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Synthesis of new trifunctional ligands based on 1,4,7,10-tetraazacyclododecane.
Publication1,4,7,10-tetraazacyklododekan jest cykliczną tetraaminą. Selektywne wprowadzenie różnych podstawników jest dość trudnym zadaniem. W pracy przedstawiono syntezę pozwalającą na wprowadzenie trzech różnych podstawników z wysokimi wydajnościami. Substratem w reakcji był dichroniony cyklen, który następnie wykorzystano do selektywnej substytucji podstawnika chinolinowego i długiego łańcucha alifatycznego, zakończonego grupą hydroksylową.Następnie...
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New approach to localization of clicks in archive speech signals.
PublicationPrzedstawiono problem lokalizacji zniekształceń impulsowych w archiwalnych sygnałach mowy. Pokazano, że detekcja oparta na dwuzakresowym modelu autoregresyjnym i przetwarzanie dwukierunkowe pozwala uzyskać znaczącą poprawę działania w stosunku do istniejących metod lokalizacji zniekształceń.
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Database systems for tomorrow: new challenges and research areas
PublicationZaprezentowano nowe obszary badawcze w dziedzinie baz danych, które będą rozwijane w najbliższej przyszłości. Omówiono takie obszary jak systemy typu ''Plug and Play'', duże systemy sfederowane, nowe architektury systemów baz danych oparte na dużych buforach pamięciowych, integracja danych i aplikacji oraz bazy danych semistrukturalnych.
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New vitamin D analogs as potential therapeutics in melanoma
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Trends in the new generation of green solvents in extraction processes
PublicationAnalytical chemistry, like other scientific fields, has undergone a number of changes to make it more consistent with the concept of sustainable development. Among the various steps of chemical analysis, without a doubt, sample preparation is the bottleneck in regard to following a green protocol, especially in terms of solvent consumption. Therefore, many attempts have been made to improve the environmental friendliness of this...
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OVERALL SET OF BANDSAW TEETH VERSUS METHODS OF MEASUREMENTS
PublicationThis article deals with the impact of the manual methods of measurement on the overall set measurement results. It describes the results of the measurement of bandsaw teeth kerf with the use of a micrometer and a digital calliper. It is commonly known that the cutting process causes the wear of cutting tools. The wear of the cutting edge depends on the cutting conditions as well as on the mechanical properties of the processed...
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New algorithms for wow and flutter detection and compensation in audio
PublicationW referacie przedstawiono nowe metody dyskryminacji naturalnych efektów muzycznych i pasożytniczych zniekształceń drżenia dźwięku. Dodatkowo, opisano w nim metody wyznaczania przebiegu zniekształceń drżenia. Wśród nich znajdują się: detekcja okresowości sygnału w poszczególnych ramkach czasowych, śledzenie zmian przydźwięku sieciowego wykorzystujące modelowane AR widma sygnału, śledzenie zmian wysokoczęstotliwościowego prądu podkładu....
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Domination numbers in graphs with removed edge or set of edges
PublicationW artykule przedstawiony jest wpływ usuwania krawędzi lub zbioru krawędzi na liczby dominowania spójnego i słabo spójnego.
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New product practices and performance of German appliances companies
PublicationArtykuł prezentuje wyniki badań odnośnie stosowanych praktyk i wyników uzyskiwanych w rozwoju nowych produktów. Badania dotyczyły niemieckich producentów sprzętu gospodarstwa domowego, zaś podstawową metodą gromadzenie danych była ankieta pocztowa. Rezultaty badań wskazują, że wysokie wyniki rozwoju nowych produktów uzyskują producenci, którzy stosują: strategię pioniera, badania koncepcji, przegląd koncepcji, plan marketingowy...
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Container Cargo Safety. New solutions and future trends
PublicationThe smoothness and flexibility of distribution of goods by containers are teh most important impulses for the development in these means of transport. But the second main reason for the growing containerization of freifht is cargo safety.
