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Wyniki wyszukiwania dla: SAMPLE-AND-HOLDING METHOD
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SAMPLE-AND-HOLDING METHOD FOR GAS SENSING APPLIED FOR RESISTANCE GAS SENSORS
PublikacjaThe DC resistance of a Taguchi gas sensor is influenced by the ambient gas. To improve the selectivity and sensitivity of a sensor the fluctuation enhanced sensing (FES) was used. The paper proposes a novel methodology of utilizing FES technique that sample composition of an ambient atmosphere and hold it for further processing (sample-and-holding technique). The method uses the heated gas sensor to sample an ambient atmosphere...
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SPME as a method of sample preparation for GC analysis of VFAs
PublikacjaW niniejszym artykule omówiono szczegółowo technikę mikroekstrakcji do fazy stacjonarnej, stosowaną na etapie przygotowania próbek, w celu oznaczania lotnych kwasów tłuszczowych.
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Quechers sample preparation method variants for analysis of pesticide residues in fruits and vegetables
PublikacjaThis article describes the comparison of different versions of an easy, rapid and low-cost sample preparation approach for the determination of pesticide residues in fruits and vegetables by concurrent use of gas and liquid chromatography coupled to MS or ECD for detection. The sample preparation approach is known as QuEChERS, which stands for quick, easy, cheap, effective, rugged and safe. It is a combination of liquid-liquid...
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Determination of pesticide residues in fruits and vegetables using QuEChERS sample preparation method
PublikacjaThe intensive development of agriculture means that more and more toxic organic and inorganic compounds are entering the environment. Because of their widespread use, environmental stability, selective toxicity and bioaccumulative capability, pesticides belong to the most hazardous substances contaminating the environment. They are particularly dangerous in fruits and vegetables, because they are one of the reasons why people are...
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A Robust Method for Sample Preparation of Gastrointestinal Stromal Tumour for LC/MS Untargeted Metabolomics
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Seeking genetic signature of radiosensitivity - a novel method for data analysis in case of small sample sizes
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Analysis of pesticide residues in fruits and vegetables using QuEChERS sample preparation method and gas chromatography with electron capture detection
PublikacjaPesticides are a numerous and diverse group of chemical compounds. They are some of the most toxic substances contaminating the environment, which are used to eliminate pests in agriculture and the household. Despite considerable progress in the development of methods for preparing samples for analysis and for the final determination of analytes, the analysis of pesticides in biological samples continues to present challenges to...
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Hanging drop cathode-atmospheric pressure glow discharge as a new method of sample introduction for inductively coupled plasma-optical emission spectrometry
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Can matrix solid phase dispersion (MSPD) be more simplified? Application of solventless MSPD sample preparation method for GC–MS and GC–FID analysis of plant essential oil components
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Justyna Płotka-Wasylka dr hab. inż.
OsobyUrodziła się w Słupsku (24.03.1986).W 2005 roku ukończyła I Liceum Ogólnokształcące im. Jana II Sobieskiego w Wejherowie i rozpoczęła studia na Wydziale Chemicznym Politechniki Gdańskiej. Po ich ukończeniu w 2010 rozpoczęła pracę naukową na tej uczelni, uzyskując w 2014 roku stopień doktora nauk chemicznych. Tematem jej rozprawy doktorskiej, wykonywanej pod kierunkiem prof. Marka Biziuka oraz dr Caluma Morrisona (Uniwersytet w...
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The new concept of product. Cooling band
PublikacjaThe chapter below presents the innovative solution consist in applying the cooling band to help holding the hot object. The solution was found through substitute inputs analysis and brain storm method. The new product was submitted in Polish Patent Office under the No. W.120905.
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THEORETICAL AND EXPERIMENTAL INVESTIGATION OF THIN-WALLED BEARING SHELL’S DESIGN PARAMETERS AND ASSEMBLY CONDITIONS ON THE HOLDING TORQUE INSIDE A HOUSING BORE OF A CONNECTING ROD
PublikacjaThe aim of the work was the experimental and theoretical evaluation of the influence of the most important parameters determining the holding torque of a thin-walled bearing shell inside a housing bore of a connecting rod. The main investigated parameters were defned by authors experience in this feld. In the frst stage of research, a special test stand was designed in order to allow measuring the real values of the friction torque...
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Rafał Leszczyna dr hab. inż.
OsobyDr hab. inż. Rafał Leszczyna jest profesorem uczelni na Wydziale Zarządzania i Ekonomii Politechniki Gdańskiej. W lipcu 2020 r., na podstawie osiągnięcia naukowego w obszarze zarządzania cyberbezpieczeństwem infrastruktur krytycznych w sektorze elektroenergetycznym, uzyskał stopień doktora habilitowanego w dziedzinie nauk inżynieryjno-technicznych, dyscyplina informatyka techniczna i telekomunikacja. W latach 2004–2008 pracował...
