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Search results for: STALE CR-MO
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Ocena stanu trójnika rurociągu pary świeżej ze stali 13HMF metodą emisji magnetoakustycznej
PublicationZbadano trójnik w rurociągu pary świeżej ze stali 13HM o czasie eksploatacji około 66 tyś. godzin. Mierzono: natężenie emisji magneto akustycznej (EMA), twardość HV, współczynnik tłumienia fal ultradźwiękowych (dB/mm). W przypadku badania EMA do magnesowania użyto grubościenny elektromagnes jarzmowy o adaptowanych ramionach a sygnał napięciowy z szerokopasmowej sondy był filtrowany w celu eliminacji zakłóceń przemysłowych. Porównawcza...
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Strength deterioration of 26H2MF and 34HNM steels used in ship engines: hydrogen factor
PublicationBadano podatność stali 26H2MF i 34HNM poddanych różnej obróbce cieplnej na niszczenie wodorowe. Badania wykonano metodą powolnego rozciągania z szybkością 10-6 s-1. Określano wytrzymałość, wydłużenie, przewężenie i energię zniszczenia. Stwierdzono znaczna degradację w 0,01 M kwasie siarkowym z dodatkiem arszeniku. Wykazano istnienie korelacji między obróbką cieplną i stopniem degradacji. Efekty przypisano pułapkowaniu wodoru.
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Elektrochemiczne badania korozyjne stali do azotowania.Electrochemical corrosion tests of nitriding steels
PublicationPrzedstawiono badania elektrochemiczne podatności na korozję stali do azotowania gatunków 31CrMoV9 i 34CrAlNi7-10 oraz warstw azotowanych jarzeniowo. Badania wykonano metodą potencjoskokową w środowisku słabo kwaśnym.
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Nieniszczące magnetyczne metody badania stanu eksploatowanych w energetyce stali o własnościach ferromagnetycznych.
PublicationOpisano podstawy fizyczne i przykłady zastosowania magnetycznych metod badań stanu mikrostruktury stali eksploatowanych w energetyce. Zmiany mikrostruktury wynikały z procesu degradacji. Stosowano takie metody badań jak: pomiar pętli histerezy B(H)oraz pomiar natężenia efektu Barkhausena i emisji magnetoakustycznej. Wykazano, iż najbardziej zasadne jest wykorzystanie do badań nieniszczących efektu emisji magnetoakustycznej.
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Chromium (III) removal by perennial emerging macrophytes in floating treatment wetlands
PublicationFloating treatment wetlands (FTWs) are a sustainable solution to treat polluted water, but their role in chromium (Cr(III)) removal under neutral pH conditions remains poorly understood. This study evaluated the potential of FTWs planted with two perennial emergent macrophytes, Phragmites australis and Iris pseudacorus, to remove Cr(III) and nutrients (N and PO4-P) from water containing 7.5 mg/L TN, 1.8 mg/L PO4-P, and Cr(III)...
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Zagrożenie powodziowe polderu oruńskiego w Gdańsku 2001.
PublicationW roku 2001 nastąpiła powódź na polderze oruńskim, w południowej części miasta. Polder położony jest poniżej poziomu morza i stale odnawiany mechanicznie. Jest to byłe dno jeziora, stale zagrożone topielą, otoczone wałami przeciwpowodziowymi.
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Optimization of adsorption of methyl orange from aqueous solution by magnetic CoFe2O4/ZnAl-layered double hydroxide composite using response surface methodology
PublicationThe CoFe2O4/ZnAl-layered double hydroxide (LDH) composite was successfully developed through a facile co-precipitation method, characterized, and applied as an effective adsorbent for the removal of methyl orange (MO) dye from aqueous solutions. The central composite design (CCD) of the response surface methodology (RSM) was employed to estimate and optimize process variables such as initial MO concentrations, solution pH, adsorbent...
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Enabling simultaneous redox transformation of toxic chromium(VI) and arsenic(III) in aqueous media—A review
PublicationSimultaneous conversion of most harmful As(III) and Cr(VI) to their less toxic counterparts is environmentally desirable and cost-effective. It has been confirmed that simultaneous oxidation of As(III) to As(V) and reduction of Cr(VI) to Cr(III) can occur via free radical or mediated electron transfer processes. While Cr(VI) is reduced by reacting with H•, eaq−, photoelectron directly or undergoing ligand exchange with H2O2 and...
