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Search results for: capital gap
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Analysis of pesticide residues in fruits and vegetables using QuEChERS sample preparation method and gas chromatography with electron capture detection
PublicationPesticides are a numerous and diverse group of chemical compounds. They are some of the most toxic substances contaminating the environment, which are used to eliminate pests in agriculture and the household. Despite considerable progress in the development of methods for preparing samples for analysis and for the final determination of analytes, the analysis of pesticides in biological samples continues to present challenges to...
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Biofilm Production and Presence of ica and bap Genes in Staphylococcus aureus Strains Isolated from Cows with Mastitis in the Eastern Poland
PublicationThe aim of the study was phenotypic and genotypic analysis of 132 S. aureus strains isolated from mastitis in eastern Poland in respect to their biofilm formation ability. The analysis of the size polymorphism of fragment X in the gene encoding protein A (spa) revealed high genetic differentiation of the analyzed group of isolates. The ability of biofilm formation by the isolates was tested using two phenotypic methods. The Congo...
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Determination of fuel combustion product in airport runoff water samples using liquid–liquid extraction with gas chromatography–spectrometry
PublicationDetermination of xenobiotics in samples of airport runoff water is both a complex and indispensable task due to an increasing threat resulting from the activities of numerous airports. The aim of this study was to develop, optimize, and validate a procedure based on liquid–liquid extraction (LLE) coupled with gas chromatography–mass spectrometry (GC–MS) for the determination of polycyclic aromatic hydrocarbons (PAHs). So far, no...
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Selecting wells for an optimal design of groundwater monitoring network based on monitoring priority map: A Kish Island case study
PublicationThis paper presents a novel approach, i.e. a combination of gamma test and monitoring priority map, for optimal design of groundwater monitoring network (GMN) by considering the cumulative effects of industries, human activities, and natural factors on the groundwater quality. The proposed method was successfully applied to design an optimal network for groundwater salinity monitoring on Kish Island, Persian Gulf. The priority...
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Membrane-SPME the best 'green' sample preparation technique for the gas chromatographic determination polar organic pollutants in polar media
PublicationOne of the most popular technique for sample preparation, which fulfill requirements of green analytical chemistry, is solid phase microextraction (SPME). Because of the undoubted advantages of SPME technique, solvent-free character of the extraction process and the enormous potential in analytical practice, a series of studies has been undertaken to develop new technical solutions, where improving the sensitivity and the extraction...
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Specificity of automatic control of micro-turbines (steam or gas -driven and expanders) in dispersed generation system of heat and electric power
PublicationThis paper presents specific problems of automatic control of steam micro-turbines and expanders intended for the dispersed, combined generating of heat and electric power. The investigations concern ensurance of certainty of energy supply and its required quality.
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Experimental investigation of performance and emission characteristics of a miniature gas turbine supplied by blends of kerosene and waste tyre pyrolysis oil
PublicationFossil fuels are non-renewable sources of energy that could be depleted in the near future, giving rise to amajor energy crisis. Scientists from all over the world are working on new technologies to produce fuelnot only from renewable sources but also from waste. This article is concerned with: (i) waste tyremanagement by means of the pyrolysis process, (ii) investigation of physico-chemical parameters ofwaste tyre pyrolysis oil...
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Feasibility Study GaN Transistors Application in the Novel Split-Coils Inductive Power Transfer System with T-Type Inverter
PublicationA promising solution for inductive power transfer and wireless charging is presented on the basis of a single-phase three-level T-type Neutral Point Clamped GaN-based inverter with two coupled transmitting coils. The article focuses on the feasibility study of GaN transistor application in the wireless power transfer system based on the T-type inverter on the primary side. An analysis of power losses in the main components of the...
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Monolithic capsule phase microextraction prior to gas chromatography-mass spectrometry for the determination of organochlorine pesticides in environmental water samples
PublicationIn this study, a capsule phase microextraction (CPME) protocol followed by gas chromatography-mass spectrometry is proposed for the accurate and sensitive monitoring of organochlorine pesticides (OCPs) in environmental water samples. Different monolithic sol–gel encapsulated sorbents were compared and monolithic sol–gel poly(ethylene glycol)-based sorbent incorporated into porous microextraction capsules resulted in the highest...
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Monitoring the gas turbine start-up phase on the platform using a hierarchical model based on Multi-Layer Perceptron networks
PublicationVery often, the operation of diagnostic systems is related to the evaluation of process functionality, where the diagnostics is carried out using reference models prepared on the basis of the process description in the nominal state. The main goal of the work is to develop a hierarchical gas turbine reference model for the estimation of start-up parameters based on multi-layer perceptron neural networks. A functional decomposition...
