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Search results for: ULTRA-FAST GC
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Application of gas chromatography,mass spectrometry and olfactometry for quality assessment of selected food products = Zastosowanie chromatografii gazowej, spektrometrii mas i olfaktometrii w ocenie jakości wybranych produktów spożywczych
PublicationStosując mikroekstrakcję do fazy stacjonarnej z fazy nadpowierzchniowej jako metodę przygotowania próbek i chromatografię gazową (GC) ze spektrometrią mas (MS) i olfaktometrią (O) jako metodę oznaczeń końcowych oznaczono lotne związki w spirytusach i miodach. Identyfikację przeprowadzono przez porównanie widm masowych z widmami z biblioteki NIST. Dodatkowo, wykrywane przez panel oceniający związki zapachowe rejestrowano w formie...
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Potentiometric Solid-Contact Ion-Selective Electrode for Determination of Thiocyanate in Human Saliva
PublicationA new solid-contact potentiometric ion-selective electrode for the determination of SCN− (SCN-ISE) has been described. Synthesized phosphonium derivative of calix[4]arene was used as a charged ionophore. The research included selection of the ion-selective membrane composition, determination of the ISEs metrological parameters and SCN-ISE application for thiocyanate determination in human saliva. Preparation of the ISEs included...
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Blood concentrations of a new psychoactive substance 4-chloromethcathinone (4-CMC) determined in 15 forensic cases
PublicationPurpose: The 4-chloromethcathinone (4-CMC) is a synthetic derivative of cathinone and belongs to new psychoactive substances. Neither data on the effects of 4-CMC on the human body, nor on nontoxic, toxic and lethal concentrations in biological materials have been published in the literature. This paper describes the results of an analysis of the blood concentrations of 4-CMC determined in 15 forensic cases related to nonfatal...
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Green capsule phase microextraction employing hydrophobic monolithic sol-gel octadecyl siloxane platforms for the monitoring of organophosphorus pesticides in environmental water samples
PublicationIn this study, a novel, facile and green capsule phase microextraction (CPME) method is presented for the extraction and preconcentration of organophosphorus pesticides (i.e., chlorpyrifos, disulfoton, ethoprophos, fenchlorphos, prothiofos, and parathion-methyl) from environmental water samples. Monolithic sol-gel octadecyl siloxane (sol-gel C18) sorbent encapsulated within porous polypropylene capsules was synthesized, characterized,...
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Substrate-integrated waveguide (SIW) filter design using space mapping
PublicationIn this paper, we present a fast technique for an automated design of microwave filters in substrate integrated wave (SIW) technology. The proposed methodology combines the space mapping technique with a cost function defined using the location of complex zeros and poles of filter’s transfer and reflection function and uses a rectangular waveguide as a surrogate model. The effectiveness of the proposed technique is presented with...
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A structure and simulation-driven design of compact CPW-fed UWB antenna
PublicationIn this letter, a structure of a miniaturized ultra-wideband CPW-fed antenna and its design proce-dure are presented. The antenna is a modified version of the design previously proposed in the literature, with additional degrees of freedom introduced in order to improve the structure flexibility. The small size is achieved by executing a rigorous optimization procedure that consists of two stages: (i) smart random search carried...
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On-line measurement of wood surface smoothness
PublicationThe latest progress in the field of optics and microelectronics resulted in development of new generation vision systems capable of scanning surface topography with very high sampling frequencies. The blue color of illuminating light as well as novel systems for controlling ultra-thin laser line thickness allows measurement of the porous surface of wood with a triangulation method. Three alternative sensors were tested here in...
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The Current State-of-the-Art in the Determination of Pharmaceutical Residues in Environmental Matrices Using Hyphenated Techniques
PublicationSeveral thousand tons of pharmaceuticals and their transformation products (metabolites and degradation products) are introduced into the environment each year. They affect both human health and the environment, therefore, analytical procedures enabling the determination of a wide range of pharmaceuticals at trace levelswithminimal effort, time, and energy are required. Nowadays, hyphenated techniques are commonly applied in pharmaceutical...
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Analiza sieci bezprzewodowych serii IEEE 802.15.x - Bluetooth (BT), UWB i ZigBee - z transmisją wieloetapową. Część I
PublicationW artykule zaprezentowano ogólną koncepcję pracy bezprzewodowych sieci mesh (Wireless Mesh Networks - WMNs), tj. sieci ad hoc z topologią złożoną (kratową) i z transmisją wieloetapową. Opisano podstawowe problemy projektowania i implementacji sieci WMN. Przedstawiono ogólne założenia nowego standardu IEEE 802.15.5 - WPAN Mesh. Skoncentrowano się przy tym na opisie i analizie bezprzewodowych sieci złożonych typu WPAN, realizowanych...
