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Professor Janusz Rachoń official address at the Kapodistrian University of Athens
PublicationWystąpienie na uroczystości jubileuszu 170. rocznicy National Kapodistrian University of Athens, Ateny 3 maja 2007
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Design and testing of a radial-axial microturbine for domestic applications
PublicationIn the paper presented is a new design of the radial-axial microturbine of 3-4kW capacity for operation with ethanol as working fluid
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Synthetic, Structural, and Spectroscopic Characterization of a Novel Family of High-Spin Iron(II) [(β-Diketiminate)(phosphanylphosphido)] Complexes
PublicationThis work describes a series of iron(II) phosphanylphosphido complexes. These compounds were obtained by reacting lithiated diphosphanes R2PP(SiMe3)Li (R = t-Bu, i-Pr) with an iron(II) β-diketiminate complex, [LFe(μ2-Cl)2Li(DME)2] (1), where DME = 1,2-dimethoxyethane and L = Dippnacnac (β-diketiminate). While the reaction of 1 with t-Bu2PP(SiMe3)Li yields [LFe(η1-Me3SiPPt- Bu2)] (2), that of 1 with equimolar amounts of i-Pr2PP(SiMe3)Li,...
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Heteroleptic tri-tert-butoxysilanethiolate complexes of manganese(II) - thermal studies
PublicationThe thermal behavior of Mn(II) silanethiolate series [Mn(SR)2L(MeOH)n], where R=SSi(OBut)3, L=heterocyclic nitrogen base and n=0, 1 or 2 has been comparatively investigated using differential scanning calorimetry (DSC), thermogravimetry (TG) and TG-infrared spectoscopy (IR) techniques. The TG curves indicate the differences in the thermal decomposition due to presence of distinct N-donor ligands and labile MeOH molecules coordinated...
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Ultrafast Intramolecular Relaxation and Wave-Packet Motion in a Ruthenium-Based Supramolecular Photocatalyst
PublicationThe hydrogen-evolving photocatalyst [(tbbpy)2 Ru(tpphz)Pd(Cl)2 ](2+) (tbbpy=4,4'-di-tert-butyl-2,2'-bipyridine, tpphz=tetrapyrido[3,2-a:2',3'-c:3'',2''-h:2''',3'''-j]phenazine) shows excitation-wavelength-dependent catalytic activity, which has been correlated to the localization of the initial excitation within the coordination sphere. In this contribution the excitation-wavelength dependence of the early excited-state relaxation...
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First Copper(I) and Silver(I) Complexes Containing Phosphanylphosphido Ligands
PublicationThree new complexes with phosphanylphosphido ligands, [Cu4{μ2-P(SiMe3)-PtBu}4](1), [Ag4{μ2-P(SiMe3)-PtBu2}4](2) and [Cu{η1-P(SiMe3)-PiPr2}2]–[Li(Diglyme)2] (3) were synthesized and structurally characterized by X-ray diffraction, NMR spectroscopy, and elemental analysis. Complexes 1 and 2 were obtained in the reactionsof lithium derivative of diphosphane tBu2P-P(SiMe3)Li·2.7THF withCuCl and [iBu3PAgCl]4, respectively....
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Ratowanie elewacji
PublicationOmówienie prac konserwatorskich przy elewacji budynku mieszkalnego przy ul.3 Maja 27-31 w Gdyni.
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Otrzymywanie oraz zbadanie właściwości tri-tert-butoksysilanotiolanów i tri-tert-butoksysilanolanów chromu(II) i chromu(III)"
PublicationW badaniach nad chemią związków wywodzących się z kwasu ortokrzemowego niezwykle użyteczne okazały się ligandy tri-tert-butoksysilanotiolanowe - SSi(OtBu)3 oraz tri-tert-butoksysilanolanowe - OSi(OtBu)3. Nadrzędnym celem pracy było otrzymanie tri-tert-butoksysilanotiolanowych i tri-tert-butoksysilanolanowych kompleksów chromu i określenie ich struktury za pomocą rentgenowskiej analizy strukturalnej. W wyniku przeprowadzonych badań...