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Chapter 8. New composite materials for electrochemical capacitors
PublicationW pracy zaprezentowano materiały hybrydowe składające się z polimeru przewodzącego elektronowo połączonego z nieorganiczną siecią typu redoks. Te materiały to poli(3,4-etylenodioksytiofen) modyfikowany heksacyjanożelazianem (II/III) żelaza (pEDOT/Fehcf), kobaltu (pEDOT/Cohcf) i niklu (pEDOT/Nihcf).Materiały elektrodowe scharakteryzowano metodami elektrochemicznymi w elektrolitach niewodnych. Otrzymane materiały hybrydowe cechują...
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Enhancing the set of experience knowledge structure as a reflexive ontology
PublicationPrzedstawiono mechanizm wspomagania reprezentacji wiedzy wyrażonej w postaci zbioru doświadczeń przy pomocy ontologii.
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New concept of a measurement probe for high impedance spectrocopy
PublicationArtykuł przedstawia nową koncepcję sondy pomiarowej służącej jako obwód wejściowy analizatora do spektroskopii wysokoimpedancyjnej. Dzięki wykorzystaniu przetwornika prąd na napięcie uzyskano najmniejszy możliwy wpływ pojemności kabli dołączających mierzony obiekt na wynik pomiaru. Przeprowadzono analizę sondy biorąc pod uwagę najważniejsze parametry wpływające na dokładność pomiaru: pojemności pasożytnicze oraz rzeczywiste parametry...
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Next generation automatic IP configuration deployment issues
PublicationAlthough Dynamic Host Configuration Protocol for IPv6 (DHCPv6) protocol was defined in 2003, it was designed as a framework rather than a complete solution to the automatic configuration in IPv6 networks. There are still some unsolved problems and new options yet to be defined. One example of such case is Fully Qualified Domain Name (FQDN) option, which final version has been published in late 2007. It describes DHCPv6 client...
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The New LM-PCR/Shifter Method for the Genotyping of Microorganism
PublicationTechniques relies on the ligation of appropriates adapters (LM-PCR) as AFLP, PCR MP and ADSRRS are successfully used for epidemiological studies for prokaryotic and eukaryotic microorganisms. In this study we propose a new method, called the LM-PCR/Shifter, based on the use of a Class IIS restriction enzyme giving restriction fragments with different 4 base 5' overhangs (Shifter) and the ligation of appropriate oligonucleotide...
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Analytical characteristics of a new amperometric sulfur dioxide sensor
PublicationZaprojektowano i skonstruowano wyposażony w układ trójelektrodowy amperometryczny czujnik ditlenku siarki. Elektroda pracująca czujnika była napylona bezpośrednio na powierzchnię membrany. Zbadano charakterystyki czujnika z membranami z mikroporowatego Teflonu oraz Nafionu. Porównano parametry statyczne i dynamiczne tych czujników wypełnionych roztworami elektrolitów wewnętrznych, zawierających dodatek dimetylosulfotlenku.
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A New Heuristic Algorithm for Effective Preemption in MPLS Networks
PublicationW artykule opisano nowy algorytm wywłaszczania przeznaczony dla sieci MPLS. Umożliwia on alokację zasobów sieci dla nowej ścieżki uwzględniając koszt usuniętych jednej lub wielu istniejących już ścieżek. Proponowany heurystyczny algorytm wybiera ścieżki do wywłaszczenia wykorzystując informację o topologii sieci. Używa funkcji optymalizacji minimalizującej stratę pasma na poziomie sieci. Przedstawiono i omówiono wyniki badań symulacyjnych...
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Production of new non-matrix reference material of ethene
PublicationThe main objective of the research is to produce new non-matrix reference materials of ethene. The study are based on thermal decomposition of surface compound chemically bonded with the surface of glass fibers coated with thin layer of aluminum. Positivehomogeneity test, stability test and organization of inter-laboratory comparison are leading to find new non-matrix reference materials which are indispensable tools in the analysis...
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A New Approach For High Speed Data Transmission Monitoring
PublicationW artykule przedstawiono nowatorski sposób monitorowania szybkiej transmisji danych. Technika została zaprezentowana dla przypadku transmisji różnicowej na płycie drukowanej. Cechą szczególną rozwiązania jest możliwość pomiaru jakości transmisji w linii bez konieczności montowania dedykowanych złącz pomiarowych, które mogłyby degradować transmisję.
