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wszystkich: 547
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Wyniki wyszukiwania dla: BADANIA IN SITU
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Electrophoretic co-deposition of Fe2O3 and Mn1,5Co1,5O4: Processing and oxidation performance of Fe-doped Mn-Co coatings for solid oxide cell interconnects
PublikacjaThe “in-situ” Fe-doping of the manganese cobalt spinel was achieved by electrophoretic co-deposition of Mn1,5Co1,5O4 and Fe2O3 powders followed by a two-step reactive sintering treatment. The effects on the coating properties of two different Fe-doping levels (5 and 10 wt.% respectively) and two different temperatures of the reducing treatment (900 and 1000 °C) are discussed. Samples with Fe-doped coatings demonstrated a lower...
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Ammonia Gas Sensors: Comparison of Solid-State and Optical Methods
PublikacjaHigh precision and fast measurement of gas concentrations is important for both understanding and monitoring various phenomena, from industrial and environmental to medical and scientific applications. This article deals with the recent progress in ammonia detection using in-situ solid-state and optical methods. Due to the continuous progress in material engineering and optoelectronic technologies, these methods are among the most...
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Architecture of ecumenical spaces in public buildings in the 21st century: Links among the architecture of multi-faith spaces, their names, and the functions they serve in Polish airports
PublikacjaThis study explores the architecture and arrangement of prayer spaces in public buildings. It examines whether Polish airports have prayers spaces and whether a correlation exists between the name (e.g., “multi-faith space,” “place of prayer,” and “place of focus”) and design. The study is supported by analyses of ecumenical spaces, which have recently been brought into service andwhere a visible symbiosis exists between their...
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Transformation of bimetallic Ag–Cu thin films into plasmonically active composite nanostructures
PublikacjaFormation of plasmonically active silver, copper and composite silver-copper nanostructures were studied in this paper. Metallic nanostructures were fabricated by thermal disintegration, so called dewetting, of the thin films in an argon atmosphere. The formation process of the nanostructures was in-situ observed by a novel method, based on resistance measurements. The influence of the material and thickness of the initial thin...
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The effective elastic properties of human trabecular bone may be approximated using micro-finite element analyses of embedded volume elements.
PublikacjaBoundary conditions (BCs) and sample size affect the measured elastic properties of cancellous bone. Samples too small to be representative appear stiffer under kinematic uniform BCs (KUBCs) than under periodicity-compatible mixed uniform BCs (PMUBCs). To avoid those effects, we propose to determine the effective properties of trabecular bone using an embedded configuration. Cubic samples of various sizes (2.63, 5.29, 7.96, 10.58...
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Monitoring system of the road embankment
PublikacjaThe paper presents the monitoring system of the embankment supported on concrete columns and overlaid by a load transfer platform (LTP) with the embedded steel grid. This field investigation was to study the complex inter-action between the columns, the LTP layer, and steel reinforcement via full-scale in situ measurements during erection of the embankment. The study was focused on the behaviour of steel reinforcement and the behaviour...
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Immunoanalityka – użyteczne podejście analityczne w badaniach środowiska
PublikacjaWażnym krokiem w rozwoju bezpośrednich metodyk analitycznych było opracowanie technik immunoanalitycznych. Początkowo znalazły one zastosowanie praktyczne w analityce medycznej a później także w analityce środowiskowej. Dzięki temu możliwe jest ilościowe oznaczenie stosunkowo szerokiego spektrum ksenobiotyków w próbkach charakteryzujących się złożonym składem matrycy bez praco- i czasochłonnego etapu przygotowania tych próbek do...
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Ocena nośności oraz naprawy zarysowanych bloków oporowych wiaduktu sprężonego.
PublikacjaW trakcie prac wykończeniowych na nowym wiadukcie sprężonym zauważono, wzbudzające niepokój, rysy w okolicach bloków oporowych kabli sprężających. Przedstawiono metodykę i wyniki badań nad określaniem nośności zakotwień oraz sposób naprawy występujących tam rys. Od strony teoretycznej przeprowadzono numeryczne symulacje wytężenia bloków stref zakotwień. Wyniki teoretyczne uzupełniono badaniami obiektu in situ. Dla określenia...
