of mixed ligand ruthenium(II) complex
PublicationIn order to obtain a potential chemotherapeutic which is not affected on the normal BALB/3T3 cell line, a new arene ruthenium(II) complex {[RuCl(L1)(η6-p-cymene)]PF6}2 · H2O has been synthesized by a direct reaction of precursor, [{(η6-p-cymene)Ru(μ-Cl)}2Cl2], with N,N-chelating ligand (L1 - 2,2′-bis(4,5-dimethylimidazole). The compound has been fully characterized by elemental analysis, X-ray diffraction, IR, UV–Vis and 1H, 13C...
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Preparation and Characterization of Defective TiO2. The Effect of the Reaction Environment on Titanium Vacancies Formation
PublicationAmong various methods of improving visible light activity of titanium(IV) oxide, the formation of defects and vacancies (both oxygen and titanium) in the crystal structure of TiO2 is an easy and relatively cheap alternative to improve the photocatalytic activity. In the presented work, visible light active defective TiO2 was obtained by the hydrothermal reaction in the presence of three different oxidizing agents: HIO3, H2O2, and...
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Projekt Trasy Henryka Sucharskiego.
PublicationMost III Tysiąclecia im. Jana Pawła II jest elementem Trasy Sucharskiego w Gdańsku, łączącej ul. Elbląską od strony południowej nad Martwą Wisłą z węzłem Wosia Budzysza i dalej portem Północnym. Most oddano do użytku w październiku 2001r. Jego budowa była, z punktu widzenia realizacji, przedsięwzięciem wysoce oryginalnym w skali kraju, gdyż to właśnie tutaj po raz pierwszy w Polsce zastosowano montaż wspornikowy przy budowie mostu...
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Badania odbiorcze mostu (próbne obciążenie).
PublicationMost III Tysiąclecia im. Jana Pawła II jest elementem Trasy Sucharskiego w Gdańsku, łączącej ul. Elbląską od strony południowej nad Martwą Wisłą z węzłem Wosia Budzysza i dalej portem Północnym. Most oddano do użytku w październiku 2001r. Jego budowa była, z punktu widzenia realizacji, przedsięwzięciem wysoce oryginalnym w skali kraju, gdyż to właśnie tutaj po raz pierwszy w Polsce zastosowano montaż wspornikowy przy budowie mostu...
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Regional quality contests based on business excellence models – Pomeranian case study
PublicationCompetitions based on models of organizational excellence have significant potential. Organizations participating in these initiatives have the chance not only to get marketing benefits, but also gain comprehensive knowledge about their management systems. Moreover, thanks to the structure of models of excellence an organization can plan in detail the improvement activities in its main processes. The aim of the authors is to analyze...
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Cement kiln dust
PublicationThe volume of cement production in the world has remained at the level of approxi mately 4.1 billion tons/year. The cement production process is energy intensive and is the world’s leading emitter of carbon dioxide. Therefore, the main activities cement plants are aimed at introducing technologies changes in production of clinkier.The construction industry is responsible for the majority of CO2 emissions to the atmosphere: the...
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Monometallic nanoparticles decorated and rare earth ions doped KTaO3/K2Ta2O6 photocatalysts with enhanced pollutant decomposition and improved H2 generation
PublicationNew, monometallic nanoparticles (MNPs) decorated surface and rare earth (RE) ions doped lattice of perovskite-type (KTaO3)/pyrochlore-type (K2Ta2O6) photocatalysts were successfully prepared by facile hydrothermal incorporation of RE ions into KTaO3/K2Ta2O6 lattices followed by photodeposition of MNPs. The impact of noble metal type (MNPs = Au, Pt, Rh) and rare earth dopant type (RE = Er, Pr) on the physicochemical properties correlated...
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Sawing of frozen wood with narrow-kerf saws.
PublicationPrzedstawiono wyniki badań eksperymantalnych skrawania drewna sosnowego mrożonego na pilarce ramowej PRW15M za pomocą cienkich pił. Badano opory skrawania, chropowatość powierzchni po przecinaniu, dokładność przecinania oraz przeprowadzono analize granulometryczna wiórów. Zaobserwowano wzrost oporów skrawania w raz ze spadkiem temperatury,któremu towarzyszyła również niższa dokładność przeciania w odniesieniu do drewna obrabianego...