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Działanie na szkodę spółki zależnej - aspekty prawne
PublikacjaCelem artykułu jest prezentacja prawnych aspektów funkcjonowania grup kapitałowych w Polsce. Opracowanie dotyczy prawa grup spółek rozpatrywanego z punktu widzenia potrzeb działalności gospodarczej, z uwzględnieniem ochrony akcjonariuszy mniejszościowych, wierzycieli i menedżerów spółek tworzących holding, w szczególności spółek zależnych. Wykazano, że polski system prawa grup spółek nie spełnia zupełnie potrzeb współczesnego obrotu...
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Study on the prevalence of mobile phone use by car drivers – the case of Poland
Publikacja: Distracted driving is a significant factor affecting road safety and it can occur as a result of using mobile phones while driving. The aim of the current research is to present the prevalence of mobile phone use by Polish car drivers, based on the roadside and online survey. The field study showed that 11.6% of 1867 drivers were using mobile phones while being in motion and 26.1% of 203 drivers when stopped in front of traffic...
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Public valuation of social impacts. The comparison between mega and non-mega sporting events
PublikacjaThe main aim of this study is to assign value to intangible effects,including social impacts, which appear when organising sportingevents of various scales in the city of Gdansk located in northernPoland. A survey was conducted to determine the city residents’willingness-to-pay (WTP) using the contingent valuation method(CVM). The average WTP values, which ranged between PLN 6.04and PLN 46.34, show that the scale of the sporting...
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Use of Modified Cuckoo Search algorithm in the design process of integrated power systems for modern and energy self-sufficient farms
PublikacjaIn the face of increasingly stringent pollutant emission regulations, designing an agricultural holding becomes a difficult challenge of connecting a large number of coefficients that describe an energy system of a farm in regard to its ecological and economic efficiency. One way to cope with this issue is to design an energy self-sufficient farm that integrates various technologies, including renewable energy. However, the selection...
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A novel approach for processing CaAlSiON glass-ceramics by spark plasma sintering: Mechanical and electrical properties
PublikacjaLithium containing glassy materials can be used as solid electrolytes or electrode materials for lithium-ion batteries due to their high energy density. Conventional melt-quenched Ca11Al14Si16O49N10 glass powder containing 24 e/o N, doped with Li-ions (1, 3, and 6 wt. %) and sintered by spark plasma sintering technique (SPS) was studied. The benefits of using SPS to produce glass-ceramics are rapid heating rates compared to conventional...
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Ocena efektywności monitoringu obiektów inżynierskich za pomocą sieci Bayesa
PublikacjaW swojej pracy autorzy zaproponowali zastosowanie sieci Bayesa do projektowania monitoringu i podejmowania decyzji w działaniach eksploatacyjnych. Ponadto pokazano dwie metody oceny wartości informacji diagnostycznych. Pierwszą z nich jest wartość oczekiwana EVSI (ang. Expected Value of Sample Information), która stanowi podstawę do wyboru spośród alternatywnych obserwacji symptomów zmiennej diagnostycznej. Natomiast drugą metodą...
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Attributes of Entrepreneurial Teams as Elements of a Mental Model
PublikacjaAn entrepreneurial team can be defined as a small group of individuals holding ownership or control positions who create or develop an entrepreneurial venture and have shared commitments towards each other. Entrepreneurial teams start numerous new ventures or affect the performance of firms due to their social capital based on some characteristic attributes. The mental models of teams refer to internal, organised representation...
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The Role of Proteins in Food
PublikacjaThis chapter describes the effect of proteins on the sensory attributes and the biological value and safety of foods. The role of proteins depends on their amino acid composition and structure, on changes due to storage and processing, as well as on interactions with other food components. The effect on the sensory quality of foods is brought about by hydrophobicity, solubility, water holding capacity, gelling, film formation,...
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Investigation of Microbes in the Stratosphere – Stardust Project
PublikacjaThe stratospheric microbiota has been investigated many times using the methods of classical microbiology. In this research a few modern methods, including NGS sequencing and multiple displacement amplification of DNA, were in use. The analysis of metagenome helped to determine the content of various species of bacteria in the sample collected in the stratosphere by a hydrogen-filled balloon holding...
