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Search results for: HS-SPME
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Porous material-based sorbent coatings in Solid-phase microextraction technique: Recent trends and future perspectives
PublicationThe use of porous materials as sorbents in sample preparation techniques has gained recent scientific attention in the context of developing novel fibers for the Solid-phase microextraction (SPME) technique. SPME requires the appropriate selection of a robust sorbent for successful utilization under variable conditions. A deeper understanding of the nature of newly developed porous SPME coatings and the impact of their structures...
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Nanosorbents as Materials for Extraction Processes of Environmental Contaminants and Others
PublicationThe aim of this work focuses on the application of nanomaterials (NMs) in different sorp- tive extraction techniques for the analysis of organic contaminants from environmental samples of distinct matrix compositions. Without any doubt, the integration of specific NMs such as carbona- ceous nanomaterials, magnetic nanoparticles (MNPs), metal–organic frameworks (MOFs), silica na- noparticles, and ion-imprinted NPs with so lid-phase...
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Autoprezentacja, poznanie i zarządzanie talentami oraz umiejętnościami zawodowymi (DK 00171 HS ), W, ogólnoakademicki, humanistyczno-społeczny, sem. letni 23/24
e-Learning CoursesZapoznanie studenta z meandrami autoprezentacji, optymalnej komunikacji z rynkiem pracy oraz elementami procesu zarządzania talentami pracowniczymi.
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Ionic liquids in the microextraction techniques: the influence of ILs structure and properties
PublicationIonic liquids (ILs) are composed entirely of ions thus they possess unique properties, including negligible volatility, a liquid state in a broad range of temperatures and ability to change them depending on the chosen type of anion and cation, which make ILs unique and useful for many applications in sample preparation techniques. A deeper understanding of the nature of ILs and the impact of their structure on their parameters...
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Nowe rozwiązania metodyczne i techniczne w zakresie techniki mikroekstrakcji do fazy stracjonarnej
PublicationSample preparation has been recognized as a critical step of the analytical process, being even considered as the bottleneck of the overall process. Enrichment of target compounds, transfer of the analytes into a solvent compatible with the analytical instrumentation, minimization of potential interferences, and efficient sample clean-up, are among the main aims of sample preparation techniques. In this regard, liquid-liquid extraction...
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Piotr Lorens prof. dr hab. inż. arch.
PeopleProf. Piotr Lorens - PhD, DSc., urban planner. Lecturer in urban design and development and - since 2007 - Head of the Department of Urban Design and Regional Planning at the Faculty of Architecture, Gdansk University of Technology. His university activities also include coordination of the research and EU Social Fund projects. Based on these projects he was responsible for organization and coordination of the post-graduate studies...
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Effective configuration of a double triad planar parallel manipulator for precise positioning of heavy details during their assembling process
PublicationIn the paper, dynamics analysis of a parallel manipulator is presented. It is an atypical manipulator, devoted to help in assembling of heavy industrial constructions. Few atypical properties are required: small workspace; slow velocities; high loads. Initially, a short discussion about definition of the parallel manipulators is presented, as well as the sketch of the proposed structure. In parallel, some definitions, assumptions...
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An annotated timeline of sensitivity analysis
PublicationThe last half a century has seen spectacular progresses in computing and modelling in a variety of fields, applications, and methodologies. Over the same period, a cross-disciplinary field known as sensitivity analysis has been making its first steps, evolving from the design of experiments for laboratory or field studies, also called ‘in-vivo’, to the so-called experiments ‘in-silico’. Some disciplines were quick to realize the...
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Research project I (February 2024)
e-Learning CoursesThis is the course for English-speaking students of Research project I. Access code: KSiSR2024 If you have some problem with access to the course please sent me e-mail to: slagaj@eti.pg.edu.pl (give me the name and your id number).
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Application of IR UWB Spectrum Shaping to IEEE 802.15.4a Standard
PublicationCoexistence of existing narrowband systems and new ultra wideband devices in the same frequency range requires using some interference mitigation techniques, for example based on spectrum shaping. This paper presents efficiency of impulse radio spectrum shaping methods, applied to IEEE 802.15.4a UWB alternate physical layer signals. Basic parameters of 802.15.4a signal structure and outline of proposed spectrum shaping methods...
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Impact of Spatial Noise Correlation on Bearing Accuracy in DIFAR Systems
PublicationDIFAR type underwater passive systems are one of the more commonly used tools for detecting submarines. At the design stage, which usually uses computer simulations, it is necessary to generate acoustic noise of the sea. It has been shown that correlating noise significantly reduces these errors compared to the assumption that noise is uncorrelated. In addition, bearing errors have been shown to be the same in systems with a commonly...
