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Chromatografia gazowa z detekcją olfaktometryczną (GC-O) w analizie żywności. Cz. I. Charakterystyka metody
PublicationW ostatnich latach prowadzone są intensywne badania nad aktywnością sensoryczną poszczególnych składników zapachów żywności, a także napojów alkoholowych i nad zależnościami pomiędzy zapachem, a składem chemicznym lotnej frakcji tych produktów. Z oczywistych powodów największe zastosowanie w oznaczaniu lotnych substancji zapachowych znajduje chromatografia gazowa z różnymi wariantami detekcji. Większość osiągnięć w tej dziedzinie...
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Skażenia żywności. Rozdział 5
PublicationW rozdziale 5 przedstawiono podstawowe wiadomości z toksykologii: definicja i zakres toksykologii żywności, trucizny - definicje, zatrucia, kryteria oceny higieniczno-toksykologicznej związków chemicznych, toksykologię związków chemicznych występujących w żywności, wchłanianie, przemiany substancji w organizmie, wydalanie i wydzielanie, czynniki wpływające na wchłanianie z przewodu pokarmowego, mechanizm przemian i wynik działania...
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Wykorzystanie ciepła niskotemperaturowego do procesu suszenia peletu ze słomy z wykorzystaniem mikrostrugowego wymiennika ciepła
PublicationW artykule przedstawiono wpływ temperatury medium suszącego na zmiany względnej oraz bezwzględnej zawartości wilgoci podczas suszenia peletu ze słomy. Proces suszenia przeprowadzono przy stałym ciśnieniu atmosferycznym i różnych wartościach temperatury powietrza, jako czynnika suszącego, wynoszących odpowiednio: 40℃, 60℃, 80℃, 100℃ oraz 120℃. Badania eksperymentalne wykonywano na innowacyjnym stanowisku wyposażonym w mikrostrugowy...
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Zastosowanie elektronicznych zmysłów w analizie żywności - cz. 1
PublicationW dzisiejszych czasach konsumenci zwracają dużą uwagę na takie cechy żywności jak: zapach, smak i wygląd. Ze względu na to naukowcy od wielu lat podejmują próby naśladowania ludzkich narządów zmysłów za pomocą urządzeń określanych jako elektroniczne zmysły. Zaliczamy do nich elektroniczny nos i język oraz komputerowy system rozróżnienia barw i kształtów. Elektroniczny nos jest najbardziej rozwiniętym i najczęściej stosowanym sztucznym...
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HPLC-DAD in identification and quantification of selected coumarins in crude extracts from plant cultures of Ammi majus and Ruta graveolens.
PublicationW pracy opisano wyniki badań nad opracowaniem metody rozdzielania, identyfikacji i oznaczania wybranych kumaryn i funarokumaryn w surowych ekstraktach roślinnych z Ammi majus i Ruta graveolens hodowanych pojedynczo lub w kokulturach. Zbadano przydatność trzech głównych składników eluentu, stosowanych w układach faz odwróconych i różnych programów elucji: woda- acetonitryl(ACN)- metanol (MeOH)- tetrahydrofuran (THF). W optymalnej...
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Technological improvements in food production in the context of food quality and health safety.
PublicationW rozdziale wykazano sprzeczność pomiędzy szczytnymi celami Prawa Żywnościowego UE mającymi na celu absolutna ochronę zdrowia konsumenta a praktyką i wpływem wielkich organizacji przemysłowych skutkiem działań których, liczba dodatków do żywności z ok. 260 dozwolonych w RP przed wstąpieniem do UE wzrosła do ponad 330 wg aktów prawnych UE. Stosowanie dodatków do żywności ma przede wszystkim na celu przedłużenie okresu "shelf life"...
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Modelowanie numeryczne rozprzestrzeniania się zanieczyszczeń ropopochodnych
PublicationZ uwagi na właściwości związków BTEX, jak również częste ich występowanie w sąsiedztwie obszarów zanieczyszczonych substancjami ropopochodnymi, modelowano numerycznie transport benzenu i jego pochodnych jako związków reprezentujących substancje ropopochodne zanieczyszczające środowisko wodno-gruntowe. Jako narzędzie zastosowano program MODFLOW z modułem MT3D umożliwiającym trójwymiarową symulację transportu rozpuszczonych w wodzie...