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Measuring and Analyzing Audio Levels in Film, Commercials, and Movie Trailers Using Leq(A) Values and the LUFS Loudness Model . Analiza pomiarów dźwięku w filmie oraz w reklamach filmowych z wykorzystaniem modelu głośności
PublicationThe purpose of this paper is to describe the measurement of loudness levels in movies, movie trailers, and commercials displayed before feature films at movie theaters. In the initial section, the paper discusses the issues related to measurement of loudness levels, provides recommendations regarding permissible loudness levels during movie screenings, and mentions the applied units of measurement. The following section of the...
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High Temperature Corrosion Evaluation of Porous Hastelloy X Alloy in Air and Humidified Hydrogen Atmospheres
PublicationIn this work a commercially available porous Hastelloy X alloy is characterized in terms of high temperature corrosion resistance. The alloy was oxidized in the temperature range from 500C to 900C in air and humidified hydrogen for 100 hours. Corrosion rates and porosity changes were measured. Microstructural characterization was performed using X-ray diffractometry and scanning electron microscopy. Results show that porous alloys...
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Nano-structured Pt embedded in the acidic salts of heteropolymolybdate matrices: MS XAFS study
PublicationMultiple-scattering extended X-ray absorption fine structure (MS EXAFS) study combined with TEM and XRD analysis of a novel Pt-based catalyst operating at low temperature fuel cells (FCs) is presented. Innovation in the case of the considered catalyst resides in the use of a porous inorganic matrix of acidic heteropolymolybdate salts as a catalyst support. Obtained results show the relation between the matrix composition and the...
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Impedance Studies of Phosphate-iron Glasses Containing Niobium and Titanium
PublicationThe ac and dc conductivity in phosphate-iron-niobate glasses with addition of titanium oxide was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD), scanning electron microscopy (SEM), and confocal microscopy methods. The obtained results show that all samples are amorphous but they...
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Podatkowe uwarunkowania rozwoju przedsiębiorczości w Polsce
PublicationPrzedsiębiorczość jest podstawowym czynnikiem wzrostu aktywności gospodarczej. Jest również elementem i narzędziem gdy konkurencyjnej. W związku z tym każdy kraj stara się stworzyć jak najlepsze warunki rozwoju przedsiębiorczości. Procesy te napotykają jednak na szereg barier z których najważniejszymi są bariery podatkowe.System podatkowy powinien być tak konstruowany aby z jednej strony zapewniał spełnienie funkcji fiskalnych...
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Rzeczywista nośność pali w gruntach ilastych z zastosowaniem zaleceń PN-EN 1997-1:2004
PublicationObecnie co raz więcej obiektów posadawianych jest w gruntach słabych bądź o specyficznych parametrach, do takich gruntów zalicza się iły. Jedną z podstawowych możliwości posadowienia w gruntach ilastych jest posadowienie na palach. Projektowanie fundamentów na palach dla takich warunków wymaga specjalnego i indywidualnego podejścia. W pracy przedstawiono przegląd metod i uwag w oparciu o PN-EN 1997-1:2004, którymi należy kierować...
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Projekt przebudowy nawierzchni betonowej z zastosowaniem technologii rozkruszania
PublicationW artykule przedstawiono projektowanie i technologię przebudowy starej nawierzchni z betonu cementowego drogi krajowej nr 22 na odcinku Chojnice - Tczew poprzez rozkruszanie na miejscu starych płyt betonowych (ang. rubblizing) i wbudowaniu nakładki asfaltowej. Technologię "rubblizingu" zaprojektowano po raz pierwszy w Polsce. Omówiono wady i zalety technologii rubblizingu, przedstawiono wydajność, jak i orientacyjne ceny jednostkowe....