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Farzin Kazemi Ph.D. Student at Gdansk University of Technology
PeopleHis main research areas are seismic performance assessment of structures and seismic hazard analysis in earthquake engineering. He performed a comprehensive study on the effect of pounding phenomenon and proposed modification factors to modify the seismic collapse capacity of structures or predict the seismic collapse capacity of structures which were retrofitted with linear and nonlinear Fluid Viscous Dampers (FVDs). His current...
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Application of Ionic Liquids in Amperometric Gas Sensors
PublicationThis article presents an analysis of available literature data on metrological parameters of the amperometric gas sensors containing ionic liquids as an electrolyte. Four mechanism types of signal generation in amperometric sensors with ionic liquid are described. Moreover, this article describes the influence of selected physico-chemical properties of the ionic liquids on the metrological parameters of these sensors. Some metrological...
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Rengel Cane Sia Doctoral Candidate
PeopleI’m Rengel, born and raised in the Philippines. As an undergraduate I did kinetic modeling on Copper-catalyzed atom transfer radical addition (ATRA). Then I was inspired to do both theoretical and experimental studies, which led me to propose my master’s thesis on Synthesis, Computational, Electrochemical, and Photoconductivity Studies on Naphthalene and its derivatives. This led to a master’s degree in Chemistry in the Mindanao...
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Entrepreneurship Today: Selected Aspects
PublicationAt its very beginning, entrepreneurship was a purely economic notion. However, this growing interest in entrepreneurship-related problems prompted other sciences to participate in explaining the entrepreneurship phenomenon. Nowadays, entrepreneurship is analyzed through multiple theoretical lenses of economics, management, psychology, sociology – just to name a few. Therefore, it would be difficult to find a notion that could be...
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Distance learning trends: introducing new solutions to data analysis courses
PublicationNowadays data analysis of any kind becomes a piece of art. The same happens with the teaching processes of statistics, econometrics and other related courses. This is not only because we are facing (and are forced to) teach online or in a hybrid mode. Students expect to see not only the theoretical part of the study and solve some practical examples together with the instructor. They are waiting to see a variety of tools, tutorials,...
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Jarosław Guziński prof. dr hab. inż.
PeopleJaroslaw Guzinski received M.Sc., Ph.D. and D.Sc. degrees from the Electrical Engineering Department at Technical University of Gdansk, Poland in 1994, 2000 and 2011 respectively. Since 2016 he is Associate Professor at Gdansk University of Technology. Currently he is the head of the Department of Electric Drives and Energy Conversion. From 2006 to 2009 he was involved in European Commission Project PREMAID Marie Curie, ‘Predictive...
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UAV Design and Construction for Real Time Photogrammetry and Visual Navigation
PublicationA unmanned aerial vehicles applications in photogrammetry have increased rapidly last years. A fast data gathering and processing in real time in some cases become crucial and desired in some application. In the paper, a real time solution is proposed. A real time photogrammetry from UAV is proposed, where image data are gathered and processed on board UAV and finally reconstructed 3D model and measurements are delivered. The paper...
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Implementation of control system and tracking objects in a Quadcopter
PublicationIn this paper, we implement a quadcopter assembly with control and navigation module. The project also includes the design of the control panel for the operator which consists of a set of the micro-controller and the glove equipped with sensors and buttons. The panel has a touch screen which displays current parameters such as vehicle status, including information about orientation and geographical coordinates. The concept of quadcopter...
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Ekstrakcja do fazy stałej niejedno ma imię
PublicationW czasach, gdy we wszystkich przejawach aktywności człowieka trzeba się odnieść do przesłanek leżących u podstaw zrównoważonego rozwoju trudno jest uzasadnić stosowanie w praktyce analitycznej takich procedur i operacji, które pociągają za sobą konieczność:użycia dużych ilości rozpuszczalników i odczynników chemicznychdużych nakładów energii czy też przyczyniają się do wzrostu ekspozycji pracowników laboratoriów na niekorzystne...
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Determination of volatile organic compounds using solventless sample preparation techniques and gas chromatography
PublicationIn this paper the latest advances in the determination of volatile organic compounds using solvent-free extraction techniques in the sample preparation step are presented. A paper is focus mainly on one of the most popular sample preparation technique: solid-phase microextraction technique (SPME) combined with different detection systems and its applications to sampling of VOCs from the samples with different matrices. This paper...