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On the independence number of some strong products of cycle-powers
PublicationIn the paper we give some theoretical and computational results on the third strong power of cycle-powers, for example, we have found the independence numbers alpha((C^2_10)^⊠3) = 30 and alpha((C^4 _14)^⊠3) = 14. A number of optimizations have been introduced to improve the running time of our exhaustive algorithm used to establish the independence number of the third strong power of cycle-powers. Moreover, our results establish...
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Tuftsin-Properties and Analogs
PublicationImmunomodulation is one of the significant therapeutic strategies. It includes both stimulation or suppression of the immune system by a variety of substances called immunomodulators, designed to regulate the immune response of the organism to infections of varying etiology. An example of such a substance is tuftsin (TKPA) 3 (Fig. (1)). Tuftsin is an endogenous immunomodulator of a wide spectrum of biological activity. Tetrapeptide...
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Preparation of 1-[Ω-(1,4,5,6-Tetrahydropyrimidin-2-yl)alkyl]thymines
PublicationOne-stage prepn. of the hydrochloride salts of 1-[ω-(1,4,5,6-tetrahydropyrimidin-2-yl)alkyl]-thymines, e.g. I, from 1-(ω-cyanoalkyl)thymines and a 1:1-mixt. of 1,3-diaminopropane and ethanol satd. with hydrogen sulfide is described. 1-(2-Cyanoethyl)-thymine gave a facile reversal of the Michael reaction to thymine under the conditions used. The reaction of 1,3-bis(3-cyanobenzyl)thymine with the above reagent produced 1,3-bis[3-(1,4,5,6-tetrahydropyrimidin-2-yl)benzyl]thymine.
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Application of Survey Simulator for Museums
Publication“Virtual Museum” is currently a very popular form of presenting museums’ collections of artefacts as well as an approach to archaeological research [1], [2], [3]. The term “virtual” can be understood in many ways – from a simple collection of on-line photographs, through multidirectional viewable panorama pictures, to complete interactive models of the real world, including 3-dimensional (3D) geometry, physical properties and many...
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Reconfiguring Minimum Dominating Sets in Trees
PublicationWe provide tight bounds on the diameter of γ-graphs, which are reconfiguration graphs of the minimum dominating sets of a graph G. In particular, we prove that for any tree T of order n ≥ 3, the diameter of its γ-graph is at most n/2 in the single vertex replacement adjacency model, whereas in the slide adjacency model, it is at most 2(n − 1)/3. Our proof is constructive, leading to a simple linear-time algorithm for determining...
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Graphs with isolation number equal to one third of the order
PublicationA set D of vertices of a graph G is isolating if the set of vertices not in D and with no neighbor in D is independent. The isolation number of G, denoted by \iota(G) , is the minimum cardinality of an isolating set of G. It is known that \iota(G) \leq n/3 , if G is a connected graph of order n, , distinct from C_5 . The main result of this work is the characterisation of unicyclic and block graphs of order n with isolating number...
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Zjawisko interakcji idącego człowieka i drgającego podłoża konstrukcji inży-nierskiej. W: Projektowanie, budowa i estetyka kładek dla pieszych. Ed. K.Flaga, W. Średniawa. Kraków: P. Krak. Wydz. Inż. Ląd. Kated. Bud. Mostów i Tuneli**2003 s. 51-70, 11 fot. 4 rys. 21 wykr. bibliogr. 12 poz. Cykl seminariów: Projektowanie, Budowa i Estetyka Kładek dla Pieszych. Kra-ków, 8 października, 5 listopada, 3 grudnia 2003 r.
PublicationPrzedstawiono podstawy mechaniki chodu, wyniki badań eksperymentalnych i propozycję matematycznego opisu zjawiska dostosowania kroku człowieka do drgań konstrukcji. W części eksperymentalnej przedstawiono stanowisko badawcze wyposażone w bieżnię stacjonarną umieszczoną naplatformie pomiarowej podłączo-nej do siłownika wywołującego drgania o zadanej częstotliwości i amplitudzie. Porównano wyniki symulacji numerycznej z pomiarami...
