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Enhanced acceptor concentration, proton conductivity, and hydration in multicomponent rare‐earth ortho‐niobates
PublikacjaThe structural properties of (La0.2Nd0.2Sm0.2Gd0.2Eu0.2)1−xCaxNbO4−δ (x = 0–0.05) series have been studied by X-ray powder diffraction at room temperature. The thermal properties were investigated using thermogravimetry, from which the concentration of proton defects was determined. Additionally, dilatometry studies were carried out, from which the thermal expansion coefficients and the phase transition temperature between low-...
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Preparation, characterization, and manufacturing of new polymeric materials for 3D printing for medical applications
PublikacjaThis work concerns the synthesis, formation, and characteristics of new filaments for 3D printing in FDM™/FFF technology for medical purposes. Two types of filaments were developed, i.e. degradable polyurethane and biodegradable polylactide-starch. The influence of the 3D printing process on selected filament properties was investigated. A detailed analysis of the filament formation process by the extrusion method was carried out,...
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Development of novel (BiO)2OHCl/BiOBr enriched with boron doped-carbon nanowalls for photocatalytic cytostatic drug degradation: Assessing photocatalytic process utilization in environmental condition
PublikacjaIn this work, a series of novel (BiO)2OHCl/BiOBr-x%B:DGNW (x = 0%, 1%, 1.5%, 2%) composites with different content of boron-doped diamond/graphene nanowalls (B:DGNW) were fabricated by simple solvothermal synthesis. A boron-doped diamond/graphene nanowalls (B:DGNW) were prepared by CVD method. A series of analyses: XRD, XPS, SEM, and TEM showed that the photocatalyst (BiO)2OHCl/BiOBr-x%B:DGNW with a “flower-like” morphology was...
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Development of Intelligent Road Signs with V2X Interface for Adaptive Traffic Controlling
PublikacjaThe objective of this paper is to present a practical project of intelligent road signs, under which a series of new products for the regulation of traffic is being created. The engineering part of the project, described in this paper, was preceded by a series of experimental studies, the results of which were described in another paper accepted for publication at the MTS-ITS conference 2019, entitled "Comparative study on the effectiveness...
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World Politics
Kursy OnlineThe course aims to familiarize stdnets with the most important theories of the international relations. This instrument will enable them to understand a series of case studies that will be presented starting with the first wordl war and going until today. The case studies will include the main aspects of the Cold War period, the role of USA and Soviet Union in shaping the international relations according to a political and ideological...
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Hydrodynamic Pressure Field of a Ship on Shallow Water
PublikacjaResults of calculations of the hydrodynamic pressure field around the ship were obtained by application of the boundary element method. Hydrodynamic field was calculated for a Polish Navy’s tugboat and transport ship using a program called SHiPP and compared with measurements of the field taken on river near Swinoujscie for two identical tugs H-4 and H-10. Next, a series of HPF calculations was carried out on planes situated at...
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A method for counting people attending large public events
PublikacjaThe algorithm for people counting in crowded scenes, based on the idea of virtual gate which uses optical flow method is presented. The concept and practical application of the developed algorithm under real conditions is depicted. The aim of the work is to estimate the number of people passing through entrances of a large sport hall. The most challenging problem was the unpredicted behavior of people while entering the building....
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KTaO3-based nanocomposites for air treatment
PublikacjaThe advantage is that photocatalytic methods allow removing VOCs, NOx, SO2, deodorants, and microorganisms at the same system. The new third generation of photoactive materials activated by low powered and low cost irradiation sources (such as LEDs or black fluorescent UV lamps) can be used as photocatalysts in air purification systems. A series of single semiconductors and their nanocomposites combination were prepared using hydrothermal...
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Problems and Solutions of Software Design in Scrum Projects
PublikacjaThe aim of the paper is to identify the problems and solutions of the software design in Scrum project as well as to analyze the effectiveness of the solutions. Through a series of workshops with 4 experts from IT industry and academia we have identified 52 problems and 99 unique solutions. In this paper we present a list of 10 common problems and 5 solutions for each problem selected by the number of sources. The effectiveness...
