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Search results for: FAST/FLASH GC
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Accelerated solvent extraction-gas chromatographic determination of acidic herbicides in soil
PublicationPrzyspieszona ekstrakcja rozpuszczalnikiem z wykorzystaniem wody jako ekstraktanta okazała się skutecznym sposobem izolacji herbicydów kwasowych (MCPP, MCPA, 2,4-D, 2,4,5-T, PCP, dinoseb, dinoterb) z próbek gleby. Wysoka zawartość substancji iłowych powodowała problemy techniczne, które udało się pokonać poprzez zwiększenie stosunku piasku do gleby w celce ekstrakcyjnej. Anality przenoszono z ekstraktu wodnego do rozpuszczalnika...
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Sample preparation procedure for the determination of polycyclic aromatic hydrocarbons in petroleum vacuum residue and bitumen
PublicationThis paper describes a novel method of samplepreparation for the determination of trace concentrations ofpolycyclic aromatic hydrocarbons (PAHs) in high-boilingpetroleum products. Limits of quantitation of the investigatedPAHs in materials of this type range from tens ofnanograms per kilogram to <20 μg/kg. The studies revealedthat in order to separate most of interferences from theanalytes without a significant loss of PAHs, it...
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Contamination of Runoff Water at Gdańsk Airport (Poland) by Polycyclic Aromatic Hydrocarbons (PAHs) and Polychlorinated Biphenyls (PCBs)
PublicationAirport runoff can contain high concentrations of various pollutants, in particular polycyclic aromatic hydrocarbons (PAHs) and polychlorinated biphenyls (PCBs), the environmental levels of which have to be monitored. Airport runoff water samples, collected at the Gdańsk-Rębiechowo Airport from 2008 to 2009, were analysed for PAHs and PCBs by gas chromatography. The aromatic fractions were separated by liquid-liquid extraction...
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Interaction of human serum albumin with volatiles and polyphenols from some berries
PublicationHeadspace solid-phase microextraction coupled with comprehensive two-dimensional gas chromatography with time-of-flight mass spectrometry (HS-SPME/GC GCeTOFMS) identified 19 and quantified 6 monoterpenes in gooseberries, blueberries and cranberries. As a protein model human serum albumin (HSA) was used in interaction with terpenes. Specific binding of terpenes to HSA under the physiological conditions was a result of the formation...
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The Sonocatalytic Activation of Persulfates on Iron Nanoparticle Decorated Zeolite for the Degradation of 1,4-Dioxane in Aquatic Environments
PublicationIn the chemical industry, 1,4-diethylene dioxide, commonly called dioxane, is widely used as a solvent as well as a stabilizing agent for chlorinated solvents. Due to its high miscibility, dioxane is a ubiquitous water contaminant. This study investigates the effectiveness of catalyst- and ultrasound (US)-assisted persulfate (PS) activation with regard to degrading dioxane. As a first step, a composite catalyst was prepared using...
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Rapid Design Tuning of Miniaturized Rat-Race Couplers Using Regression-Based Equivalent Network Surrogates
PublicationA simple technique for fast design tuning of compact rat-race couplers is presented. Our approach involves equivalent circuit representation, corrected by nonlinear functions of frequency with coefficients extracted through nonlinear regression. At the same time, the tuning process connects two levels of coupler representation: EM simulation of the entire circuit and re-optimization of the coupler building blocks (slow-wave cells...
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Airstrip Ground Improvement Works by Blasting Charge Technique and Dredged-Ash Material Mixture
PublicationSoil improvement by blasting charge technique is known in geotechnics as one of the efficient and inexpensive method. It can be used in preparing of underground to found road construction and buildings as well. The technique proves usefulness especially when dynamic load is applied. It is because of non-stiff or rather resilient type soil after improvement. In noncohesive or organic soil, blasting charge...