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Sample ecourse
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ZASTOSOWANIE FILTRACJI CZĄSTECZKOWEJ DO ESTYMACJI POŁOŻENIA W SYSTEMIE LOKALIZACYJNYM UWB
PublikacjaNiniejszy artykuł dotyczy kwestii poprawy dokładności estymacji położenia w systemie lokalizacji wewnątrzbudynkowej, bazującym na radiowych pomiarach odległości realizowanych przez modemy UWB. Proponuje się zastosowanie metody filtracji cząsteczkowej do zmniejszenia błędu wyznaczania pozycji obiektu przy braku bezpośredniej widoczności ze stacją referencyjną. W artykule opisano algorytm filtru cząsteczkowego, jego przykładową implementację...
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Logistics of Transnational Corporations as the Basis of Cooperation Between Ukraine and EU (for Poland Example)
PublikacjaThe article describes the scientific and theoretical basis for the organization of logistics management of modern international corporations, owning by assets in mining and metallurgical business in Ukraine and Poland; it had been analyzed the influence of transfer pricing mechanism as one of the main factors affecting on the efficiency of the organization of supply chain of resources (Ukrainian semi-finished goods) to ensure uninterrupted...
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Ewolucyjne planowanie bezpiecznych trajektorii statków oparte na zmodyfikowanym diagramie Cockcrofta.
PublikacjaArtykuł przedstawia kontynuację badań autora nad planowaniem bezpiecznych trajektorii statków za pomocą algorytmów ewolucyjnych. Prezentowana metoda poszukuje optymalnego zbioru bezpiecznych trajektorii wszystkich statków biorących udział w spotkaniu. Bieżąca wersja metody zakłada ograniczoną widoczność i obowiązywanie Prawidła 19 Międzynarodowych Przepisów o Zapobieganiu Zderzeniom na Morzu (MPZZM) zamiast Prawideł 11 – 18. Artykuł...
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A Tutorial on AGREEprep an Analytical Greenness Metric for Sample Preparation
PublikacjaSample preparation is a key step in the analytical procedure and a critical component for achieving analytical greenness. AGREEprep is the first metric intended for evaluating the environmental impact of sample preparation methods. The approach consists of ten steps of assessment that correspond to the ten principles of green sample preparation and uses a user-friendly open-source software to calculate and visualize the results....
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Technological and Media Platforms: Redefinition of Meanings as Symbolic Power over the Discourse
PublikacjaRedefining the meanings of such social terms as “likes” and “friends” on Facebook is a popular practice. In terms of consistency, the (auto)-redefinition of the term “platform” is itself particularly important from a media management perspective. The article proposes to consider the redefinition of meanings as a form of wielding non-transparent power over discourse. From this perspective, redefining a meaning is a form of holding...
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Identifying and Mitigating the Negative Effects of Power in Organizations
PublikacjaThis article investigates the possible negative effects of power in organizations. It demonstrates how holding power may affect an individual’s perception of others, actions, and cognition. Ways in which power may have a detrimental effect on different aspects of a manager’s functioning within an organization, including building relationships, communication, and performance are analyzed. It is argued that individuals are unaware...
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Virtual Engineering Objects (VEO): Designing, Developing and Testing Models
PublikacjaIn this article, the development and implementation of the concept of Virtual Engineering Object (VEO) is described. A VEO is a computerized real world representation of an engineering object. VEO will act as a living representation of the object capable of adding, storing, improving and sharing knowledge through experience, in a way similar to an expert of that object. In this paper, it is shown through test models how the concept...
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Herbarium of Division of Marine Biology and Ecology University of Gdańsk (DMBE)
Dane BadawczeHerbarium of Division of Marine Biology and Ecology University of Gdańsk (DMBE) is a research herbarium encompassing specimens of vascular plants and algae hosted by the Laboratory of Marine Plant Ecology at University of Gdańsk, Poland. The aim of Herbarium is to preserve marine plant and algae collections mostly from the Gulf of Gdańsk, but the herbarium...
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Statistics 2022_23
Kursy Online1.Elements of probability. The axioms of the probability theory 2. Random variables and their distributions. Discrete and continuous random variables 3. Parameters of random variables: expected value, moments 4. Selected distributions of random variables (Bernoulli, Poison, Gaussian) 5.The distribution in the sample. Visualisation by histograms 6. Measures of statistical location: arithmetic mean, median, quantiles. 7. Measures...
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Green sample preparation 2023
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Confidence, Financial Literacy and Investment in Risky Assets: Evidence from the Survey of Consumer Finances
PublikacjaWe employ recent Survey of Consumer Finances (SCF) microdata from the US to analyze the impacts of confidence in one's own financial knowledge, confidence in the economy, and objective financial literacy on investment in risky financial assets (equity and bonds) on both the extensive and intensive margins. Controlling for a rich set of covariates including risk aversion, we find that objective financial literacy is positively...