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Wykorzystanie techniki mikroekstrakcji do fazy stacjonarnej w analityce środowiskowej.**2002, 122 s. 25 rys. 31 tab. bibliogr. 465 poz. maszyn. Rozprawa doktorska /10.12.2002/ Wydz. Chem. PG Promotor: prof. dr hab. inż. Jacek Namieśnik
PublicationPrzeprowadzone badania obejmowały: opracowanie podstaw metodycznych oznacza-nia lotnych amin alifatycznych w powietrzu za pomocą GC ze wzbogacaniem te-chniką SPME; określenie warunków oraz parametrów pracy urządzenia do SPME wwarunkach badań modelowych; zbadanie wpływu temperatury, wilgotności i stę-żenia gazowej mieszaniny wzorcowej na efektywność procesu wzbogacania anali-tów z wykorzystaniem urządzenia do SPME; porównanie...
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Ireneusz Kreja dr hab. inż.
PeopleGraduated from the mathematical class at the Nicolaus Copernicus High School in Gdańsk (1974). Master of Sciences in Civil Engineering after studies at Gdansk University of Technology (GUT), Poland (1974-1979). Since 1979 became an employee of the GUT. In 1989 earned a Ph.D. degree in Civil Engineering (with grade "Summa cum Laude") from the GUT. In 2008 obtained a D. Sc. (Habilitation) degree in Civil Engineering (with grade...
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Comparing phylogenetic trees using a minimum weight perfect matching
PublicationA phylogenetic tree represents historical evolutionary relationshipbetween different species or organisms. There are various methods for reconstructing phylogenetic trees.Applying those techniques usually results in different treesfor the same input data. An important problem is to determinehow distant two trees reconstructed in such a wayare from each other. Comparing phylogenetic trees is alsouseful in mining phylogenetic information...
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Low-energy positron scattering from gas-phase uracil
PublicationQuantum scattering calculations are presented for the interaction of low energy positrons with the uracil molecule, an important component of biological systems. The rotational elastic and inelastic cross sections and vibrational inelastic cross sections are reported and compared with existing experiments, indicating a general trend of the cross sections different from the experimental findings and in line with what should be expected...
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A novel method of time-frequency analysis: an essential spectrogram
PublicationA novel precise method of time-frequency analysis is presented. In the algorithm, a new energy distribution is estimated by simultaneously discard or displacement of the classical spec- trogram energy. A channelized instantaneous frequency and a local group delay are used in order to replacement in the same manner as formulated by Kodera et al. [1, 2]. Additionally, new representations: a channelized instantaneous bandwidth and...
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Modeling DAC Application Execution Time
PublicationAn application written in the Divide And Conquer paradigm is more difficult to model than SPMD application because of complex algorithm, causing use of many coefficients in a computational complexity function. Processors are divided into various layers, each layer contains different number of processors. Data packets processed in different layers and transferred between layers have different length. Moreover first layer processors use...
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Mass spectrometric identification of 13C-Labeled metaboloites during anaerobic propanoic acid oxidation
PublicationBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Mass Spectrometric Identification of 13C-Labeled Metabolites DuringAnaerobic Propanoic Acid Oxidation
PublicationBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Próba oceny efektów projektowania układów geometrycznych toru z wykorzystaniem komercyjnych programów komputerowych
PublicationW pracy podjęto kwestię dokładności uzyskiwanej w projektowaniu układów geometrycznych toru z wykorzystaniem komercyjnych programów komputerowych typu CAD. Opisano w sposób ogólny funkcjonowanie wybranego programu. Do celów weryfikacji wykorzystano własną, analityczną metodę projektowania układów torowych. W analizie porównawczej rzędnych poziomych rozpatrzono trzy warianty układu geometrycznego zawierającego łuk koszowy z trzema...
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state aid for projects on heritage conservation
Open Research DataThe dataset encompassed a choice of the most important legal acts in EU law, a list of selected bibliography, together with a list of some interesting individual EC decisions issued on the topic of state aid for heritage conservation in Poland and some UE countries in the period 2007-2013. The reader gets the possibility to acquire basic information...
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Proof of Concept of Indoor Location System Using Long RFID Readers and Passive Tags
PublicationThe paper proposes a system for persons and objects location with the use of long radio-frequency identifications (RFIDs) readers. In order to investigate all aspects of the proposed location system, several key elements had to be analyzed, including the distance from which the tagged objects and the possibility of using more than one tag within one RFID range at the same time. When designing the system, it is also necessary to...