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Minimizing Distribution and Data Loading Overheads in Parallel Training of DNN Acoustic Models with Frequent Parameter Averaging
PublicationIn the paper we investigate the performance of parallel deep neural network training with parameter averaging for acoustic modeling in Kaldi, a popular automatic speech recognition toolkit. We describe experiments based on training a recurrent neural network with 4 layers of 800 LSTM hidden states on a 100-hour corpora of annotated Polish speech data. We propose a MPI-based modification of the training program which minimizes the...
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Anticancer and antimicrobial properties of novel η6-p-cymene ruthenium(ii) complexes containing a N,S-type ligand, their structural and theoretical characterization
PublicationRuthenium(II) complexes are lately of great scientific interest due to their chemotherapeutic potential asanticancer and antimicrobial agents. Here we present the synthesis of new pyrazole carbothioamidederivatives and their four arene–ruthenium complexes. The title compounds were characterized with theapplication of IR, NMR, mass spectrometry, elemental analysis and X-ray diffraction. Additionally, for newcomplexes DFT calculations...
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Structural and dynamic insights on the EmrE protein with TPP+ and related substrates through molecular dynamics simulations
PublicationEmrE is a bacterial transporter protein that forms an anti-parallel homodimer with four transmembrane helices in each monomer. EmrE transports positively charged aromatic compounds, such as TPP+ and its derivatives. We performed molecular dynamics (MD) simulations of EmrE in complex with TPP+, MeTPP+, and MBTPP+ embedded in a membrane. The detailed molecular properties and interactions were analysed for all EmrE-ligand complexes....
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THE PROTECTIVE MEASURES AGAINST SARS-COV-2 INFECTION IN THE SEAFOOD COMPANY FROM THE PERSPECTIVE OF THE EMPLOYEES
PublicationPurpose: To identify and discuss the protective measures implemented to prevent SARS-CoV-2 infection among employees. Design/methodology/approach: The four-stage course of research. Case study and structured interviews with all employees, directly and indirectly, involved in food processing. Research questions: (R1) What measures have been taken to prevent the risk of infection among employees? (R2) What activities and responsibilities...
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Peculiarities associated with testing polyetheretherketone (PEEK) in a model rolling contact
PublicationPolyetheretherketone (PEEK) was investigated using a modified version of the four-ball tester in which the upper forth ball was replaced by a cone in such a way that kinematics of the four-ball configuration were fully preserved. Rotation of the cone enforced orbiting and rolling of the ceramic balls around the polymer cup. The results produced some unexpected peculiarities in the wear of ceramic balls which, in principle, should...
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Numerical Study of the Impinging Jets Formed by an Injector with Different Nozzle Diameters
PublicationThe collision of two or more liquid jets may provide considerable atomisation and efficient mixing of injected substances at the same time. This phenomenon is used, among others, in rocket engines, where the fuel and oxidiser are introduced separately and almost immediately mixed through self-impingement. Depending on the injection and operating conditions, diverse configurations of impinging jets are used, such as doublets,...
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Double layer adhesive silicone dressing as a potential dermal drug delivery film in scar treatment
PublicationThe present studies focused on the evaluation of design of an adhesive silicone film intended for scar treatment. Developed silicone double layer film was examined in terms of its future relevance to therapy and applicability on the human skin considering properties which included in vitro permeability of water vapor and oxygen. In order to adapt the patches for medical use in the future there were tested such properties as...
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Whether Carbon Nanotubes Are Capable, Promising, and Safe for Their Application in Nervous System Regeneration. Some Critical Remarks and Research Strategies
PublicationCarbon nanotubes are applied in or considered for different fields of medicine. Among them is the regeneration or rebuilding of nervous system components, which still lack substantial progress; this field is supported by carbon nanotubes to a great extent as the principal material. The limited research on this issue has involved PU/silk/MWCNTs, PCL/silk/MWCNTs, PCL/PGS/CNTs, chitin/CNTs, PGF/CNTs, CNTs/PGFs/PLDLA,MWCNTs chitosan,MWCNTs/PPy,...
