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Search results for: audyt brd
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Nonlinear and linear impedance of bismuth vanadate ceramics and its relation to structural properties
PublicationThe nonlinear and linear electrical properties, topography, and microstructure of bismuth-vanadate ceramics, were studied. The structurewas observed with the use of X-ray diffraction (XRD), scanning electronmicroscopy (SEM), atomic force microscopy (AFM) and confocal microscopy methods. The obtained results showed that ceramic is porous. Two phase transitionswere determinedwith the use of DSC measurements. The linear and nonlinear ac...
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The influence of thermal conditions on V2O5 nanostructures prepared by sol-gel method
PublicationThis work presents the result of structure investigations ofV 2O5 nanorods grown from thin films and powders prepared by sol-gel method. To examine the best temperature of nanorods crystallization, thin films deposited by spin-coating method on quartz glass or silicon substrates and bulk xerogel powders were annealed at various temperatures ranging from 100∘C to 600∘C. The structure of the samples was characterized by X-ray diffraction...
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Luminescence properties of Eu3+ and Tb3+ doped silica-based xerogels
PublicationPure SiO2 xerogels and SiO2 xerogels containing SrF2: Eu3+/: Tb3+ crystals were prepared using sol-gel method. Luminescent spectra showed excitation and emission peaks characteristic to Eu3+ and Tb3+ 4f - 4f transitions. ET Tb3+→Eu3+ has been observed. XRD pattern of SiO2 matrix confirmed lack of long range order. Patterns of SiO2-SrF2:Eu3+ and SiO2-SrF2:Tb3+ showed peaks corresponding to SrF2. SEM images have shown agglomerates...
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Ti-Fe2O3/In2O3 as photoactive material: The role of the substrate in photoelectrochemical water oxidation
PublicationThe layers of Ti-Fe2O3/In2O3 were prepared on the different substrates using hydrothermal method: Ti/TiO2 nanotubes, Ti foil, FTO and FTO/TiO2. Materials were characterized using scanning electron microscopy, XRD, Raman, UV-Vis, and X-ray photoelectron spectroscopy and tested as photoanodes for water oxidation under illumination. The formation of heterojunction on the TiO2 nanotubes increases photocurrent of water oxidation at...
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Electrical conductivity of NbN-SiO2 films obtained by ammonolysis of Nb2O5-SiO2 sol-gel derived coatings
PublicationW pracy przedstawiono badania przewodnictwa elektrycznego (w zakresie 5-280K) warstw NbN-SiO2 o grubości 450 nm. Warstwy uzyskano poprzez azotowanie otrzymanych metodą zol-żel warstw Nb2O5-SiO2, o różnym stosunku molowym Nb2O5/SiO2. Azotowanie takich warstw w temperaturze 1200C prowadzi do otrzymania metalicznych granul NbN w amorficznej matrycy SiO2. Struktura warstw była badana mikroskopem sił atomowych (AFM) oraz metodą dyfrakcji...
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The efficiency of pollutants removal and concepts on improvement for single-family TWs
PublicationIn the rural areas building of sewerage systems and central wastewater treatment plants (WWTPs) often brings too high costs, due to high distances from one farm to another and terrain configuration. Individual treatment systems for each farm are a good solution. Theteratment wetlands for nine individual farms were constructed in Kaszubian Lake District in summer and autumn 2009. Three configurations of hydrophyte beds were chosen....
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Electrolytic deposition of reactive element thin films on Crofer 22 APU and evaluation of the resulting high-temperature corrosion protection properties at 700 °C–900 °C
PublicationThis article presents electrolytic deposition of thin Rare Earth (RE) coatings on Crofer 22 APU stainless steel substrates for high temperature applications, such as interconnects in solid oxide cell stacks. The deposition of coatings based on yttrium-, gadolinium-, lanthanum-, and cerium nitrates is discussed. The high temperature corrosion properties of surface-modified steels were examined using thermogravimetry and electrical...
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The effect of Sr and Mg substitutions on structure, mechanical properties and solubility of fluorapatite ceramics for biomedical applications
PublicationIonic substitutions play important role in the modifications of biological apatites. Recently, attention has been focused on the co-doping effects on the functional properties of apatite-based biomaterials. In this research work, the dense samples of fluorapatites, Ca10(PO4)6F2 and Ca8MgSr(PO4)6F2, were produced after sintering at 1250 °C for 6 h in air. Structural characterization carried out with XRD, IR, Raman and SEM, confirmed...
