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Combination of homogeneous liquid–liquid extraction and vortex assisted dispersive liquid–liquid microextraction for the extraction and analysis of ochratoxin A in dried fruit samples: Central composite design optimization
PublikacjaThis paper presents a new analytical procedure based on combination of homogeneous liquid–liquid extraction (HLLE) and vortex-assisted dispersive liquid–liquid microextraction (VA-DLLME) for the accurate and reliable determination of ochratoxin A (OTA) in dried fruit samples. To enable selective extraction of the OTA, six hydrophobic deep eutectic solvents (hDESs) were prepared and tested as extraction solvents. Optimization of...
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Synthesis, characterization and application of cross-linked functional terpolymer through epoxy group as sorbent for extraction of cadmium from waters and foods: Multivariate optimization
PublikacjaThe purpose of this study was to develop a selective sorbent for cadmium ions (Cd(II)) enrichment in orbital shaker assisted solid phase microextraction (OS-SPME) from different aqueous and food samples. A maleic anhydride-styrene-glycidyl methacrylate (MA-St-GMA) terpolymer was synthesized and characterized in detail. Experimental variables of sample preparation step were optimized using a central composite design (CCD). The final...
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Analysis of measurement uncertainty for contact-less method used to measure the position of catenary contact wire, performed with the use of Monte Carlo method
PublikacjaCurrently the majority of main railway lines in Europe are electrified, and electric trains have the biggest share in the entire amount of rail transport. Reliability of electrified railways is closely related to the issue of supplying traction vehicles with energy. The problems connected with diagnostics of energy consumption node, namely the contact line and the current collector, are therefore of fundamental importance for maintaining...
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Study on the Positioning Accuracy of the GNSS/INS System Supported by the RTK Receiver for Railway Measurements
PublikacjaCurrently, the primary method for determining the object coordinates is positioning using Global Navigation Satellite Systems (GNSS) supported by Inertial Navigation Systems (INS). The main goal of this solution is to ensure high positioning availability, particularly when access to satellite signals is limited (in tunnels, areas with densely concentrated buildings and in forest areas). The aim of this article is to determine whether...
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The selective salinity and hydrazine parameters for the start-up of non-anammox-specific biomass SBR
PublikacjaThe presence of ammonium (NH 4+ ) in wastewater above the permissible limits leads to undesirable ecological impact and public health concerns. In this study, the anaerobic ammonium oxidizing (anammox) bacteria-mediated nitrogen removal was investigated using a sequential batch reactor (SBR). Effects of different salinity levels were evaluated on the bacterial activity at: mild (below 0.2 g NaCl/L), elevated (18.2 g NaCl/L) and...
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Optimization of Train Energy Cooperation Using Scheduled Service Time Reserve
PublikacjaThe main aim of the paper was to develop an innovative approach to the preliminary estimation possibility of train energy cooperation based on data from timetables, without traction calculations. The article points out the need to strive for sustainable and environmentally friendly transport. It was pointed out that rail transport using electric traction is one of the more ecological branches of transport. It also offers a number...
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Modification of quaternary structure of Candida albicans GlcN-6-P synthase and its desensitization to inhibition by UDP-GlcNAc by site-directed mutagenesis
PublikacjaSite-directed mutagenesis of the CaGFA1 gene encoding glucosamine-6-phosphate synthase from Candida albicans was performed. Desensitization of the enzyme to inhibition by UDPGlcNAc was achieved upon T487I and H492F substitutions at the UDP-GlcNAc binding site, exchange of D524, S525 and S527 for Ala at the dimer:dimer interface and construction of the tail-lock array (L434R and L460A) at the C-tail region. The first two sets if...
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Optimisation of conditions for precipitation of collagen from solution using kappa-carrageenan. Studies on collagen from the skin of Baltic cod (Gadus morhua)
PublikacjaZbadano wpływ stężenia kolagenu (0,012-3%) wyekstrahowanego ze skór dorsza bałtyckiego (Gadus morhua) i stężenia kappa-karagenu w obecności NaCl (0-5%) na wydajność strącania włókien kolagenowych z roztworu przy pH 2,2-8. Stwierdzono, że wydajność strącania włókien jest wprost proporcjonalna do masowego stosunku kappa-karagen : kolagen w zakresie niższym od 0,4. Kolagen rozpuszczony w kwasie cytrynowym jest całkowicie strącony,...