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Prophylaxis of Non-communicable Diseases: Why Fruits and Vegetables may be Better Chemopreventive Agents than Dietary Supplements Based on Isolated Phytochemicals?
PublicationThe World Health Organization (WHO) report from 2014 documented that non-communicable socalled civilization diseases such as cardiovascular disease, chronic respiratory diseases, cancer or type 2 diabetes are responsible for over 50% of all premature deaths in the world. Research carried out over the past 20 years has provided data suggesting that diet is an essential factor influencing the risk of development of these diseases....
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Determination of long-chain aldehydes using a novel quartz crystal microbalance sensor based on a biomimetic peptide
PublicationThere is an increasingly popular trend aimed at improvement of fundamental metrological parameters of sensors via implementation of materials mimicking biological olfactory systems. This study presents investigation on usefulness of the peptide mimicking HarmOBP7 region as a receptor element of the piezoelectric sensor for selective analysis of long-chain aldehydes. Identification of odorant binding proteins creates new possibilities...
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Using On-line Measurement by Electronic Nose and Computer Simulations for Real-time Control at WWTP
PublicationContinuous investigation of wastewater quality can be carried out by a device called an e-nose. One important feature of the proposed real-time control system for WWTP is that using on-line measurements by e-nose together (Figure 1) with technological sets picked on this basis by means of computer models, it is possible to change treatment process parameters, depending on the current quality of wastewater. It can be used for the...
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Monitoring of odors emitted from stabilized dewatered sludge subjected to aging using proton transfer reaction–mass spectrometry
PublicationOne of the potential emission sources of odorous compounds from wastewater treatment plants is sludge processing. The odorous compounds released from dewatered sludge can result in odor nuisance. This study concerns the use of flux hood chamber combined with proton transfer reaction—time of flight—mass spectrometry (PTR-MS) technique for periodical monitoring of odorous compounds emitted from aged, stabilized dewatered sludge samples...
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Comprehensive Evaluation of the Biological Properties of Surface-Modified Titanium Alloy Implants
PublicationAn increasing interest in the fabrication of implants made of titanium and its alloys results from their capacity to be integrated into the bone system. This integration is facilitated by different modifications of the implant surface. Here, we assessed the bioactivity of amorphous titania nanoporous and nanotubular coatings (TNTs), produced by electrochemical oxidation of Ti6Al4V orthopedic implants’ surface. The chemical composition...
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Electrochemical oxidation of PFOA and PFOS in landfill leachates at low and highly boron-doped diamond electrodes
PublicationPolyfluorinated alkyl substances (PFASs) may reach landfill leachates (LLs) due to improper waste management. In this study perfluorooctanoate (PFOA) and perfluorooctane sulphonate (PFOS) were used as representatives of PFASs in the decomposition on boron-doped diamond electrodes (BDDs) with high (10k ppm) and low (0.5k ppm) boron doping concentrations. The result shows that although better COD removal efficacies are obtained on...
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Therapeutic Potential of Carnosine and Its Derivatives in the Treatment of Human Diseases
PublicationDespite significant progress in the pathogenesis, diagnosis, treatment, and prevention of cancer and neurodegenerative diseases, their occurrence and mortality are still high around theworld. The resistance of cancer cells to the drugs remains a significant problem in oncology today,while in the case of neuro-degenerative diseases, therapies reversing the process are still yet to be found. Furthermore, it is important to seek new...
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The newest researches and applications of treatment wetlands in sewage sludge management
PublicationIn the paper the newest researches and applications of treatment wetlands conducted by re-searchers of Civil and Environmental Faculty are presented. Among others it was proved that this technology could be successfully implemented for highly polluted wastewater treatment. Within the research project two multistage treatment wetlands, one for landfill leachate and the second for reject water from digested sewage sludge centrifugation,...
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Capillary gas chromatography using a -cyclodextrin forenantiomeric separation of methylamphetamine, its precursors andchloro intermediates after optimization of the derivatization reaction
PublicationtThe enantiomeric ratio of methylamphetamine (MAMP) is closely related to the optical activity of precur-sors and reagents used for the synthesis and this knowledge can provide useful information concerningthe origins and synthetic methods used for illicit manufacture. The information can be utilized for reg-ulation of the precursors and investigation of the manufacturing sources but this requires analyticalprocedures to determine...
