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Search results for: FINGERPRINTING CHARACTERIZATION
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Partial characterization of white cabbages (Brassica oleracea var. capitata f. alba) from different regions by glucosinolates, bioactive compounds, total antioxidant activities and proteins
PublicationW pracy przedstawiono wyniki oznaczeń glukozynolanów (GLS), aktywności przeciwutleniającej (TRSA) oraz białek w próbkach białej kapusty pochodzącej z różnych rejonów geograficznych Europy. Glukobrassycyna i sinigryna były dominującymi GLS we wszystkich próbkach kapusty. Całkowita zawartość GLS mieściła się w zakresie od 3,3-7,7 µmol/g sm. Aktywność przeciwulteniająca próbek kapusty została oszacowana za pomocą testów ABTS,...
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Effect of alumina oxide nano-powder on the wear behaviour of CrN coating against cylinder liner using response surface methodology: processing and characterizations
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Can cornelian cherry mask bitter taste of probiotic chocolate? Human TAS2R receptors and a sensory study with comprehensive characterisation of new functional product
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Tailoring diamondised nanocarbon-loaded poly(lactic acid) composites for highly electroactive surfaces: extrusion and characterisation of filaments for improved 3D-printed surfaces
PublicationA new 3D-printable composite has been developed dedicated to electroanalytical applications. Two types of diamondised nanocarbons - detonation nanodiamonds (DNDs) and boron-doped carbon nanowalls (BCNWs) - were added as fillers in poly(lactic acid) (PLA)-based composites to extrude 3D filaments. Carbon black served as a primary filler to reach high composite conductivity at low diamondised nanocarbon concentrations (0.01 to 0.2...
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RF Indoor Positioning System Supported by Wireless Computer Vision Sensors
PublicationIn this paper the possibility of increase the accuracy of RF fingerprinting indoor tracking system by the use of additional information from simple vision system is examined. As the distances in signal space differs from ones in real environment the ambiguity in decision process of fingerprinting algorithm can occur when set of closest distances between tag and map points in signal space corresponds to big distances differences...
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Induction Assisted Hybrid Friction Stir Welding of Dissimilar Materials AA5052 Aluminium Alloy and X12Cr13 Stainless Steel
PublicationThis research aimed to study the induction in-situ heated hybrid friction stir welding (IAFSW) method to join AA5052 aluminium alloy with X12Cr13 stainless steel (SS) to enhance joint strength. The potency of this method on the mechanical properties and microstructural characterizations were also investigated. The results show that the transverse tensile strength gained was 94% of the AA5052 base metal that is 229.5 MPa. This superior...
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Effect of particle size and weight fraction of SiC on the mechanical, tribological, morphological, and structural properties of Al-5.6Zn-2.2Mg-1.3Cu composites using RSM: fabrication, characterization, and modelling
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Surface-enhanced Raman scattering (SERS) and tip-enhanced Raman scattering (TERS) in label-free characterization of erythrocyte membranes and extracellular vesicles at the nano-scale and molecular level
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Characterization of GM3 Gangliosides in Human Milk throughout Lactation: Insights from the Analysis with the Use of Reversed-Phase Liquid Chromatography Coupled to Quadrupole Time-Of-Flight Mass Spectrometry
PublicationGangliosides are complex lipids found in human milk that play important structural and biological functions. In this study, we utilized reversed-phase liquid chromatography coupled to quadrupole time-of-flight mass spectrometry to evaluate the molecular distribution of GM3 in human milk samples collected at distinct lactation stages, ranging from colostrum to advanced lactation samples. Throughout lactation, GM3 d40:1 emerged as...
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Electrophoretic deposition and characterization of composite chitosan/Eudragit E 100 or poly(4-vinylpyridine)/mesoporous bioactive glass nanoparticles coatings on pre-treated titanium for implant applications
PublicationTitanium implants are surface-modified to achieve bioactivity and often antibacterial properties. Such surface coatings may increase corrosion degradation and be weakly attached to the substrate. In the present research, biodegradable composite coatings, investigated so far as smart environment-sensitive, slowly releasing silver to the implant neighborhood, were produced as a combination of chitosan (CS) with Eudragit E 100 (EE100)...
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Synthesis and characterization of mononuclear Zn(II), Co(II) and Ni(II) complexes containing a sterically demanding silanethiolate ligand derived from tris(2,6-diisopropylphenoxy)silanethiol
PublicationFour heteroleptic complexes of zinc(II), cobalt(II) and nickel(II) containing a monodentate silanethiolate ligand derived from tris(2,6-diisopropylphenoxy)silanethiol (TDST), were prepared and characterized. The geometries of ligands in the complexes are typical: distorted tetrahedral in zinc and cobalt(II) complexes and square planar in nickel(II) compound. Magnetic studies performed for Ni(II) and Co(II) compounds confirm the...