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Zastosowanie mieszania wgłębnego i iniekcji strumieniowej do wzmocnienia podłoża pod budynkiem basenu.
PublikacjaPrzedstawiono jeden z pierwszych przykładów zastosowania w Europie nowoczesnej technologii wgłębnego mieszania gruntu na mokro (ang. wet Deep Soil Mixing) w celu posadowienia budynku basenu na uwarstwionym podłożu zawierającym grunt organiczny. Technologia DSM, wprowadzona w Polsce przez firmę Keller, polega na mechanicznym mieszaniu in situ gruntu z zaczynem cementowym i pozwala na formowanie w gruncie kolumn z cementogruntu w...
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Wykładnicze równanie Arrheniusa jako funkcja dojrzałości twardniejącego betonu
PublikacjaPoprawne określenie funkcji dojrzałości dla mieszanki betonowej warunkuje powodzenie szacowania wytrzymałości na ściskanie na bazie pomiarów temperatury in situ. W artykule omówiono zastosowanie równania Arrheniusa do opisu funkcji dojrzewania twardniejącego betonu. Szczególną uwagę zwrócono na zależności szybkości zachodzenia reakcji w odmiennych warunkach temperaturowych. Przedstawiono wyniki własnych badań na kostkach zaprawy...
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Dynamic Electrochemical Impedance Spectroscopy (DEIS) as a Tool for Analyzing Surface Oxidation Processes on Boron-Doped Diamond Electrodes
PublikacjaSurface oxidation processes play a key role in understanding electrochemical properties of boron-doped diamond (BDD) electrodes. The type of surface termination groups, which create the potential window of electrolytic water stability or hydrophobicity, influences such properties. In this study the kinetics of oxidation process under anodic polarization were studied in situ by means of Dynamic Electrochemical Impedance Spectroscopy...
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MONITORING SYSTEM OF THE ROAD EMBANKMENT
PublikacjaThe paper presents the analysis of the monitoring system of the embankment supported on concrete columns and overlaid by a load transfer platform with the embedded steel grid. This field investigation was to study the complex interaction among the columns, the load transfer platform layer, and steel grid via in situ measurements during erection and live loading of the embankment. The study was focused on the behaviour of steel...
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3D polypyrrole structures as a sensing material for glucose detection
PublikacjaIn this work, 3D polypyrrole (PPy) structures as material for glucose detection is proposed. Polypyrrole was electrochemically polymerized on platinum screen-printed electrode from an aqueous solution of lithium perchlorate and pyrrole. The growth mechanism of such PPy structures was studied by ex-situ scanning electron microscopy. Preliminary studies show that studied here PPy film is a good candidate as a sensing material for...
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Geospatial Coverage and Signal Quality Measurements of Terrestrial DAB+ Network in Northern Poland
PublikacjaModern signal coverage maps are prepared based on industry-standard radio propagation models, which take into account a number of parameters, including: type of antenna, distance from the transmitter, type of terrain, etc. However, such simulations are prone to location-specific inaccuracies, and should be verified with in-situ measurements. This paper presents results of a field test of a terrestrial DAB+ (Digital Audio Broadcasting...
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Study of various machine learning approaches for Sentinel-2 derived bathymetry
PublikacjaIn recent years precise and up-to-date information regarding seabed depth has become more and more important for companies and institutions that operate on coastlines. While direct, in-situ measurements are performed regularly, they are expensive, time-consuming and impractical to be performed in short time intervals. At the same time, an ever-increasing amount of satellite imaging data becomes available. With these images, it...
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Modelowanie wymiany wody w zbiornikach hodowlanych przy użyciu zmodyfikowanego modelu tłokowego na przykładzie basenów hodowlanych dla fok
PublikacjaNiniejszy artykuł opisuje sposób prostego modelowania wymiany wody w basenach hodowlanych fokarium Stacji Morskiej Instytutu Oceanografii Uniwersytetu Gdańskiego. W celu rozpoznania warunków wymiany wody oraz udziału stref zastoiskowych w basenach posłużono się dwiema uzupełniającymi się metodami. Były to badania traserowe z wykorzystaniem znacznika fluororescencyjnego oraz komputerowe obliczenia rozkładu linii prądu z użyciem...