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Samotestowanie toru analogowego ze wzmacniaczem w pełni różnicowym w elektronicznych systemach wbudowanych sterowanych mikrokontrole-rami
PublikacjaPrzedstawiono nową metodę samotestowania toru analogowego opartego na wzmacniaczu w pełni różnicowym w elektronicznych systemach wbu-dowanych sterowanych mikrokontrolerami. Bazuje ona na nowej metodzie diagnostycznej opartej na przekształceniu transformującym próbki odpo-wiedzi czasowej badanej części analogowej na pobudzenie "ujemnym" impulsem prostokątnym na wejściu Vocm na krzywe identyfikacyjne w przestrzeni pomiarowej. Metoda...
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Glaciers as an Important Element of the World Glacier Monitoring Implemented in Svalbard
PublikacjaGlaciers are not only contributors to the sea level rise but also important players in the circulation of pollutants. Over a billion people apply glacial waters for domestic purposes; hence, both the quality and quantity of this water should be monitored. In this chapter, we concentrate on the archipelago Svalbard in the Arctic, a typical target area for xenobiotics from long range atmospheric transport (LRAT), holding an important share...
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Finite Element Method
Kursy OnlineItem Name : Finite Element Method- Abaqus learning Field of study : Civil Engineering Faculty : Faculty of Civil and Environmental Engineering Education level : Second degree studies Form of studies : Full-time studies Year of studies : 1 Study semester : 2 Start of the semester : November 2021 Academic year of the course : 2021/2022 Form of classes : Lecture, Laboratory
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Green Sample Collection
PublikacjaThe term of “green sample collection” is directly associated with both passive and dynamic analytical tools which allow for simultaneous management of the stage of collection and isolation and/or enrichment of a broad spectrum of chemical compounds from environmental samples. The use of passive sampling techniques at the stage of sample collection makes it possible to obtain in a simple yet inexpensive manner an analytical information...
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Metoda f-chart w zastosowaniu do projektu instalacji solarnej w budownictwie jednorodzinnym
PublikacjaW artykule przedstawiono algorytm obliczeń cieplnych związanych z konwersją promieniowania cieplnego oraz analizę efektów pracy instalacji solarnej przy użyciu metody korelacyjnej f-chart. Zaprezentowany algorytm obliczeń cieplnych oraz omówiona w artykule podstawowa odmiana metody f-chart zostały poparte przykładem obliczeniowym dla instalacji solarnej, która wykorzystywana jest do wspomagania układu przygotowania c.w. dla potrzeb...
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Quality Expectations of Mobile Subscribers
PublikacjaMobile systems, by nature, have finite resources. Radio spectrum is limited, expensive and shared between many users and services. Mobile broadband networks must support multiple applications of voice, video and data on a single IP-based infrastructure. These converged services each have unique traffic holding and quality requirements. A positive user experience must be obtained through efficient partitioning of the available wireless...
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Finite Element Method Applications - winter 2022/2023
Kursy OnlineFinite Element Method Applications - summer 2022/2023 Seminar.
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Finite Element Method Applications - summer 2022/2023
Kursy OnlineFinite Element Method Applications - summer 2022/2023 Seminar.
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Finite Element Method Applications - winter 2023/2024
Kursy OnlineFinite Element Method Applications - winter 2022/2023 Seminar.
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Finite Element Method Applications 2023/2024 Summer
Kursy OnlineFinite Element Method Applications - summer semester 2023/2024 Seminar.
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On Sample Rate Conversion Based on Variable Fractional Delay Filters
PublikacjaThe sample rate conversion algorithm based on variable fractional delay filters is often used if the resampling ratio cannot be expressed as the ratio of small integer numbers or if it is not constant. The main advantage of such solution is that it allows for arbitrary resampling ratios which can even be changed during the resampling process. In this paper a discussion on influence of different approaches to fractional filter...
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Green Analytical Chemistry Approaches in Sample Preparation
PublikacjaThis chapter presents environmentally friendly solutions for sample preparation. Attention is focused on extraction techniques and the minimization of organic solvent consumption, as the large quantitiesused in analytical laboratories are a pressing environmental problem. Solventless sample preparation techniques, alternative solvents, mediated extractions are discussed. The principle of each technique isbriefly described, together...
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Tuning the Laser-Induced Processing of 3D Porous Graphenic Nanostructures by Boron-Doped Diamond Particles for Flexible Microsupercapacitors
PublikacjaCarbon (sp3)-on-carbon (sp2) materials have the potential to revolutionize fields such as energy storage and microelectronics. However, the rational engineering and printing of carbon-on-carbon materials on flexible substrates remains a challenge in wearable electronics technology. This study demon-strates the scalable fabrication of flexible laser-induced graphene (LIG)-boron doped diamond nanowall (BDNW) hybrid nanostructures...