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Evaluation of Gas Chromatography Stationary Phases Based on Morpholinium Ionic Liquids by McReynolds Constants and Activity Coefficients at Infinite Dilution
PublicationIn this work, four ionic liquids (ILs) based on the N-alkyl-N-methylmorpholinium cation ([Mor1,R], in which R = 2, 4, 8, or 10) and bis (trifluoromethanesulfonyl)imide anion were synthesized. Using GLC, a number of parameters describing the sorption properties of the investigated ILs were determined. The values of Kovats indices, McReynolds constants, and activity coefficients at infinite dilution were the basis for the evaluation...
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Reprezentacja map procesów biznesowych Rummlera-Brache'a w języku PMDL na potrzeby agentów monitorujących proces wytwórczy.
PublicationW artykule przedstawiono zastosowanie technologii Web Farming do procesów zarządzania projektami informatycznymi w firmie komputerowej. Proces wytwórczy definiowany jest w formie hierarchicznego zbioru procesów biznesowych opisywanych zgodnie z formalizmemzaproponowanym przez Rummlera-Brache'a. Zbiór ten odwzorowany jest na zapis w języku PMDL, z którego generowany jest kod agentów monitorujących proces wytwórczy.
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Partition coefficients of selected environmentally important volatile organic compounds determined by gas - liquid chromatography with polydimethylsiloxane stationary phase
PublicationPrzedstawiono wartości współczynników podziału (stałych podziału) 14 lotnych związków organicznych istotnych dla stanu środowiska (często oznaczanych w powietrzu w pomieszczeniach zamkniętych) między fazą gazową (N2) a ciekłą (PDMS). Wyznaczano je dwiema technikami (izotermiczną i z liniowo programowanym wzrostem temperatury). Dowiedziono, że istnieje możliwość wyznaczania współczynników podziału techniką LTPRI w oparciu o skalę...
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Deep learning for ultra-fast and high precision screening of energy materials
PublicationSemiconductor materials for energy storage are the core and foundation of modern information society and play important roles in photovoltaic system, integrated circuit, spacecraft technology, lighting applications, and other fields. Unfortunately, due to the long experiment period and high calculation cost, the high-precision band gap (the basic characteristic parameter) of semiconductor is difficult to obtain, which hinders the...
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Organic Agriculture
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Adaptive Positioning Systems Based on Multiple Wireless Interfaces for Industrial IoT in Harsh Manufacturing Environments
PublicationAs the industrial sector is becoming ever more flexible in order to improve productivity, legacy interfaces for industrial applications must evolve to enhance efficiency and must adapt to achieve higher elasticity and reliability in harsh manufacturing environments. The localization of machines, sensors and workers inside the industrial premises is one of such interfaces used by many applications. Current localization-based systems...
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Electrical and noise responses of graphene/AlGaN/GaN field-effect transistor for nitrogen dioxide, teatrahydrofuran, and acetone sensing
Open Research DataThis data set consists of raw and modified data concerning current-voltage characteristics and low-frequency noise spectra measured for graphene/AlGaN/GaN field-effect transistor in the ambiance of selected gases (laboratory air, dry and wet synthetic air, nitrogen dioxide, tetrahydrofuran, and acetone). The data show that sensor responses are enhanced...
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FTIR spectra of gas mixtures from the process of biogas dry reforming using Al2O3/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using AlOOH/1%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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FTIR spectra of gas mixtures from the process of biogas dry reforming using CeO2/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using CeO2/5%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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FTIR spectra of gas mixtures from the process of biogas dry reforming using Al2O3/5%Cu catalyst
Open Research DataThe dataset contains the FTIR spectra collected during the catalytic measurements of dry reforming of biogas (60/40 CH4-CO2) using Al2O3 (TMDAR)/5%Cu nanocatalyst. The specatra were collected every 1 minute from 800C to 500C. Reagent flow was set to 20ml/min.
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Rekonstrukcja światowego rozkładu dochodów na podstawie minimalnej informacji statystycznej
PublicationCelem pracy jest uzyskanie próby ze światowego rozkładu dochodów (WID). Zakładamy, że krajowe rozkłady dochodów są log-logistyczne z jednostkową średnią. Stąd wynika, że takie rozkłady są całkowicie określone przez indeks Giniego. Oceny indeksu Giniego dla 119 krajów w latach 1990-2005uzyskaliśmy z baz danych Deningera-Squire’a, WID2 i innych baz. Wygenerowaliśmy próbę losową z każdego rozkładu i przemnożyliśmy jej wartości przez...