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A Simple Replica Method as the Way to Obtain a Morphologically and Mechanically Bone-like Iron-Based Biodegradable Material
PublicationPorous iron-based scaffolds were prepared by the simple replica method using polyurethane foam as a template and applying the sintering process in a tube furnace. Their surface morphology was characterized using scanning electron microscopy (SEM) and phase homogeneity was confirmed using X-ray diffraction (XRD). Corrosion behavior was determined using immersion and potentiodynamic polarization methods in phosphate buffered saline...
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Luminescent properties of Ln3+ doped tellurite glasses containing AlF3
PublicationThe low-phonon energy tellurite glasses TeO2-BaO-Bi2O3 and TeO2-BaO-Bi2O3-AlF3 triply doped with Eu3+, Tb3+, Tm3+ ions in two different molar ratios were synthesized using melt-quenching technique. Their structure and luminescence properties were widely investigated by X-ray Diffraction (XRD), Differential Scanning Calorimetry (DSC), Fourier Transform Infrared Spectroscopy (FTIR) and Photoluminescence Spectroscopy (PL). The luminescence...
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Release and Transport of Toxic, Mobile Organic Compounds (Formaldehyde and Phenols) on an Arctic Glacier
PublicationAs a result of current deglaciation, the chemical cycles of many compounds, including toxic formaldehyde and phenols, are changing. However, the processes by which these chemicals are released have yet to be studied in situ. Here, we quantify fluxes of HCHO and phenols in a glacial catchment within one summer season, obtaining a net release from the glacier of 0.106 · 106 g formaldehyde and 0.255 · 106 g phenols, which can be interpreted...
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WPŁYW METODY SYNTEZY NA WŁAŚCIWOŚCI STRUKTURALNE I KATALITYCZNE ZWIĄZKU Ce0.9Pr0.1O2-δ PODCZAS WYSOKOTEMPERATUROWEJ PRACY W BIOGAZIE
PublicationTlenkowe ogniwa paliwowe zasilane biogazem degradują się pod wpływem węgla osadzającego się na anodzie. Aby wyeliminować ten efekt, szuka się warstw katalitycznych, które nałożone na anodę powstrzymują osadzanie się węgla i zmniejszają straty wydajności ogniwa. Związkiem użytym w tym celu jest Ce0,9Pr0,1O2-δ wytworzony dwiema metodami: Pechiniego i metodą strącania z odwróconej emulsji. Aby zbadać wpływ metody syntezy na właściwości...
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Modified Preisach model of hysteresis in multi air gap ferrite core medium frequency transformer
PublicationThis article presents the modified Preisach model of hysteresis for a 3-phase medium frequency transformer in a 100 kW dual active bridge converter. The transformer magnetic core is assembled out of ferrite I-cores, which results in multiple parasitic air gaps. For this transformer, the hysteresis loops were measured and parameters of the Preisach model were determined. The Preisach distribution function is approximated with a...
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Effect of MAO coatings on cavitation erosion and tribological properties of 5056 and 7075 aluminum alloys
PublicationTwo ceramic coatings have been applied on 5056 and 7075 aluminum alloy by microarc oxidation (MAO) technology. The mass losses, surface morphologies and the phase constituents of the MAO coatings before and after cavitation tests were examined by means of digital scales, scanning electron microscopy (SEM) and X-ray diffraction (XRD), respectively. In order to assess the impact of the mechanical properties of the surface layer on...
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Realizacja układu SZR na bazie sterownika PLC WAGO PFC200
PublicationArtykuł opisuje projekt i wykonanie układuSamoczynnego Załączania Rezerwy (SZR), który został zrealizowany z wykorzystaniem sterownika PLC WAGO PFC200 i jest wdrażany w systemie stacji elektroenergetycznej Laboratorium LINTE^2 na Politechnice Gdańskiej.
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Tellurite based glass doped by Eu3+ ions - XPS measurements
Open Research DataEu3+ doped tellurite glass ceramics containing SrF2 nanocrystals were prepared using melt quenching technique and subsequent heat treatment of glass in 370 °C for different time periods. Thermal properties of glass matrix have been determined based on DSC measurements. XRD and XPS results confirmed formation of SrF2 nanocrystals in glass matrices after...