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Distributed Evacuation in Graphs with Multiple Exits
PublikacjaWe consider the problem of efficient evacuation using multiple exits. We formulate this problem as a discrete problem on graphs where mobile agents located in distinct nodes of a given graph must quickly reach one of multiple possible exit nodes, while avoiding congestion and bottlenecks. Each node of the graph has the capacity of holding at most one agent at each time step. Thus, the agents must choose their movements strategy...
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Scientific Research Method
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AGREEprep – Analytical greenness metric for sample preparation
PublikacjaThis work proposes for the first time, a metric tool that gives prominence to sample preparation. The developed metric (termed AGREEprep) was based on 10 categories of impact that were recalculated to 0 e1 scale sub-scores, and then used to calculate the final assessment score. The criteria of assessment evaluated, among others, the choice and use of solvents, materials and reagents, waste generation, energy consumption, sample...
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Sample Rate Conversion Based on Frequency Response Masking Filter
PublikacjaThe sample rate conversion with high resampling ratios requires low-pass digital filters with very narrow transition band which results in high computational complexity and makes filter design problematic. Therefore in this work we propose to use the FRM method, which breaks the filter with a narrow transition band into a group of filters with reduced design requirements. These decreases the number of non-zero coefficients and...
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Evaluation of Green Sample Preparation Techniques for Organic Compounds
PublikacjaNowadays, Green Analytical Chemistry (GAC) idea is of high importance, with impact on the rapid growth in the sample preparation area with special emphasis on sample preparation simplification, miniaturization and automation. Due to the fact that GAC is of high importance today, this study is focused on the evaluation of green sample preparation techniques for organic compounds. It is well known that sample preparation is considered...
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Sample Rate Conversion with Fluctuating Resampling Ratio
PublikacjaIn this paper a sample rate conversion with continuouslychanging resampling ratio has been presented. The proposed implementation is based on variable fractional delay filter implemented using a Farrow structure. It have been demonstrated that using the proposed approach instantaneous resampling ratio can be freely changed. This allows for simulation of audio recored on magnetic tape with nonuniform velocity as well as removal...
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Sample Rate Conversion with Fluctuating Resampling Ratio
PublikacjaIn this paper a sample rate conversion with continuously changing resampling ratio has been presented. The proposed implementation is based on variable fractional delay filter implemented using a Farrow structure. It have been demonstrated that using the proposed approach instantaneous resampling ratio can be freely changed. This allows for simulation of audio recored on magnetic tape with nonuniform velocity as well as removal...
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The effect of aeration mode (intermittent vs. continuous) on nutrient removal and greenhouse gas emissions in the wastewater treatment plant of Corleone (Italy)
PublikacjaThe paper reports the results of an experimental study aimed at comparing two configurations of a full-scale wastewater treatment plant (WWTP): conventional activated sludge (CAS) and oxic-settling-anaerobic process (OSA) with intermittent aeration (IA). A comprehensive monitoring campaign was carried out to assess multiple parameters for comparing the two configurations: carbon and nutrient removal, greenhouse gas emissions, respirometric...
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Mechanisms of Damage to DNA Labeled with Electrophilic Nucleobases Induced by Ionizing or UV Radiation
PublikacjaHypoxia—a hallmark of solid tumors—makes hypoxic cells radioresistant. On the other hand, DNA, the main target of anticancer therapy, is not sensitive to the near UV photons and hydrated electrons, one of the major products of water radiolysis under hypoxic conditions. A possible way to overcome these obstacles to the efficient radio- and photodynamic therapy of cancer is to sensitize the cellular DNA to electrons and/or ultraviolet...
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New analytical sample preparation techniques in food flavour analysis
PublikacjaIn this chapter sample preparation techniques were broadly characterized and their applications in field of food analysis were presented. Usefulness of three extraction methods: SPME, SAFE and SDE for isolation of aroma compounds from complex food matrices was compared. Additionally, requirements for sample preparation methods using in food flavour analysis were detailed.
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Progress in development of molecularly imprinted polymers as sorbents for sample preparation
PublikacjaSample preparation has been one of the most often investigated steps in analytical procedures.These investigations are focused on problems such as isolation of analytes from the sample matrix, matrix implification, analyte enrichment to the level above the detection limit of the instrumentation used, and the removal of interfering species to improve the final determination. Techniques based on solid (adsorption) and pseudo liquid...