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Analiza sieci bezprzewodowych serii IEEE 802.15.x - Bluetooth (BT), UWB i ZigBee - z transmisją wieloetapową. Część II
PublicationW artykule zaprezentowano ogólną koncepcję pracy bezprzewodowych sieci mesh (Wireless Mesh Networks - WMNs), tj. sieci ad hoc z topologią złożoną (kratową) i z transmisją wieloetapową. Opisano podstawowe problemy projektowania i implementacji sieci WMN. Przedstawiono ogólne założenia nowego standardu IEEE 802.15.5 - WPAN Mesh. Skoncentrowano się przy tym na opisie i analizie bezprzewodowych sieci złożonych typu WPAN, realizowanych...
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ENHANCED MASTER CYCLE - SIGNIFICANT IMPROVEMENT OF STEAM RANKINE CYCLE
PublicationThe present paper focuses on an enhancement of the Master Cycle. In the first part, the paper presents a classical Master Cycle which is a modification of the double reheat Rankine cycle. This modification allows to slightly increase efficiency, resolves problems caused by superheated steam on bleeds and decreases mass flow rate of steam directed to reheat. These improvements include the implementation of a tuning turbine from...
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Analiza siłowni nadkrytycznych oraz ultranadkrytycznych
PublicationNiniejszy artykuł zawiera przegląd istniejących rozwiązań siłowni nadkrytycznych oraz ultra nadkrytycznych. Przedstawiono historię rozwoju bloków na parametry nadkrytyczne. Obecny stan technologii został zaprezentowany – są to następujące parametry pary świeżej: 650°C oraz 330 bar. W Polsce istnieje 8 bloków pracujących na parametry nadkrytyczne. Ich parametry pracy zostały przedstawione w tekście. Z kolei elektrownią parową posiadającą...
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Nos elektroniczny - użyteczne narzędzie w analizie żywności
PublicationW artykule przedstawiono nowoczesne instrumentalne techniki stosowane w analizie związków zapachowych obecnych w żywności, a także ich przydatność w kontroli jakości produktów spożywczych. Główną uwagę poświęcono elektronicznym nosom. Opisano zasadę działania, zjawiska fizyczne i fizykochemiczne wykorzystywane przez czujniki takich urządzeń oraz metody analizy sygnału. Porównano tę metodę z techniką chromatografii gazowej sprzężonej...
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Impact of pollution derived from ship wrecks on the marine environment on the basis of s/s ''Stuttgart'' (Polish coast, Europe)
PublicationW 1943 roku niemiecki statek szpitalny, s/s Stuttgart (Lazaretschiff ''C'') został zatopiony w pobliżu portu w Gdyni. Doprowadziło to do zanieczyszczenia dna morskiego paliwem. Podczas badań przeprowadzonych w 2009 r. pobranych zostało 11 próbek osadów powierzchniowych i wody morskiej oraz 4 rdzenie. Próbki poddano analizie na zawartość zanieczyszczeń priorytetowych należących do grupy wielopierścieniowych węglowodorów aromatycznych...
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Determination of the substances potentially allergenic in water
PublicationPersonal care chemicals are continuously released into environment through domestic and industrial wastewater, causing adverse effects on human health. Their presence can be detected in different environmental compartments. A group of chemicals included in most personal care products are the allergen fragrances. In the present work, simple and rapid methodology based on ultrasound-assisted emulsification-microextraction (USAEME)...
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Studies on solid phase microextraction-gas chromatographic determination of volatile chloroorganic pollutants in soil. badanie lotnych związków chloroorganicznych w glebie przy użyciu techniki mikroekstrakcji do fazy stacjonarnej i chromatografii gazowej.
PublicationLotne związki chloroorganiczne (VOXs) mogą być obecne w powietrzu, wodzie i glebie. Związki te mają właściwości kancerogenne, dlatego też ich ilość w środowisku powinna być monitorowana. W pracy przedstawiono badania nad możliwością zastosowania techniki izolacji i wzbogacania jaką jest mikroekstrakcja do fazy stacjonarnej, jej przydatność w analizie lotnych węglowodorów chloroorganicznych w różnych typach gleb z wykorzystaniem...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,4 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,4 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,5 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,5 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec (1 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,4 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,4 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec in order to examine the fast fluctuations of sample temperature during charging - discharging...
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Tuning a Hybrid GPU-CPU V-Cycle Multilevel Preconditioner for Solving Large Real and Complex Systems of FEM Equations
PublicationThis letter presents techniques for tuning an accelerated preconditioned conjugate gradient solver with a multilevel preconditioner. The solver is optimized for a fast solution of sparse systems of equations arising in computational electromagnetics in a finite element method using higher-order elements. The goal of the tuning is to increase the throughput while at the same time reducing the memory requirements in order to allow...