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Decisional experiance: a new approach to intelligent knowledge representation
PublicationOmowiono nowe podejscie do reprezentacji wiedzy oparte na modelowaniu i formalizacji doswiadczen decyzyjnych
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Decisional DNA based embedded systems: a new perspective
PublicationOmówiono nowe kierunki i perspektywy badań w zakresie systemów podporządkowanych opartych na decyzyjnym DNA.
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A few steps more towards NPT bound entanglement
PublicationIn this paper, existence of bound entangled states with nonpositive partial transpose (NPT) is considered. As one knows, existence of such states would in particular imply nonadditivity of distillable entanglement. Moreover, it would rule out a simple mathematical description of the set of distillable states. The particular state, known to be 1-copy nondistillable and supposed to be bound entangled, is considered. The problem of...
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GreedyMAX-type Algorithms for the Maximum Independent Set Problem
PublicationA maximum independent set problem for a simple graph G = (V,E) is to find the largest subset of pairwise nonadjacent vertices. The problem is known to be NP-hard and it is also hard to approximate. Within this article we introduce a non-negative integer valued functionp defined on the vertex set V(G) and called a potential function of agraph G, while P(G) = max{vinV(G)| p(v)} is called a potential of G. For any graph P(G) <= D(G),...
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A New Model for context aware applications analysis and design
PublicationW artykule zostały opisane aplikacje kontekstowe, które działają w przestrzeniach inteligentnych, oraz zostały przeanalizowane ich właściwości. Na podstawie analizy zaproponowano nowe podejście do ich modelowania które zapewnia oddzielenie logiki aplikacji w zakresie adaptacji (do zmian środowiska) od jej realizacji. Zostały wykorzystane MVC i modele zmian stanu. Zaproponowano ilościową miarę poziomu kontekstowości a także sposób...
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Comparison of new position estimation algorithm for indoor environment
PublicationIn the paper a new position estimation algorithm based on distance measurements is presented. This algorithm is dedicated for indoor environments. In the paper the new algorithm is compared with Chan algorithm. For the comparison were used real measurements conducted inside a building.
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FURTHER REMARKS ON THE NEO-CLASSICAL NAVIER-STOKES EQUATIONS
PublicationThe seminal Navier-Stokes equations have been stated yet before creation of principles of thermodynamics and the first and second laws. In the literature there is the common opinion that the Navier-Stokes equations cannot be taken as a thermodynamically correct model of “working fluid” which is able to describe transformation of “ heat” into “work” and vice versa. Therefore, in the paper, a new exposition of thermodynamically...
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New trends in development of micro heat exchangers for ORC's
PublicationIn the paper, new trends in development of micro heat exchangers for CHP are presented. Main attention is concentrated on the question, how channels size and thermal development lenght affect the heat transfer. New types of micro heat exchangers developed at the Institute of Fluid-Flow Machinery PAS and the methoda of their design are presented. The new experimental testing methods of the micro-channel heat exchangers, new algorithms...
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New developments in preparation and use of standard gas mixtures
PublicationStandard gas mixtures are commonly applied in all stages of analytical work related to the analysis of gaseous samples. Numerous techniques for generating standard gas mixtures are in use. In this article, we present new developments regarding the production of standard gas mixtures, with particular focus on improvements in the application of dynamic techniques for generating them. Furthermore, we describe the application of new...
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Sound Art and Architecture: New Horizons for Architecture and Urbanism
PublicationThe article discusses the crossroad between art and architecture. It sketches out the theoretical and practical aspects of involving art into architecture and multisensory dimensions of space. The analysis is based on examples of innovative experimental activities for architecture: educational projects such as workshops, seminars and courses, combining art and architecture, with special emphasis on sound art, and the consequences...
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A NEW WORK SAFETY MANAGEMENT SYSTEM IN CONSTRUCTION SITES
PublicationThe hazards on the list are assessed on two levels, namely as minor and serious, and the risk relating to work at the site at three levels: small, average and high, within the range from 1 to 10, where 1 is the lowest value meaning a small risk, and 10 the value meaning a high risk.