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Crystal structure and physical properties of a novel ternary compound La15MoxGe9
PublicationWe present the synthesis, structural characterization and physical properties measurements of a new compound, La15MoxGe9 in Mn5Si3-type derived structure with interstitial Mo. The sample was synthesized by arc-melting method. La15MoxGe9 crystallizes in non-centrosymmetric hexagonal structure P63mc (#186) with lattice parameters a = b = 15.495(5) Å and c = 6.917(2) Å. The refinement on single X-ray diffraction data show that interstitial...
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Concentration‐Induced Hetero‐Valent Partial‐Inverse Occupation of Infrared Phosphor
PublicationInfrared luminescent materials have evoked much attention from chemists and material scientists. Although substantial progress is made in materials design, the luminescent mechanism remains ambiguous in the complex structures, presenting major barriers to developing novel infrared luminescent materials. Herein, this study aims to deliberate a complete discussion on infrared phosphors with concentration-induced hetero-valent partial-inverse...
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High-temperature kinetics study of 430L steel powder oxidized in air at 600–850 °C
PublicationThe 430L stainless steel powder with a mean particle size of 95 μm was studied to determine its high-temperature oxidation properties. Continuous thermogravimetric measurements were carried out for 100 h in air at temperatures in the range of 600–850 °C. Even though a considerable amount of Cr (up to ˜5 wt.% Cr) inside the grains was depleted – especially inside small grains – no breakaway oxidation was observed. This indicates...
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Potential of nanocomposites of zero valent copper and magnetite with Eleocharis dulcis biochar for packed column and batch scale removal of Congo red dye
PublicationThe current study is the first attempt to prepare nanocomposites of Eleocharis dulcis biochar (EDB) with nano zero-valent Copper (nZVCu/EDB) and magnetite nanoparticles (MNPs/EDB) for batch and column scale sequestration of Congo Red dye (CR) from synthetic and natural water. The adsorbents were characterized with advanced analytical techniques. The impact of EDB, MNPs/EDB and nZVCu/EDB dosage (1–4 g/L), pH (4–10), initial concentration...
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Degradation of cefadroxil drug by newly designed solar light responsive alcoholic template-based lanthanum ferrite nanoparticles
PublicationIn this work, lanthanum ferrite nanoparticles were synthesized via a simple co-precipitation method. Two different templates, namely sorbitol and mannitol, were used in this synthesis to tune the optical, structural, morphological, and photocatalytic properties of lanthanum ferrite. The synthesized lanthanum ferrite-sorbitol (LFOCo-So) and lanthanum ferrite-mannitol (LFOCo-Mo) were investigated through Ultraviolet–Visible (UV–Vis),...
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Effect of SiC on the corrosion behaviour of chromium coatings
PublicationWarstwy kompozytowe Cr-SiC osadzono z kąpieli zawierającej Cr(VI) oraz zielony proszek SiC. Zawartość SiC w warstwie chromowej wynosiła od 0,1-0,9% wag. Badania XPS wykazały iż SiC pokrywała warstwa SiO2, która powstała w wyniku utleniania SiC za pomocą Cr(VI). Przeprowadzono badania potencjodynamiczne i badania za pomocą spektroskopii impedancyjnej w celu określenia właściwości korozyjnych warstw Cr-SiC w środowisku kwaśnym....
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The role of microbial coagulants on the physicochemical, proteolysis, microstructure and sensory properties of low-fat Edam cheese manufactured from ultrafiltered buffalo milk
PublicationThis work investigates the influence of using microbial coagulants, including Rhizomucor miehei (MCR) protease and Cryphonectria parasitica (MCC) protease, on the quality characteristics of low-fat Edam cheese made from ultrafiltered buffalo milk (LFUE). Concurrently, a benchmark with calf rennet (CR) has been also performed. Throughout a 90-day ripening period, the cheeses were assessed for their physicochemical features, proteolysis,...
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A fast time-frequency multi-window analysis using a tuning directional kernel
PublicationIn this paper, a novel approach for time-frequency analysis and detection, based on the chirplet transform and dedicated to non-stationary as well as multi-component signals, is presented. Its main purpose is the estimation of spectral energy, instantaneous frequency (IF), spectral delay (SD), and chirp rate (CR) with a high time-frequency resolution (separation ability) achieved by adaptive fitting of the transform kernel. We...