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Characterisation of Escherichia coli isolates from the blood of haematological adult patients with bacteraemia: translocation from gut to blood requires the cooperation of multiple virulence factors
PublicationThe aim of the study was to investigate whether there are unique pathotypes of Escherichia coli capable of transmission from the gastrointestinal tract to the vascular bed. The study included E. coli strains isolated from clinical materials collected from 115 patients suffering from haematologic malignancies diagnosed with bacteraemia. The genotyping techniques established that 89 E. coli isolates from the blood had the same genotype...
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A multi-analytical approach to the characterization of natural organic dyestuffs and inorganic substrates present in the 19th-century artistic oil paints manufactured by a French art materials supplier Richard Aines
PublicationThis paper presents a comprehensive analysis of artistic paints produced in the 19th century by a French art materials supplier Richard Ain`es. Improved mild extraction with hydrofluoric acid enabled the observation of intact organic dyes. Reversed-phase liquid chromatography with diode-array and mass spectrometry detection was utilised for the identification of 35 dyes present in yellow and red paint samples, and in selected plant...
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Single-Anchor Indoor Localization Using ESPAR Antenna
PublicationIn this paper a new single-anchor indoor localization concept employing Electronically Steerable Parasitic Array Radiator (ESPAR) antenna has been proposed. The new concept uses a simple fingerprinting algorithm adopted to work with directional main beam and narrow minimum radiation patterns of ESPAR antenna that scans 360° area around the base station, while the signal strength received from a mobile terminal is being recorded...
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Synthesis, characterization and application of a zirconium-based MOF-808 functionalized with isonicotinic acid for fast and efficient solid phase extraction of uranium(VI) from wastewater prior to its spectrophotometric determination
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Characterization of single-stranded DNA-binding proteins from the psychrophilic bacteria Desulfotalea psychrophila, Flavobacterium psychrophilum, Psychrobacter arcticus, Psychrobacter cryohalolentis, Psychromonas ingrahamii, Psychroflexus torquis, and Photobacterium profundum
PublicationBackground: Single-stranded DNA-binding proteins (SSBs) play essential roles in DNA replication, recombination and repair in Bacteria, Archaea and Eukarya. In recent years, there has been an increasing interest in SSBs, since they find numerous applications in diverse molecular biology and analytical methods. Results: We report the characterization of single-stranded DNA-binding proteins from the psychrophilic bacteria Desulfotalea...
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Principles and applications of Ligation Mediated PCR methods for DNA-based typing of microbial organisms
PublicationA significant number of DNA-based techniques has been introduced into the field of microorganisms’ characterization and taxonomy. These genomic fingerprinting methods were developed to detect DNA sequence polymorphisms by using general principles, such as restriction endonuclease analysis, molecular hybridization, and PCR amplification. In recent years, some alternative techniques based on ligation of oligonucleotide adapters before...
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Evaluation of structural and electrical properties of multicomponent spinel oxide thin films deposited via spray pyrolysis technique
PublicationThis work reports the preparation of (Mn,Co,Fe,Ni,Cr)3O4 high-entropy spinel oxide in the form of a ~ 500 nm thin film utilising a facile spray pyrolysis technique. The structural and electrical properties of the layers were characterised after exposure to temperatures in the range of 400–900 ◦C. The as-deposited layers were amorphous, and crystallised upon heat treatment at 500 ◦C. Microstructural analyses proved a homogeneous...
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Effect of processing parameters on the cyclic behaviour of aluminium friction stir welded to spark plasma sintered aluminium matrix composites with bimodal micro-and nano-sized reinforcing alumina particles
PublicationUnderstanding the cyclic behaviour of Alumina reinforced Aluminium composites (Al-A2O3) was of critical importance, for their further application in the different industrial sectors. The present study is focussing on the cyclic behaviour of the Al-Alumina nanocomposite produced through the combination of spark plasma sintering (SPS) method and friction stir welding (FSW). The added Alumina with total content of 10% is the combination...
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Experimental investigations of damage evolution in concrete during bending by continuous micro-CT scanning
PublicationThe paper describes experimental investigation results of fracture in notched concrete beams under quasi-static three-point bending. To visualize 3D fracture in concrete under bending, an extended X-ray micro-computed tomography system was used, i.e. the tomography system SkyScan 1173 was connected to the loading machine ISTRON 5569. This combined system enabled to shot images of deforming concrete beams during a continuous deformation...