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Manganese(III) Promoted Cyclization of N-alkenyl-N-(2-hydroxyethyl) amides to Iso-Oxacepham Potent β-Lactamase Inhibitors
PublicationBackground: β-Lactams are still a subject of interest of organic chemists. The main reason for this interest is due to their application as a chemotherapeutic. β-Lactam antibiotics are still the most commonly used drugs in bacterial infections. Method: Methods using 4-exo-trig radical cyclization leading to β-lactams are an alternative to classical Staudinger`s β-Lactams formation. We prepared N-alkenyl-N-(2-hydroxyethyl)amides...
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Iridium 5d -electron driven superconductivity in ThIr3
PublicationA polycrystalline sample of superconducting ThI r 3 was obtained by arc-melting Th and Ir metals. Powder x-ray diffraction revealed that the compound crystalizes in a rhombohedral crystal structure (R-3m, s.g. #166) with the lattice parameters: a = 5.3394 ( 1 ) Å and c = 26.4228 ( 8 ) Å . Normal and superconducting states were studied by magnetic susceptibility, electrical resistivity, and heat capacity measurements. The results...
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Numerical Modeling and Simulation of Vehicular Crashes into Three-Bar Metal Bridge Rail
PublicationAdvanced finite element (FE) modeling and simulations were performed on vehicular crashes into a three-bar metal bridge rail (TMBR). The FE models of a sedan, a pickup truck, and a TMBR section were adopted in the crash simulations subject to Manual for Assessing Safety Hardware (MASH) Test Level 2 (TL-2) and Test Level 3 (TL-3) requirements. The test vehicle models were first validated using full-scale physical crash tests conducted...
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Janusz Nieznański prof. dr hab. inż.
PeopleJanusz Nieznański born in 1957 in Gdańsk. He received the M.Sc. degree in 1981, the Ph.D. degree in 1990, and the D.Sc. (‘habilitation’) degree in 1999, all from the Gdańsk University of Technology. Since 1981 he has been with the above university, where he is currently Professor of Electrical Engineering. His research and teaching interests include control, diagnostics, modeling and simulation of power electronic converters and...
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Structure-function analysis of decay-accelerating factor: identification ofresidues important for binding of the Escherichia coli Dr adhesin and complement regulation
PublicationZidentyfikowano ważne dla wiązania adhezyny Dr uropatogennych Escherichiacoli reszty aminokwasowe w ludzkim receptorze DAF SCR-3.
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Electrochemical sensor for measurement of volatile organic compounds = Elektrochemiczny czujnik do oznaczania lotnych związków organicznych
PublicationPrzedstawiono rezultaty badań prototypowego czujnika do oznaczania benzaldehydu i formaldehydu w powietrzu. Określono czułość wskazań czujnika i jego granice oznaczalności wykorzystując jako technikę detekcyjną woltamperometrię fali prostokątnej (SWV). Elektrodę roboczą i przeciwelektrodę stanowiły elektrody z Pt. Elektrolitem wewnętrznym były ciecze jonowe: chlorek 1-heksylo,3- metyloimidazolinowy i bis(trifluorometylosulfonylo)imidek...
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Synthesis, spectroscopy and crystal structure determination of heteroleptic cobalt(II) silanethiolates with pyridine derivatives
PublicationCztery nowe tri-tert-butoksysilanotiolanowe kompleksy kobaltu(II) z 3- i 4-metylopirydyną zostały zsyntetyzowane i scharakteryzowane. Monometaliczne kompleksy otrzymano w reakcji bimetalicznego kompleksu [Co(SSi(OtBu)3(NH3)]2, który posłużył jako substrat kobaltu(II). Nowe związki zostały scharakteryzowane przy użyciu rentgenografii strukturalnej oraz spektroskopii UV-vis i FT-IR, a także za pomocą analizy elementarnej. Kompleksy...
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Modulacja 3D-SVPWM z kompensacją napięcia niezrównoważenia i balansowaniem napięć DC dla czterogałęziowego falownika 3L-NPC
PublicationPrzedstawiono realizację algorytmu modulacji napięcia 3D-SVPWM (ang. 3-Dimensional Space Vector Pulse Width Modulation) z kompensacją napięcia niezrównoważenia dla trójpoziomowego czterogałęziowego falownika 3L-NPC (ang. 3-Level Neutral-Point-diode-Clamped Converter). Do wyznaczania współczynników wypełnień w modulacji szerokości impulsów zastosowano liniowe funkcje kształtu czworościennego elementu skończonego z węzłami, których...