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Application of virtual gate for counting people participating in large public events
PublikacjaThe concept and practical application of the developed algorithm forpeople counting in crowded scene is presented. The aim of the work is to estimatethe number of people passing towards entrances of a large sport hall. Thedetails of implemented the Virtual Gate algorithm are presented. The video signalfrom the camera installed in the building constituted the input for the algorithm.The most challenging problem was the unpredicted...
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Intelligent equalizer solution employing music genre and the room characteristics analysis
PublikacjaThe paper presents an intelligent equalizer solution based on room acoustic conditions and music genre analysis. A series of acoustic characteristic measurements are performed for checking the concept proposed. White noise (reference signal) and audio excerpts belonging to six music genres are utilized as excitation signals in measurements. This results in registration of frequency responses of rooms and reverberation times. Signals...
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REWIZJA PRZYBLIŻONYCH METOD OBLICZANIA OPORU CAŁKOWITEGO KADŁUBA W OPARCIU O BADANIA MODELOWE WYBRANEGO JACHTU ŻAGLOWEGO
PublikacjaRewizja opiera się na weryfikacji wybranych przybliżonych metod prognozowania oporu całkowitego gołego kadłuba opracowanych w wyniki badań systematycznej serii kadłubów jachtów żaglowych w latach od 1973 do 2010 znanych, jako The Delft Systematic Yacht Hull Series (DSYHS). Zademonstrowano wyniki otrzymane w oparciu o wzory przybliżone (Metoda Delft), obliczenia numeryczne (CFD) i badania modelowe dla wybranego jachtu żaglowego...
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A Three-Step Approach to Estimation of Reduction Potentials of Natural Mixtures of Antioxidants Based on DPPH Test; Illustration for Catechins and Cocoa
PublikacjaThe aim of this study is to propose a methodology to assess electrochemical properties of complex mixtures of antioxidants, such as plant extracts, based on the results of simple and popular DPPH test. The first, most difficult step, involves determinations of standard reduction potentials (E0) for the series of purified compounds (here catechins). The next step is the calculation of stoichiometric values (n10) based on the results...
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Design, synthesis, and molecular docking of new 5-HT reuptake inhibitors based on modified 1,2-dihydrocyclopenta[b] indol-3(4H)-one scaffold
PublikacjaA new group of serotonin reuptake inhibitors containing 1,2-dihydrocyclopenta[b]indol-3(4H)-one scaffoldwas synthesized, starting from indole 5-((1H-indol-3-yl)(1,3-dioxane-4,6-diones as a key intermediates. Following three transformations including intramolecular cyclization and formation of imines, a series of new ligand for human serotonin transporter was obtained. The ability of these ligands to inhibit human TS3 serotonin transporter...
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Synthesis and biological activity of novel ester derivatives of N3-(4-metoxyfumaroyl)-(S)-2,3-diaminopropanoic acid containing amide and keto function as inhibitors of glucosamine-6-phosphate synthase
PublikacjaA short series of novel ester derivatives of N3-4-methoxyfumaroyl-(S)-2,3-diaminopropanoic acid (FMDP) containing amido or keto functions have been designed and synthesized. Their antifungal activity and inhibitory properties toward fungal glucosamine-6-phosphate synthase has also been evaluated. The obtained compounds 11-13 and 15-17 demonstrated good antifunga activity against Candida albicans. Compounds 11-13 displayed also...
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Applying Fuzzy Logic of Expert Knowledge for Accurate Predictive Algorithms of Customer Traffic Flows in Theme Parks
PublikacjaThis study analyzes two forecasting models based on the application of fuzzy logic and evaluates their effectiveness in predicting visitor expenditure and length of stay at a popular theme park. The forecasting models are based on a set of more than 600 decision rules constructed in the form of a complex series of IF-THEN statements. These algorithms store expert knowledge. A descriptive instrument that records the individual visitor's...