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Synchrotron radiation photoemission spectroscopy of the oxygen modified CrCl3 surface
PublicationWe investigate the experimentally challenging CrCl3 surface by photon energy dependent photoemission (PE). The core and valence electrons after cleavage of a single crystal, either in a ultrahigh vacuum (UHV) or in air, are studied by keeping the samples at 150 1C, aiming at confirming the atomic composition with respect to the expected bulk atomic structure. A common spectroscopic denominator revealed by data is the presence of...
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The effect of PEDOT morphology on hexavalent chromium reduction over 2D TiO2/PEDOT photocatalyst under UV–vis light
PublicationThe present study represents an approach to apply organic-inorganic hybrid materials for photocatalytic removal of heavy metals from the aqueous environment. The photocatalytic activity of the semiconductor modified with the conjugated polymer may depends on the conjugated polymer type, its amount and morphology. Therefore, in the present study the effect of poly (3, 4-ethylenedioxythiophene) (PEDOT) morphology on adsorption and photoreduction...
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Stress corrosion cracking of the 26H2MF and 34HNM constructional allaysteels of different heat treatment in hydrocarbons
PublicationBadane są dwie stale stopowe 26HZMF i 34HNM o różnych właściwościach mechanicznych w różnych środowiskach.
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Domain segmentation for low-cost surrogate-assisted multi-objective design optimisation of antennas
PublicationAbstract: Information regarding the best possible design trade-offs of an antenna structure can be obtained through multiobjective optimisation (MO). Unfortunately, MO is extremely challenging if full-wave electromagnetic (EM) simulation models are used for performance evaluation. Yet, for the majority of contemporary antennas, EM analysis is the only tool that ensures reliability. This study introduces a procedure for accelerated...
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Zachowania starszych klientów na rynku usług on-line
PublicationOsoby starsze stanowić będą w przyszłości stale zwiększający się rynek konsumencki. Jednocześnie stale rośnie rynek usług online. Dlatego problem korzystania osób starszych z usług on-line nabiera szczególnego znaczenia. W artykule przedstawione zostały wyniki badania sposobu korzystania z usługi pośrednictwa pracy w serwisach internetowych, uzyskane z wykorzystaniem badań okulograficznych - nagrań Gaze Plot oraz wywiadów ThinkAloud....
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Nowe rozwiązania materiałowe w konstrukcji barek na wody płytkie
PublicationScharakteryzowano takie rozwiązania, jak konstrukcje sandwiczowe SPS, elastomery na części podwodne, stale niskostopowe na barki o płytkim zanurzeniu.
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Reactivity of Diimido Complexes of Molybdenum and Tungsten towards Lithium Derivatives of Diphosphanes and Triphosphanes
PublicationThe reaction of R2P–P(SiMe3)Li (R = tBu, iPr) with the diimido molybdenum complex [(ArN)2MoCl2·dme] (Ar = 2,6-iPr2C6H3; dme = 1,2-dimethoxyethane) yielded the side-oncoordinated phosphanylphosphinidene anionic complexes [(2,6-iPr2C6H3N)2Mo(Cl)(η2-P=PR2)]– (7Mo, 8Mo). The thermal decomposition of [(2,6-iPr2C6H3N)2M(Cl)(η2-P=PR2)]–[M = Mo (7Mo), W (8W)] to [(2,6-iPr2C6H3N)2M(Cl)(1,2-η-tBu2P=P–PtBu2)] [M = Mo (3Mo), W (3W)] was investigated...
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Crystallization kinetics study of dynamically vulcanized PA6/NBR/HNTs nanocomposites by nonisothermal differential scanning calorimetry
PublicationInvestigation of crystallization behavior and kinetics of thermoplastic elastomer nanocomposites was the subject of limited works because of complexities associated with semiexperimental modeling of such phenomenon in a system containing components having completely different behavior in the molten state. Nonisothermal crystallization kinetics of dynamically vulcanized PA6/NBR/HNTs thermoplastic elastomer nanocomposites was mathematically...