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Koncepcja zarządzania systemem ładowania sterowanego do akumulatorów samochodów elektrycznych
PublicationPraca magisterska Wraz ze wzrostem liczby pojazdów elektrycznych na drogach, ładowanie akumulatorów samochodów elektrycznych będzie miało coraz większy wpływ na systemy elektroenergetyczne. Nieograniczone czasowo ładowanie wywoła konieczność poniesienia dodatkowych kosztów rozbudowy systemu elektroenergetycznego.Rozwiązaniem tego problemu jest sterowanie ładowaniem akumulatorów samochodów elektrycznych, co umożliwi...
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The Bridge of Data Project Objectives
PublicationOpen Research Data (ORD) is one of the emerging trends for researchers across the globe. However, it has to be stressed that the level of implementation and awareness of ORD varies between countries. Many initiatives have been created in Polish scientific institutions to support the process of opening publications. These are mainly Open Access (OA) repositories, implementing the so-called green road of OA. However, only a few universities...
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The microbial community, its biochemical potential, and the antimicrobial resistance of Enterococcus spp. in Arctic lakes under natural and anthropogenic impact (West Spitsbergen)
PublicationThe sustainable management of small human communities in the Arctic is challenging. In this study, both a water supply system (Lake 1) under the natural impact of a bird-nesting area, and a wastewater receiver (Lake 2) were analysed in the vicinity of the Polish Polar Station on West Spitsbergen. Microbial community composition, abundance and activity were assessed in samples of the treated wastewater, lake water and sediments...
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A new simple approach to prepare rare-earth metals-modified TiO2 nanotube arrays photoactive under visible light: Surface properties and mechanism investigation
PublicationApplication of Ti90RE10 alloys (RE = Ho, Er, Nd, Y, Ce, Tm) as a working electrode, instead of Ti pure foil in anodic oxidation in a fluoride-based electrolyte, resulted in formation of well-ordered nanotubes made of TiO2 and RE2O3 mixture, which could be efficiently used for pollutant removal from water and air phase upon UV and visible irradiation and easily separable from the reaction mixture to recycle. The as-prepared NTs...
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Kinetics of Cross-Linking Reaction of Epoxy Resin with Hydroxyapatite-Functionalized Layered Double Hydroxides
PublicationThe cure kinetics analysis of thermoset polymer composites gives useful information about their properties. In this work, two types of layered double hydroxide (LDH) consisting of Mg2+ and Zn2+ as divalent metal ions and CO32− as an anion intercalating agent were synthesized and functionalized with hydroxyapatite (HA) to make a potential thermal resistant nanocomposite. The curing potential of the synthesized nanoplatelets in the...
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Spectroscopic studies of Nb-doped tricalcium phosphate glass-ceramics prepared by sol-gel method
PublicationCalcium-phosphate based glasses and glass-ceramics play a crucial role in the tissue engineering development. Apart from their high biocompatibility and excellent ability to undergo varying degrees of resorbability1, they exhibit relatively high bioactivity and due to that they are commonly used as bone and dental implants. A substantial research effort is devoted to improve calcium-phosphate materials physico-chemical properties...
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Analiza spostrzeżeń podczas audytów w przedsiębiorstwach z branży spożywczej
PublicationAnalizowano dane z 54 przedsiębiorstw potwierdzających zgodność z wdrożonym systemem ISO 22000 w latach 2005–2013 przez jednostkę certyfikującą DNV GL–BA. Przedstawiono najczęściej spotykane kategorie niezgodności stwierdzane podczas audytów certyfikujących w przedsiębiorstwach należących do łańcucha żywnościowego. Przeanalizowano występujące problemy wpływające na bezpieczeństwo żywności podczas procesu produkcyjnego. Obliczono...
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Rain Gardens SW quality dataset
Open Research DataThis dataset contains the results of parameters of storm water runoff and storm water quality in rain garden units. Samples were collected from 4 different rain gardens in Gdansk, Poland.
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Thickness and structure change of titanium (IV) oxide thin films synthesized by the sol–gel spin coating method
PublicationTitanium dioxide is a well-known material in nanotechnology, while it provides new opportunities due to its interesting properties, for example, as a semiconductor with a quite significant forbidden band gap energy of 3.2 eV. In this study, thin films of titanium dioxide (TiO2) were synthesized in amorphous and crystallographic systems using the sol–gel process. Atomic Force Microscopy (AFM), Raman spectroscopy and X-ray diffraction...