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Imidazolium silanethiolates relevant to the active site of cysteineproteases. A cooperative effect in a chain of NH(+)...S(-) hydrogenbonds
PublicationThree imidazolium silanethiolates relevant to the active site of cysteine proteases have been synthesized and investigated by X-ray diffraction, IR spectroscopy and computational methods. As indicated by crystallographic and FT-IR data in the solid state, the transfer of proton from thiol to imidazole takes place and a thiolato-imidazolium ion pair is formed. The FT-IR spectra of crystalline imidazolium silanethiolates exhibit...
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Superconducting properties of vn-sio 2 sol-gel derived thin films
Publicationin this work studies of structure and superconducting properties of vnsio2 films are reported. the films were obtained through thermal nitridation (ammonolysis) of solgel derived v2o3sio2 coatings (in a proper v2o3/sio2 ratio) at 1200 ◦c. this process leads to the formation of disordered structure with vn metallic grains dispersed in the insulating sio2 matrix. the structural transformations occurring in the lms as a result...
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Syntheses and structures of the first terminal phosphanylphosphido complexes of molybdenum(IV)
PublicationThe reactions of R2P-P(SiMe3)Li (R = tBu, iPr2N) with [Cp2MoCl2] yield terminal phosphanylphosphido complexes formally via the insertion of the phosphinidene P-atom into the C - H bond of a cyclopentadienyl ring and the migration of the hydrogen atom or SiMe3 moiety to the molybdenum centre. Solid state structures of [Cp(C5H4P-PtBu2)MoH], [Cp(C5H4P-PtBu2)Mo(SiMe3)] and [Cp{C5H4P-P(NiPr2)2}Mo(SiMe3)] were established by single crystal...
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Functionalized azobenzocrown ethers as sensor materials—The synthesis and ion binding properties
PublicationNew 13- and 16-membered azobenzocrown ethers with aromatic amino, amide, ether–ester or ether–amide residue in para position to an azo moiety were obtained. Acid–base properties and ion binding ability of the colored compounds were studied by spectroscopic methods: UV–vis, fluorimetry and 1H NMR spectroscopy. Selected azobenzocrowns were tested as ionophores in ion-selective membrane electrodes (ISEs) – classic and miniature all...
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Expedited two-objective dimension scaling of compact microwave passives using surrogate models
PublicationGeometry scaling of compact microwave structures is a challenging problem because of complex relationships between the physical dimensions and electrical characteristics, mostly caused by considerable cross-couplings in densely arranged layouts. Here, a procedure for expedited dimension scaling of compact microwave couplers with respect to two independent criteria has been presented. Our approach involves inverse surrogate models...
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XXVIII Aukcja Wielkie Serce
PublicationAukcja to wyjątkowa okazja dla miłośników i kolekcjonerów polskiej sztuki współczesnej. Kolejny raz będzie można obcować z dziełami artystów, którzy tworzą kanon, są „żywą encyklopedią” grafiki i malarstwa polskiego. Od początku lat 90. ubiegłego stulecia, organizatorzy aukcji szczycą się i zaufaniem najwybitniejszych polskich twórców. Pieniądze z licytacji ich dzieł, jak co roku, przekazane zostaną na rzecz wychowanków Specjalnego...
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Depth Determination Accuracy of the Modified Prony Method in a Swath Mapping Application
PublicationThis article presents the performance of the modified Prony method in a swath mapping application. Depth determination accuracy is assessed by processing raw signal acquired by an EdgeTech 6205 swath bathymetry system over flat seafloor. An updated version of the method, proposed previously by the authors, is used to determine the number of signal echoes. The number of signal echoes is essential for performing the low-rank approximation...
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Analysis of Roughness, the Material Removal Rate, and the Acoustic Emission Signal Obtained in Flat Grinding Processes
PublicationIn this work, the analysis of the acoustic emission (AE) signal in grinding processes is addressed. The proposed analysis method decomposes the acoustic signal into three frequency ranges. The total energy of each range is determined, as well as the highest frequency. Different grinding experiments were carried out, according to a full factorial design of experiments (DOE), in which feed speed, depth of cut, and transversal step...