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The fate and contamination of trace metals in soils exposed to a railroad used by Diesel Multiple Units: Assessment of the railroad contribution with multi-tool source tracking
PublicationSoil samples from cut slopes from lightly loaded railway lines used by Diesel Multiple Units for 5 years in Gdansk (Poland) were collected and analyzed for trace metals (TMs): Zn, Pb, Cd, Ni, Cr, Cu, and Fe. The main aim was to assess soil enrichment, contamination status, and distribution of TMs relative to the distance from the railway track. Extensive source tracking analyses were performed using cluster analysis (CA) and the...
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Rapid Multi-Criterial Antenna Optimization by Means of Pareto Front Triangulation and Interpolative Design Predictors
PublicationModern antenna systems are designed to meet stringent performance requirements pertinent to both their electrical and field properties. The objectives typically stay in conflict with each other. As the simultaneous improvement of all performance parameters is rarely possible, compromise solutions have to be sought. The most comprehensive information about available design trade-offs can be obtained through multi-objective optimization...
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Syntheses and structures of the first terminal phosphanylphosphido complexes of molybdenum(IV)
PublicationThe reactions of R2P-P(SiMe3)Li (R = tBu, iPr2N) with [Cp2MoCl2] yield terminal phosphanylphosphido complexes formally via the insertion of the phosphinidene P-atom into the C - H bond of a cyclopentadienyl ring and the migration of the hydrogen atom or SiMe3 moiety to the molybdenum centre. Solid state structures of [Cp(C5H4P-PtBu2)MoH], [Cp(C5H4P-PtBu2)Mo(SiMe3)] and [Cp{C5H4P-P(NiPr2)2}Mo(SiMe3)] were established by single crystal...
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Methods of Assessment of Metal Contamination in Bottom Sediments (Case Study: Straszyn Lake, Poland)
PublicationThe concentrations of six metals (Zn, Cu, Pb, Ni, Cr, and Cd) were investigated in bottom sediments of Straszyn Lake (North Poland). This study was designed to determine a total content of metals and to assess their mobility and bioavailability. The sequential extraction was used to fractionate metals into five fractions: exchangeable, bound to carbonates, bound to Fe–Mn oxides, bound to organic matter, and residual. The evaluation...
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Przegląd własności nowych stali chromowych.
PublicationOpisano mikrostruktury oraz właściwości mechaniczne i eksploatacyjne stali chromowych typu 9-12% Cr.
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Rapid multi-objective optimization of antennas using nested kriging surrogates and single-fidelity EM simulation models
PublicationEver increasing performance requirements make the design of contemporary antenna systems a complex and multi-stage process. One of the challenges, pertinent to the emerging application areas but also some of the recent trends (miniaturization, demands for multi-functionality, etc.), is the necessity of handling several performance figures such as impedance matching, gain, or axial ratio, often over multiple frequency bands. The...
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Optymalizacja podatkowa przedsiębiorców – granice prawa a granice bezpieczeństwa
PublicationOptymalizacja podatkowa jest kategorią niezbędną w działalności każdego podmiotu gospodarczego. Niestety przepisy prawa podatkowego nie wyzna-czają zakresu dopuszczalnych prawem działań optymalizujących. Działaniom takim nie sprzyjają: niejasne i niestabilne przepisy prawne, ukierunkowanie sytemu podatkowego wyłącznie na cele fiskalne, brak strategii podatkowych wobec przedsiębiorców oraz niewystarczający poziom edukacji podatkowej....
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Low-cost multi-criterial design optimization of compact microwave passives using constrained surrogates and dimensionality reduction
PublicationDesign of contemporary microwave circuits is a challenging task. Typically, it has to take into account several performance requirements and constraints. The design objectives are often conflicting and their simultaneous improvement may not be possible; instead, compromise solutions are to be sought. Representative examples are miniaturized microwave passives where reduction of the circuit size has a detrimental effect on its electrical...
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Current and future emissions of selected heavy metals to the atmosphere from anthropogenic cources in Europe
PublicationPrzedstawiono wyniki obliczeń emisji As, Cd, Cr, Ni i Pb do powietrza ze źródeł antropogennych w Europie. Obecnie spalanie paliw jest głównym źródłem emisji As, Cd, Cr i Ni (powyżej 50 % ogólnej emisji tych metali), natomiast spalanie benzyny jest głównym źródłem emisji Pb. Zaobserwowano ciągłą redukcje emisji tych metali w Europie w ciagu ostatnich 40 lat. Powiększający się stan wiedzy nt. źródeł, emisji oraz transportu i zachowania...