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Validation and Regulatory Issues for Sample Preparation in: Comprehensive Sampling and Sample Preparation
PublikacjaW rozdziale opisano podstawowe terminy związane z walidacja procedury analitycznej. Szczególnie zwrócono uwagę na etapy pobierania i przygotowania próbek do analizy. Podano także rolę i znaczenie poszczególnych składowych procesu kontroli i zapewnienia jakości wyników pomiarów analitycznych.
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Method and Theory in the Study of Religion
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JOURNAL OF ARCHAEOLOGICAL METHOD AND THEORY
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“Green” nature of the process of derivatization in analytical sample preparation
PublikacjaNowadays, the idea of Green Analytical Chemistry (GAC) is of high importance what impacts on the rapid growth in the sample preparation area with special emphasis on sample preparation simplification, miniaturization, and automation. Because the derivatization process is often an essential element of the analytical procedure, it should be important to focus on this issue from GAC perspective and conduct a series of experiments...
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Physics Research Method IV
Kursy Online{mlang pl} Dyscyplina: Nauki Fizyczne Zajęcia obowiązkowe dla doktorantów II roku Prowadzący: prof. Julien Guthmuller Liczba godzin: 15 h Forma zajęć: wykład/seminarium {mlang} {mlang en} Discipline: Phisical Sciences Obligatory course for 2nd year PhD students Academic teacher: prof. Julien Guthmuller Total hours of training: 15 teaching hours Course type: lecture/seminar {mlang}
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Solventless sample preparation techniques based on solid- and vapour-phase extraction
PublikacjaThe main objective of this review is to critically evaluate recent developments in solventless sample preparation techniques. The potential of a variety of sample preparation techniques based on solid- and vapour-phase extraction techniques is evaluated. Direct thermal extraction and derivatization processes to facilitate the extraction of analytes in different areas are included. The applicability, disadvantages and advantages...
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Chemical identification of rubber fender sample and hardness and density measurements
PublikacjaScope of testing: Chemical identification of rubber fender sample and hardness and density measurements. - Raport z badań zleconych - Numer umowy: 031178
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Green Aspects of Miniaturized Sample Preparation Techniques
PublikacjaCorrect monitoring and control of the state of the environment and scientific research on the subject of environmental protection often require that determinations of compounds present at very low concentrations be made in samples characterized by a matrix of complex composition (e.g., biological samples, water and soil samples). Moreover, due to the limited number of analytical techniques which are sufficiently sensitive to conduct...
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Effect of ultrasound treatment on water holding properties and microstructure of beef (m. semimembranosus) during ageing
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Sample Preparation in Foodomics: Miniaturized Solid-Phase Extraction
PublikacjaAnalytical chemists face a challenge to bring comprehensive information on a given food and biological sample by using the best available analytical techniques and meet the requirements of sustainable development and green chemistry at the same time. A key objective of this chapter is to review selected literature data on the utilization of solid-phase extraction techniques with special attention to their miniaturized modes in...
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Dynamic Headspace Sampling as an Initial Step for Sample Preparation in Chromatographic Analysis
PublikacjaThis work represents a brief summary of the use of dynamic headspace (DHS) as a technique for sample preparation in chromatographic analysis. Despite numerous developments in the area of analyte isolation and enrichment, DHS remains one of the fundamental methods used with GC. In our opinion, interest in this technique will not diminish significantly because it conforms to stipulations of green analytical chemistry. Moreover, DHS...
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Variable Ratio Sample Rate Conversion Based on Fractional Delay Filter
PublikacjaIn this paper a sample rate conversion algorithm which allows for continuously changing resampling ratio has been presented. The proposed implementation is based on a variable fractional delay filter which is implemented by means of a Farrow structure. Coefficients of this structure are computed on the basis of fractional delay filters which are designed using the offset window method. The proposed approach allows us to freely...
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New sample preparation strategies for comprehensive lipidomics of human breast milk
PublikacjaGLOBAL PROFILING ANALYSIS OF HUMAN BREAST MILK (HBM) LIPIDS IS HINDERED BY COMPLEX COMPOSITION OF HBM. THIS PROBLEM IS HUGE FROM ANALYTICAL POINT OF VIEW, SINCE DUE TO THAT DETECTION OF ALL HBM LIPIDS DURING ONE ANALYTICAL RUN IS LIMITED. THUS, SAMPLE PREPARATION STEP CONSTITUTES A CRUCIAL STEP IN UNTARGETED LIPIDOMIC ANALYSIS OF HBM, ESPECIALLY WHEN SEMI-QUANTITATIVE ANALYSIS IS ASSUMED. HEREIN, WE PRESENT A COMPARISON OF PUBLISHED...