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Investigation on water infiltration and water content changes in a large-scale experimental test dike
PublikacjaThe paper presents result of series of experiments made within the DREDGDIKES project, performed on a test dike built from composite soil. The composite is produced by mixing fly ash (by-product of energetics) with dredged material (sand) taken from the mouth of The Vistula river. The test dike, located near Gdansk in Poland, was subjected to hydraulic load in several flooding time scenarios and the unsaturated unsteady flow was...
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Characterization of Corrosion-Induced Fracture in Reinforced Concrete Beams Using Electrical Potential, Ultrasound and Low-Frequency Vibration
PublikacjaThe paper deals with the non-destructive experimental testing of the reinforced concrete beams under progressive corrosion. A series of experiments using electrical potential, ultrasound and low-frequency vibrations techniques are reported. Electrical potential and natural frequencies were used to characterise and monitor the corrosion process at its initial state. The P-wave velocity measurements were proved to be effective in...
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Bezpieczeństwo transferu zestrukturalizowanych plików xml w sieci grid w oparciu o usługi web service poprzez protokół soap
PublikacjaNiezależny protokół SOAP (ang. Simple Object Access Protocol) działający głównie ponad protokołem HTTP (inne protokoły transportowe to np. MSMQ, MQ Series, SMTP lub TCP/IP) posiada na dzień dzisiejszy wiele rozwiązań dotyczących bezpieczeństwa transferu zestrukturalizowanych plików XML (ang. Extensible Markup Language). W rozdziale zaprezentowano sposoby zapobiegania nieautoryzowanym dostępom do danych przesyłanych w sieci grid...
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Heterogeneous distribution of surface electrochemical activity in polycrystalline highly boron-doped diamond electrodes under deep anodic polarization
PublikacjaThe surface homogeneity of boron-doped diamond electrodes is variable and depends on anodic polarization conditions. The differentiation factor is the gradual and localized change in surface termination. A series of measurements under different polarization conditions was performed in order to investigate the scale of this effect. Nanoscale impedance microscopy (NIM) revealed large variation of surface resistance in individual...
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MONITORING OF PERMANENT GPS STATIONS AT THE SUDETY MOUNTAINS
PublikacjaThe aim of this paper is to show time-dependent baseline variation between GPS stations situated in South-East Poland. This study was based on daily data analysis of selected GPS stations: WROC, GOPE, MOPI, KRAW and KATO. The start date of the analysis is linked at every station with the beginning of its operation and the closing date of the operation is in 2006. The multiresolution signal decomposition method has been used to...
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Teoria zbiorów rozmytych w zarządzaniu ryzykiem jako utylitarne narzędzie systemu zarządzania jakością
PublikacjaDziałalność przedsiębiorstwa wiąże się z potrzebą analizowania ryzyka oddziałującego na procesy firmy. Norma PN-EN ISO 9001:2015 dokonuje identyfikacji czynników ryzyka i ich wpływu na jakość wyrobu. W szacowaniu ryzyka punktowe oceny wyrażające subiektywne opinie zastępowane są coraz częściej formalnym zapisem niepewności. Artykuł ukazuje zastosowanie rozmytego systemu wnioskującego w procesie zarządzania ryzykiem, umożliwiającego...
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Prognozowanie ostrzegawcze w małej firmie
PublikacjaW artykule pokazano możliwości zastosowania prostych metod prognostycznych do ostrzegania w małej firmie przed niekorzystnymi zjawiskami. Przedmiotem badań jest sprzedaż, a ze względu na występowanie w szeregu czasowym sezonowości, w celu wyznaczenia sygnałów ostrzegawczych dokonano porównań trendów prognozowanych i rzeczywistych w okresach jednoimiennych za pomocą pierwszych różnic. Do prognozowania sprzedaży wykorzystano proste...
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The assessment of microbiological antimicrobial properties of PE film loaded with nanozinc filler
Dane BadawczeThe dataset contains the results of a single series of determinations of the antimicrobial properties against E. coli and S. aureus of polyethylene films containing the nanozinc filler.