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Obliczenia MES zginanych belek betonowych na poziomie skali mezo
PublicationW artykule przedstawiono wyniki numeryczne MES modelowanie belek betonowych z nacięciem w czasie zginania 3-punktowego na poziomie skali mezo. Obliczenia wykonano przy wykorzystaniu modelu degradacji sztywności z nielokalnym osłabieniem. Beton został opisany na poziomie skali mezo jako stochastyczny materiał 3-składnikowy złożony z kruszywa, zaczynu cementowego oraz stref kontaktu. Zbadano wpływ rozkładu stochastycznego ziaren...
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Tomasz Wąsowicz dr hab.
PeopleTomasz Wąsowicz's research was first related to high-resolution atomic spectroscopy and focused on measurements and analysis of the transition probabilities of the forbidden lines, the hyperfine and isotopic structure of spectral lines of heavy elements, Stark effect in the helium atom. Tomasz Wąsowicz currently studies physicochemical processes occurring during interactions of various forms of radiation with atoms and molecules...
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Ion-selective electrodes based on p-tert-butyl-homooxacalixarene di(ethyl) amides
PublicationPochodne dietyloamidowe p-tert-butylodihomooksakaliks[4]arenu (1), p-tert-butyloheksahomotrioksakaliks[3]arenu (2) oraz p-tert-butylokaliks[4]arenu (3) były wykorzystane jako materiał aktywny w membranach elektrod jonoselektywnych w celu sprawdzenia detekcji kationów różnych rodzajów (Na+, K+, Cs+, Mg2+, Ca2+, Mn2+, Cu2+, Zn2+, Cd2+, Pb2+ oraz kation tetrametyloammoniowy). Wyznaczono charakterystyki elektrod oraz współczynniki...
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Synthesis of bicoumarin thiophosphate derivatives as steroid sulfatase inhibitors
PublicationBased on the frameworks of 7-hydroxy-2,3-dihydro-1H-cyclopenta[c]chromen-4-one, 3-hydroxy- 7,8,9,10-tetrahydro-6H-benzo[c]chromen-6-one and 3-hydroxy-8,9,10,11-tetrahydro-7H-cyclohepta[c] chromen-6-one, a series of bicoumarin thiophosphate analogs have been synthesized and biologically evaluated. Additionally, their binding modes have been modeled using docking techniques. The inhibitory properties of the synthesized compounds...
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Assessment of Trace Metals Leaching During Rainfall Events from Building Rooftops with Different Types of Coverage – Case Study
PublicationRunoff water is an important medium transporting various types of pollution originating from the atmosphere and washed out from roofing materials. The study presents a quality assessment of runoff from different roofs in the context of trace metal concentrations. The analysed rooftops were covered with copper, tar paper and ceramic tile. The quality of the rain water collected at the same time satisfies the demands of the first...
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Subjective and Objective Quality Evaluation Study of BPL -PLC Wired Medium
PublicationThis paper presents results of research on the effectiveness of bi-directional voice transmission in a 6 kV mine cable network using BPL-PLC (Broadband over Power Line - Power Line Communication) technology. It concerns both emergency cable state (supply outage with cable shorted at both ends) and loaded with distorted current waveforms. The narrowband (0.5 MHz–15 MHz) and broadband (two different modes, frequency range of 3 MHz–7.5...
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Roland Wesołowski Ph.D.
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Oczyszczanie ścieków zawierających ciecz jonową osadem czynnym
PublicationZbadano możliwość biologicznego oczyszczania ścieków syntetycznych zawierających tetrafluoroboran 1-butylo-3-metyloimidazoliowy w laboratoryjnym bioreaktorze z osadem czynnym.
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Jacek Krenz dr hab. inż. arch.
PeopleJacek Krenz, born in 1948 in Poznań, Poland, is an academic architect and painter. He is a professor at Gdańsk University of Technology, Faculty of Architecture, taught also at University of Fine Arts in Poznań – both in Poland – and at Universidade da Beira Interior in Covilhã, Portugal. Charter member of The Polish Watercolour Society. He is a co-founder of the Wdzydze Artists’ Village in Kaszuby, Poland, where he works in his...