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Oil removal from polluted soil by washing with surfactants solutions in dynamic conditions
PublikacjaFor washing of the oil from polluted soil surfactants solutions were applied. In a research a nonionic synthetic surfactant - polyoxyethylene ether of synthetic fatty alcohol (Rokanol NL6), rhamnolipid biosurfactant JBR 425 (Jeneil Biosurfactant Co. LLC) and their mixtures were used. Results of oil removal from peat soil and sand with mixtures of surfactants solutions at concentration 0,5 g/dm...
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Wykorzystanie techniki ekstrakcji do fazy stałej w procedurach przygotowania próbek do analizy chromatograficznej
PublikacjaKażdą procedurę analityczną można potraktować jako łańcuch złożony z ogniw, które obrazują poszczególne czynności i operacje. Zgodnie ze znanym przysłowiem, które mówi, że ''Łańcuch jest tak mocny jak jego najsłabsze ogniwo'', także i w przypadku procedur analitycznych szczególną uwagę należy zwrócić na te czynności i operacje (wykonywane zarówno w terenie, czyli in situ, jak i w laboratorium), które wymagają szczególnej troski...
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Rola związków znaczonych izotopowo w analityce środowiskowej
PublikacjaKażdą procedurę analityczną można potraktować jako łańcuch złożony z ogniw, które obrazują poszczególne czynności i operacje. Zgodnie ze znanym przysłowiem, które mówi, że ''Łańcuch jest tak mocny jak jego najsłabsze ogniwo'', także i w przypadku procedur analitycznych szczególną uwagę należy zwrócić na te czynności i operacje (wykonywane zarówno w terenie, czyli in situ, jak i w laboratorium), które wymagają szczególnej troski...
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Multimedia services applied to noise and hearing monitoring and measuring
PublikacjaThe goal of this chapter is to show a research study related to processing of data acquired by the multimedia services engineered at the multimedia systems department (MSD) of the Gdansk University of Technology. This concerns a survey on noise threat employing the multimedia noise monitoring system (MNMS) and hearing tests performed by the "I can hear. . . " system. The obtained results of the noise measurements revealed that...
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Release and Transport of Toxic, Mobile Organic Compounds (Formaldehyde and Phenols) on an Arctic Glacier
PublikacjaAs a result of current deglaciation, the chemical cycles of many compounds, including toxic formaldehyde and phenols, are changing. However, the processes by which these chemicals are released have yet to be studied in situ. Here, we quantify fluxes of HCHO and phenols in a glacial catchment within one summer season, obtaining a net release from the glacier of 0.106 · 106 g formaldehyde and 0.255 · 106 g phenols, which can be interpreted...
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Tome-lapse X-ray tomography imaging of flow patterns in versatile silo model
PublikacjaThe paper introduces a new versatile silo model that was especially designed for in situ X-ray tomography studies of silo discharge for various flow conditions, namely concentric and eccentric. The presented work focuses on organic granular materials where low fraction of short-grain white rice is mixed with spheroidal sorghum particles. The high-quality tomography images combined with adequate image processing strategy allows...
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Dynamics of the small-span railway bridge under moving loads
PublikacjaThe paper presents the results of dynamic analysis of the small-span railway bridge, subjected to an action of moving trains. Numerical simulations were performed using three different load models: series of moving forces, series of moving single-mass and double-mass oscillators. The parameters of the vehicle were taken from the existing EN57 train. The parameters of the bridge were taken from the existing steel span of 10,24 m...
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Palladium versus Platinum: The Metal in the Catalytic Center of a Molecular Photocatalyst Determines the Mechanism of the Hydrogen Production with Visible Light
PublikacjaTo develop highly efficient molecular photocatalysts for visible light-driven hydrogen production, a thorough understanding of the photophysical and chemical processes in the photocatalyst is of vital importance. In this context, in situ X-ray absorption spectroscopic (XAS) investigations show that the nature of the catalytically active metal center in a (N^N)MCl2 (M=Pd or Pt) coordination sphere has a significant impact on the...