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The new type of [Zr6(μ3-O)4 (μ3-OH)4] cluster core: Crystal structure and spectral characterization of [Zr6O4(OH)4(OOCR)12] (R = Bu^t^,C(CH3)2Et)
PublicationSześciojądrowe oxo karboksylowe kompleksy cyrkonu(IV) zostały otrzymane z Zr(OR')4 i odpowiednich kwasów organicznych HOOCR (R=t-Bu, CMe2Et) w stosunku molowym 1:2. Struktury krystaliczne dwóch związków o wzorze [Zr6O4(OH)4(OOCR)12] (1 dla R=t-Bu i 2 dla R=-CMe2Et) zostały rozwiązane w grupie przestrzennej R-3. Substancje zostały przebadane termograwimetrycznie (TGA/DTA) oraz przy użyciu spektroskopii w podczerwieni ze zmienną...
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Immunizing the Hillcast Method against the Known-Plaintext Attack using Periodic Key Exchange
PublicationThis paper considers a Joint Fingerprinting and Decryption method, called Hillcast, for the copyright protection and traitor tracing in case of Video on Demand services. Because the method is based on the Hill cipher, it is vulnerable to a known-plaintext attack. The goal of this paper is to present an efficient periodic key exchange mechanism to make this method secure without compromising its scalability, imperceptibility or...
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Etazene (N,N-diethyl-2-{[(4-ethoxyphenyl)methyl]-1H-benzimidazol-1-yl}-ethan-1-amine (dihydrochloride)): a novel benzimidazole opioid NPS identified in seized material: crystal structure and spectroscopic characterization
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Piezoresponse force microscopy and dielectric spectroscopy study of Ba0.6Sr0.4TiO3 thin films
PublicationResearch on synthesis, characterization and determination of processing – structure – property relationships of commercially important ferroelectric thin films has been performed. The sol-gel-type solution deposition technique was applied to produce good quality thin films of Ba0.6Sr0.4TiO3 (BST60/40) chemical composition on the stainless steel substrates. The thin films were characterized in terms of their microstructure, crystal...
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Research of Accuracy of RSSI Fingerprint-Based Indoor Positioning BLE System
PublicationRadio localization in indoor environment is still a challenging task due to environment volatility. In the paper are compared achieved localization accuracies for RSSI-Fingerprinting method utilizing Bluetooth Low Energy (BLE) for two different environments: large empty hall and narrow corridor. Measurements were done by 6 different smartphones of 3 different producers, which makes those measurements unique as accuracies achieved...
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Research of Accuracy of RSSI Fingerprint-Based Indoor Positioning BLE System
PublicationRadio localization in indoor environment is still a challenging task due to environment volatility. In the paper are compared achieved localization accuracies for RSSI-Fingerprinting method utilizing Bluetooth Low Energy (BLE) for two different environments: large empty hall and narrow corridor. Measurements were done by 6 different smartphones of 3 different producers, which makes those measurements unique as accuracies achieved...
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Dynamic F-free Coloring of Graphs
PublicationA problem of graph F-free coloring consists in partitioning the vertex set of a graph such that none of the resulting sets induces a graph containing a fixed graph F as an induced subgraph. In this paper we consider dynamic F-free coloring in which, similarly as in online coloring, the graph to be colored is not known in advance; it is gradually revealed to the coloring algorithm that has to color each vertex upon request as well...
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[Komentarz do artykułu] Yin, W.-Y., Wu, B., Miao, M., Doi, L.B., Li, L.-W., and Kooi, P.-S.: Experimental characterisation and modelling of on-chip capacitors and resistors on GaAs substrates.
PublicationDokonano krytycznej oceny wartości elementów schematu zastępczego rezystorów monolitycznych wykonanych na podłożu GaAs przedstawionych w pracy: Yin, W.-Y., Wu, B., Miao, M., Doi, L.B., Li, L.-W., and Kooi, P.-S.: Experimental characterisation and modelling of on-chip capacitors and resistors on GaAs substrates, IEE Proc. Microw. Antennas and Propag., 2002,149, (1), pp.50-52.