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Derivatization of single-walled carbon nanotubes with redox mediator biocatalytic oxygen electrodes
PublicationSingle-walled carbon nanotubes were covalently modyfied with a redox mediator derived from 2,2'-azino-bis-(3-ethylbenzothiazole)-6-sulfonic acid.
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Badania hydrodynamiki doświadczalnego reaktora fluidalnego na ziarno energetyczne. Cz. 2
PublicationPrzedstawiono i omówiono struktury złoża fluidalnego w zależności od 3 przypadków zasilania w powietrze, zasypanego materiału i wysokości reaktora.
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Wytwarzanie cząstek węglanu wapnia w układzie gaz-ciecz w obecności substancji organicznych
PublicationOtrzymywano węgaln wapnia w reakcji CO2 z Ca(OH)2. Do mieszaniny reakcyjnej dodawano glikol etylenowy, glicerol lun n-butanol. Cząstki węglanu wapnia strącane w obecności substancji organicznych były mniejsze niz powstałe w wyniku procesu prowadzonego tylko w mieszninie reagentów w wodzie. Najmniejsze cząstki CaCO3 otrzymywano w obecności glicerolu, wówczas średnia średnica cząstek wynosiła 3,1x10^-3 mm dla reakcji prowadzonej...
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Modulacja 3D-SVPWM dla przekształtników wielopoziomowych czterogałęziowych na bazie funkcji kształtu
PublicationPrzedstawiono realizację algorytmu modulacji napięcia 3D-SVPWM (ang. 3-Dimensional Space Vector Pulse Width Modulation) dla trójpoziomowego czterogałęziowego przekształtnika 3L-NPC (ang. 3-Level Neutral-Point-diode-Clamped Converter). Do wyznaczania współczynników wypełnień w modulacji szerokości impulsów zastosowano liniowe funkcje kształtu czworościennego elementu skończonego. Proponowany algorytm modulacji nie jest ograniczony...
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Nilpotent singularities and chaos: Tritrophic food chains
PublicationLocal bifurcation theory is used to prove the existence of chaotic dynamics in two well-known models of tritrophic food chains. To the best of our knowledge, the simplest technique to guarantee the emergence of strange attractors in a given family of vector fields consists of finding a 3-dimensional nilpotent singularity of codimension 3 and verifying some generic algebraic conditions. We provide the essential background regarding...
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Sulfurization of phosphanylphosphinidene ligand: Access to phosphinothioyltrithiophosphonato platinum(II) complexes
PublicationThe reactivity of phosphanylphosphinidene Pt(0) complexes [DppePt(η2-P–PtBu2)] (1) and [(pTol3P)2Pt(η2-P–PtBu2)] (2) toward sulfur was studied. Reactions of 1 and 2 with an excess of sulfur led to the formation of the first transition metal complexes 3 and 4 with phosphinothioyltrithiophosphonato ligands with the formula [tBu2P(=S)–P(=S)S2]2-. In contrast to previous reports on the phosphanylphosphinidene moiety sulfurization,...
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Synthesis and Spectroscopic Characterization of Selected Phenothiazines and Phenazines Rationalized Based on DFT Calculation
PublicationTwo unique structures were isolated from the phosphorylation reaction of 10H-phenothiazine.The 5,5-dimethyl-2-(10H-phenothiazin-10-yl)-1,3,2-dioxaphosphinane 2-oxide (2a) illustrates theproduct of N-phosphorylation of phenothiazine. Moreover, a potential product of 2a instability,a thiophosphoric acid 2b, was successfully isolated and structurally characterized. Molecule 2a,similarly to sulfoxide derivative...
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Three-dimensional modeling and automatic analysis of the human nasal cavity and paranasal sinuses using the computational fluid dynamics method
PublicationPurpose The goal of this study was to develop a complete workflow allowing for conducting computational fluid dynam- ics (CFD) simulation of airflow through the upper airways based on computed tomography (CT) and cone-beam computed tomography (CBCT) studies of individual adult patients. Methods This study is based on CT images of 16 patients. Image processing and model generation of the human nasal cavity and paranasal sinuses...
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Anna Kuczyńska-Łażewska dr inż.