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Adaptive Identification of Underwater Acoustic Channel with a Mix of Static and Time-Varying Parameters
PublicationWe consider the problem of identification of communication channels with a mix of static and time-varying parameters. Such scenarios are typical, among others, in underwater acoustics. In this paper, we further develop adaptive algorithms built on the local basis function (LBF) principle resulting in excellent performance when identifying time-varying systems. The main drawback of an LBF algorithm is its high complexity. The subsequently...
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Dynamic Positioning Capability Assessment for Ship Design Purposes
PublicationThe article focuses on solving a problem of optimal thrust distribution over the actuators in a ship Dynamic Positioning, according to DNV-ST-0111 standard, Level 1. The classic Quadratic Programming approach is combined with the numerical solusion used to handle the propeller with the rudder constraints in the optimization task and the influence between thrusters and skeg. It is presented as an efficient method of minimizing the...
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Ordered titania nanotubes layer selectively annealed by laser beam for high contrast electrochromic switching
PublicationThe phase conversion from amorphous into crystalline one in the selected area of as-anodized titania nanotubes was achieved via laser treatment. The optimized processing parameters enable fast, one-minute crystallization of titania within an area limited by a shadow mask and without any morphology damage of ordered TiO2 tubular film. The laser annealed titania nanotubes could be easily overgrown by a conducting polymer without...
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A Time Delay Controller Included Terminal Sliding Mode and Fuzzy Gain Tuning for Underwater Vehicle-Manipulator Systems
PublicationAn improved Time Delay Control (TDC) method for an Underwater Vehicle-Manipulator System (UVMS) is proposed. The proposed controller consists of three terms: a time-delay-estimation term that cancels nonlinearities of the UVMS dynamics, a Terminal Sliding Mode (TSM) term that provides a fast response and a PID term that reduces the tracking error. In addition the proposed controller uses fuzzy rules to adaptively tune the gains...
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Sprzętowa implementacja koprocesora dla zastosowań kryptograficznych
PublicationW pracy przedstawiono procedurę implementacji elektronicznej skrzynki podawczej z wykorzystaniem zasobów sprzętowych na płytce FPGA (Filed Programmable Gate Array) typu Virtex 4. Przedstawiono ogólna zasadę działania skrzynki podawczej oraz opisano parametry i właściwości poszczególnych modułów funkcjonalnych systemu tj.: modułu TFTP Trivia File Transfer Protocol), serwera WWW, funkcji skrótu oraz asymetrycznego algorytm kryptograficznego....
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Automated Reduced Model Order Selection
PublicationThis letter proposes to automate generation of reduced-order models used for accelerated -parameter computation by applying a posteriori model error estimators. So far,a posteriori error estimators were used in Reduced Basis Method (RBM) and Proper Orthogonal Decomposition (POD) to select frequency points at which basis vectors are generated. This letter shows how a posteriori error estimators can be applied to automatically select...
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A nine-input 1.25 mW, 34 ns CMOS analog median filter for image processing in real time
PublicationIn this paper an analog voltage-mode median filter, which operates on a 3 × 3 kernel is presented. The filter is implemented in a 0.35 μm CMOS technology. The proposed solution is based on voltage comparators and a bubble sort configuration. As a result, a fast (34 ns) time response with low power consumption (1.25 mW for 3.3 V) is achieved. The key advantage of the configuration is relatively high accuracy of signal processing,...
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Selection of excitation signals for high-impedance spectroscopy
PublicationA method of fast impedance spectroscopy of technical objects with high impedance (|Zx| > 1 GOhm) is evaluated in this paper. An object is excited with a signal generated by a digital-to-analog converter (DAC) located on the U2531A DAQ module. Response signals proportional to current flowing through and voltage across the measured object are sampled by analog-to-digital converters (ADC) in the DAQ module. The object impedance spectrum...
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Implementation of Contemporary Technologies in Naval Sonars Modernization
PublicationToday’s fast technological advancement in electronics and signal processing methods makes electronic systems, including sonars, obsolete very quickly. The Polish Navy seems to be particularly affected as its ships were built in the 1970s and 1980s. Researchers at the Gdansk University of Technology have developed a methodology for modernising Navy sonars which involves the use of new electronic sub-systems and modern, bespoke methods...