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DIGITAL HYDRAULICS CIRCUIT BASED ON PWM FUNCTION FOR CONTROLLING HYDRAULIC ACTUATOR POSITION
PublicationHydraulic systems are used in many different industries, such as multi-source hydrostatic drive systems. In traditional hydraulic systems, a proportional servo valve is used to control the position of hydraulic actuators. The low energy efficiency and high cost of these control valves are two major problems with these systems. Digital hydraulics is one of the most unique ideas on how to solve these problems. Researchers like digital...
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Wykorzystanie technik instrumentalnych do oceny jakości organoleptycznej i rozróżniania destylatów rolniczych i miodów
PublicationPodstawowym celem pracy było opracowanie nowych metod oceny jakości organoleptycznej i rozróżniania destylatów rolniczych i miodów przy wykorzystaniu wybranych technik instrumentalnych, a następnie określenie jakie związki i w jakich ilościach występują w lotnej frakcji omawianych produktów i półproduktów oraz znalezienie różnic w składzie lotnych związków zapachowych w destylatach rolniczych różnej jakości organoleptycznej i miodach...
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Wielowymiarowa chromatografia cieczowa jako technika przygotowania próbki i oznaczania składu grupowego skomplikowanych mieszanin substancji
PublicationCelem ogólnym niniejszej rozprawy doktorskiej jest opanowanie problemu doboru optymalnych warunków przygotowania próbki, z uwzględnieniem rozdzielania grupowego w celu zapewnienia możliwości oznaczania zawartości wybranych analitów lub grup analitów w materiałach stanowiących skomplikowane mieszaniny bardzo wielu substancji. W części wprowadzającej pracy dokonano przeglądu i poddano krytycznej ocenie istniejące techniki i metody...
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Szybka identyfikacja harmonicznych na podstawie oszczędnego próbkowania
PublicationW pracy przedstawiono implementację szybkiego algorytmu rekonstrukcji sygnału, opartego na teorii oszczędnego próbkowania, który może wykrywać harmoniczne w sygnale wejściowym. Zagadnienie rekonstrukcji sygnału jest problemem optymalizacyjnym rozwiązywanym za pomocą algorytmu programowania liniowego. Dodatkowo, aby przyspieszyć zbieżność rozwiązania zastosowano w rzadkiej dziedzinie sygnału filtr typu K-rank-order. Przeprowadzona...
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Marek Czachor prof. dr hab.
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IATUL Fall Seminar - Connecting in a disconnected world.
Events We invite both current community members and other people interested in IATUL's activities to the online seminar on December 15, 2021. During the meeting, we will talk about the mission and activities of the organisation, as well as the benefits of belonging to the IATUL community. In addition, Special Interest Groups (SIGs), analysing...
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Przyszłość energetyki jądrowej na świecie
PublicationProblemy dostępności paliwa jądrowego i składowania odpadów radioaktywnych skłaniają do przemian w technologii reaktorów jądrowych w kierunku generacji IV. Równolegle obserwuje się rozwój reaktorów małej i średniej mocy. Obie ścieżki wydają się być słuszne i obiecujące. W przypadku małych reaktorów jądrowych, pierwsze instalacje mogą powstać w najbliższych pięciu latach, niektóre z nich mogą zaliczać się do reaktorów IV generacji....
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Występowanie i oznaczanie lotnych kwasów tłuszczowych w próbkach środowiskowych
PublicationLotne kwasy tłuszczowe (LKT) odgrywają kluczową rolę w biologicznym oczyszczaniu ścieków. Występują one także w osadzie ściekowych, w odciekach na składowiskach odpadów. Są odpowiedzialne za tworzenie się odorów podczas hodowli trzody chlewnej. Powstają również w wielu procesach naturalnych. Ważną rolę w monitorowaniu LKT, co jest bardzo istotne, odgrywa chromatografia gazowa, która pozwala je oznaczać w postaci wolnej oraz po...
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain alkane monocarboxylic acids in aqueous samples
PublicationCelem prowadzonych badań było opracowanie metodyki oznaczania krótkołańcuchowych kwasów alkanomonokarboksylowych (KKA), opartej na ich izolowaniu i wzbogacaniu za pomocą techniki HS-SPME, a następnie oznaczaniu za pomocą chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS). Do ekstrakcji zastosowano włókno pokryte polarną fazą stacjonarną opartą na glikolu polietylenowym (PEG). Dla celów porównawczych zastosowano również...
