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Search results for: TITANIUM ALLOY TI13NB13ZR, ELECTROCHEMICAL OXIDATION, NANOTUBULAR TITANIUM OXIDES, HYDROXYAPATITE COATINGS, SEM
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The Influence of Tool Shape and Process Parameters on the Mechanical Properties of AW-3004 Aluminium Alloy Friction Stir Welded Joints
PublicationThe purpose of the following study was to compare the effect of the shape of a tool onthe joint and to obtain the values of Friction Stir Welding (FSW) parameters that provide the bestpossible joint quality. The material used was an aluminium alloy, EN AW-3004 (AlMn1Mg1). To theauthors’ best knowledge, no investigations of this alloy during FSW have been presented earlier. Fivebutt joints were made with a self-developed, cylindrical,...
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Pressure effects on the electronic structure and superconductivity of (TaNb)0.67(HfZrTi)0.33 high entropy alloy
PublicationEffects of pressure on the electronic structure, electron-phonon interaction, and superconductivity of the high entropy alloy ( TaNb ) 0.67 ( HfZrTi ) 0.33 are studied in the pressure range 0–100 GPa. The electronic structure is calculated using the Korringa-Kohn-Rostoker method with the coherent potential approximation. Effects of pressure on the lattice dynamics are simulated using the Debye-Grüneisen model and the Grüneisen...
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The scanning spreading resistance microscopy (SSRM) studies of heavy boron-doped diamond oxidation under high-temperature
Open Research DataThe dataset contains the results of scanning spreading resistance microscopy (SSRM) of heavy boron-doped diamond (BDD) electrodes subjected to high-temperature oxidation in a furnace at 600 Celsius. The micrographs reveal the local change of electric properties at certainly crystallographic orientations of BDD grains and at the grain boundaries due...
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Integrated Photocatalytic Advanced Oxidation System (TiO2/UV/O3/H2O2) for Degradation of Volatile Organic Compounds
PublicationSeveral advanced oxidation processes (AOPs) including photocatalytic processes were studied for effective treatment of complex model wastewater containing a wide variety of VOCs. The studies revealed synergistic effects of TiO2 based processes for improved degradation of the VOCs. A peroxone combined with TiO2/UV system (TiO2/UV/O3/H2O2) with a ratio between the oxygen source from the oxidant to chemical oxygen demand (COD) of...
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Photodegradation and advanced oxidation of endocrine disruptors in aqueous solutions
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Photosensitised oxidation of a water pollutant using sulphonated porphyrin
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Application of Fenton oxidation to reduce the toxicity of mixed parabens
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Post-plasma oxidation in water of graphene paper surface
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Carbonaceous catalysts from orange pulp for limonene oxidation
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Selective oxidation of metallic single-walled carbon nanotubes
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Oxidation and reduction of multiwalled carbon nanotubes — preparation and characterization
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Photo-oxidation of dissolved cyanide using TiO2 catalyst
PublicationZbadano utlenianie katalityczne jonów cyjankowych w układzie UV/TiO2. Szybkość utleniania zbadano dla różnego stężenia początkowego CN-, wartość pH, formy katalizatora, temperatury oraz wprowadzanej formy gazowej. Stwierdzono że szybkość degradacji cyjanków w układzie UV/TiO2/O2 wzrasta dwukrotnie, jakkolwiek jest niezależna od ciśnienia cząstkowego tlenu (0,2-1,0 atm.). Wzrost temperatury środowiska reakcji w zakresie od 20 do...
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Thermally activated persulfate-based Advanced Oxidation Processes — recent progress and challenges in mineralization of persistent organic chemicals: a review
PublicationThermally activated persulfate (TAP) finds application in Advanced Oxidation Processes for the removal of pollutants from contaminated water and soil. This paper reviewed the various cases of TAP in the environmental remediation. The pollutants such as individual pharmaceuticals, biocides, cyclic organic compounds, and dyes are considered in this review. It is interesting to note that most of the organic compounds undergo complete...