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Toward the next generation of air quality monitoring: Mercury
PublicationMercury is a global pollutant that is ubiquitous in the environment. Enrichment of mercury in the biosphere as the result of human activities and subsequent production of methylmercury (MeHg) has resulted in elevated concentrations in fish, wildlife and marine mammals globally. Elemental mercury (Hg0) is the most common form of mercury in the atmosphere, and the form that is most readily transported long distances from its emission...
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Mechanical properties of mosquito nets in the context of hernia repair
PublicationThe paper deals with issue of applying mosquito nets as implants in hernia repair, which have already been used in resource-poor developing countries. Uniaxial tensile tests have been conducted on polyester mosquito meshes in two orthogonal directions. Non-linear elastic constitutive laws parameters have been identified to be applied in dense net material models. Mechanical performance of tested mosquito nets has been compared...
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Synthesis and properties of new 'N,'N-phenyltetrazole podand
PublicationThe synthesis of a new chromogenic N,N-phenyltetrazole receptor is reported here. The cationbinding properties of this receptor in solution were investigated by naked-eye colour change, electrochemical methods and UV-Vis spectroscopy in various solvents (CH3CN, dimethylsulphoxide (DMSO), DMSO/H2O, CH3CN/H2O and CH3CN/MeOH). In addition, the receptor was used as a sensing material in ion-selective membrane electrodes. The selectivity...
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Music Genre Recognition in the Rough Set-Based Environment
PublicationThe aim of this paper is to investigate music genre recognition in the rough set-based environment. Experiments involve a parameterized music data-base containing 1100 music excerpts. The database is divided into 11 classes cor-responding to music genres. Tests are conducted using the Rough Set Exploration System (RSES), a toolset for analyzing data with the use of methods based on the rough set theory. Classification effectiveness...
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New clicked full agonists of the estrogen receptor β
PublicationA click chemistry approach was used to synthesize a series of 1,4-diaryl-substituted 1,2,3-triazoles designed to behave as estrogen receptor (ER) ligands. We studied their affinities for both receptors α and β, their agonist activities in a cell-based luciferase reporter assay and their effect on the proliferation of the hormone-dependent MCF-7 cell line. We found two compounds (3a and 3c) that behave as selective full agonists...
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Recykling opakowań ze szkła, aluminium i PET
PublicationW artykule porównano możliwość i korzyści wynikające z recyklingu pojemników typu puszka aluminiowa, butelka szklana i butelka PET. Ocenę przedstawiono na podstawie zebranych danych literaturowych.
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Acoustics - new services for urban planning, research and education
PublicationThe main purpose of the presented design is twofold, namely: providing detailed information about the noise threats that occur every day in city areas and preventing the noise induced hearing loss especially among young people. An experimental system designed for the continuous monitoring of the acoustic climate of urban areas was developed and implemented within the PLGrid Plus project. The assessment of environmental threats...
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New Procedures for Control of Industrial Effluents Treatment Processes
PublicationThis work presents the procedures for monitoring volatile organic compounds during treatment of industrial effluents. The investigation was carried out for a specific effluent—caustic effluent from bitumen production. The developed procedures enable more detailed control of the effectiveness of wastewater treatment than standard procedures. Caustic effluents from bitumen production have a complex physicochemical form and consist...
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ALLYING SYSTEM THINKING AND SET OF EXPERIENCE KNOWLEDGE STRUCTURE
PublicationThe approach of system thinking is completely different from traditional forms of analysis. Even the ancient meaning of word analysis is “a breaking up”. Set of Experience Knowledge Structure is an atomic record of decision event that can be grouped together and form some form of decision DNA of an organization. The question that this paper is trying to answer in how those concepts can be merged.
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Scalar and Vector acoustic fields and sources: a new look
PublicationA study of fundamental problems of the wavefields that are the reaction of fluid continuum on two kinds of primary actions in fluid, then on two kinds of elementary point sources, is presented in this paper, based on the assumption of the physical duality of linear fluid mechanics and the formal symmetry of mathematical description. The two fundamental wavefields generated in fluid by physical point sources are discussed in detail,...