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Average Size of a Suffix Tree for Markov Sources
PublicationWe study a suffix tree built from a sequence generated by a Markovian source. Such sources are more realistic probabilistic models for text generation, data compression, molecular applications, and so forth. We prove that the average size of such a suffix tree is asymptotically equivalent to the average size of a trie built over n independentsequences from the same Markovian source. This equivalenceis only known for memoryless...
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Kamila Kokot-Kanikuła mgr
PeopleKamila Kokot-Kanikuła is a digital media senior librarian at Gdańsk University of Technology (GUT) Library. She works in Digital Archive and Multimedia Creation Department and her main areas of interests include early printed books, digital libraries, Open Access and Open Science. In the Pomeranian Digital Library (PDL) Project she is responsible for creating annual digital plans, transferring files on digital platform, and promoting...
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Green Chemistry - current and future issues
PublicationW pracy przedstawiono 12 zasad Zielonej Chemii oraz wybrane przykłady stosowania zasad w życiu codziennym, przemyśle, laboratoriach i edukacji. Pokrótce opisano historię Zielonej Chemii oraz przyszłe wyzwania. ZCH dotyczy nowego podejścia do zagadnienia syntezy, przeróbki i wykorzystania związków chemicznych, związanego ze zmniejszeniem zagrożenia dla zdrowia i środowiska. Istnieje wiele publikacji opisujących metodyki analityczne...
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Corporate Governance and Ownership Structure in the Top 30 Listed Non Financial Companies in Poland
PublicationThis paper offers a first analysis of the relationships between corporate governance models and rules and ownership structure of the top 30 Polish firms listed at the WSE (not considering foreign firms and/or the Polish branches of foreign firms listed at the same stock exchange, nor the financial companies and the banks). The general picture depicted by this analysis is putting into evidence the increasing importance of institutional...
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Mass Spectrometric Identification of 13C-labeled Metabolites During anaerobic Propanoic Acid Oxidation
PublicationBiowaste digestion is a possibility to gain biogas as a renewable fuel source. However, the anaerobic food chain may be disrupted by, e.g., substrate overload or by inhibitors, leading to the accumulation of volatile fatty acids (VFAs), predominantly of propanoic acid (PA). VFA Accumulation may cause a rapid pH decrease, less biogas production, or even a total inhibition. To maintain high biogas productivity or to prevent a collapse...
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Experimental and theoretical investigation of conformational states and noncovalent interactions in crystalline sulfonamides with a methoxyphenyl moiety
PublicationFour sulfonamide derivatives with a methoxyphenyl moiety, namely N-{4-[(2-methoxyphenyl)sulfamoyl] phenyl}acetamide (1a), N-{4-[(3-methoxyphenyl)sulfamoyl]phenyl}acetamide (1b), 4-amino-N-(2- methoxyphenyl)benzenesulfonamide (2a) and 4-amino-N-(3-methoxyphenyl)benzenesulfonamide (2b), have been synthesized and characterized physiochemically by CHNS, MS, FT-IR, 1H NMR, 13C NMR, PXRD and TG methods. Crystal structures were determined...
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Oznaczanie niezmienionych form lotnych związków bromo- i chloroorganicznych w próbkach płynów biologicznych z wykorzystaniem opracowanej metodyki TLHS-DAI-GC-ECD
PublicationRozprawa doktorska dotyczyła opracowania nowej procedury analitycznej opartej na wykorzystaniu analizy fazy nadpowierzchniowej nad cienkim filmem cieczy z samoczynną generacją strumienia ciekłego sorbentu w połączeniu z chromatografem gazowym wyposażonym w detektor wychwytu elektronów (TLHS-DAI-GC-ECD). Skupiono się na :1. wykonaniu badań optymalizacyjnych poprzedzających walidację metodyki TLHS-DAI-GC-ECD (sprawdzenie trwałości...
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The Hybrid Fuzzy - SOEKS Approach to the Polish Internet Mortgage Market
PublicationThe paper presents the hybrid fuzzy- SOEKS approach to the Polish Internet mortgage market, which is treated as an example of a fast changing market. Firstly, the market and market problems are described. Then, the first approach to the market problems is presented: the complete fuzzy model which was built basing on the rules. The fuzzy model is presented on one real data case. Next, the new approach, called Set of Experience Knowledge...