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Journal of Coatings Technology and Research
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SEM micrographs of morphology evolution of VO2 and V2O3 nanostructures
Open Research DataThe DataSet contains the scanning electron microscopy (SEM) micrographs of VO2 and V2O3 nanostructures obtained by the sol-gel with different reaction conditions. The information about xerogel powder synthesis is described in the Journal of Nanomaterials. The xerogel powder was annealing under argon atmosphere in the temperature range 400-800C. The...
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Wojciech Chrzanowski dr hab. inż.
PeopleWojciech Chrzanowski was born in 1952 in Toruń. He completed his studies in Chemical Technology in 1975, getting his MSc in Inorganic Technology (specialty: Anti-Corrosion Protection) At the Faculty of Chemistry, Gdańsk University of Technology (with distinction). Later this year he was employed in the Department of Analytical Chemistry of then Institute of Chemical Engineering and Measuring Techniques, initially as a technical...
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Detection of the Plant Pathogen Pseudomonas Syringae pv. Lachrymans on Antibody-Modified Gold Electrodes by Electrochemical Impedance Spectroscopy
PublicationThe present work describes an impedimetric immunosensor for Pseudomonas syringae pv. lachrymans (Psl) detection. This pathogen infects many crop species causing considerable yield losses, thus fast and cheap detection method is in high demand. In the assay, the gold disc electrode was modified with 4-aminothiophenol (4-ATP), glutaraldehyde (GA), and anti-Psl antibodies, and free-sites were blocked with bovine serum albumin (BSA)....
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Tuning Electrochemical Performance by Microstructural Optimization of the Nanocrystalline Functional Oxygen Electrode Layer for Solid Oxide Cells
PublicationFurther development of solid oxide fuel cell (SOFC) oxygen electrodes can be achieved through improvements in oxygen electrode design by microstructure miniaturisation alongside nanomaterials implementation. In this work, improved electrochemical performance of an La0.6Sr0.4Co0.2Fe0.8O3-d (LSCF) cathode was achieved by the controlled modification of the La0.6Sr0.4CoO3-d (LSC) nanocrystalline interlayer introduced between a porous...
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The influence of welding heat input on the quality and properties of high strength low-alloy dissimilar steel butt joints
PublicationThe paper presents the results of non-destructive and destructive tests of dissimilar highstrength low-alloy S460ML and S460N steel butt joints. These steels are characterized by similar mechanical properties, but their carbon equivalent CeIIW values are much different. The joints were made using different values of heat input for each welding bead. They were tested by non-destructive methods: visual, penetrant, radiographic and...
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OPTIMAL WAVELET CHOICE IN ELECTROCHEMICAL EXPERIMENTS
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Materials for potentiometric electrochemical gas sensors
PublicationPublikacja przeglądowa na temat zasady działania oraz rodzajów czujników elektrochemicznych gazów.
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Accuracy Analysis of Measurements in Electrochemical Biosensing
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Molecular structure and electrochemical properties of alkyldithiocarbamates.
PublicationZastosowano klasyczne metody elektroanalityczne do badania właściwości redoks ditiokarbaminianów litu w środowisku dimetylosulfotlenku. Użyto elektrody z platyny i węgla szklistego. Badane związki zsyntezowano z N,N'-dimetyloetylenodiaminy, do której podstawiono jedną lub dwie grupy ditiokarbonylowe na drodze reakcji z CS2 w środowisku alkalicznym. Stwierdzono, że elektrochemiczne utlenianie ditiokarbaminianów przebiega z udziałem...
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Electrochemical analysis of aluminium passive layer
PublicationZbadano proces pękania warstwy pasywnej na aluminium dla liniowo narastających naprężeń rozciągających oraz różnych warunków elektrochemicznych. Badania prowadzono w 0.1M NaCl metodą dynamicznej elektrochemicznej spektroskopii impedancyjnej przy różnych poziomach polaryzacji anodowej. Określono progową wartość naprężeń, przy której następowało zniszczenie warstwy pasywnej wskutek działania sił rozciągających.