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SU‐E‐T‐472: Characterization of the Very High Energy Electrons, ISO ‐ 250 MeV (VHEE) Beam Generated by ALPHA‐X Laser Wakefield Accelerator Beam Line for Utilization in Monte Carlo Simulation for Biomedical Experiment Planning
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Koncepcja i analiza sensora/aktuatora piezoelektrycznego do pomiaru procesu starzenia się ludzkiej skóry
PublicationNiniejszy artykuł przedstawia nową koncepcję piezoelektrycznego sensora/aktuatora przeznaczonego do pomiaru właściwości mechanicznych tkanek miękkich a w szczególności skóry ludzkiej. Wyjaśnione jest analityczne podejście z wykorzystaniem schematu zastępczego Mason’a określającego aktuator w stanie rezonansu oraz opis metody impedancji elektromechanicznej wykorzystanej w systemie pomiarowym. Analiza z użyciem metody elementów...
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Micro-Abrasive Wear Testing of Surface Engineered Surgical Grade CoCrMo Alloy for Biotribological Applications
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Surface Characteristics of Plasma Treated and Titanium Nitride (TiN) Deposited Aluminum Alloy
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Progress on Roman and Weakly Connected Roman Graphs
PublicationA graph G for which γR(G)=2γ(G) is the Roman graph, and if γwcR(G)=2γwc(G), then G is the weakly connected Roman graph. In this paper, we show that the decision problem of whether a bipartite graph is Roman is a co-NP-hard problem. Next, we prove similar results for weakly connected Roman graphs. We also study Roman trees improving the result of M.A. Henning’s A characterization of Roman trees, Discuss. Math. Graph Theory 22 (2002)....
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Low-coherence photonic method of electrochemical processes monitoring
PublicationWe present an advanced multimodality characterization platform for simultaneous optical and electrochemical measurements of ferrocyanides. Specifcally, we combined a fber-optic Fabry– Perot interferometer with a three-electrode electrochemical setup to demonstrate a proof-ofprinciple of this hybrid characterization approach, and obtained feasibility data in its monitoring of electrochemical reactions in a boron-doped diamond flm...
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Molecular epidemiology of Serratia marcescens in two hospitals in Danzig, Poland, over a 5-year period.Molecular epidemiology of Serratia marcescens in two hospitals in Gdańsk, Poland, over a 5-year period.
PublicationW pracy badano zmiany populacji Serratia marcescens w ciągu 5 lat w dwóch szpitalach klinicznych Gdańska. Posłużono się wartościami MIC, wynikami typowania genetycznego RAPD-PCR, PFGE i nową metodą ADSRRS-fingerprinting oraz analizą beta-laktamaz o rozszerzonym spektrum substratowym (ESBL). Dzięki określeniu lekowrażliwości na najnowsze antybiotyki beta-laktamowe wykryto fenotypy wykazujące derepresję cefalosporynazy AmpC u 23%...
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Differential scanning calorimetry as a tool to assess the oxidation state of cold-pressed oils during shelf-life
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Controllable Synthesis of 3D Hollow-Carbon-Spheres/Graphene-Flake Hybrid Nanostructures from Polymer Nanocomposite by Self-Assembly and Feasibility for Lithium-Ion Batteries
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Revealing the Influence of the Shape, Size, and Aspect Ratio of ZnO Nanoparticles on Antibacterial and Mechanical Performance of Cellulose Fibers Based Paper
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Application of Electrical Capacitance Tomography for bulk solids flow analysis in silos
PublicationW artykule przedstawiono wyniki aplikacji metody ECT w analizie przepływów materiałów sypkich, zarówno bezkohezyjnych, jak również kohezyjnych. Omówiono podstawy techniczne metody ECT, przeprowadzono dyskusje parametrów zmiennych (zagęszczenie początkowe, szorstkość ścian).
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Applicability of edible Candelilla wax composite blended with Bryophyllumpinnatum extract to prolong shelf life of fruits/vegetables
PublicationCandelilla wax (CW) is a natural lipid source that can be used to make biodegradable and edible coatings and films for fruits. However, CW alone does not provide sufficient antimicrobial and antioxidant properties to prevent microbial spoilage and oxidative deterioration of fresh products. This study aims at evaluating the applicability of CW blended with Bryophyllum pinnatum extract (BPE), a plant with medicinal and phytochemical...
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Experimental investigation of the flow pattern and wall pressure distribution in a silo with double-cone insert
PublicationArtykuł opisuje przeprowadzone badania przepływów silosowych i naporu materiałów sypkich podczas napełniania i opróżniania silosu o średnicy 2.5 m wyposażonego we wkładkę "podwójny stożek". Badania przeprowadzane były w Instytucie Badawczym Tel-Tek w Norwegii. Materiałem użytym był suchy piasek. Napór na ścianę mierzony był bezpośrednio za pomocą 10 czujników wbudowanych w ścianę. Badania eksperymentalne pokazały duży wpływ wkładki...