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Rapid method for the determination of organochlorine pesticides and PCBs in fish muscle samples by microwave-assisted extraction and analysis of extracts by GC-ECD
PublicationA procedure for the multiresidue determination of organochlorine pesticides and polychlorinated biphenyls in fish muscle samples has been developed. The method is based on the microwave-assisted extraction (MAE) of food samples from an acetonitrile-water (95 + 5, v/v) mixture followed by SPE cleanup of the extracts and analysis by GC with an electron capture detector. MAE operational parameters, such as the extraction solvent,...
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The optimisation of analytical parameters for routine profiling of antioxidants in complex mixture by HPLC coupled post-column derivatisation
PublicationIntroduction: The wide application of natural and artificial antioxidants in food, cosmetic and pharmaceutical industry as well as the recognition of the importance of food antioxidants for supporting human health created demand for reliable and industrially applicable methods of determining antioxidative activity. This requirement can be fullfilled with the recently proposed HPLC-post-column derivatisation approach enabling the...
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Challenges in determination of pesticides from various chemical groups in fruits and vegetables applying QuEChERS method
PublicationPesticides are a large group of compounds with different physical and chemical properties, which place some of them among the most toxic, environmentally stable, and mobile substances. Nevertheless, their number, use, and application are continuously expanding. A consequence of their use is the possible presence of residues in treated food products. To protect consumers from exposure to unacceptable levels of pesticides Maximum...
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Metoda TrustCritic oceny wiarygodności sklepów internetowych
PublicationW artykule przedstawiono metodę oceny wiarygodności sklepów internetowych TrustCritic. Powszechnie występujące nadużycia w handlu elektronicznym sprawiają, że zaufanie do przedsiębiorcy staje się kluczowym czynnikiem decyzji konsumentów. Przedsiębiorca narażony jest na niezgodność z prawem, utratę wizerunku i klientów. Artykuł omawia problematykę nadużyć w sferze e-biznesu oraz proponuje wielokryterialny model oceny sklepu internetowego,...
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Ways of Harmonising Polish Competition Law with the Competition Law of the EU
PublicationThis article discusses the harmonisation of laws within the EU focusing on the specific ways of achieving an approximation of the Polish legal system with European competition law. It identifies and gives an overview of three specific ways of harmonising national laws with EU antitrust provisions: (1) spontaneous (or bottom-up) harmonisation; (2) judicial harmonisation and; (3) legislative harmonisation by means of EU Directives....
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Endoscopic Videos Deinterlacing and On-Screen Text and Light Flashes Removal and Its Influence on Image Analysis Algorithms' Efficiency
PublicationIn this article, deinterlacing and removing on- screen text and light flashes methods on endoscopic video images are discussed. The research is intended to improve disease recognition algorithms' performance. In the article, four configurations of deinterlacing methods and another four configurations of text and flashes removal methods are described and examined. The efficiency of endoscopic video analysis algorithms is measured...
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"SKONTEKSTOWANE. zamieszkiwanie krajobrazów", dwa tryptyki malarskie, akryl/ podobrazie płócienne, materiał video
PublicationPoruszamy się w świecie przemieszanych znaczeń. Kierowani tradycją, doświadczeniem i intuicją przemierzamy przestrzenie odnosząc je do swojego domu. W każdy otaczający krajobraz podświadomie lub celowo wpisujemy siebie. Filtrujemy obraz, dźwięk i zapach włączając wartości niesione przez życie. Dom z marzeń, dom ze wspomnień, dom, do którego tęsknimy, nasz dom: wypełniają kadry i współtworzy historię odwiedzanych miejsc. Przedstawione...
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Optimum Choice of Randomly Oriented Carbon Nanotube Networks for UV-Assisted Gas Sensing Applications
PublicationWe investigated the noise and photoresponse characteristics of various optical transparencies of nanotube networks to identify an optimal randomly oriented network of carbon nanotube (CNT)-based devices for UV-assisted gas sensing applications. Our investigation reveals that all of the studied devices demonstrate negative photoconductivity upon exposure to UV light. Our studies confirm the effect of UV irradiation on the electrical...
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What defines excellent lighting design for humans and animals?