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The stationarity characteristics of electrochemical current noise
PublicationPrzedstawiono rezultaty analizy szumu elektrochemicznego generowanego podczas korozji stali 0H18N9 w roztworze 0.1 M H2SO4+0,006 M Cl-. Rejestry uzyskano w warunkach potencjostatycznych. W szumie zaobserwowano trendy i sygnały przejściowe, charakterystyczne dla korozji wżerowej. Trend został usunięty za pomocą aproksymacji wielomianem trzeciego stopnia. Analiza statystyczna wykazała niestacjonarny bądź słabo stacjonarny charakter...
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Optimal wavelet choice in electrochemical experiments
PublicationW ostatnich latach obserwuje się wzrost zainteresowania łączeniem eksperymentów elektrochemicznych z nowoczesnymi technikami analizy sygnałów. Jednym z najbardziej obiecujących kierunków jest analiza falkowa. W omawianym przypadku istnieje wybór pomiędzy różnymi rodzinami falek w zależności od wymogów danego eksperymentu. W pracy omówione zostały wyniki zastosowania różnych typów falek do analizy szumów elektrochemicznych o różnym...
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Solid-state electrochemical gas sensors
PublicationW pracy przedstawiono budowę i zasadę działania wybranych typów elektrochemicznych czujników gazów zbudowanych na bazie elektrolitów stałych.
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The Impact of Ground Tire Rubber Oxidation with H2O2 and KMnO4 on the Structure and Performance of Flexible Polyurethane/Ground Tire Rubber Composite Foams
PublicationThe use of waste tires is a very critical issue, considering their environmental and economic implications. One of the simplest and the least harmful methods is conversion of tires into ground tire rubber (GTR), which can be introduced into different polymer matrices as a filler. However, these applications often require proper modifications to provide compatibility with the polymer matrix. In this study, we examined the impact...
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Graphene nanoflakes functionalized with cobalt/cobalt oxides formation during cobalt organic framework carbonization
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Structural phase transitions in multicomponent La0.2Nd0.2Sm0.2Gd0.2RE50.2NbO4 (RE5 = Ho, Y, Tb, Eu, Pr) oxides
PublicationIn this work, the influence of compositional complexity on the structural and thermal properties of multicomponent rare-earth ortho-niobates from the La0.2Nd0.2Sm0.2Gd0.2RE50.2NbO4 (RE5 = Ho, Y, Tb, Eu, Pr) series have been investigated. Based on X-ray powder diffraction studies using synchrotron radiation, it was found that all tested materials were pure single-phase compositions and showed stability in the monoclinic I2/c crystal...
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Electrochemical activity and characterization of hybrid material consisted of poly(3,4- ethylenedioxythiophene) and silver hexacyanocobaltate
PublicationPrac przedstawiono charakterystykę elektrochemiczną oraz powierzchniową materiału hybrydowego składającego się z polimeru przewodzącego, poli(3,4-etylenodioksytiofenu) oraz nieorganicznej sieci typu redoks, heksacyjanokobaltanu srebra. Materiał scharakteryzowano technikami jak AFM, SEM. Skład materiału oznaczono za pomocą mikroanalizy rentgenowskiej EDX. Analiza potwierdziła obecność sieci nieorganicznej w materiale. Proporcja...
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Electrochemical performance of thin free-standing boron-doped diamond nanosheet electrodes
PublicationIn the following work we describe preparation and the electrochemical performance of thin and free-standing heavy boron-doped diamond (BDD) nanosheets. The investigated foils were deposited on Ta substrate using microwave plasma-enhanced chemical vapor deposition technique (MPECVD). Foils of two B-dopant densities were investigated, obtained on the base of 10 k and 20 k ppm [B]/[C] ratio in the gas admixture. The obtained foils...
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Bartosz Woliński dr inż.
PeopleCourses Informatization strategies (winter sem. 20/21, winter sem. 22/23) IT teams technologies (winter sem. 20/21) Decision analysis (winter sem. 20/21, winter sem. 21/22, summer sem. 22/23) Controlling in IT (summer sem. 20/21, 21/22, 22/23) Projects in enterprises (summer sem. 20/21, 22/23) Integrated enterprise information systems (winter sem. 20/21) Managing enterprise IT infrastructure and security (summer sem. 2021/22) Decision...