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Assessment of image processing methods for the determination of propagation of squat-type defects in rails
PublikacjaWe demonstrate the idea of squat-type defect measurement in the rail and the concept of tracking of the defect development using the techniques of image acquisition and image processing as well as the methods of metric spaces. We introduce the concepts of a set diameter δ(A) and the metric ρ1, which come from the properties of plane figures, to compare and to observe the development of the defects. We characterize the feasibility...
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Wyznaczanie współczynnika dyspersji metodą kondultometryczną
PublikacjaW artykule przedstawiono konduktometryczną metodę wyznaczania współczynnika dyspersji w przypadku jednowymiarowym statystyczną metodą Fischera. Obliczenia wykonano na podstawie pomiarów przewodności nierozkładalnego trasera w postaci roztworu solanki (NaCl). Do tego celu wykonane zostało stanowisko pomiarowe złożone z prostego odcinka rurociągu wykonanego z polipropylenu o średnicy D=15 mm i długości L=44,05 m. Na wlocie i wylocie...
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Development of an orbital shaker-assisted fatty acid-based switchable solvent microextraction procedure for rapid and green extraction of amoxicillin from complex matrices: Central composite design
PublikacjaIn this study, a cheap, fast and simple orbital shaker-assisted fatty acid-based switchable solvent microextraction (OS-FASS-ME) procedure was developed for the extraction of amoxicillin (AMOX) in dairy products, pharmaceutical samples and wastewater prior to its spectrophotometric analysis. Fatty acid-based switchable solvents were investigated for extracting AMOX. The key factors of the OS-FASS-ME procedure were optimized using...
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Magnetic hydrophobic deep eutectic solvents for orbital shaker-assisted dispersive liquid-liquid microextraction (MAGDES-OS-DLLME) - determination of nickel and copper in food and water samples by FAAS
PublikacjaIn this work, a cheap and widely applicable dispersive liquid-liquid microextraction (DLLME) method was developed for the extraction of Ni(II) and Cu(II) from water and food samples and analysis using flame atomic absorption spectrometry. DLLME was assisted by orbital shaker, while ferrofluid as an extractant was based on deep eutectic solvent (DES). This ferrofluid was made of hydrophobic DES (hDES), composed of lauric acid and...
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Investigation of use of hydrophilic/hydrophobic NADESs for selective extraction of As(III) and Sb(III) ions in vegetable samples: Air assisted liquid phase microextraction and chemometric optimization
PublikacjaIn this paper, a green, cost-effective sample preparation method based on air assisted liquid phase microextraction (AA-LPME) was developed for the simultaneous extraction of As(III) and Sb(III) ions from vegetable samples using hydrophilic/hydrophobic natural deep eutectic solvents (NADESs). Central composite design was used for the optimization of extraction factors including NADES volume, extraction cycle, pH, and curcumin concentration....
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Nowa metoda diagnostyki stanu technicznego nakładek stykowych
PublikacjaThe current collection system, which consists of the overhead contact line and a current collector, is particularly important in electric rail vehicles, where their reliability is concerned. Faultless current collection is conditioned not only by suitable construction of these elements but also by their proper maintenance. Retaining permanent electrical contact is essential in DC systems, where current demand is relatively high. In...
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Comparison of anti-plane surface waves in strain-gradient materials and materials with surface stresses
PublikacjaHere we discuss the similarities and differences in anti-plane surface wave propagation in an elastic half-space within the framework of the theories of Gurtin–Murdoch surface elasticity and Toupin–Mindlin strain-gradient elasticity. The qualitative behaviour of the dispersion curves and the decay of the obtained solutions are quite similar. On the other hand, we show that the solutions relating to the surface elasticity model...