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Price convergence in the EU-an aggregate and disaggregate approach
PublicationThis article examines the price dispersion in the European Union (EU) over 15 years (1990-2005). An extensive overview of the literature offers inconclusive results with the half-lives of price shocks from 2.8 to 282 months. Until now, most of the empirical research has been either micro or macro based. In contrast, we conducted a complex analysis utilizing both aggregate and disaggregate price data. The macro approach is based...
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CERVIX UTERI, Uterine cervix - Female, 36 - Cell image [3010325017236511]
Open Research DataThis is the histopathological image of CERVIX UTERI cell sample obtained in Copernicus Sp z o.o., M. Copernicus Hospital in Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (40x magnification) and saved to DICOM format.
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Jakub Drewnowski dr hab. inż.
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Computational analysis of substituent effects on proton affinity and gas-phase basicity of TEMPO derivatives and their hydrogen bonding interactions with water molecules
PublicationThe study investigates the molecular structure of 2,2,6,6-tetramethylpiperidine-1-oxyl (TEMPO) and its derivatives in the gas phase using B3LYP and M06-2X functional methods. Intermolecular interactions are analyzed using natural bond orbital (NBO) and atoms in molecules (AIM) techniques. NO2-substituted TEMPO displays high reactivity, less stability, and softer properties. The study reveals that the stability of TEMPO derivatives...
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The effect of aeration mode (intermittent vs. continuous) on nutrient removal and greenhouse gas emissions in the wastewater treatment plant of Corleone (Italy)
PublicationThe paper reports the results of an experimental study aimed at comparing two configurations of a full-scale wastewater treatment plant (WWTP): conventional activated sludge (CAS) and oxic-settling-anaerobic process (OSA) with intermittent aeration (IA). A comprehensive monitoring campaign was carried out to assess multiple parameters for comparing the two configurations: carbon and nutrient removal, greenhouse gas emissions, respirometric...
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Comprehensive two dimensional gas chromatography coupled with mass spectrometry as tool for characterization of the main pollutants present in atmospheric air in Gdansk
PublicationNowadays, the technique that is commonly used to identify and quantify the chemical compounds in gas sample is gas chromatography. The separation resolution in gas chromatography can be improved by applying the modulation technique. In this paper present is the most important information regarding the pollutants present in atmospheric air. The areas in which the tests were carried out are one of the largest industrial zones in...
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THE USE OF ULTRAFAST GAS CHROMATOGRAPHY FOR CLASSIFICATION OF PLUM SPIRITS = SPOSÓB WYKORZYSTANIA ULTRASZYBKIEJ CHROMATOGRAFII GAZOWEJ DO KLASYFIKACJI OKOWIT ŚLIWKOWYCH
PublicationStan środowiska ma znaczny wpływ na jakość upraw. W konsekwencji występowanie zanieczyszczeń w powietrzu ma istotny wpływ na jakość żywności. W skutek złego stanu powietrza zewnętrznego i wewnętrznego zmieniają się m.in. walory sensoryczne i zdrowotne niektórych produktów spożywczych. Z tego powodu należy nieustannie monitorować stan środowiska za pomocą m.in. nowoczesnej aparatury analitycznej jakim jest elektroniczny nos. W...
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Thermal decomposition of surface compounds for the generation of small quantities of acetaldehyde. Calibration of a thermal desorption gas chromatography flame ionization detection.
PublicationW pracy opisano sposób wytwarzania niewielkich ilości acetaldehydu w procesie termicznego rozkładu związku powierzchniowego uzyskanego w wyniku chemicznej modyfikacji żelu krzemionkowego.Proces rozkładu prowadzony jest w temperaturze 130-190 stopni Celsjusza.Przedstawiono również sposób syntezy prowadzący do uzyskania odpowiedniego związku powierzchniowego.
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Application of gas chromatography to the study of the kinetics of reactionsin solution. Ring opening reactions for á-lactams studied using internal standard
PublicationW pracy przedstawiono metodę badania kinetyki reakcji otwarcia pierścienia á-laktamu, wykorzystującą technikę chromatografii gazowej. Na podstawie badań kinetyki reakcji w różnych temperaturach wyznaczono wartości energii aktywacji dwóch badanych reakcji. Podstawowym celem pracy było pokazanie możliwości wykorzystania GC w badaniach kinetyki reakcji prowadzonych w mikroskali.