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Structural and electrical properties of titanium-doped yttrium niobate
PublicationIn this work, the influence of the substitution of niobium by titanium in Y3Nb1-xTixO7-δ on the structural and electrical properties is reported. Several experimental techniques, i.e. X-Ray Diffraction (XRD), Scanning Electron Microscopy (SEM), X-Ray Photoelectron Spectroscopy (XPS) and Electrochemical Impedance Spectroscopy (EIS), were applied to investigate the system Y3Nb1-xTixO7-δ. Titanium in Y3Nb1-xTixO7-δ is an acceptor-type...
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Manganese Phosphatizing Coatings: The Effects of Preparation Conditions on Surface Properties
PublicationManganese phosphate coating could be used to protect the surface of steel products. However, it is essential to determine the effects which process parameters, as well as the types of additives used, have on the efficiency of coating deposition. Thus, we present here a process of phosphatization of low-alloy steel (for 15 min at 95 ◦C) in manganese/nickel baths followed by a passivation process with the use of a silicon and zircon...
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A negative effect of carbon phase on specific capacity of electrode material consisted of nanosized bismuth vanadate embedded in carbonaceous matrix
PublicationLithium-ion batteries (LIBs) are widely used all over the world. The LIBs belong to a renewable energy source and energy storage devices. The increase in energy demand causes that new materials of higher energy and higher power densities are still under investigation. Herein, we compare electrochemical properties of bismuth vanadate (BiVO4) embedded and not embedded into carbonaceous matrix as an anode material along with structural...
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Modeling and Designing Acoustical Conditions of the Interior – Case Study
PublicationThe primary aim of this research study was to model acoustic conditions of the Courtyard of the Gdańsk University of Technology Main Building, and then to design a sound reinforcement system for this interior. First, results of measurements of the parameters of the acoustic field are presented. Then, the comparison between measured and predicted values using the ODEON program is shown. Collected data indicate a long reverberation...
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Structure and electrical properties of nitrided NbN-TiN sol-gel derived films
PublicationW pracy przedstawiono rezultaty badań struktury oraz właściwości elektrycznych warstw NbN-TiN (o różnym stosunku molowym NbN/TiN)otrzymanych w wyniku termicznego azotowania warstw tlenkowych otrzymanych metodą zol-żel. Badania struktury przeprowadzono metodami AFM, XRD oraz XPS. Wynika z nich, iż głównymi fazami w wartstwach są NbN i TiN o rozmiarach ziaren około 100 nm. Jednakże zaobserwowano również istnienie niewielkiej ilości...
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Analiza pracy ujęcia infiltracyjnego w warunkach suszy hydrologicznej = Infiltration intake work analysis under hydrological drought
PublicationW publikacji przedstawiono wyniki obliczeń numerycznych przepływu wody w warstwie wodonośnej ujęcia infiltracyjnego. Do rozwiązania problemu wykorzystano równanie filtracji wody ze swobodnym zwierciadłem wody. W obliczeniach w warunkach nieustalonych warunek początkowy obliczono przy założeniu dopuszczalnej wydajności ujęcia (100 000 m3/doba). Jako warunek brzegowy, przyjęto funkcję wahania poziomu zwierciadła wody w stawach infiltracyjnych...
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Nanomateriały o właściwościach magnetycznych, fotokatalitycznych, biobójczych
PublicationTematyka badawcza pracy doktorskiej obejmuje preparatykę i charakterystykę nanomateriałów o właściwościach magnetycznych, fotokatalitycznych, biobójczych. Celem pracy była preparatyka nanomateriałów na bazie TiO2 oraz ZnFe2O4 oraz zastosowanie nanokompozytów w fotokatalizie heterogenicznej do degradacji ksenobiotyków niepodatnych na rozkład biologiczny i otrzymywania funkcjonalnych materiałów budowlanych. Otrzymane nanokompozyty...
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Influence of controlled crystallization and SrF2 content on the structure and properties of Eu3+ doped phosphate glasses
PublicationNew phosphate glasses and glass-ceramics P2O5–Bi2O3–K2O–Nb2O5-SrF2 doped with Eu were synthesized and studied in this work. The influence of the SrF2 content (0–15 mol%) and the parameters of the heat treatment on their structural and optical properties were investigated. For the above purpose, the structural characterization by FTIR spectroscopy and XRD measurements was carried out, which showed a significant effect of SrF2 on...