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Compressive Strength and Leaching Behavior of Mortars with Biomass Ash
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On effective surface elastic moduli for microstructured strongly anisotropic coatings
PublikacjaThe determination of surface elastic moduli is discussed in the context of a recently proposed strongly anisotropic surface elasticity model. The aim of the model was to describe deformations of solids with thin elastic coatings associated with so-called hyperbolic metasurfaces. These metasurfaces can exhibit a quite unusual behaviour and concurrently a very promising wave propagation behaviour. In the model of strongly anisotropic...
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Design of metamaterials: Preface
PublikacjaThis special issue “Design of metamaterials” collects several papers that have presented theoretical, numerical, and experimental studies of metamaterials.
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Transverse surface waves on a cylindrical surface with coating
PublikacjaWe discuss the propagation of transverse surface waves that are so-called whispering-gallery waves along a surface of an elastic cylinder with coating. The coating is modelled in the framework of linearized Gurtin–Murdoch surface elasticity. Other interpretations of the surface shear modulus are given and relations to so-called stiff interface and stiff skin model are discussed. The dispersion relations are obtained and analyzed.
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Role of size scale of ZnO nanoparticles and microparticles on toxicity toward bacteria and osteoblast cancer cells
PublikacjaThe specific role of size scale, surface capping, and aspect ratio of zinc oxide (ZnO) particles on toxicity toward prokaryotic and eukaryotic cells was investigated. ZnO nano and microparticles of controlled size and mor- phology were synthesized by wet chemical methods. Cytotoxicity toward mammalian cells was studied using a human osteoblast cancer cell line and antibacterial activity using Gram-negative bacteria (Escherichia...
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Bilateral multi-issue negotiation of execution contexts by proactive document agents
PublikacjaA proactive document can react to its actual environment by autonomously selecting and performing actions integrated into its body and interact with its user. When migrating over a network of execution devices it may encounter diverse execution contexts, each one set up according to temporal characteristics of a receiving device and preferences of its owner. A concept to augment proactive documents with negotiation capability is...
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Microstructural aspects of corrosion of the SUPERSTON alloy after laser treatment
PublikacjaW artykule przedstawiono rezultaty obróbki laserowej stopu SUPERSTON w warunkach kriogenicznych i jej wpływ na mikrostrukturę i odporność korozyjną. Badania korozyjne zostały zrealizowane metodą potencjostatyczną w 3% NaCl, odporność korozyjna stopu zmieniała się wraz ze zmianą parametrów nadtapiania laserowego.
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Electrostatic interface recombination in the system of disordered materials characterized by different permittivities
PublikacjaWe report on the analysis of an electrostatic interface recombination in a system consisting of disordered organic materials. This process is a consequence of the polarization effect which takes place at the interface of two phases characterized by different permittivities. In this paper, the impact of tail and deep localized states on the recombination order is demonstrated. We also discuss the influence of temperature on this...
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Charakterystyka korozyjna stopów miedzi stosowanych na śruby okrętowe po obróbce laserowej w warunkach kriogenicznych
PublikacjaW artykule przedstwiono wpływ nadtapiania laserowego w warunkach kriogenicznych na właściwości korozyjne stopów MM55 i SUPERSTON, stosowanych na śruby okrętowe. Uzyskane wyniki potwierdzają możliwość rozdrobnienia mikrostruktury w warstwie nadtopionej oraz znaczącego podwyższenia właściwości korozyjnych badanych stopów w środowisku 3%NaCl.
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Naprężeniowe pękanie korozyjne złączy spawanych nowego stopu Al-Mg ALUSTAR
PublikacjaWykonano pomiary wytrzymałości na rozciąganie, wydłużenia, czasu do zniszczenia, przewężenia i energii zniszczenia stopu rozciąganego z małą szybkością w powietrzu i 3,5 roztworze NaCl. Oceniono podatność złączy spawanych na korozję naprężeniową oraz możliwość zastosowania stopu ALUSTAR w budowie jednostek pływających.