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In silico assessment and sonochemical synthesis of 2-alkynyl 3-chloropyrazines as prospective ligands for SARS-CoV-2
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Spectral and photophysical properties of some imidazo[1,2-a]purine derivatives related to acyclovir
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Formation of novel nanostructures using carbon nanotubes as a frame
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Jerusalem artichoke (Helianthus tuberosus L.) as a medicinal plant and its natural products
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Report of the ISMIS 2011 Contest : Music Information Retrieval
PublicationThis report presents an overview of the data mining contestorganized in conjunction with the 19th International Symposiumon Methodologies for Intelligent Systems (ISMIS 2011), in days betweenJan 10 and Mar 21, 2011, on TunedIT competition platform. The contestconsisted of two independent tasks, both related to music information retrieval:recognition of music genres and recognition of instruments, for agiven music sample represented...
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Application of commercial supercapacitor modules in autonomic photovoltaic installations
PublicationDynamiczny rozwój technologii i konstrukcji superkondensatorów, napędzany głównie potrzebami przemysłu motoryzacyjnego pozwala na stwierdzenie, że stają się one coraz bardziej realną alternatywą dla konwencjonalnych akumulatorów stosowanych w autonomicznych instalacjach fotowoltaicznych.Za ich stosowaniem przemawiają takie zalety jak: możliwość szybkiego ładowania i rozładowania, wielokrotnie wyższa trwałość, bezobsługowość eksploatacji...
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The Importance of Demand and Environment for Defining and Establishing the Role of Data Stewards
PublicationData stewardship is now a central part of FAIR research data management. Although various types of positions called data stewards have been created at academic institutions over the last years, no demand-oriented, formal model of data stewardship and the associated roles exist so far. This workshop report presents the outcomes of the panel discussion “The Importance of Demand and Environment for Defining Data Stewardship” held...
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Application of Nanomaterials for Cadmium Adsorption for Sustainable Treatment of Wastewater: a Review
PublicationMany heavy metals, particularly cadmium, are detrimental to both people and the environment when present in large quantities. In wastewater treatment plants, several conventional approaches are employed for cadmium abatement to restore the ecosystem, food supplies, and health of people and animals. Ion exchange, coagulation, membrane filtration, and chemical precipitation are a few examples of ways for removing heavy metals from...
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Synthesis and hydrogen evolving catalysis of a panchromatic photochemical molecular device
PublicationA dinuclear hydrogen evolution photocatalyst [(tbbpy)2Os(tpphz)PtI2](PF6)2 (tbbpy = 4,4′-tert-butyl-2,2′-bipyridine; tpphz = tetrapyrido[3,2-a:2′,3′-c:2′′,3′′-h:2′′′,3′′′-j]phenazine) is synthesized in order to make use of the broader range of visible light absorption mitigated by the osmium center. In a first step, the activity of the complex for hydrogen evolution is investigated by evaluating the role of different electron donors...
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Superconductivity on a Bi Square Net in LiBi
PublicationWe present the crystallographic analysis, superconducting characterization and theoretical modeling of LiBi, that contains the lightest and the heaviest nonradioactive metal. The compound crystallizes in a tetragonal (CuAu-type) crystal structure with Bi square nets separated by Li planes (parameters a = 3.3636(1)Å and c = 4.2459(2) Å, c/a = 1.26). Superconducting state was studied in detail by magnetic susceptibility and heat...
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Using of carbon nanotubes and nano carbon black for electrical conductivity adjustment of pressure-sensitive adhesives
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Udział złotego w mechanizmie stabilizowania kursu a ryzyko wystąpienia kryzysu walutowego w Polsce
PublicationWśród szeregu niepożądanych zjawisk wynikających z zastąpienia złotego walutą euro, uwaga najczęściej skupiona jest na tych, które oddziałują już po przystąpieniu do jednowalutowego obszaru. Rzadziej dokonuje się analizy zagrożeń w fazie przygotowawczej, jeszcze przed formalnym przystąpieniem do obszaru euro. Jednym z takich niebezpieczeństw jest ryzyko wystąpienia kryzysu walutowego w czasie realizacji przez państwo kandydujące...