PublicationWhat defines excellent lighting design for humans and animals? The answer to the above question is more than complex. It is not enough nowadays to design a project to make it aesthetically pleasing. Nor is it sufficient to create nicely lit environments, or simply to achieve the light levels required by the lighting norms or standards. With the new scientific research of the last few decades that relates directly or indirectly...
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WEAR OF Si OR B DOPED AMORPHOUS CARBON COATINGS
PublicationThe paper describes a complex wear research on DLC (amorphous carbon) moped with boron (B) and silicone (Si). The tests were carried out in two different sliping systems: flat–on–flat (ring contact, unidirectional sliding) and ball–on–flat (reciprocating sliding). Water and medical saline solutions were used as lubricants. A comparative analysis of the results revealed differences in the initiation and progress of wear and the...
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9-Cyano-10-methylacridinium hydrogen dinitrate
PublicationThe title compound, C15H11N2+·HN2O6−, crystallizes in the monoclinic space group C2/c with four molecules in the unit cell. The planar 9-cyano-10-methylacridinium cations lie on crystallographic twofold axes and are arranged in layers, almost perpendicular to the ac plane, in such a way that neighbouring molecules are positioned in a `head-to-tail' manner. These cations and the hydrogen dinitrate anions are linked through C—H⋯O...
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Zastosowanie testu biologicznego Microtox do oceny skuteczności działania oczyszczalni ścieków bytowo-przemysłowych
PublicationOcena efektywności procesu oczyszczania ścieków z zastosowaniem biotestu Microtox® na przykładzie wybranej oczyszczalni Powszechnie praktykowanym sposobem wprowadzania ścieków oczyszczonych do środowiska jest ich punktowy zrzut do wód powierzchniowych. Różnorodność działalności prowadzonej w ramach współczesnej gospodarki sprawia, że do oczyszczalni docierają nie tylko substancje, których oznaczanie jest wymagane przez przepisy...
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Wikipedia and WordNet integration based on words co-occurrences
PublicationThe article presents a method for automatic integration of two lexical resources: semantic dictionary WordNet and electronic encyclopaedia Wikipedia. Our goal is to add automatically an semantic tags - a WordNet synset identifier to the title of the Wikipedia article. We've analyze several different ap-proaches to these problem and implement our own solution, based on word occurrences in synsets descriptions and the article body....
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Discovering relationships between data in an enterprise information system using log analysis
PublicationEnterprise systems are inherently complex and maintaining their full, up-to-date overview poses a serious challenge to the enterprise architects’ teams. This problem encourages the search for automated means of discovering knowledge about such systems. An important aspect of this knowledge is understanding the data that are processed by applications and their relationships. In our previous work, we used application logs of an enterprise...
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The Influence of Sulfate on Anaerobic Ammonium Oxidation in a Sequencing Batch Reactor
PublicationAnaerobic ammonia-oxidizing bacteria have a more comprehensive metabolism than expected - there may be other electron acceptors that oxidize ammonium nitrogen under anaerobic conditions, in addition to the well-known nitrite nitrogen, one of which is sulfate in the sulfammox process. Sulfate-containing compounds are part of the medium for the anammox process, but their concentrations are not particularly high (0.2 g MgSO4 ∙ 7H2O/dm3...
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Topical delivery of pharmaceutical and cosmetic macromolecules using microemulsion systems
PublicationMicroemulsions are transparent, thermodynamically stable colloidal systems. Over the recent years, they have been increasingly investigated due to their potential as skin delivery vehicles for a wide range of drug molecules. The nanoscale particle size and the specificity of microemulsion components are the main features determining the skin permeation process. However, in order to effectively cross the skin barrier, the active...
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Forced Degradation Studies of Ivabradine and In Silico Toxicology Predictions for Its New Designated Impurities
PublicationAll activities should aim to eliminate genotoxic impurities and/or protect the API against degradation. There is a necessity to monitor impurities from all classification groups, hence ivabradine forced degradation studies were performed. Ivabradine was proved to be quite durable active substance, but still new and with insufficient stability data. Increased temperature, acid, base, oxidation reagents and light were found to cause...