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Thermal and Mechanical Properties of Microporous Polyurethanes Modified with Reduced Graphene Oxide
PublikacjaMicroporous polyurethanes (MPU) were modified by adding 0.25%–1.25 wt% of reduced graphene oxide (RGO). The materials were prepared without solvent via in situ polymerization. From a technological point of view, it is very important to obtain functional materials by using reacting compounds only. The thermal characteristics of obtained MPU were investigated using TGA, DSC, and DMA techniques. In comparison to nonmodified microporous...
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Sulfate‐reducing bacteria‐assisted hydrogen‐induced stress cracking of 2205 duplex stainless steels
PublikacjaThe paper presents the results of a laboratory investigation of the microbiologically assisted hydrogen‐induced stress cracking (HISC) of 2,205 duplex stainless steel (DSS). The testing of susceptibility toward HISC was performed with two different methods. Precharged in sulfate‐reducing bacteria (SRB), inoculated medium samples were subjected to slow strain‐rate testing in artificial seawater. In situ constant load tests were...
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Diagnostyka i wyjaśnienie aktualnego stanu 40-letniego wiaduktu kolejowego
PublikacjaPraca zawiera krótką ocenę stanu technicznego, opis przeprowadzonych badań nieniszczących in-situ oraz wykonanych modeli MES, służących do przeprowadzenia analiz na poziomie globalnym jak i lokalnym. Przedstawiono i omówiono wyniki analiz numerycznych, wykorzystanych do oceny stanu konstrukcji i mających na celu rozwiązanie sformułowanych problemów badawczych. Wykonane obliczenia na poziomie globalnym z uszczegółowieniem w obrębie...
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A Perspective on Missing Aspects in Ongoing Purification Research towards Melissa officinalis
PublikacjaMelissa officinalis L. is a medicinal plant used worldwide for ethno-medical purposes. Today, it is grown everywhere; while it is known to originate from Southern Europe, it is now found around the world, from North America to New Zealand. The biological properties of this medicinal plant are mainly related to its high content of phytochemical (bioactive) compounds, such as flavonoids, polyphenolic compounds, aldehydes, glycosides...
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Understainding solid-phase microextraction: key factors influencing the extraction process and trends in improving the technique
PublikacjaAnalytical chemists are faced with the daunting challenges of accurately monitoring the state of the environment and the processes taking place in it and of determining an enormous range of analytes often present in trace and ultratrace amounts in sample matrixes with complex or variable compositions. Further challenges are presented by the need to introduce new methodologies into current analytical practice and equipment to comply...
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Investigation of H2:CH4 plasma composition by means of spatially resolved optical spectroscopy
PublikacjaThe system based on spatially resolved optical emission spectroscopy dedicated for in situ diagnostics of plasma assisted CVD processes is presented in this paper. Measurement system coupled with chemical vapour deposition chamber by dedicated fiber-optic paths enables investigation of spatial distribution of species densities (Hx, H+, CH, CH+) during chemical vapour deposition process. Experiments were performed for a various...
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Koherentna tomografia optyczna wykorzystująca źródło o przestrajalnej długości fali.
PublikacjaOptyczne metody pomiarowe odgrywają w ostatnich latach coraz większą rolę w badaniach i diagnostyce medycznej. Mają one szereg zalet, do których zaliczyć można odporność na promieniowanie elektromagnetyczne, bezinwazyjność,bezpieczeństwo pomiaru oraz wysoką rozdzielczość. Jedną z najważniejszych technik stosowanych w diagnostyce medycznej jest koherentna tomografia optyczna (OCT). Jest to wysokorozdzielcza metoda obrazowania...
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Ultrahigh-resolution detection techniques for biomedical applications of optical coherent tomography.
PublikacjaOptyczne metody pomiarowe odgrywają w ostatnich latach coraz większą rolę w badaniach i diagnostyce medycznej. Mają one szereg zalet, do których zaliczyć można odporność na promieniowanie elektromagnetyczne, bezinwazyjność, bezpieczeństwo pomiaru oraz wysoką rozdzielczość. Jedną z najważniejszych technik stosowanych w diagnostyce medycznej jest koherentna tomografia optyczna (OCT). Jest to wysokorozdzielcza metoda obrazowania wewnętrznych...