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Low-frequency tripping characteristics of residual current devices
PublicationFast development of various types of converters makes their utilization in industry and in domestic installations very common. Due to converters, an earth fault current waveform in modern circuits can be distorted or its frequency can be different than 50/60 Hz. Frequency of earth fault (residual) current influences tripping of residual current devices which are widely used in low voltage systems. This paper presents the behaviour...
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Smart Innovation Engineering: Toward Intelligent Industries of the Future
PublicationKnowledge-based Engineering Systems are founded upon integration of knowledge into computer systems and are one of the core requirements for the future Industry 4.0. This paper presents a system called Smart Innovation Engineering (SIE) capable of facilitating product innovation process semi-automatically. It enhances decision-making processes by using the explicit knowledge of formal decision events. The SIE system carries the...
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Pareto Ranking Bisection Algorithm for Expedited Multi-Objective Optimization of Antenna Structures
PublicationThe purpose of this letter is introduction of a novel methodology for expedited multi-objective design of antenna structures. The key component of the presented approach is fast identification of the initial representation of the Pareto front (i.e., a set of design representing the best possible trade-offs between conflicting objectives) using a Pareto-ranking bisection algorithm. The algorithm finds a discrete set of Pareto-optimal...
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Cost-efficient simulation-driven design of compact impedance matching transformers
PublicationIn this paper, an algorithmic framework for cost-efficient design optimization of miniaturized impedance matching transformers has been presented. Our approach exploits a bottom-up design that involves translating the overall design specifications for the circuit at hand to its elementary building blocks (here, compact microstrip resonant cells, CMRCs), as well as fast surrogate-assisted optimization of the cells followed by simulation-based...
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Geometry Parametric Model Order Reduction with Randomly Generated Projection Bases
PublicationIn this work, a reduced-order model for geometry parameters and fast frequency sweep is proposed. The Finite Element Method is used to solve time-harmonic Maxwell’s equations. Taking into account the electromagnetic field does not arbitrarily vary as a function of frequency and geometry parameters, a low dimension system manifold is identified. Thus, the original Finite Element problem can be approximated by a model of reduced...
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Rapid surrogate-assisted statistical analysis of compact microstrip couplers
PublicationIn this paper, a technique for low-cost statistical analysis and yield estimation of compact microwave couplers has been presented. The analysis is executed at the level of a fast surrogate model representing selected characteristic points of the coupler response that are critical to determine satisfaction/violation of the prescribed design specifications. Because of less nonlinear dependence of the characteristic points on geometry...
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Magnetoacoustic Heating of Plasma Caused by Periodic MagnetosoundPerturbations with Discontinuities in a Quasi-Isentropic Magnetic Gas
PublicationThe magnetoacoustic heating of plasma by harmonic or periodic saw-tooth perturbations at a trans-ducer is theoretically studied. The planar fast and slow magnetosound waves are considered. The wavevector may form an arbitrary angleθwith the equilibrium straight magnetic field. In view of variableθand plasma-β, the description of magnetosound perturbations and appropriate magnetosound heatingis fairly difficult. The scenario of...
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A Generalized SDP Multi-Objective Optimization Method for EM-Based Microwave Device Design
PublicationIn this article, a generalized sequential domain patching (GSDP) method for efficient multi-objective optimization based on electromagnetics (EM) simulation is proposed. The GSDP method allowing fast searching for Pareto fronts for two and three objectives is elaborated in detail in this paper. The GSDP method is compared with the NSGA-II method using multi-objective problems in the DTLZ series, and the results show the GSDP method...
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Prediction of manoeuvring abilities of 10000 DWT pod-driven coastal tanker
PublicationThis paper aims to present a new approach in the prediction of manoeuvring abilities of pod-driven ships. A new mathematical model of motions based on MMG methodology was developed and a new type of description of forces acting on azimuth drives is presented. Captive model tests of medium-size coastal tanker and pod open water tests were carried out in CTO S.A. (Ship Design and Research Centre S.A.) to obtain hull hydrodynamic derivatives...