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Advances in Sample Preparation
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Influence of plastic deformation on stray magnetic field distribution of soft magnetic steel sample
PublikacjaThe effect of various combinations of conditions, i.e., presence of the Earth’s magnetic field during and after deformation on the distribution of stray magnetic field of S355 steel sample, which is locally deformed, was investigated. Some of the stages of the experiment were carried out in zero magnetic field. Compensation of the Earth’s magnetic field was obtained by the application of a pair of Helmholtz coils. These coils are...
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Miniaturized methods of sample preparation
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Surfactants application in sample preparation techniques: Insights, trends, and perspectives
PublikacjaSince the implementation of Green Chemistry into analytical practice, significant efforts have been made to improve the sustainability of chemical analysis. These include reducing the use of hazardous chemicals and solvents, minimizing waste, and improving energy efficiency. Surfactants can be applied in chemical analysis as an environmentally friendly alternative to conventional solvents and chemicals. The use of surfactants can...
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Ultrasound-Assisted Solvent Extraction of a Porous Membrane Packed Sample for the Determination of Tobacco-Specific Nitrosamines in the Replacement Liquids for E-Cigarettes
PublikacjaThe content of tobacco-specific nitrosamines (TSNAs) possessing carcinogenic properties has been an important area of research since replacement liquids were introduced for e-cigarettes. A method for determining N′-nitrosonornicotine (NNN), 4-(methylnitrosamino)-1-(3-pyridyl)-1-butanone (NNK), N′-nitrosoanatabine (NAT), and N′-nitrosoanabasine (NAB) in replacement liquids for electronic cigarettes was developed using liquid chromatography–tandem...
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International Journal of Research & Method in Education
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How does stakeholder pressure influence CSR-practices? A construction industry model based on a European sample
PublikacjaThe stakeholder pressure is one of the most vital powers which determines CSR implementation and can provide organizations with the motivation to adopt corporate social responsibility (CSR) strategy, as the stakeholder theory claims. The current investigation replications Kowalczyk’s (2019) study, who examined the same structure of relations based on the Polish sample. The essence of this replication is to find out whether CSR-...
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Coacervative extraction as a green technique for sample preparation for the analysis of organic compounds
PublikacjaOne of the present trends in analytical chemistry is miniaturization, which is one of the methods of green analytical chemistry application. A particular emphasis is placed on the elimination of the use of large amounts of organic solvents which are toxic and harmful to the environment, maintaining high efficiency of the extraction process, high recovery values and low values of quantification (LOQ) and detection (LOD) limits....
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New Trends in Sample Preparation Techniques for the Analysis of the Residues of Pharmaceuticals in Environmental Samples
PublikacjaPharmaceutical residues in the environment is a field of special interest due to the adverse effects to either human health or aquatic and soil environment. Pharmaceuticals have been already detected in underground, surface and wastewaters, soils, manure and sediments. The growing awareness of environmental pollution arising from human activity forces the need for their comprehensive determination. Environmental samples are complex...
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Sample preparation techniques for determination of pesticide residues in food samples
PublikacjaPesticides are very important in increasing the efficiency and quality of agricultural production. They are applied in many spheres of life, not only in agriculture, and their applications are expanding. Despite their numerous merits, pesticides are some of the most toxic substances contaminating our environment and have a negative impact on the human health. Properties of pesticides such as stability, ability to bioaccumulation...
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Introductory Chapter: Evolution of Sample Preparation
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Validation and Regulatory Issues for Sample Preparation
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Introductory Chapter: Evolution of Sample Preparation
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A framework estimating the minimum sample size and margin of error for maritime quantitative risk analysis
PublikacjaThe average accident frequency is essential for quantitative risk analysis and is conventionally estimated from accident statistics. This paper has systematically synthesised the knowledge on statistical errors and offered the missing instructions, a framework, for determining the minimum sample size and the margin of error (MOE) when calculating the average accident frequency from an accident database at hand. We have applied...
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Sample preparation procedure for the determination of polycyclic aromatic hydrocarbons in petroleum vacuum residue and bitumen
PublikacjaThis paper describes a novel method of samplepreparation for the determination of trace concentrations ofpolycyclic aromatic hydrocarbons (PAHs) in high-boilingpetroleum products. Limits of quantitation of the investigatedPAHs in materials of this type range from tens ofnanograms per kilogram to <20 μg/kg. The studies revealedthat in order to separate most of interferences from theanalytes without a significant loss of PAHs, it...
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Evaluation of the impact of geometry and plastic deformation on the stray magnetic field around the bone shaped sample
PublikacjaInfluence of two factors: the variable cross-section and the localized plastic deformation, which affect the stray magnetic field profile of a ferromagnetic sample have been studied. Evaluation of an effect size is based on the analysis of the stray magnetic field component which is tangential to the longest dimension of a sample. However, in order to describe the nature of the stray magnetic field, the normal component (perpendicular...