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Pre-oxidation of porous ferritic Fe22Cr alloys for lifespan extension at high-temperature
PublicationPre-oxidation of porous ferritic Fe22Cr alloys was extensively studied in this paper. Weight gain measurements and SEM analysis revealed that pre-oxidation performed at 900◦C for 40 min increased the lifespan of the alloy. A Cr evaporation study did not disclose any significant influence of the pre-oxidation process on the Cr content in the alloy. For a more detailed assessment, TEM imaging and X-ray tomography measurements of...
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Coastal cliff erosion as a source of toxic, essential and nonessential metals in the marine environment
PublicationDue to the rising environmental awareness, emissions and releases of pollutants, including metals, have been considerably reduced in the last decades. Therefore, the remobiliza-tion of natural and anthropogenic contaminants is gaining importance in their biogeochemical cycle. In the marine coastal zone, this process occurs during the erosion of a shore, especially the most vulnerable cliffs. The research was conducted in the...
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Study on polymer modified road asphalt mixture
PublicationThe formulation of ternary asphalt-additives blend composed of crumb rubber : low-density polyethylene (CR : LDPE) and crumb rubber : textile fiber (CR : TF) couples, and quaternary asphalt additives-blend composed of (CR : LDPE : TF) triplets on the virgin asphalt to optimize the asphalt basic and rheological properties and to use the extrusion process of two or three additives to obtain composite materials of them, as well as...
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Low-Dimensional Magnetic Semimetal Cr0.65Al1.35Se3
PublicationWhile exploring novel magnetic semiconductors, the new phase Cr0.65Al1.35Se3 was discovered and characterized by both structural and physical properties. Cr0.65Al1.35Se3 was found to crystallize into orthorhombic CrGeTe3-type structure with space group Pnma (no. 62). Vacancies and mixed occupancies were tested, and the results show that one of the 4c sites accommodates a mixture of Cr and Al atoms, while the other 4c site is fully...
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High-temperature Corrosion of ~ 30 Pct Porous FeCr Stainless Steels in Air: Long-Term Evaluation Up to Breakaway
PublicationIn this work, a long-term (up to 6000 hours) corrosion evaluation of three porous (~ 30 pct of initial porosity) ferritic iron-chromium alloys with different Cr contents (20, 22, and 27 wt pct of Cr) was carried out at 600 C, 700 C, 800 C, and 900 C in air. Mass gain measurements and SEM analyses revealed that at temperatures above 600 C, all alloys exhibit breakaway corrosion, whereas at 600 C, none of the alloys were heavily...
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Elektrownie jądrowe- historia i przegląd typów reaktorów
PublicationElektrownie jądrowe stanowią jedno ze źrodeł produkcji energii. Produkują one duże ilości energii z małej ilości surowca. Reaktry jądrowe są stale rowijane technologicznie, po to aby byly one jeszcze bezpieczniejsze, a także aby pracowały z coraz to wyższymi sprawnościami
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O możliwości spawania elementów kształtowych giętych na zimno ze stali typu S355
PublicationCelem pracy jest ocena wpływu gięcia na zimno profili na własności spoin usytuowanych w rejonie gięcia. Praca obejmuje opis tych zagadnień z punktu widzenia budowy strukturalnej i warunków sprzyjających procesowi starzenia jak i technologii spawania w odniesieniu do stali S355. Własności mechaniczne elementów giętych na zimno są niehomogeniczne wzdłuż obwodu z powodu różnic w umocnieniu powstającego w trakcie gięcia na zimno. w...
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Generalized Pareto ranking bisection for computationally feasible multi-objective antenna optimization
PublicationMulti-objective optimization (MO) allows for obtaining comprehensive information about possible design trade-offs of a given antenna structure. Yet, executing MO using the most popular class of techniques, population-based metaheuristics, may be computationally prohibitive when full-wave EM analysis is utilized for antenna evaluation. In this work, a low-cost and fully deterministic MO methodology is introduced. The proposed generalized...