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Classification of objects in the LIDAR point clouds using Deep Neural Networks based on the PointNet model
PublicationThis work attempts to meet the challenges associated with the classification of LIDAR point clouds by means of deep learning. In addition to achieving high accuracy, the designed system should allow the classification of point clouds covering an area of several dozen square kilometers within a reasonable time interval. Therefore, it must be characterized by fast processing and efficient use of memory. Thus, the most popular approaches...
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Power efficient thrust allocation algorithms in design of dynamically positioned ships
PublicationAssessment of power consumption on a Dynamically Positioned (DP) ship in the early design stage can assist crucial design choices. The study presents a comparison between two algorithms of optimal thrust allocation in a propulsion system for an over-actuated DP ship. Applied algorithms were Quadratic Programming (QP) and Non- dominated Sorting Genetic Algorithm II (NSGAII). Based on both approaches, tools were developed for ship...
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Application of regularized Savitzky–Golay filters to identification of time-varying systems
PublicationSavitzky–Golay (SG) filtering is a classical signal smoothing technique based on the local least squares approximation of the analyzed signal by a linear combination of known functions of time (originally — powers of time, which corresponds to polynomial approximation). It is shown that the regularized version of the SG algorithm can be successfully applied to identification of time-varying finite impulse response (FIR) systems....
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Very accurate time propagation of coupled Schrödinger equations for femto- and attosecond physics and chemistry, with C++ source code
PublicationIn this article, I present a very fast and high-precision (up to 33 decimal places) C++ implementation of the semi-global time propagation algorithm for a system of coupled Schrödinger equations with a time-dependent Hamiltonian. It can be used to describe time-dependent processes in molecular systems after excitation by femto- and attosecond laser pulses. It also works with an arbitrary user supplied Hamiltonian and can be used...
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Szybkie uziemniki do ograniczania skutków zwarć łukowych w okrętowych rozdzielnicach SN
PublicationW artykule scharakteryzowano moc i napięcie łuku, jak również przedstawiono model termodynamiczny służący do obliczania ciśnienia i temperatury gazów w otoczeniu łuku zwarciowego. Przedstawiono przykładowy układ elektrowni okrętowej i zasilania najważniejszych odbiorników na statku do przewozu gazu ziemnego w stanie ciekłym. Na podstawie parametrów prądnic i silników odbiorników zasilanych z rozdzielnicy głównej obliczono prądy...
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Wizyjny system monitoringu stanu nakładek stykowych odbieraków prądu
PublicationEksploatowane do niedawna w Polsce nakładki pantografów kolejowych były wykonywane w postaci styków miedzianych. Na początku 2011 r. przeprowadzono kompleksową zmianę typu nakładek stykowych, stosowanych przez operatorów korzystających z infrastruktury PKP PLK S.A., z miedzianych na metalizowane węglowe. Wraz z wprowadzeniem nakładek węglowych istnieje potrzeba opracowania nowych metod diagnostyki tego istotnego elementu toru zasilania...
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System do prototypowania bezprzewodowych inteligentnych urządzeń monitoringu audio-video
PublicationW komunikacie przedstawiono system prototypowania bezprzewodowych urządzeń do monitoringu audio-video. System bazuje na układach FPGA Virtex6 i wielu dodatkowych wspierających urządzeniach jak: szybka pamięć DDR3, mała kamera HD, mikrofon z konwerterem A/C, moduł radiowy WiFi, itp. Funkcjonalność systemu została szczegółowo opisana w komunikacie. System został zoptymalizowany do pracy pod kontrolą systemu operacyjnego Linux, zostały...
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Kontrola jakości i analityka techniczna [Moduł dyscyplinarny, grupa B]
e-Learning CoursesProwadzący: Dr hab. inż. Grzegorz Boczkaj prof. PG Terminy realizacji: 25 marca, 1 kwietnia, 15 kwietnia, 22 kwietnia, 13 maja w godz. od 09:15 do 12-tej /zajęcia online Tematyka realizowanego przedmiotu obejmuje: Pobieranie próbek do badań (on-line, off-line, at-line, in-line) Przygotowanie próbek do badań (techniki i przykłady metodyk dla próbek stałych, ciekłych i gazowych) Techniki i wybrane metodyki klasyczne (miareczkowanie,...