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Assessment of Subsoil Subsidence Under the Railway Surface with the Use of Fuzzy Sets
PublicationThe cause of the subsidence of the railway track is the subsidence of the track bed itself and it is often related to the subsidence of the subsoil. Such settlement leads to: uneven longitudinal railways and track twist. These phenomena have a negative impact on the comfort and safety of driving, and in extreme cases lead to a train derailment. It has been shown that the magnitude of these settlements is determined by many parameters...
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Ocena wpływu parametrów nadtapiania laserowego w warunkach kriogenicznych na strukturę warstwy wierzchniej na stopie Ti-6Al-4V
PublicationW pracy zostały przedstawione efekty przetapiania laserowego w warunkach kriogenicznych stopu tytanu Ti-6Al-4V. W celu określenia wpływu obróbki laserowej wykonano analizę mikrostruktury (SEM), składu fazowego (XRD), oraz pomiary mikrotwardości uzyskanych warstw. Stwierdzono, że zmiany podstawowych parametrów przetapiania laserowego - mocy wiązki lasera i prędkości skanowania istotnie wpływają na grubość i mikrostrukturę otrzymanych...
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Effect of crystallinity on structural, thermal, and in vitro dissolution properties of Na2O-CaO-Nb2O5/MgO-P2O5 glass-ceramics
PublicationThe impact of the crystallinity on structural, thermal, and in vitro dissolution properties were examined for Na2O- CaO-Nb2O5/MgO-P2O5 glasses/glass-ceramics. Glass-ceramics were synthesized via a spontaneous crystallization process. The Nb content in the materials increased with melting temperature, furthermore, the crystallinity is proportional to the Nb content. The presence of crystalline niobates and phosphates is confirmed...
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Hydrothermal Cobalt Doping of Titanium Dioxide Nanotubes towards Photoanode Activity Enhancement
PublicationDoping and modification of TiO2 nanotubes were carried out using the hydrothermal method. The introduction of small amounts of cobalt (0.1 at %) into the structure of anatase caused an increase in the absorption of light in the visible spectrum, changes in the position of the flat band potential, a decrease in the threshold potential of water oxidation in the dark, and a significant increase in the anode photocurrent. The material...
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MgPdSb─An Electron-Deficient Half-Heusler Phase
PublicationThe half-Heusler family consists of many semiconducting intermetallic compounds, virtually all of them having a valence electron count (VEC) of 18. We have studied an electron-deficient (VEC = 17) phase MgPdSb and its Pd-stuffed variant MgPd1.25Sb. The cubic F4̅3m crystal structure was confirmed by the Rietveld refinement of powder X-ray diffraction (XRD) data. The lattice parameter is a = 6.284 and 6.335 Å for MgPdSb and MgPd1.25Sb,...
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Preparation and characterisation of iron substituted Mn1.7Cu1.3-xFexO4 spinel oxides (x = 0, 0.1, 0.3, 0.5)
PublicationSpinel oxides with the general formula Mn1.7Cu1.3-xFexO4 (x= 0, 0.1, 0.3, 0.5) were prepared and evaluated in this work for their properties at high temperatures. The effect of partially substituting Cu by Fe has not been studied so far for this group of materials and is thus evaluated in this work. Mn1.7Cu1.3-xFexO4 powders were synthesised by a soft chemistry process and studied in terms of crystallographic phase analysis, electrical...
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Compression test results of fused filamend fabricated polylactyde and polylactyde with carbon fiber filler
Open Research DataThe DataSet contains the results of the mechanical behaviour of cube specimens with dimensions 30 x 30 x 30 cm3. The specimens were additively manufactured with the fused filament fabrication (FFF) method. They used two different materials polylactide (PURE PLA) and polylactide with carbon fibre filler (PLA+CF). The specimens were segregated into three...