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Pilot scale degradation study of 16 selected volatile organic compounds by hydroxyl and sulfate radical based advanced oxidation processes
PublicationThe studies of effective technologies for complete degradation of the volatile organic compounds (VOCs), are very important due to the high biotoxicity of the VOCs which makes the biological technologies ineffective. It also increases the risk of VOCs emission instead of their treatment when using open air biological technologies. In the present study, different types of Advanced Oxidation Processes (AOPs) were investigated for...
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SEM images of MXene catalysts
Open Research DataData contain results SEM measurements of the Ti3C2Tx MXenes produced via acidic etching aluminum from MAX Phase (Ti3C2-Al-Ti3C2-Al-Ti3C2) using different etching agents, HF/HCl and HF/H2SO4 with different weight ratios (1:3, 1:4, and 1:5). The samples were labeled as MXene HF/HCl X:Y and MXene HF/H2SO4 X:Y, where X:Y means the acids weight ratios. MAX...
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Analysis of the properties of the YSTF ceramics materials before and after reduction
Open Research DataThe valence of titanium in reduced YSTF ceramics materials was investigated. Ceramics were reduced by annealing in a hydrogen atmosphere. For comparison unreduced sample was also measured. Valance state was measured by XPS method.
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Electrochemical determination of neurotransmitter serotonin using boron/nitrogen co-doped diamond-graphene nanowall-structured particles
PublicationElectrode fouling is a major issue in biological detection due to the adhesion of the protein itself and polymerization of biomolecules on the electrode surface, impeding the electron transfer ability and decreasing the current response. To overcome this issue, the use of anti-fouling material, especially boron-doped diamond (BDD) electrode, is an alternative way. However, the electrocatalytic activity of BDD is inadequate compared...
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Ni/cerium Molybdenum Oxide Hydrate Microflakes Composite Coatings Electrodeposited from Choline Chloride: Ethylene Glycol Deep Eutectic Solvent
PublicationCerium molybdenum oxide hydrate microflakes are codeposited with nickel from a deep eutectic solvent-based bath. During seven days of exposure in 0.05 M NaCl solution, the corrosion resistance of composite coating (Ni/CeMoOxide) is slightly reduced, due to the existence of some microcracks caused by large microflakes. Multielemental analysis of the solution, in which coatings are exposed and the qualitative changes in the surface...
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Cyclic Behavior of Masonry Shear Walls Retrofitted with Engineered Cementitious Composite and Pseudoelastic Shape Memory Alloy
PublicationThe behavior of masonry shear walls reinforced with pseudoelastic Ni–Ti shape memory alloy (SMA) strips and engineered cementitious composite (ECC) sheets is the main focus of this paper. The walls were subjected to quasi-static cyclic in-plane loads and evaluated by using Abaqus. Eight cases of strengthening of masonry walls were investigated. Three masonry walls were strengthened with different thicknesses of ECC sheets using...
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Validity of impedance spectra obtained by dynamic electrochemical impedance spectroscopy verified by Kramers-Kronig transformation.
PublicationArtykuł przedstawia weryfikację wiarygodności widm impedancyjnych otrzymanych za pomocą niedawno wprowadzonej techniki eksperymentalnej - Dynamicznej Elektrochemicznej Spektroskopii Impedancyjnej (Dynamic Electrochemical Impedance Spectroscopy, DEIS). Technika ta zakłada, że badany system jest pseudostacjonarny jeśli czas pomiaru jest odpowiednio krótki. Czas potrzebny na otrzymanie pojedynczego spektrum zależy od długości okna...