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Evaluation of Terpene Decomposition in Kaffir Lime Juice during Storage Using Gas Chromatography–Mass Spectrometry and Proton Transfer Reaction–Mass Spectrometry
PublicationKaffir lime juice, often treated as production waste, can be a good source of terpenes. These compounds undergo various decomposition processes under the influence of external factors, especially during transportation and storage. In this paper, it was possible to monitor changes in the terpene profile of kaffir lime juice under different storage conditions, namely, 4 ◦C, 20 ◦C, and 35 ◦C. The identification of key decomposition...
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Evaluation of the Impact of Storage Conditions on the Biogenic Amines Profile in Opened Wine Bottles
PublicationA survey of biogenic amine (BA) profiles in opened wine bottles has been established to monitor the level of biogenic amines (BAs) in opened bottles against time and other conditions. Bottles of red and white wine were submitted to different temperatures, stopper type (screw cap, cork), and use of vacuum devices. A total of six wines made from a variety of grapes were obtained from vineyards from regions across Poland. Dispersive...
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The extended version of restriction analysis approach for the examination of the ability of low-molecular-weight compounds to modify DNA in a cell-free system
PublicationOne of the primary requirements in toxicology is the assessment of ability of chemicals to induce DNA covalent modification. There are several well-established methods used for this purpose such as 32P-Postlabeling or HPLC-MS. However, all of these approaches have difficult to overcome limitations, which prevents their use in genotoxin screening. Here, we describe the simple protocol exploiting specificity of restriction enzymes...
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Determination of volatile organic compounds in water samples using membrane-solid phase microextraction (M-SPME) (headspace version)
PublicationThe results of a study on the use of membrane-solid phase microextraction (M-SPME) for sampling volatile organic compounds (VOCs) from the headspace above the liquid medium are presented. The sampled VOCs were subsequently quantified by gas chromatography (GC). Two systems were compared in this study, i.e. a novel two-phase sorption system (M-SPME), and a commercial fibre. Headspace sampling using SPME was optimized with respect...
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Comprehensive determination of flavouring additives and nicotine in e-cigarette refill solutions. Part II: Gas-chromatography–mass spectrometry analysis
PublicationFlavouring compounds are an essential part of e-liquid products for cigarettes. In general, they are regarded as safe for ingestion, but they may have unrecognized risks when they are inhaled. In some cases, manufactures do not currently abide by the Tobacco Products Directive (2014/40/EU) and do not declare the detailed contents of e-liquids on their labels. To help evaluate the health impact of flavouring substances, there is...
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Determination of phenol biodegradation pathways in three psychrotolerant yeasts, Candida subhashii A011, Candida oregonensis B021 and Schizoblastosporion starkeyi-henricii L012, isolated from Rucianka peatland
PublicationIn this study, three psychrotolerant phenol-degrading yeast strains Candida subhashii (strain A011), Candida oregonenis (strain B021) and Schizoblastosporion starkeyi-henricii (strain L012) isolated from Rucianka peatland were examined to determine which alternative metabolic pathway for phenol biodegradation is used by these microorganisms. All yeast strains were cultivated in minimal salt medium supplemented with phenol at 500,...
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Theory and application of Near-infrared spectroscopy
PublicationIn recent years one can observe a significant increase in the requirements on quality control in all industrial sectors. The growing number of involved analyses makes the traditional, time consuming, requiring use of large quantities of reagents, thus expansive methods inconvenient especially for industrial applications. Fortunately, there is a very fast, cheap and not invasive analytical method that is increasingly used in qualitative...