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Annihilation rates of low-energy positron scattering from simple diatomic molecules
PublikacjaWe discuss the calculations of Zeff coefficients for a series of diatomic molecules over the range of energies below the positronium formation. During the development of a general code for polyatomic, nonlinear molecules colliding with positrons, it was discovered that the earlier one, employed only for diatomic molecules, had an error. The error is corrected and the corrected results are presented here. We also discuss a way of...
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A robust 18-pulse diode rectifier with coupled reactors
PublikacjaThe article presents the principle of operation and selected results of simulation and laboratory tests of the 18-pulse rectifier system with coupled reactors and small series active power filter. The presented system makes it possible to reduce, especially in distribution supply networks, undesired higher current harmonics. The 18-pulse nature of operation of the rectifier is reached using a set of coupled three-phase network...
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Positron binding to alkali-metal hydrides: The role of molecular vibrations
PublikacjaThe bound vibrational levels for J=0 have been computed for the series of alkali-metal hydride molecules from LiH to RbH, including NaH and KH. For all four molecules the corresponding potential-energy curves have been obtained for each isolated species and for its positron-bound complex (e+XH). It is found that the calculated positron affinity values strongly depend on the molecular vibrational state for which they are obtained...
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Towards Audio Signal Equalization Based on Spectral Characteristics of a Listening Room and Music Content Reproduced
PublikacjaThis study presents investigations of the influence of the room acoustics on the frequency characteristic of the audio signal playback. First, the concept of a novel spectral equalization method of the room acoustic conditions is introduced. On the basis of the room spectral response, a system for room acoustics compensation based on an equalizer designed is proposed. The system settings depend on music genre recognized automatically....
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TS-based RSM-aided design of cold-formed steel stiffened C-sectional columns susceptible to buckling
PublikacjaThe paper focuses on joint-performance analysis of a built-up cold-formed thin-walled C-sectional column with a fillister (stiffener) of the same type, interconnected with a series of bolts located along the length of the compressed members in specific spacing. The quantity of bolts and the non-connected starting distance of the fillister are considered random variables of the problem. Optimal distribution of joints on the stiffener...
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Accuracy analysis of the RSSI BLE SensorTag signal for indoor localization purposes
PublikacjaIn this paper we describe possibility of use the RSSI signal (Radio Signal Strength Indication) from Texas Instruments SensorTag CC2650 for indoor positioning purposes. This idea is not a new but in our opinion it is possible to use SensorTags with Bluetooth LE wireless interface for positioning inside buildings in such applications as people findings in hospitals, senior come care, etc. RSSI is mostly selected as the sensor localization...
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Enthalpies of formation of rare earth niobates, RE3NbO7
PublikacjaHigh-temperature oxide melt solution calorimetry was used to investigate energetics of a series of rare earth niobates RE3NbO7. All of investigated compounds were found to be stable in enthalpy in respect to their oxides. The enthalpy of formation from oxides becomes more exothermic as the size of the RE cation increases, a trend seen previously in other RE compounds including pyrochlores, perovskites, and phosphates. For smaller...
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Synthesis and biological evaluation of fluorinated 3-phenylcoumarin-7-O-sulfamate derivatives as steroid sulfatase inhibitors
PublikacjaIn the present work, we report the initial results of our study on a series of 3-phenylcoumarin sulfamate-based compounds containing C-F bonds as a novel inhibitors of steroid sulfatase (STS). The new compounds are potent STS inhibitors, possessing more than 10 times higher inhibitory potency than coumarin-7-O-sulfamate. In the course of our investigation, compounds 2b and 2c demonstrated the highest inhibitory effect in the enzymatic...
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Differentiating patients with obstructive sleep apnea from healthy controls based on heart rate-blood pressure coupling quantified by entropy-based indices
PublikacjaWe introduce an entropy-based classification method for pairs of sequences (ECPS) for quantifying mutual dependencies in heart rate and beat-to-beat blood pressure recordings. The purpose of the method is to build a classifier for data in which each item consists of two intertwined data series taken for each subject. The method is based on ordinal patterns and uses entropy-like indices. Machine learning is used to select a subset...