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Identification of diagnostic parameter sensitivity during dynamic processes of a marine engine
PublicationChanging some parameters of the engine structure alters the emission of harmful components in the exhaust gas. This applies in particular to the damage of charge exchange system as well as fuel system and engine supercharger. These changes are much greater during the dynamic states and their accompanying transitional processes. The different sensitivity of diagnostic parameters to the same force, coming from the engine structure, but...
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Iwona Kochańska dr hab. inż.
PeopleIwona Kochańska is a graduate of Faculty of Electronics, Telecommunications and Informatics, Gdansk University of Technology. She received M.Sc. degree in Automation Control and Robotics, specializing in the mobile objects control. In 2012 she received Ph.D. degree in hydroacoustics. In the same year she started working as an assistant professor in the Department of Marine Electronic Systems. The main area of interest is hydroacoustis, ...
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Can we rely on the pulse transit time - pressure relationship - models comparison
PublicationAn unobtrusive, noninvasive and continuous pressure measurement is invaluable however, still being under research and development. There are many attempts proposing an appropriate relationship between pulse pressure velocity and pressure. Fifteen different formulas, both theoretical and experimental, describing relation between blood pressure and crosssectional area of the vessel were examined. Using these formulas the relation...
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Affective computing and affective learning – methods, tools and prospects
PublicationEvery teacher knows that interest, active participation and motivation are important factors in the learning process. At the same time e-learning environments almost always address only the cognitive aspects of education. This paper provides a brief review of methods used for affect recognition, representation and processing as well as investigates how these methods may be used to address affective aspect of e-education. The paper...
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On the correlation between magnetoacoustic emission and magnetostriction dependence on the applied magnetic field
PublicationThe correlation between magnetoacoustic emission signal envelopes and magnetostriction curves is investigated. Two sets of samples are being considered: tempered martensitic steel and plastically deformed ferritic steel. It is shown that even though some general relations may be observed, as was demonstrated in the literature, the correlation is not always present. One may not expect to change both quantities in the same way if...
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Shape-Memory Polyurethane Polymers
PublicationPolyurethanes (PUs) are one of the most widely used polymers in research and industry. They can be synthesized from chemical sources and natural sources. PUs are a very useful class of polymers and exhibit many desirable properties that can be exploited in various applications. PUs are formed by the reaction between polyols and isocyanates. A wide variety of polyols and isocyanates are available for synthesis, and hence we can...
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The estimation of total volatile organic compounds emissions generated from peroxide cured natural rubber/polycaprolactone blends
PublicationNatural rubber (NR)/polycaprolactone (PCL) blends at the ratio of 90/10% wt. (NR/PCL90/10) and 70/30% wt. (NR/PCL70/30), with a constant amount of dicumyl peroxide, were prepared by compounding in an internal mixer. Obtained NR/PCL bio-based blends were cured at three different temperatures (150 °C, 160 °C and 170 °C). The total content of volatile organic compounds (TVOC) as a function of the NR/PCL blends ratio, and their curing...
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Synthesis and photoelectrochemical behaviour of hydrogenated titania nanotubes modified with conducting polymer infiltrated by redox active network
PublicationIn this work, we show preparation of ordered inorganic-organic composite electrode material where hydrogenated titania nanotubes H-TiO2 with tubularly developed surface modified with poly(3,4-ethylenedioxythiophene) matrix permeated by Prussian Blue (PB) inorganic redox network in order to reach highly photoactive heterojunction. The polymer deposition was realized via two subsequent processes covering: i) potentiostatic polymerization...
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FEM modelling of screw displacement pile interaction with subsoil
PublicationPredicting the-settlement characteristics of piles is an important element in the designing of pile foundations. The most reliable method in evaluating pile-soil interaction is the static load test, preferably performed with instrumentation for measuring shaft and pile base resistances. This, however, is a mostly post-implementation test. In the design phase, prediction methods are needed, in which numerical simulations play an...
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Membrane Solid Phase Microextraction - a new concept of sorbent preparation
PublicationOpracowano nowy układ sorpcyjny do izolacji i/lub wzbogacania polarnych analitów organicznych z próbek wody z zastosowaniem techniki solid phase microextraction (SPME). Układ bazuje na oddzieleniu sorbentu polarnego od próbki za pomocą membrany hydrofobowej. Próbnik membrane-SPME (M-SPME) sporządzono z zastosowaniem polietylenoglikolu (PEG)o masie cząsteczkowej 20 kDa. Polimer ten jest rozpuszczalny w wodzie i w typowych warunkach...