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Asymptotic behaviour in the set of nonhomogeneous chains of stochastic operators
PublicationWe study different types of asymptotic behaviour in the set of (infinite dimensional) nonhomogeneous chains of stochastic operators acting on L1(μ) spaces. In order to examine its structure we consider different norm and strong operator topologies. To describe the nature of the set of nonhomogeneous chains of Markov operators with a particular limit behaviour we use the category theorem of Baire. We show that the geometric structure...
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Weldability of high strength steels in wet welding conditions
PublicationIn this paper are characterized problems of high strength steel weldability in underwater wet welding conditions. Water as a welding environment intensifies action of unfavourable factors which influence susceptibility to cold cracking of welded steel joints. The susceptibility to cold cracking of S355J2G3 steel and S500M steel in wet conditions was experimentally estimated (by using Tekken test). It was concluded that the steels...
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Three phase transient model of wet coal pyrolysis
PublicationA one-dimensional transient mathematical model was developed to describe the thermal and flow phenomena during coal pyrolysis in a coke oven. The model was solved numerically using partly implicit methods for gas flow and heat transfer problems. It was successfully validated with industrial-scale measurements of temperature change in the middle-plane of the coke oven chamber. The evolution of temperature and pressure, distributions...
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A new quaternion-based encryption method for DICOM images
PublicationIn this paper, a new quaternion-based lossless encryption technique for digital image and communication on medicine (DICOM) images is proposed. We have scrutinized and slightly modified the concept of the DICOM network to point out the best location for the proposed encryption scheme, which significantly improves speed of DICOM images encryption in comparison with those originally embedded into DICOM advanced encryption standard...
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New Approach to Arc Fitting for Railway Track Realignment
PublicationThis article presents a new method of arc fitting for railway track realignment. The theoretical foundations are presented, along with a detailed algorithm of the iterative computational process. This method is based on solving a set of linearized pseudo-observation equations. The formulas of the functional model of the fitting problem were derived, and a special form of objective function is proposed. An iterative method for optimization...
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A new diagnostic method for evaluation of cardiosurgery wound healing
PublicationOne of important and still unsolved problems in medicine is the question of objective and quantitative evaluation of post-surgery wound healing. The aim of this research is to analyse possibility and value of using the newly elaborated infrared imaging procedure – Active Dynamic Thermography (ADT) – for quantitative description of wound healing processes in cardiosurgery. Both, classical thermal figures of merit as well as ADT...
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In search for new urban planning education and research formulas
PublicationThis paper shows research and educational urban planning projects based on international and mutlicultural cooperation including innovative elements to conduct research on built environment. Their common aim is to search for a new perspective on the city development and challenges resulting from changing conditions.
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Structural and spectroscopic analysis of a new family of monomeric diphosphinoboranes
PublicationWe present a series of amino- and aryl(diphosphino)boranes R2PB(R’’)PR’2, where R2P, R’2P = tBu2P, tBuPhP, Ph2P, Cy2P, and R’’ = iPr2N, Ph, which were obtained via the metathesis reaction of iPr2NBBr2 or PhBBr2 with selected lithium phosphides. The structures of isolated diphosphinoboranes were characterized in the solid state and in solution by means of X-ray diffraction and NMR spectroscopy, respectively. The utility of these...
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Hydrodynamic Model of the New Waterway through the Vistula Spit
PublicationThe decision to build a new waterway (strait) in the Polish part of the Vistula Spit was made in 2017. The new connection between the Gulf of Gdańsk and the Vistula Lagoon is planned as an artificial navigable channel with a lock and a small port. During storm surges and wind tides in the gulf or in the lagoon, sluicing will be re-quired for vessels to tackle the Vistula Spit. This procedure does not require significant water flow...
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NEW DESIGNS OF MAGNETIC FLUID SEALS FOR RECIPROCATING MOTION
PublicationT he operating conditions of magnetic fluid seals during reciprocating motion are so different from those observed in rotating motion that the use of their conventional structures for reciprocating motion seals yields no good results. The analysis of the sealing mechanism of magnetic fluid seals in reciprocating motion shows that the operation of these seals is affected by the carry-over phenomenon and magnetic fluid...