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Normal stress distribution in built‑up cold‑formed column in relation to interconnecting bolt spacing
PublikacjaIn order to increase a stiffness of cold-formed steel (CFS) elements it is practised to built-up the cross-section. In the analysed case, a main element is strengthened by adding extra chord in contact partially along the column. This additional chord acts as a longitudinal stiffener connected with the main section by series of bolts. Authors check whether rules applied over the years, for hot-rolled elements, can be indiscriminately...
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Validation of dynamic electrochemical impedance spectrograms using autocorrelation function
PublikacjaValidation of impedance data is essential for checking the reliability of experimental data. Kramers – Kronig transformation is used to verify data obtained from classical Electrochemical Impedance Spectroscopy (EIS) measurements. Data obtained from Dynamic Electrochemical Impedance Spectroscopy (DEIS) could be validated in the same way, but in this case, there is no information about internal consistency between every single spectrum...
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Ocena zastosowania wybranych reguł wymiany narzędzi w systemie produkcyjnym
PublikacjaIn this paper, an integrated analytical and simulation modelling framework has been developed with the objective to explore total system planning and operational issues. It enables in particular structuring the alternative process flow in manufacturing systems and their extended investigation under different tool exchange rules with limited number of tool inventory. Simulation studies performed with the proposed rules in the environment...
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Mechanical characterization of a gravel column in a calibration chamber operating as a triaxial cell
PublikacjaA series of tests considering the behavior of gravel columns was performed. A segment of column with a height of 1 m and a diameter of 0.53 m was modelled in a calibration chamber used as a triaxial cell at three different lateral stress applied. The vertical load transferred on the column head was simulated with steady increase of water pressures in the upper and lower membranes. During the loading the volumetric changes in the...
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Monitoring the fracture process of concrete during splitting using integrated ultrasonic coda wave interferometry, digital image correlation and X-ray micro-computed tomography
PublikacjaThe paper deals with the continuous-time monitoring of mechanical degradation in concrete cubes under splitting. A series of experiments performed with integrated coda wave interferometry (CWI) and digital image correlation (DIC), supported with X-ray micro-computed tomography (micro-CT) is reported. DIC and micro-CT techniques were used to characterize the fracture process in detail. CWI method was proved to be effective in the...
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The Reactivity of the Imine Bond within Polynuclear Nickel(II) Complexes
PublikacjaThree novel Ni complexes with the Schiff base ligand 2-methoxy-6-(E-2-pyridyliminomethyl)-phenol (L1) are described. In comparison with the similar 2-(pyridine-2-ylimino-methyl)phenol (pymp), the mode of coordination of L1 is altered due to the presence of methoxy substituent introducing the sterical hindrance. During the synthesis of the complexes, partial hydrolysis of the ligand was observed. Since such immediate hydrolysis...
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Computational Complexity and Its Influence on Predictive Capabilities of Machine Learning Models for Concrete Mix Design
PublikacjaThe design of concrete mixtures is crucial in concrete technology, aiming to produce concrete that meets specific quality and performance criteria. Modern standards require not only strength but also eco-friendliness and production efficiency. Based on the Three Equation Method, conventional mix design methods involve analytical and laboratory procedures but are insufficient for contemporary concrete technology, leading to overengineering...
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Synthesis, structural characterization, and thermal properties of Ca‐ and La‐doped soda‐lime glasses by laser melting
PublikacjaLaser melting techniques have been used in the preparation of unconventional glass compositions with high melting temperatures. Thus, we wanted to test the feasibility of using a CO2 laser in the preparation of nitrogen-rich oxynitride glasses and nitride silicate glasses. Melting from oxides and metallic raw materials, we wanted to study first glass formation and possible evaporation losses of the glass components. Two glass series...
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Reactions of cobalt(ii) chloride and cobalt(ii) acetate with hemisalen-type ligands: ligand transformation, oxidation of cobalt and complex formation. Preliminary study on the cytotoxicity of Co(ii) and Co(iii) hemisalen complexes
PublikacjaSeveral molecular cobalt(II) complexes, one Co(II) coordination polymer, and one ionic cobalt(III) complex with imine hemisalen ligands were synthesized. The hemisalen ligands were synthesized from o-vanillin (oVP) and diverse aminopyridines (compounds HL1–HL4) or aminophenol (compound HL5). It was observed that cobalt(II) chloride in dry acetonitrile catalyzes a transformation of HL1 and HL3 instead of complex formation. The conversion...