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Enhanced Electrochemical Performance of MnCo1.5Fe0.5O4Spinel for Oxygen Evolution Reaction through Heat Treatment
PublikacjaMnCo1.5Fe0.5O4 spinel oxide was synthesized using the sol−gel technique, followed by heat treatment at various temperatures (400, 600, 800, and 1000 °C). The prepared materials were examined as anode electrocatalysts for watersplitting systems in alkaline environments. Solid-state characterization methods, such as powder X-ray diffraction and X-ray absorption spectroscopy (XAS), were used to analyze the materials’ crystallographic...
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Structural and catalytic properties of ceria layers doped with transition metals for SOFCs fueled by biogas
PublikacjaThe aim of this paper was to investigate an influence of the nanocrystalline Ce0.8A0.2O2-δ (A = Mn, Fe, Co, Ni, Cu) materials on the direct internal reforming of biogas in SOFC. Structural analysis of fabricated compounds has been done. An in-situ analysis of a composition of outlet gases from operating SOFC was performed using FTIR spectroscopy with simultaneous electrical tests. It was found out, that type of dopant strongly...
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Impedance monitoring of fuel cell stacks
PublikacjaThis paper presents an innovative, electrochemical impedance method for monitoring of electrochemical behaviour of a multi-cell, direct methanol fuel cell (DMFC) device. This method not only provides classical voltage changes at successive cells but also allows their detailed impedance behaviour to be presented. Impedance characteristics of individual cells within a fuel cell stack (depending on actual operating conditions) are...
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Grafting and reactive extrusion technologies for compatibilization of ground tyre rubber composites: Compounding, properties, and applications
PublikacjaChemical modification of ground tyre rubber (GTR) to compatibilize it with the matrix is a well-known approach. Based on our recent review of the surface etching methods used in GTR modification, the purpose of the current work is to take a deeper look into more advanced methods such as grafting and reactive extrusion. While grafting is more efficient in achieving compatibility, however, it usually involves multi-step synthesis...
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Design and implementation of an illumination system to mimic skyglow at ecosystem level in a large‐scale lake enclosure facility
PublikacjaLight pollution is an environmental stressor of global extent that is growing exponentially in area and intensity. Artificial skyglow, a form of light pollution with large range, is hypothesized to have environmental impact at ecosystem level. However, testing the impact of skyglow at large scales and in a controlled fashion under in situ conditions has remained elusive so far. Here we present the first experimental setup to mimic...
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Finite element modelling of a historic church structure in the context of a masonry damage analysis
PublikacjaThe paper includes a case study of modelling a real historic church using the finite element method (FEM) based on laser scans of its geometry. The main goal of the study was the analysis of the causes of cracking and crushing of masonry walls. An FEM model of the structure has been defined in ABAQUS. A non-linear dynamic explicit analysis with material model including damage plasticity has been performed. A homogenization procedure...
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On the current state of dovetail wall-corner joints in wooden Greek Catholic churches in Polish Subcarpathia with structural and sensitivity analyses
PublikacjaThis paper describes the current condition of some dovetail joints which form the wall corners of two Greek Catholic churches of wooden construction in Polish Subcarpathia. It also gives the historical background of the sacral architecture of that region. The two structures, which represent the same type of log corner joints are situated in Chotylub and Cewków. The buildings were examined e.g. for damage, wood moisture content,...
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Short and Long Term Measurements in Assessment of FRP Composite Footbridge Behavior
PublikacjaThe paper presents application of different sensors for the purpose of short and long term measurements, as well as a structural health monitoring (SHM) system to assess the behavior of a novel fiber reinforced plastics (FRP) composite footbridge. The aim is to present a thorough and concise description of these sensors networks and results gathered with their aid during in situ measurement of strains, displacements, and vibrations,...
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Detection of Objects Buried in the Sea Bottom with the Use of Parametric Echosounder
PublikacjaThe paper contains results of a in situ research main task of which was to detect objects buried, partially or completely, in the sea bottom. Object detecting technologies employing acoustic wave sources based on nonlinear interaction of elastic waves require application of parametric sound sources. Detection of objects buried in the sea bottom with the use of classic hydroacoustic devices such as the sidescan sonar or multibeam...