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An air-assisted dispersive liquid phase microextraction method based on a hydrophobic magnetic deep eutectic solvent for the extraction and preconcentration of melamine from milk and milk-based products
PublikacjaIn the current research, a fast and sustainable air-assisted hydrophobic magnetic deep eutectic solvent-based dispersive liquid phase microextraction followed by UV–Vis spectrophotometry measurements was optimized for the extraction and determination of melamine in milk and milk-based products. The central composite design was applied for the optimization of factors affecting the recovery of melamine. Quantitative extraction of...
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Ultrasound assisted dispersive solid phase microextraction using polystyrene-polyoleic acid graft copolymer for determination of Sb(III) in various bottled beverages by HGAAS
PublikacjaA new polyoleic acid-polystyrene (PoleS) block/graft copolymer was synthesized and applied as adsorbent for ultrasound assisted dispersive solid phase microextraction (UA-DSPME) of Sb(III) in different bottled beverages and analysis using hydride generation atomic absorption spectrometry (HGAAS). Adsorption capacity of the PoleS was 150 mg g−1. Several sample preparation parameters such as sorbent amount, solvent type, pH, sample...
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Wpływ przechyłki na zjawisko postępowania zużycia bocznego szyn kolejowych w łukach poziomych
PublikacjaDegradacja elementów nawierzchni kolejowej jest zagadnieniem bardzo złożonym, w które uwikłane jest wiele czynników związanych między innymi z układem geometrycznym toru kolejowego, właściwościami trybologicznymi poszczególnych elementów nawierzchni, jak również z parametrami podłoża gruntowego, a także z właściwościami samych pojazdów szynowych. W artykule omówiono jeden z powyższych problemów, tj. wpływ ukształtowania toru kolejowego...
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Electrochemical analysis of aluminium passive layer
PublikacjaZbadano proces pękania warstwy pasywnej na aluminium dla liniowo narastających naprężeń rozciągających oraz różnych warunków elektrochemicznych. Badania prowadzono w 0.1M NaCl metodą dynamicznej elektrochemicznej spektroskopii impedancyjnej przy różnych poziomach polaryzacji anodowej. Określono progową wartość naprężeń, przy której następowało zniszczenie warstwy pasywnej wskutek działania sił rozciągających.
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Reprezentation of mechanic hysteresis in a railway track using the Preisach model
PublikacjaThis paper presents an implementation of the classic scalar Preisach model to describe the hysteresis phenomenon created in a railway track subjected to lateral (in the horizontal plane) displacements. The principles of the Preisach theory and the scalar mathematical model of the mechanical hysteresis that is based on statistically distributed modified hysteresis operators are briefly presented. This article presents the characteristic...
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Interlayer defect evolution in an coating system on steel under hydromechanical loading
PublikacjaZaprezentowano wyniki pomiarów impedancyjnych obszaru międzywarstwowego w systemie powłokowym poddanym naprężeniom. Przedstawiono nowy sensor który jest zdolny do detekcji defektów w obszarze międzywarstwowym. Dwuwarstwowy system powłokowy przeznacziony do zastosowań morskich zbadano w celu określenia jego odporności na oddziaływanie cyklicznych naprężeń i zanurzeń w 3% roztworze NaCl.
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Influence of the heat treatment on corrosion characteristics of the Superston alloy
PublikacjaW artykule przedstawiono wpływ hartowania i odpuszczania na twardość i właściwości korozyjne stopu Superston, stosowanego na śruby okrętowe. Stwierdzono, iż hartowanie z temperatury 900 st.C i odpuszczanie w temperaturze 550 st.C znacząco podwyższa odporność na korozję stopu Superston w 3% roztworze NaCl w porownaniu ze stanem odlanym.
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Shaping of the turnout diverging track with variable curvature sections
PublikacjaThe paper presents an analytical method of shaping the turnout diverging railroad track with variable curvature segments on its length, which in an evident way distinguished it from a typical solution, made up of a single circular arc with no transition curves. Two separate causes including a linear and a nonlinear curvature one in the form of a polynomial have been examined. The obtained solutions of the problem have a universal...