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Inspection of rubber linings operating in flue gas desulphurisation units. Inspekcje wykładzin gumowych w warunkach instalacji odsiarczania spalin.
PublicationPomiary metodą EIS wykładzin gumowych przeprowadzono w warunkach polowych.Stwierdzono, że najlepszym miernikiem jakości powłoki jest pojemność elektryczna powłoki. Sposób wyznaczania zwartości wilgoci w powłoce oparty został na równaniu Brashera-Kingsbury´ego. Wyniki porównano z oznaczeniami wilgoci w wykładzinie metodami niszczącymi przeprowadzonymi w tych samych miejscach co badania elektrochemiczne.
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Diagnostic Analysis of Exhaust Gas with A Quick-Changing Temperature from a Marine Diesel Engine Part II / Two Factor Analysis
PublicationThe article presents a continuation of research carried out to determine the effect of input parameters (changes in engine structure parameters) on selected output parameters (diagnostic measures), based on quickly changing exhaust gas temperature. A method of determining the simultaneous influence of two input factors (the structure parameter and the engine load) on one output factor was presented, as well as an evaluation...
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Beyond the helium buffer: 12C−2 rotational cooling in cold traps with H2 as a partner gas: interaction forces and quantum dynamics
Publicationabstract = { The scattering cross-sections and corresponding rate coefficients for rotationally inelastic collisions of $^{12}$C$_2$^-$ ($^2 \Sigma_g^+$) with H$_2$ ($^1 \Sigma_g^+$) are presented over a broad range of cold-trap temperatures. They have been calculated using quantum scattering theory that employs a new ab initio potential energy surface. The rate coefficients for the inelastic processes in the anionic partner are...
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Characterization of diatomaceous earth coated with nitrated asphaltenes as superior adsorbent for removal of VOCs from gas phase in fixed bed column
PublicationAsphaltenes isolated from bitumen possess unusual adsorption characteristics that can be further enhanced by chemical modifications to promote interactions with VOCs’. Herein, nitrated asphaltenes are used as an active layer coated on a surface of a diatomaceous earth, in order to prepare an efficient adsorbent (AsfNitro). Breakthrough experiments with benzene, pyridine, and 1-nitropropane revealed significant increase in adsorption...
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Process control of air stream deodorization from vapors of VOCs using a gas sensor matrix conducted in the biotrickling filter (BTF)
PublicationThis article presents the validity, advisability and purposefulness of using a gas sensor matrix to monitor air deodorization processes carried out in a peat-perlite-polyurethane foam-packed biotrickling filter. The aim of the conducted research was to control the effectiveness of air stream purification from vapors of hydrophobic compounds, i.e., n-hexane and cyclohexane. The effectiveness of hydrophobic n-hexane and cyclohexane...
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Statistical radii associated with amino acids to determine the contact map: fixing the structure of a type I cohesin domain in theClostridium thermocellumcellulosome
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Activation of the Normal Human Skin Cells by a Portable Dielectric Barrier Discharge-Based Reaction-Discharge System of a Defined Gas Temperature
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Rapid and sensitive determination of acrylamide in potato crisps using reversed-phase direct immersion single drop microextraction-gas chromatography
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Analysis of the biological stability of tap water on the basis of risk analysis and parameters limiting the secondary growth of microorganisms in water distribution systems
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Process Control and Investigation of Oxidation Kinetics of Postoxidative Effluents Using Gas Chromatography with Pulsed Flame Photometric Detection (GC-PFPD)
PublicationThis article presents the results of investigations on the use of headspace analysis and gas chromatography with pulsed flame photometric detection (HSA-GC-PFPD) to evaluate the effectiveness of oxidation of postoxidative effluents from the production of bitumens. Samples of effluents from the bitumen oxidation unit were used in the experiments. In addition, the kinetics of effluent oxidation was also investigated. The content...
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Technical and economical analysis of combined cycles of gas turbine -steam turbine on pipeline compressor stations. Part II - Economic analysis
PublicationW pracy przedstawiono zagadnienie nadbudowy zespołów turbosprężarkowych, znajdujących się na tłoczni gazu ziemnego, odzyskowymi blokami parowymi. W analizie tego przedsięwzięcia wzięto pod uwagę kilka wariantów konfiguracji układu parowego oraz kilka wariantów uwzględniających zmienność obciążenia turbin gazowych napędzających kompresory. Dla układu parowego dobrano wszystkie podstawowe parametry, a następnie wykonano obliczenia...