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Social media as an opportunity or a blind alley in social communication and forest education? – Experiences from Poland
PublikacjaThe article characterizes the experiences, problems, and prospects for the development of forest education on social media, which in Poland has been carried out by the Państwowe Gospodarstwo Leśne Lasy Państwowe (National Forest Holding ‘State...
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Determination of volatile organic compounds using solventless sample preparation techniques and gas chromatography
PublikacjaIn this paper the latest advances in the determination of volatile organic compounds using solvent-free extraction techniques in the sample preparation step are presented. A paper is focus mainly on one of the most popular sample preparation technique: solid-phase microextraction technique (SPME) combined with different detection systems and its applications to sampling of VOCs from the samples with different matrices. This paper...
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Application of modern sample-preparation techniques to the determination of chloropropanols in food samples
PublikacjaChloropropanols are heat-induced food toxicants that recently caused concern among industrial and scientific experts. World and European organizations related to food safety asked researchers to investigate mitigation strategies regarding these contaminants. The essential objective of this project was development of fast analytical methods enabling reliable determination and quantification of 3-monochloropropane-1,2-diol, 2-monochloropropane-1,3-diol...
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Finite Element Method - winter 2022/2023
Kursy OnlineCivil Engineering, Studia Stacjonarne II Stopień, II semestr
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Finite Element Method - winter 2023/2024
Kursy OnlineCivil Engineering, Studia Stacjonarne II Stopień, II semestr
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Experimental Evaluation of ND: YAG Laser Parameters and Sample Preparation Methods for Texturing Thin AISI 316L Steel Samples
PublikacjaIn mechanical and material engineering, the effect of laser texturing depends on many factors besides device specification, primarily the properties of the materials being processed, and, secondly, the preparation of the sample. Laser texturing of thin (<5 mm) samples is mostly performed utilizing short-pulse lasers, but depending on the power of the laser beam, the process can also be performed by using continuous operation lasers....
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State of the art in sample preparation for human breast milk metabolomics—merits and limitations
PublikacjaHuman breast milk (HBM) contains metabolites that are diverse in chemical structure and concentration. These metabolites range from high-abundance to low-abundance compounds and from polar to nonpolar. This complex nature of HBM makes HBM samples difficult to analyze, especially in global metabolomic studies for the determination and characterization of complete sets of metabolites. In this review, the state of the art in sample...
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Pre-analytical aspects in metabolomics of human biofluids – sample collection, handling, transport, and storage
PublikacjaMetabolomics is the field of omics research that offers valuable insights into the complex composition of biological samples. It has found wide application in clinical diagnostics, disease investigation, therapy prediction, monitoring of treatment efficiency, drug discovery, or in-depth analysis of sample composition. A suitable study design constitutes the fundamental requirements to ensure robust and reliable results from the...
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Modern Sample Preparation Techniques: A Brief Introduction
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Marek Tobiszewski dr hab. inż.
OsobyUrodzony 07.04.1984 roku w Gdańsku. W 2012 roku obronił z wyróżnieniem doktorat, w 2017 roku uzyskał habilitację na podstawie osiągnięcia naukowego „Opracowanie służących do oceny uciążliwości środowiskowej procedur analitycznych i rozpuszczalników”. Pracuje w Katedrze Chemii Analitycznej od 2012 roku. Jego zainteresowania naukowe łączą analitykę chemiczną, zwłaszcza analityka związków organicznych w próbkach środowiskowych, z...
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Determination of Pesticide Residues in Honeybees using Modified QUEChERS Sample Work-Up and Liquid Chromatography-Tandem Mass Spectrometry
PublikacjaIncreasing emissions of chemical compounds to the environment, especially of pesticides, is one of factors that may explain present honeybee colony losses. In this work, an analytical method employing liquid chromatography-tandem mass spectrometry (LC-MS/MS) was optimized for the simultaneous screening of 19 pesticides which have not been yet determined in honeybee samples from northern Poland (Pomerania). The sample preparation,...
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GTM Method of Structural Studies Lecture and Laboratory
Kursy Online -
Solventless and solvent-minimized sample preparation techniques for determining currently used pesticides in water samples: A review
PublikacjaThe intensification of agriculture means that increasing amounts of toxic organic and inorganic compounds are entering the environment. The pesticides generally applied nowadays are regarded as some of the most dangerous contaminants of the environment. Their presence in the environment, especially in water, is hazardous because they cause human beings to become more susceptible to disease. For these reasons, it is essential to...