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Comparative Analysis of Metabolic Variations, Antioxidant Profiles and Antimicrobial Activity of Salvia hispanica (Chia) Seed, Sprout, Leaf, Flower, Root and Herb Extracts
PublikacjaThe purpose of this study was to evaluate the phytochemical profiles of the seeds, sprouts, leaves, flowers, roots and herb of Salvia hispanica and to demonstrate their significant contribution to antioxidant and antimicrobial activities. Applied methods were: HPLC-DAD coupled with post-column derivatization with ABTS reagent, untargeted metabolomics performed by LC-Q-Orbitrap HRMS, and two-fold micro-dilution broth method, which...
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Nitrogen-doped diamond thin films: potential application in Fabry-Pérot interferometer
PublikacjaIn this paper we present results of preliminary research of using nitrogen-doped diamond (NDD) films as reflective layer in Fabry-Pérot interferometer. NDD films were deposited on Si substrates by Microwave Plasma Enhanced Chemical Vapor Deposition (MPECVD) with the use of CH4, H2 and N2 gas mixtures. During deposition process methane flow rate varied while nitrogen flow was constant. We performed series of measurements which showed...
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Enhancing capabilities of Atomic Force Microscopy by tip motion harmonics analysis
PublikacjaMotion of a tip used in an atomic force microscope can be described by the Lennard-Jones potential, approximated by the van der Waals force in a long-range interaction. Here we present a general framework of approximation of the tip motion by adding three terms of Taylor series what results in non-zero harmonics in an output signal. We have worked out a measurement system which allows recording of an excitation tip signal and its...
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R&D of satellite pumps and motors with small geometrical displacement supplied with oil and non-flammable liquids
PublikacjaThe newest construction of satellite motors and self-suction satellite pumps with small geometrical displacement have been described in this article. The characteristics of volumetric and total efficiency of one satellite motor, selected from the series, supplied with oil have been presented. These characteristics have been compared with the orbital motors' characteristics. The remaining specifications of these motors were also...
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Magnetic and capacitive couplings influence on power losses in double circuit high voltage overhead transmission line
PublikacjaPurpose – The paper aims to discuss problems of power and energy losses in a double-circuit overhead transmission line. It was observed from energymeters’ readings, that in such a line, active power losses can be measured as “negative”. The “negative” active power losses appear when the active power injected to the circuit is lower than the active power received at the circuit end. The purpose of this paper is to explain this phenomenon. Theoretical...
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Music signal equalization in a changing environment
PublikacjaThe paper presents the concept of an automatic system for music signal correction, considering room frequency response and music genre being played. The proposed algorithm, based on the room frequency response, compensates acoustic conditions surrounding the sound source. Additionally, the compensation process considers the signal content by recognizing music genre. As part of the described research, a series of subjective tests...
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Application of auto calibration and linearization algorithms to improve sound quality of computer devices
PublikacjaAn application of auto calibration and linearization algorithms designed for correcting acoustic characteristics of selected computer devices was presented in the paper. The functionality of the algorithms were presented for two kind of computer devices: ultrabook class computer and portable device of All-In-One type. The algorithms were adjusted for the given type of the device on the basis of series of measurements conducted...
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KTaO3-based nanocomposites for air treatment
PublikacjaA series of single semiconductors and their nanocomposites combination (such as KTaO3 + CdSe + SrTiO3; KTaO3 + CdS +WO3; KTaO3 + CdS + MoS2) were prepared using hydrothermal route. Photocatalytic activity of as-prepared nanocomposites was estimated by photocatalytic degradation of toluene in the gas phase using light-emitting diodes (LEDs, 375 nm) in four subsequent cycles. The nanocomposites were characterized by scanning electron...