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Investigations of porosity changes during granular silo flow using Electrical Capacitance Tomography (ECT) and Particle Image Velocimetry (PIV)
PublicationArtykuł omawia pomiary zmian porowatości podczas przepływu silosowego materiału granulowanego. Zastosowano 2 techniki: tomografie i optoelektroniczną DIC. Pomiary wykonano dla różnych początkowych zagęszczeń oraz szorstkości ścian.
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A new synthetic entry to phosphinophosphinidene complexes. Synthesis and structural characterisation of the first side-on bonded and the first terminally bonded phosphinophosphinidene zirconium complexes[mu-(1,2:2-eta-tBu2PLP){Zr(Cl)Cp2}2] and [{Zr(PPhMe2)Cp2}(eta^1^-P-P-tBu2)].
PublicationPodano nową metodę syntezy kompleksów fosfinofosfinidenowych polegającą na reakcji dichlorku cyrkonocenu z solą litową difosfanu t-Bu2P-P(SiMe3)Li. Otrzymano pierwsze kompleksy fosfanofosfinidenowe cyrkonu z ligandem związanym w sposób boczny i ligandem związanym terminalnie.
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Some variations of perfect graphs
PublicationWe consider (ψk−γk−1)-perfect graphs, i.e., graphs G for which ψk(H) =γk−1(H) for any induced subgraph H of G, where ψk and γk−1 are the k -path vertex cover number and the distance (k−1)-domination number, respectively. We study (ψk−γk−1)-perfect paths, cycles and complete graphs for k≥2. Moreover, we provide a complete characterisation of (ψ2−γ1)-perfect graphs describing the set of its forbidden induced subgraphs and providing...
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Quantum-correlation breaking channels, broadcasting scenarios, and finite Markov chains
PublicationOne of the classical results concerning quantum channels is the characterization of entanglementbreakingchannels [M. Horodecki et al., Rev. Math. Phys 15, 629 (2003)]. We address the questionwhether there exists a similar characterization on the level of quantum correlations which may gobeyond entanglement. The answer is fully affirmative in the case of breaking quantum correlationsdown to the, so called, QC (Quantum-Classical)...
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A new assay based on terminal restriction fragment length polymorphism of homocitrate synthase gene fragments for Candida species identification
PublicationCandida sp. have been responsible for an increasing number of infections, especially in patients with immunodeficiency. Species specific differentiation of the Candida sp. is difficult in routine diagnosis. This identification can have a highly significant association in therapy and prophylaxis. This work has shown a new application of terminal restriction fragment length polymorphism (t-RFLP) method in molecular identification...
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Manganese–Cobalt Based Spinel Coatings Processed by Electrophoretic Deposition Method: The Influence of Sintering on Degradation Issues of Solid Oxide Cell Oxygen Electrodes at 750 °C
PublicationThis paper seeks to examine how the Mn–Co spinel interconnect coating microstructure can influence Cr contamination in an oxygen electrode of intermediate temperature solid oxide cells, at an operating temperature of 750 °C. A Mn–Co spinel coating is processed on Crofer 22 APU substrates by electrophoretic deposition, and subsequently sintered, following both the one-step and two-step sintering, in order to obtain significantly...
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Coronas and Domination Subdivision Number of a Graph
PublicationIn this paper, for a graph G and a family of partitions P of vertex neighborhoods of G, we define the general corona G ◦P of G. Among several properties of this new operation, we focus on application general coronas to a new kind of characterization of trees with the domination subdivision number equal to 3.
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Prediction of the Biogenic Amines Index of Poultry Meat Using an Electronic Nose
PublicationThe biogenic amines index of fresh chicken meat samples during refrigerated storage was predicted based on the headspace analysis using an electronic nose equipped with an array of electrochemical sensors. The reference biogenic amines index values were obtained using dispersive liquid–liquid microextraction–gas chromatography–mass spectrometry. A prototype electronic nose with modular construction and a dedicated sample chamber...
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Structure of the Resource Theory of Quantum Coherence
PublicationQuantum coherence is an essential feature of quantum mechanics which is responsible for the departure between the classical and quantum world. The recently established resource theory of quantum coherence studies possible quantum technological applications of quantum coherence, and limitations that arise if one is lacking the ability to establish superpositions. An important open problem in this context is a simple characterization...