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Trace elements content of surface peat deposits in the Solovetsky Islands (White Sea)
PublicationPeatlands form environmental archives of trace element deposition. In this regard they are particularly valuable for areas such as the Arctic, where regular pollution monitoring is either impossible or extremely costly. The aim of this study was to assess pollution in the Solovetsky Islands (65° 05' N, 35° 53' E) by examining the spatial variability in trace element content of the uppermost layer of peat, immediately below the...
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The speciation of selected heavy metals in sewage sludge stabilized in reed basins
PublicationThe aim of the work was to determine influence of time on organic matter content, nutrients concentrations as well as speciation of selected heavy metals (Cd, Pb, Ni, Cr, Cu and Zn) in sewage sludge stabilized in reed basins during 7-15 years. The analyzed sewage sludge was collected from reed basins from four municipal WWTPs located in Denmark serving from 9 000 to 40 000 pe in Vallo, Rudkøbing, Nakskov and Helsinge. Sewage...
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A universal NDT method for examination of low energy impact damage in CFRP with the use of TLC film
PublicationThe article presents an attempt to use a sheet of laminated thermochromic liquid crystal film (TLC film) for non-destructive testing of the impact damage (energy values: 1J, 2J, 3J and 4J) in carbon fibre-reinforced polymer (CFRP). This is a new, alternative NDT approach based on the thermo-optical effect. The main advantages of this method are a) the low cost of TLC film, b) the low cost of recording devices due to the usage of...
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Magazynowanie energii elektrycznej i gospodarka wodorowa
PublicationW artykule dokonano przegl ą du aktualnych technologii magazynowania energii elektrycznej oraz zestawiono uzyskiwane parametry w aspekcie zastosowa ń w zasobnikach systemowych. Przedstawiono studium mo ż liwo ś ci magazynowania energii z odnawialnych ź róde ł energii (O Ź E) w zasobnikach akumulatorowych i elektrowniach szczytowo-pompowych w Polsce. Omówiono tak ż e mo ż liwo ś ci wykorzystania...
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Wykorzystanie surowców odnawialnych i odpadowych w syntezie poliuretanów
PublicationNa podstawie literatury i badañ w³asnych przedstawiono stan wiedzy na temat mo¿liwooeci stosowania w syntezie poliuretanów surowców odnawialnych i odpadowych, g³ównie polioli pochodzenia rooelinnego, gliceryny odpadowej z produkcji biodiesla i oleju talowego.
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Spatial and vertical distribution analysis of heavy metals in urban retention tanks sediments: a case study of Strzyza Stream
PublicationConcentrations of seven heavy metals (HMs): Zn, Cu, Pb, Cd, Ni, Cr, and Fe in core samples of bottom sediments from four retention tanks (RTs) located along the Strzyza Stream in northern Poland (Gdansk) were measured to obtain a general view of sediment quality. The recognition of contamination and potential environmental impacts is the main aim of this paper. A total of 96 sediment samples were collected from eight sampling sites...
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S-scheme heterojunction Bi2O3-ZnO/Bentonite clay composite with enhanced photocatalytic performance
PublicationThe industrial waste water is always a bottleneck problem in the modern civilization of the present era. In a quest to develop effective methods for the elimination of lethal pollutants from the waste water and water remediation, this work is focused on the development of a rapid and proficient approach for preparing supported binary metal oxide catalyst for photocatalytic advance oxidation process used in waste water treatment...
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Systemy hydrofitowe w oczyszczaniu wód opadowych
PublicationStale postępujący rozwój miast oraz stosunkowo niedawna zmiana stanowiska w kwestii konieczności szybkiego odprowadzania wód deszczowych z powierzchni utwardzanych czynią problem oczyszczania ścieków deszczowych ciągle aktualnym. Obecnie celem priorytetowym jest minimalizacja powierzchni utwardzanych oraz stworzenie warunków do infiltracji wód deszczowych do gruntu.
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Krystaliczne struktury supramolekularne z udziałem cyklicznych ditioimidów oraz pirydyn
PublicationInżynieria kryształów z uwagi na możliwość praktycznych zastosowań jest istotną i stale rozwijającą się gałęzią chemii supramolekularnej. Praca dotyczy krystalicznych struktur supramolekularnych powstających z udziałem cyklicznych ditioimidów i pochodnych pirydyny. Wykazuje możliwość występowania w ciele stałym słabych wiązań wodorowych C-H--S