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Experimental test of nonclassicality with arbitrarily low detection efficiency
PublicationWe theoretically introduce and experimentally demonstrate the realization of a nonclassicality test that allows for arbitrarily low detection efficiency without invoking an extra assumption of independence of the devices. Our test and its implementation is set in a prepare-and-measure scenario with an upper limit on the classical communication capacity of the channel through which the systems are communicated. The essence for our...
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Electrical Stimulation Modulates High Gamma Activity and Human Memory Performance
PublicationDirect electrical stimulation of the brain has emerged as a powerful treatment for multiple neurological diseases, and as a potential technique to enhance human cognition. Despite its application in a range of brain disorders, it remains unclear how stimulation of discrete brain areas affects memory performance and the underlying electrophysiological activities. Here, we investigated the effect of direct electrical stimulation...
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Increased Certification of Semi-device Independent Random Numbers using Many Inputs and More Postprocessing
PublicationQuantum communication with systems of dimension larger than two provides advantages in information processing tasks. Examples include higher rates of key distribution and random number generation. The main disadvantage of using such multi-dimensional quantum systems is the increased complexity of the experimental setup. Here, we analyze a not-so-obvious problem: the relation between randomness certification and computational requirements...
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Quality Evaluation of Speech Transmission via Two-way BPL-PLC Voice Communication System in an Underground Mine
PublicationIn order to design a stable and reliable voice communication system, it is essential to know how many resources are necessary for conveying quality content. These parameters may include objective quality of service (QoS) metrics, such as: available bandwidth, bit error rate (BER), delay, latency as well as subjective quality of experience (QoE) related to user expectations. QoE is expressed as clarity of speech and the ability...
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Chemical and biological stability of polyene macrolides
PublicationThe polyene macrolide antibiotics have been used in an-tifungal therapy since first o f them were discovered in 1950's. Up to now, four polyene macrolides are being used in medical practice, namely amphotericin B, nystatin, candi-cidin and pimaricin.The antifungal activity and mode of ac-tion of polyene macrolides is determined by their structure, chemical and physical properties.The main fragment of polyene...
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New patterns in the position of CEE countries in global value chains: functional specialisation approach
PublicationResearch background: High servitisation of manufacturing makes it impossible to separate services from manufactured goods properly, which implies difficulties in the assessment of the position of the country on the smile curve, i.e. in the proper assignment of products or services to one of the industrial process steps: pre-production, pure fabrication or post-production services. Therefore, we propose to use the business functions...
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High-Efficacy Global Optimization of Antenna Structures by Means of Simplex-Based Predictors
PublicationDesign of modern antenna systems has become highly dependent on computational tools, especially full-wave electromagnetic (EM) simulation models. EM analysis is capable of yielding accurate representation of antenna characteristics at the expense of considerable evaluation time. Consequently, execution of simulation-driven design procedures (optimization, statistical analysis, multi-criterial design) is severely hindered by the...
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Wpływ produkcji butelek z tworzyw sztucznych na środowisko naturalne. Cz. I. Zastosowanie metody oceny ReCiPe 2016 w celu identyfikacji problemów środowiskowych
PublicationDokonano oceny wpływu opakowań na środowisko naturalne. Głównym celem było przeprowadzenie analizy cyklu życia (LCA) butelki do napojów wykonanej z poli(tereftalanu etylenu) (PET). Za jednostkę funkcjonalną przyjęto łącznie 1000 szt. butelek PET o pojemności 1 L. Granica przyjętego systemu obejmowała kroki od momentu dostarczenia preform do zakładu produkcyjnego aż do ich prawidłowego ukształtowania w procesie produkcyjnym. Z systemu...
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Efektywność działania środków przeciwstarzeniowych w procesie przyśpieszonego starzenia cieplnego
PublicationPrzedmiotem przedstawionych badań są wulkanizaty kauczuku naturalnego i butadienowo-styrenowego. Celem pracy było zbadanie efektywności działania środków przeciwstarzeniowych w procesie przyspieszonego starzenia cieplnego (w czasie 7 i 14 dni w temperaturze 70°C). Do badań wykorzystano dwie substancje przeciwstarzeniowe: komercyjnie dostępny przeciwutleniacz IPPD (N–fenylo-N′-izopropylo-p-fenylenodiamina) oraz ekologiczny przeciwutleniacz...