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Framework for extracting rails and setting-out railway line axis based on UAV photogrammetric measurements
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Framework for extracting rails and setting-out railway line axis based on UAV photogrammetric measurements
PublikacjaTechnical diagnostics enables assessing the current technical condition of a railway line and adjacent infrastructure, and forecasting its changes over a specific time horizon. One of its elements is the periodic monitoring of rail position and their geometry. This article presents a new framework for the setting-out of a railway track axis. The process presented in the manuscript is based on the specific filtration and extraction...
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Evaluating Security and Resilience of Critical Networked Infrastructures after Stuxnet
PublikacjaThe chapter presents the current configuration of the simulation environment for the evaluations of the security and resilience of critical networked infrastructures, which enables simulations of Stuxnet-like attacks. The configuration includes new features added to the MAlSim - Mobile Agent Malware Simulator after the advent of Stuxnet in reference to the experiments aiming at the security evaluation of a power plant which we...
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Development of a vortex-assisted switchable-hydrophilicity solvent-based liquid phase microextraction for fast and reliable extraction of Zn (II), Fe (II), Pb (II), and Cd (II) from various baby food products
PublikacjaThis manuscript describes the development of a novel liquid phase microextraction (LPME) method for the extraction and determination of Zn (II), Fe (II), Pb (II), and Cd (II) in various infant/baby food and supplements products. The method is based on vortex-assisted extraction combined with a switchable-hydrophilicity solvent (SHS) sample preparation. The SHS, which undergoes reversible phase changes triggered by pH change, enables...
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KOOPERACYJNA TRANSMISJA DANYCH W SIECIACH BEZPRZEWODOWYCH
PublikacjaW referacie przedstawiono zagadnienia związane z transmisją kooperacyjną w sieciach bezprzewodowych. Transmisja kooperacyjna polega na wykorzystaniu termi-nali ruchomych jako stacji przekaźnikowych w celu po-prawy jakości transmisji, poprawy wydajności sieci i zmniejszenia zużycia energii. W referacie zaprezentowano metody stosowane do realizacji transmisji kooperacyjnej oraz rodzaje sieci kooperacyjnych.
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Multi-agent large-scale parallel crowd simulation with NVRAM-based distributed cache
PublikacjaThis paper presents the architecture, main components and performance results for a parallel and modu-lar agent-based environment aimed at crowd simulation. The environment allows to simulate thousandsor more agents on maps of square kilometers or more, features a modular design and incorporates non-volatile RAM (NVRAM) with a fail-safe mode that can be activated to allow to continue computationsfrom a recently analyzed state in...
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Use of a Least Squares with Conditional Equations Method in Positioning a Tramway Track in the Gdansk Agglomeration
PublikacjaSatellite measurement techniques have been used for many years in different types of human activity, including work related to staking out and making use of rail infrastructure. First and foremost, satellite techniques are applied to determine the tramway track course and to analyse the changes of its position during its operation. This paper proposes using the least squares with conditional equations method, known in geodesy (LSce)....
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Trwałość kompozytów popiołowo-cementowych modyfikowanych dodatkiem włókien szklanych i stalowych
PublikacjaKonieczność ochrony nieodtwarzalnych zasobów surowców mineralnych stwarza potrzebę wykorzystania surowców mniej wartościowych - piasków oraz odpadowych - popiołów lotnych. Wzrost wartości właściwości technicznych drobnoziarnistych kompozytów z popiołami postanowiono uzyskać przez modyfikację tych kompozytów niewielkimi dodatkami włókien szklanych i stalowych oraz domieszkę superplastikalną. Zbadano trwałość kompozytów poddanych...
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Water Solubilization Using Nonionic Surfactants from Renewable Sources in Microemulsion Systems
PublikacjaIn this study the effect of temperature, NaCl andoils (hydrocarbons: C8-C16) on the formation and solubilizationcapacity of the systems of oil/monoacylglycerols(MAG):ethoxylated fatty alcohols (CEO20)/propylene glycol(PG)/water was investigated. The effects of the surfactantmixture on the phase behavior and the concentration ofwater or oil in the systems were studied at three temperatures(50, 55, 60 C) and with varied NaCl solutions...