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Zarządzanie zapasami dla praktyków
PublicationDążenie do redukcji zapasów jest naturalnym trendem wszystkich przedsiębiorstw dbających o dostęp do tzw. wolnej gotówki. 11 lat prowadzonych przeze mnie obserwacji w toku realizowanych kilkuset projektów wskazuje, że tylko ok 0,5% przedsiębiorstw (w danym momencie) nie zajmuje się pracą nad obniżeniem zapasów. Jak ta redukcja zapasów zazwyczaj się odbywa? Szef stawia cel swojemu zespołowi: „dziś rotacja naszego zapasu...
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Spectroscopic evaluation on pseudopolymorphs of sodium naproxen
PublicationThis paper demonstrates the assessment of vibrational spectroscopy methods such as middle infrared, near infrared and Raman spectroscopy (FTIR, FT-NIR, Raman) for the identification of pseudopolymorphic forms of a model active pharmaceutical ingredient (API) - sodium naproxen (NpxNa). NpxNa, in the form of three different pseudopolymorphs, was investigated by methods dedicated for solid state characterization: DSC (differential...
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Marcin Wekwejt dr inż.
PeopleMarcin Wekwejt, absolwent studiów inżynierskich w inż. biomedycznej (2016; Politechnika Bydgoska im. J. i J. Śniadeckich & Collegium Medicum im. L. Rydygiera), studiów magisterskich w inż. mechaniczno-medycznej (2018; Politechnika Gdańska & Gdański Uniwersytet Medyczny) oraz studiów doktoranckich w dyscyplinie inż. materiałowej (2021, Politechnika Gdańska). Uzyskał z wyróżnieniem stopień naukowy doktora nauk inżynieryjno-technicznych...
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Production of fuel briquette from solid waste biomass using natural resin as a binder
PublicationBackground: This research aimed to evaluate the use of natural resin as a binder for the production of fuel briquette from solid waste biomass.Methods: Proximate analyses were made for fuel briquette prepared from solid waste biomass using natural resin as a binder in comparison with using starch as a binder.Results: The results for density, percent content of moisture, percent content of volatile matter, percent...
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Dzień Kariery OFFSHORE na Politechnice Gdańśkiej
EventsZapraszamy studentów, absolwentów oraz osoby zainteresowane morską energetyką wiatrową do udziału w Dniu Kariery OFFSHORE, który odbędzie się w dniu 16 stycznia 2024r., w godz. 10-14, w budynku WIMiO (bud. nr 30)
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Agnieszka Szuta dr inż. arch.
PeopleAgnieszka Szuta jest absolwentką Wydziału Architektury Politechniki Gdańskiej. Tytuł inżyniera architekta uzyskała w 2016 roku. W czasie studiów pracowała jako inżynier budowy m.in. obiektu wielofunkcyjnego w Gdańsku i zespołu zabytkowych kamienic w Toruniu. Pracę magisterską obroniła w 2017 roku jednocześnie rozpoczynając studia doktoranckie.Wśród jej głównych zainteresowań naukowych znajdują się zagadnienia związane z tematyką...
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Milena Marycz dr inż.
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Impact of the anion and chalcogen on the crystal structure and properties of 4,6-dimethyl-2-pyrimido(thio)nium halides
PublicationBy the reaction of urea or thiourea, acetylacetone and hydrogen halide (HF, HBr or HI), we have obtained seven new 4,6-dimethyl-2-pyrimido(thio)nium salts, which were characterized by single-crystal X-ray diffraction, namely, 4,6-dimethyl-2-oxo-2,3-dihydropyrimidin-1-ium bifluoride, C₆H₉N₂O⁺·HF₂⁻ or (dmpH)F₂H, 4,6-dimethyl-2-oxo-2,3-dihydropyrimidin-1-ium bromide, C₆H₉N₂O⁺·Br⁻ or (dmpH)Br, 4,6-dimethyl-2-oxo-2,3-dihydropyrimidin-1-ium...
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Instalacje bud-san, niestacj. 2022/2023
e-Learning CoursesW ramach przedmiotu (wykłady + ćwiczenia) omawiane są instalacje branży sanitarnej, stąd nazwa przedmiotu "Instalacje budowlane sanitarne". Instalacje te obejmują: instalacje wody zimnej, instalacje ciepłej wody użytkowej, instalacje przeciwpożarowe, instalacje kanalizacji sanitarnej i kanalizacji deszczowej, instalacje gazu, instalacje grzewcze wodne a także elementy instalacji wentylacyjnych i klimatyzacyjnych. Podawane...
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WILiŚ - Bud. - e-test 2018/19
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