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Localized impedance measurements of AA2024 and AA2024-T3 performed by means of AFM in contact mode
PublikacjaPurpose: The purpose of this paper is to present the results of an atomic force microscopy (AFM) based approach to local impedance spectroscopy (LIS) measurement performed on AA2024 and AA2024-T3 aluminium alloys. Design/methodology/approach: AFM-LIS measurements were performed ex-situ without the electrolyte environment, so in fact the electrical not electrochemical impedance was obtained. Findings: Relative local impedance values...
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Pressure-induced phase transitions in LnTe (Ln=La, Gd, Ho, Yb) and AmTe
PublikacjaThe structural behaviour under compression of different lanthanide (La, Gd, Ho, Yb) and actinide (Am) monochalcogenides is studied by means of in situ high-pressure x-ray diffraction. All the investigated compounds crystallize at ambient conditions within a cubic (B1) NaCl-type structure but show different behaviours at high pressures. LaTe and AmTe undergo B1 to B2 (CsCl-type structure) phase transitions, starting at 9 GPa and...
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Passive sampling as a tool for obtaining reliable analyticalinformation in environmental quality monitoring
PublikacjaSpośród technik pobierania próbek analitów technika dozymetrii pasywnej wydaje się być interesującą alternatywą w stosunku do powszechnie stosowanych technik dynamicznych. Dozymetria pasywna łączy w sobie etap pobierania próbki z etapem izolacji i wzbogacania analitów, które są zatrzymywane w odpowiednim medium zatrzymującym. Prowadzi to do znacznego uproszczenia operacji analitycznych wykonywanych in situ. W odróżnieniu od aktywnych...
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Chapter 8 – Active Sampling of Air
PublikacjaThis chapter reviews the literature information on analytical techniques and laboratory equipment used for active sampling of air (atmospheric and indoor) in regular monitoring research. It describes popular analytical devices applied for sample collection using various types of polymeric bags, e.g. Tedlar bags, Teflon or Nafion bags, and/or stainless steel vacuum containers. It reviews literature data about the application of...
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Encapsulation of Cs3Bi2Br9 perovskite photocatalyst with polythiophene for prolonged activity in oxidizing and humid environment
PublikacjaDespite their growing popularity in modern technology, halide perovskites suffer from susceptibility to oxidation, limiting their applications. Our aim was to enhance Cs3Bi2Br9 perovskite's performance in humid environments through polythiophene encapsulation. This extended its lifespan while preserving photocatalytic abilities, as demonstrated in toluene decomposition experiments. We confirmed the stability of Cs3Bi2Br9 encapsulated...
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A dynamic vehicle-bridge model based on the modal identification results of an existing EN57 train and bridge spans with non-ballasted tracks
PublikacjaThis paper addresses the methodology of the bridge-vehicle dynamic model definition based on the free response measurements of an existing train and existing bridge spans. In the case of the railway vehicle, the methodology uses the impulse excitations of a single car by means of the wedge method. In the case of the bridge spans, free responses are collected after the passages of trains. The global modal parameters (frequencies...
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Reactive extrusion of biodegradable aliphatic polyesters in the presence of free-radical-initiators: A review
PublikacjaNowadays, growing attention is being paid to the environment and sustainability, what fully justified research works focused on modification of biodegradable polymers and their composites. In this field of research reactive extrusion seems to be the most promising approach, which fits well to sustainable development strategy. In In the present work, the in-situ modification of biodegradable aliphatic polyesters and the compatibilization...
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Shear resistance of low height precast concrete lintels
PublikacjaThe scope of the paper is to investigate analytically and determine experimentally the shear resistance of low height reinforced precast concrete lintels. The chosen procedures included in national and international standards applied for the design of structural concrete elements to an estimation of shear behaviour of reinforced concrete elements are described. The characteristic and designed shear strength of precast concrete...
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Investigation of praseodymium and samarium co-doped ceria as an anode catalyst for DIR-SOFC fueled by biogas
PublikacjaThe Pr and Sm co-doped ceria (with up to 20 mol.% of dopants) compounds were examined as catalytic layers on the surface of SOFC anode directly fed by biogas to increase a lifetime and the efficiency of commercially available DIR-SOFC without the usage of an external reformer. The XRD, SEM and EDX methods were used to investigate the structural properties and the composition of fabricated materials. Furthermore, the electrical...