PeopleAnna Kuczyńska-Łażewska graduated from the Faculty of Chemistry of the Gdańsk University of Technologyin the field of Chemistry (1st degree) and Environmental Protection Technologies, specialization: environmental protection systems (2nd degree). She completed an internship at the Leibniz-Institut für Katalyse in Rostock. She defended her doctorate in recycling of 1st and 2nd generation modules in 2018 at the Department of Energy...
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Badania nośności na zginanie innowacyjnego kształtownika giętego na zimno typu GEB
PublicationLekkie konstrukcje metalowe wytwarzane z kształtowników giętych na zimno to jedna z najszybciej rozwijających się dyscyplin w zakresie budownictwa. Do niedawna profile gięte na zimno stosowano wyłącznie jako elementy drugorzędne, czyli płatwie oraz rygle. Nowo opatentowany przekrój typu GEB ma być wykorzystywany jako element nośny konstrukcji ramowych. Jednak jego zaistnienie na rynku budowlanych konstrukcji metalowych jest uwarunkowane...
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Photofragmentation of tetrahydrofuran molecules in the vacuum-ultraviolet region via superexcited states studied by fluorescence spectroscopy
PublicationPhotofragmentation of tetrahydrofuran molecules in the vacuum-ultraviolet region, producing excited atomic and molecular fragments, has been studied over the energy range 14-68 eV using photon-induced fluorescence spectroscopy. Excited hydrogen atoms H(n), n = 3-11, have been detected by observation of the Hα to Hı lines of the Balmer series. The diatomic CH(A2Δ), CH(B2Σ-) and C2(d3Πg) fragments, which are excited to low vibrational...
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Sense of safety and opinions about COVID-19 vaccinations in Polish school teachers: The role of conspiracy theories belief and fear of COVID-19
PublicationThe co-occurrence of COVID-19 conspiracy theories (CCT) and fear of the coronavirus (FCV) can be linked to how safe people feel and how much they endorse vaccinations. School teachers were one of the vaccination priority groups in Poland. We conducted three cross-sectional studies (N1 = 1006; N2 = 1689; N3 = 627) to find out the potential interactive effects of CCT belief and FCV in predicting sense of safety (SoS; Studies 1-3),...
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Badanie przemian chemicznych i fizykochemicznych tłuszczów smażalniczych skomponowanych na bazie oleju rzepakowego
PublicationNa bazie oleju rzepakowego przygotowano 6 tłuszczów do smażenia: 3 produkty częściowo uwodornione oraz 3 zawierające dodatki stabilizujące - przeciwutleniacze i substancję antypieniącą polidimetylosiloksan. Jako próby odniesienia stosowano olej rzepakowy bez dodatków oraz 2 frytury handlowe. Tłuszcze poddawano ogrzewaniu w temp. 190 C, przez 3 dni, po 6 godz. dziennie. Badano przemiany chemiczne (LK, zawartość oraz skład frakcji...
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Ryszard Katulski prof. dr hab. inż.
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Silicon carbide application issues
PublicationThe main goals of Task 3 and Task 4 of the ordered project ''New technologies based on silicon carbide and their application in HF, high power and high temperature electronics'' are presented
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Podejście procesowe do zarządzania jakością. Część II - opis, nadzorowanie i doskonalenie procesów
PublicationPrzedstawiono kolejne 3 etapy tworzące metodykę wdrażania podejścia procesowego do zarządzania jakością - opis przebiegu, bieżące nadzorowanie oraz doskonalenie procesów w firmie.
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Anna Danuta Dettlaff dr inż.
PeopleShe received her Master of Science degree in engineering with honours in 2013 at the Gdańsk University of Technology at the Department of Analytical Chemistry. In 2013-2017, she was a PhD student in the field of Chemical Technology at Faculty of Chemistry. Her doctoral dissertation was entitled “Nanocomposites based on conducting polymer and carbon materials for supercapacitor application”. In 2015, she was doing a three-month...
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Control design for slow speed positioning
PublicationThe problem under study is a synthesis of position and heading control system for low frequency model of surface vessel described by 3 DOF mathematical model. The recursive vectorial backstepping control design was used to keep fixed position and heading in presence of wave disturbances. The controller has been simulated on computer model of scaled supply vessel. It has been assumed that the actuators produce generalized forces...