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SiC-based T-type modules for multi-pulse inverter with coupled inductors
PublicationThe paper presents SiC-based three-level T-type modules designed for a high-performance 30kVA DC/AC inverter operating at high frequency 85 kHz with low THD of the output voltage. This inverter system consists of two integrated parts. The first part is active and contains three parallelconnected three-phase T-type modules built with fast-switching SiC power transistors. The second, passive part of the system is a set of inductors...
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Magnetoacoustic Heating in Nonisentropic Plasma Caused by Different Kinds of Heating-Cooling Function
PublicationThe nonlinear phenomena which associate with magnetoacoustic waves in a plasma are analytically studied. A plasma is an open system with external inflow of energy and radiation losses. A plasma’s flow may be isentropically stable or unstable. The nonlinear phenomena occur differently in dependence on stability or instability of a plasma’s flow. The nonlinear instantaneous equation which describes dynamics of nonwave entropy mode...
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Rapid design closure of microwave components by means of feature-based optimization and adjoint sensitivities
PublicationIn this article, fast design closure of microwave components using feature-based optimization (FBO) and adjoint sensitivities is discussed. FBO is one of the most recent optimization techniques that exploits a particular structure of the system response to “flatten” the functional landscape handled during the optimization process, which leads to reducing its computational complexity. When combined with gradient-based search involving...
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Airfoil Design Under Uncertainty Using Non-Intrusive Polynomial Chaos Theory and Utility Functions
PublicationFast and accurate airfoil design under uncertainty using non-intrusive polynomial chaos (NIPC) expansions and utility functions is proposed. The NIPC expansions provide a means to efficiently and accurately compute statistical information for a given set of input variables with associated probability distribution. Utility functions provide a way to rigorously formulate the design problem. In this work, these two methods are integrated...
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On-line Search in Two-Dimensional Environment
PublicationWe consider the following on-line pursuit-evasion problem. A team of mobile agents called searchers starts at an arbitrary node of an unknown network. Their goal is to execute a search strategy that guarantees capturing a fast and invisible intruder regardless of its movements using as few searchers as possible. As a way of modeling two-dimensional shapes, we restrict our attention to networks that are embedded into partial grids:...
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Numerical assessment of ultimate strength of severe corroded stiffened plates
PublicationThe objective of this work is to investigate numerically (using the non-linear FEM and the approach stipulated by the Common Structural Rules) the severe nonuniform corrosion degradation effect on the ultimate strength of stiffened plates and compare the results to the already published experimental works. Different factors governing structural behavior of corroded stiffened plates are investigated, such as corrosion degradation level,...
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Neural modelling of dynamic systems with time delays based on an adjusted NEAT algorithm
PublicationA problem related to the development of an algorithm designed to find an architecture of artificial neural network used for black-box modelling of dynamic systems with time delays has been addressed in this paper. The proposed algorithm is based on a well-known NeuroEvolution of Augmenting Topologies (NEAT) algorithm. The NEAT algorithm has been adjusted by allowing additional connections within an artificial neural network and...
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Discovering interactions between applications with log analysis
PublicationApplication logs record the behavior of a system during its runtime and their analysis can provide useful information. In this article, we propose a method of automated log analysis to discover interactions taking place between applications in an enterprise. We believe that such an automated approach can greatly support enterprise architects in building an up-to-date view of a governed system in a modern, fast-paced development...
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Microextraction by packed sorbent: Uncommon detection techniques, sorbents, samples and analytes
PublicationAmong sample preparation approaches, the most desirable are procedures that ensure high efficiency and reproducibility, that are cheap, fast and simple, that minimize the number of operational steps and that require a small amount of sample and solvent and are thus environmentally friendly. Microextraction by packed sorbent (MEPS) is a miniaturized form of solid-phase extraction, the use of which has been continuously expanding...
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CNN Architectures for Human Pose Estimation from a Very Low Resolution Depth Image
PublicationThe paper is dedicated to proposing and evaluating a number of convolutional neural network architectures for calculating a multiple regression on 3D coordinates of human body joints tracked in a single low resolution depth image. The main challenge was to obtain a high precision in case of a noisy and coarse scan of the body, as observed by a depth sensor from a large distance. The regression network was expected to reason about...