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Występowanie bakterii siarkowych a jakość wód podziemnych ujęcia Osowa
PublicationAbstrakt. Microorganisms that live in groundwater should be considered not only from the sanitary-hygienic point of view but also in terms of adverse changes in groundwater chemistry in the aquifer layer and its negative influence on the installed devices. For these reasons, it is important to correct approach to the problem of bacterial contamination of groundwater. The paper presents selected results of physicochemical and bacteriological...
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Macromodeling techniques for accelerated finite element analysis
PublicationThis paper deals with the Model Order Reduction applied locally in the Finite Element Method (FEM) analysis. Due to the reduction process, blocks of FEM system matrices associated with selected subregions of the computational domain are projected onto the subspaces spanned by the vectors of suited orthogonal projection basis. In effect, large and sparse FEM matrices are replaced with small and dense ones, called macromodels. This...
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Microstructure and Dielectric Properties of Barium-vanadate Glasses
PublicationThe ac and dc conductivity in barium-vanadate glasses was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD) and scanning electron microscopy (SEM) methods. The XRD results show that all samples are amorphous but microscopy investigation reveals that glasses with greater amount of V2O5...
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Badanie techniczne pojazdu zabytkowego
PublicationW artykule przedstawiono wyniki pomiarów sił hamowania oraz opóźnienia hamowania samochodów o dopuszczalnej masie całkowitej nie przekraczającej 3,5 tony. Badania wykonano dla pojazdów współczesnych oraz dla pojazdów zabytkowych. Pomiary są elementami składowymi okresowego badania technicznego każdego pojazdu przeprowadzanego raz do roku na Stacjach Kontroli Pojazdów. Omówiono zasady dopuszczania pojazdów\ zabytkowych do ruchu...
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Silver complexes stabilized by large silanethiolate ligands – crystal structures and luminescence properties
PublicationBulky silanethiolate and disiladithiolate ligands were applied to synthesize one mononuclear and three trinuclear silver complexes including two cyclic “microclusters” and a linear tri-nuclear silanethiolate complex. All obtained compounds are characterized by X-ray diffraction and FT-IR. NMR and emission spectroscopies were used where possible. The first trinuclear anionic silver thiolate is structurally characterized. The influence...
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High temperature monoclinic-to-tetragonal phase transition in magnesium doped lanthanum ortho-niobate
PublicationMagnesium doped lanthanum ortho-niobate (La0.98Mg0.02NbO4) was prepared by the molten salt synthesis method. X-ray diffraction and dilatometry methods were used to study high temperature behavior of the ceramic material. Special attention was paid to the phase transition between the monoclinic and tetragonal phases. The values of spontaneous strain on the basis of unit cell parameter, obtained by Rietveld refinement, have been...
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Neural Networks and the Evolution of Environmental Change
PublicationZmiany środowiskowe na Ziemii są odwieczne i liczą około 4 miliardy lat. Homo sapiens wpłynął na każdy aspekt środowiska ziemskiego w wyniku rozwoju ludzkości na przestrzeni ostatnich milionów lat. Ale nic tak nie wpłynęło na wzrost i szybkość zmian na Ziemi jak ludzka aktywność w ciągu ostatnich dwóch stuleci. Po raz pierwszy zmiany ekosystemów były tak intensywne i zachodziły na tka wielką skalę i z taką szybkością jak nigdy...
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Diagnostyka i modernizacja konstrukcji nawierzchni drogowych
PublicationPotrzeby w zakresie utrzymania i remontów dróg są w Polsce ogromne. Nasz kraj ma znaczne opóźnienia i zaniedbania w tym zakresie w porównaniu ze ''starymi'' krajami Unii Europejskiej. Istniejące nawierzchnie w znacznej ich części są w złym stanie, mają usterki funkcjonalne utrudniające ruch (koleiny, nierówności podłużne, niski współczynnik tarcia, spękania, wyboje, nadłamane krawędzie, wykruszenia powierzchni itp.). Wzrastające...