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Technical and economical analysis of combined cycles of gas turbine - steam turbine on pipeline compressor stations. Part I - Technical analysis
PublicationW pracy przedstawiono zagadnienie nadbudowy zespołów turbosprężarkowych, znajdujących się na tłoczni gazu ziemnego, odzyskowymi blokami parowymi. W analizie tego przedsięwzięcia wzięto pod uwagę kilka wariantów konfiguracji układu parowego oraz kilka wariantów uwzględniających zmienność obciążenia turbin gazowych napędzających kompresory. Dla układu parowego dobrano wszystkie podstawowe parametry, a następnie wykonano obliczenia...
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Technical and economical analysis of combined cycles of gas turbine - steam turbine on pipeline compressor stations. Part II - Economic analysis
PublicationW pracy przedstawiono zagadnienie nadbudowy zespołów turbosprężarkowych, znajdujących się na tłoczni gazu ziemnego, odzyskowymi blokami parowymi. W analizie tego przedsięwzięcia wzięto pod uwagę kilka wariantów konfiguracji układu parowego oraz kilka wariantów uwzględniających zmienność obciążenia turbin gazowych napędzających kompresory. Dla układu parowego dobrano wszystkie podstawowe parametry, a następnie wykonano obliczenia...
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Determination of PCBs in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry -method validation
PublicationOpracowano procedurę oznaczania wybranych analitów z grupy PCB w próbkach osadu dennego z wykorzystaniem techniki przyspieszonej ekstrakcji za pomocą rozpuszczalnika (PLE) w połączeniu z chromatografią gazową z detektorem spektrometrii mas. Opracowana procedura analityczna została wykorzystana do analizy próbek morskiego osadu dennego, które stanowiły przedmiot badań międzylaboratoryjnych organizowanych przez Comité Consultatif...
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Experimental Investigation Of Using Latent Thermal Energy Storage System Comprising Of Magnesium Chloride Hexahydrate (MgCl2.6H2O) With Domestic Gas Heater
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Reducing the number of periodic points in the smooth homotopy class of a self-map of a simply-connected manifold with periodic sequence of Lefschetz numbers
PublicationLet f be a smooth self-map of an m-dimensional (m >3) closed connected and simply-connected manifold such that the sequence of the Lefschetz num- bers of its iterations is periodic. For a fixed natural r we wish to minimize, in the smooth homotopy class, the number of periodic points with periods less than or equal to r. The resulting number is given by a topological invariant J[f] which is defned in combinatorial terms and is...
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Capillary gas chromatography using a -cyclodextrin forenantiomeric separation of methylamphetamine, its precursors andchloro intermediates after optimization of the derivatization reaction
PublicationtThe enantiomeric ratio of methylamphetamine (MAMP) is closely related to the optical activity of precur-sors and reagents used for the synthesis and this knowledge can provide useful information concerningthe origins and synthetic methods used for illicit manufacture. The information can be utilized for reg-ulation of the precursors and investigation of the manufacturing sources but this requires analyticalprocedures to determine...
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On energy, exergy, and environmental aspects of a combined gas-steam cycle for heat and power generation undergoing a process of retrofitting by steam injection
PublicationThe paper presents a study of retrofitting of a combined heat and power (CHP) plant aimed to increase the electric to heating power ratio. The modification would involve diverting part of the steam to the gas turbine, instead of letting it go to the steam turbine, using injection technique into a combustion chamber. Therefore, two potential retrofitting approaches are analyzed: steam injection gas turbine (STIGT) and combined steam...
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Comprehensive determination of flavouring additives and nicotine in e-cigarette refill solutions. Part II: Gas-chromatography–mass spectrometry analysis
PublicationFlavouring compounds are an essential part of e-liquid products for cigarettes. In general, they are regarded as safe for ingestion, but they may have unrecognized risks when they are inhaled. In some cases, manufactures do not currently abide by the Tobacco Products Directive (2014/40/EU) and do not declare the detailed contents of e-liquids on their labels. To help evaluate the health impact of flavouring substances, there is...
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Comparing combined gas tubrine/steam turbine and marine low speed piston engine/steam turbine systems in naval applications
PublicationPorównano układy napędowe okrętowe kombinowane turbina gazowa- turbina parowa oraz spalinowy okrętowy silnik tłokowy wolnoobrotowy - turbina parowa. Porównywano moce oraz zużycie paliwa oraz parametry pary świeżej układu turbiny parowej.