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Physicochemical properties of Mn1.45Co1.45Cu0.1O4 spinel coating deposited on the Crofer 22 H ferritic steel and exposed to high-temperature oxidation under thermal cycling conditions
PublicationThe Crofer 22 H ferritic steel substrate was coated with an Mn1.45Co1.45Cu0.1O4 spinel by means of electrophoresis. After high-temperature oxidation under thermal cycling conditions, the physicochemical properties of the obtained system were evaluated. During 48-h cycles that involved heating the samples up to temperatures of either 750 or 800 °C, the oxidation kinetics of both coated and unmodified steel approximately obeyed...
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SEM of TiO2 heated at 400-600oC in Ar or H2
Open Research DataData contain some SEM images of TiO2 taken after its heat treatment in Ar or H2 at 400-600oC. Treated TiO2 was crystalline anatase phase with 3-4 % of rutile nclei.
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UV-Vis measurements and SEM images of Ag nanostructures
Open Research DataUv-vis and SEM of Ag nanostructures. Structures were obtained by dewetting thin films. Various fabrication conditions i.e. temperature, time of the annealing and thickness of the initial layer were subsequently changed.
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The electrochemical determination of isatin at nanocrystalline boron-doped diamond electrodes: stress monitoring of animals
PublicationUltra-thin nanocrystalline boron-doped diamond electrodes (B:NCD) were used for the electrochemical determination of isatin in dog urine samples using cyclic voltammetry and square wave voltammetry in a phosphate buffer saline, pH = 7.2. No additional modification or pretreatment of the electrode surface was required in this approach, being of high importance for the facile detection procedure. The increase of the peak current...
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Structural, optical and electrochemical performance of black phosphorus and black arsenic-phosphorus nanostructures
PublicationBlack phosphorus (BP)-based nanostructures have drawn a lot of attention due to their tunable bandgap and extraordinary properties such as: high surface-to-volume ratio, large number of active sites, and prominent edges. However, low dimensional structures of black phosphorus oxidize easily, which hamper their application on a broader scale. One way to overcome these difficulties is to modify the black phosphorus structure by substituting...
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Modified Manganese Phosphate Conversion Coating on Low-Carbon Steel
PublicationConversion coatings are one of the primary types of galvanic coatings used to protect steel structures against corrosion. They are created through chemical reactions between the metal surface and the environment of the phosphating. This paper investigates the impact that the addition of new metal cations to the phosphating reaction environment has on the quality of the final coating. So far, standard phosphate coatings have contained...
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The bismuth vanadate thin layers modified by cobalt hexacyanocobaltate as visible-light active photoanodes for photoelectrochemical water oxidation
PublicationBismuth vanadate thin films deposited using the pulsed laser deposition technique were modified using cobalt hexacyanocobaltate (Cohcc). The 2-step method of Cohcc nanocubes preparation was applied: i) metallic cobalt deposition and ii) cobalt electrooxidation in Co(CN)63− containing electrolyte. The presence of CN stretching vibrations was confirmed by Raman spectroscopy. The energy band gap was equal to 2.5 eV and was estimated...
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The effect of lyophilization on selected biologically active components (vitamin c, catalase, lysozyme), total antioxidant capacity and lipid oxidation in human milk
PublicationHuman milk is rich in polyunsaturated fatty acids, as well as lysozyme, vitamin C and other bioactive compounds. The effect of lyophilization on the content of antioxidants (vitamin C and catalase CAT), bactericidal compounds (lysozyme), total antioxidant capacity (TAC) and lipid peroxidation in human milk was investigated in this study. Samples of mature human milk were collected from five healthy women who gave birth on the scheduled...
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Defining efficient modes range for plasma spraying coatings
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On the use of bilinear transformation for parameter identification of anticorrosion coatings
PublicationW artykule przedstawiono metodę identyfikacji parametrów powłok antykorozyjnych modelowanych wieloelementowymi układami zastępczymi. Metoda wykorzystuje właściwości przekształcenia biliniowego, które umożliwia przedstawienie funkcji układowej wieloparametrowego modelu jako funkcji każdego indywidualnego parametru. Odwrotne przekształcenie biliniowe pozwala na wyznaczenie wartości każdego z parametrów modelu z osobna na podstawie...