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Learning sperm cells part segmentation with class-specific data augmentation
PublikacjaInfertility affects around 15% of couples worldwide. Male fertility problems include poor sperm quality and low sperm count. The advanced fertility treatment methods like ICSI are nowadays supported by vision systems to assist embryologists in selecting good quality sperm. Computer-Assisted Semen Analysis (CASA) provides quantitative and qualitative sperm analysis concerning concentration, motility, morphology, vitality, and fragmentation....
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Increase of the effective energy from the radiant tube equipped with regenerative system in comparison with conventional recuperative system
PublikacjaPrzedstawiono wyniki badań eksperymentalnych spalania HiTAC (High Temperature Air Combustion) z użyciem rury promieniującej w celu porównania systemu palników regeneracyjnych z konwencjonalnym systemem rekuperacyjnym.
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Approaches to Static Digestion Models
PublikacjaIt is not possible to look in detail at the wide range of static digestion methods that have been used to date. However, this section looks at some of the general approaches that have been used to look at the digestion of various nutrients and bioactives. I have focussed on the two main nutrients that undergo digestion in the upper GI tract, namely protein and lipid. In the case of protein, the research has largely been driven...
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Method of sacrificial anode dual transistor-driving in stray current field
PublikacjaIn order to control a magnesium anode in a stray current interference field, a dual transistor driving system has been proposed. It consisted of a combination of PNP and NPN transistors. Dual transistor driven system and direct anode to cathode connection were electrochemically tested in 3% NaCl solution. The dual transistor driven system increased the anode efficiency and reduced hydrogen evolution and the risk of embrittlement....
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Simple Fractal Calculus from Fractal Arithmetic
PublikacjaNon-Newtonian calculus that starts with elementary non-Diophantine arithmetic operations of a Burgin type is applicable to all fractals whose cardinality is continuum. The resulting definitions of derivatives and integrals are simpler from what one finds in the more traditional literature of the subject, and they often work in the cases where the standard methods fail. As an illustration, we perform a Fourier transform of a real-valued...
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Friction and wear behaviour of self mated DLC and DLC-W coatings in water or salt in water solution lubricated sliding
PublikacjaPrzedstawiono wyniki badań powłok ceramicznych DLC oraz DLC z wolframem (DLC-W) nałożonych na podłoże ze stali nierdzewnej,przy tarciu ślizgowym , w modelowym skojarzeniu o styku konforemnym (płaskie czoło obracającej się względem swojej osi tulei - powierzchnia płaska). Badania prowadzono stosując smarowanie wodą destylowaną albo wodnym roztworem soli - NaCl. Wyznaczano współczynniki tarcia oraz intensywność zużywania ceramicznej...
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Novel method of initiation stage of stress corrosion cracking monitoring with respect to marine constructions
PublikacjaKorozja konstrukcji morskich i jednostek pływających stanowi bardzo ważny problem w odniesieniu do aspektów bezpieczeństwa, gdyż w całym okresie eksploatacji narażone są na działanie bardzo agresywnego środowiska i innych czynników eksploatacyjnych. W rezultacie prowadzi to do niespodziewanych kolizji i wypadków. Praca przedstawia zastosowanie dynamicznej elektrochemicznej spektroskopii impedanycjnej (DEIS) do badania inicjacji...
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Zarządzanie zdarzeniami na platformie KASKADA
PublikacjaZdefiniowano pojęcie zdarzenia i opisano proces obsługi zdarzeń w ramach platformy KASKADA, wprowadzając pojęcia strumieni zdarzeń, filtrów zdarzeń i kanałów zdarzeń typu e-mail i JMS. Przedstawiono sposób monitorowania zdarzeń bieżących i przeszłych. Wyszczególniono rozwiązania implementacyjne procesu przetwarzania zdarzeń uwzględniające komponentową architekturę platformy KASKADA, uwypuklając ich elastyczność w przypadku rozwoju...