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Methods of assaying volatile oxygenated organic compounds in effluent samples by gas chromatography—A review
PublicationThe paper is a review of the procedures for the determination of volatile and semivolatile oxygenated organic compounds (O-VOCs) in effluent samples by gas chromatography. Current trends and outlook for individual steps of the procedure for the determination of O-VOCs in effluents are discussed. The available sample preparation techniques and their limitations are described along with GC capillary columns used for O-VOCs separation...
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Wpływ kierowcy na opór toczenia samochodu
PublicationW pracy omówiono wpływ zachowań kierowcy na opory toczenia pojazdu w ruchu drogowym. Można tu wyróżnić styl jazdy kierowcy oraz jego dbałość o pojazd. Przedstawiono wzrost oporu toczenia w aspekcie dynamicznego przyspieszania oraz szybkiej jazdy na zakręcie. Przeanalizowano także wpływ na opór toczenia takich czynników jak: ciśnienie w ogumieniu obciążenie promieniowe, zbieżność kół jezdnych samochodu oraz zużycie ogumienia.
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ALDAMS Lifetime extension of high chromium ferritic porous alloys by application of ultra-thin aluminium oxide coatings
ProjectsProject realized in Katedra Inżynierii Materiałów Funkcjonalnych WETI according to UMO-2022/45/N/ST8/03351 agreement from 2023-01-16
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Modal parameters identification with Particle Swarm Optimization
PublicationThe paper presents method of the modal parameters identification based on the Particle Swarm Optimization (PSO) algorithm [1]. The basic PSO algorithm is modified in order to achieve fast convergence and low estimation error of identified parameters values. The procedure of identification as well as algorithm modifications are presented and some simple examples for the SISO systems are provided. Results are compared with the results...
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On various modelling approaches to real-time visualisation of blood flow
PublicationThis paper reviews various modelling approaches to real-time visualisation of blood flow. These include classic, macroscale approach based on the momentum conservation equation together with a proper constitutive equation. Moreover, modern micro- and mesoscale approaches, such as molecular dynamics and dissipative particle dynamics, are discussed. Advantages and disadvantages of the discussed methods are highlighted with particular...
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Isolation of xanthone and benzophenone derivatives from Cyclopia genistoides (L.) Vent. (honeybush) and their pro-apoptotic activity on synoviocytes from patients with rheumatoid arthritis
PublicationA fast and efficient method for the isolation of the C-glucosidated xanthones mangiferin and isomangiferin from the South-African plant Cyclopia genistoides was developed for the first time. Two benzophenone derivatives: 3-C-β-glucosides of maclurin and iriflophenone, were isolated from C. genistoides extracts using semi-preparative. The structures of the compounds were determined by 1D and 2D NMR experiments and/or LC-DAD-ESI–MS.
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Investigation on air quality of specific indoor environments—spa salons located in Gdynia, Poland
PublicationDue to excessive application of essential oils and scented products in spa salons during aromatherapy and massage sessions, the elevated concentration of total volatile organic compounds (TVOCs), particularly terpenes, which are known as secondary organic aerosol (SOA) precursors, is expected there. This study was aimed at determination of VOCs with a particular regard to terpenes in air samples collected in selected spa salons...
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Determination of MDPBP in postmortem blood samples by gas chromatography coupled with mass spectrometry
PublicationMDPBP (1-(3,4-methylenedioxyphenyl)-2-(1-pyrrolidinyl)-1-butanone) is a new psychoactive substance sold on the black market. It has been a controlled drug of abuse in Poland and China since 2015 as some toxic and fatal cases connected with use of synthetic cathinone derivatives were observed. The fatal case outlined here concerns a 19 year-old man, who was found dead with an envelope containing white powder lying nearby the cadaver....
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Influence of steam cooking on pro-health properties of Small and Large variety of Momordica charantia
PublicationSteam cooking is one of the most common preparations of Momordicacharantia dishes. This method improved the tastiness of the fruits but at the same time, some changes occurred in the volatile and non-volatile parts of their food matrices. In this study, for the first time these properties were correlated with the found substances affecting the bioactivity of this fruit. Two varieties of Momordicacharantia were analysed and compared....
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Multi-objective design optimization of antennas for reflection, size, and gain variability using kriging surrogates and generalized domain segmentation
PublicationCost-efficient multi-objective design optimization of antennas is presented. The framework exploits auxiliary data-driven surrogates, a multi-objective evolutionary algorithm for initial Pareto front identification, response correction techniques for design refinement, as well as generalized domain segmentation. The purpose of this last mechanism is to reduce the volume of the design space region that needs to be sampled in order...
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The electrochemical determination of isatin at nanocrystalline boron-doped diamond electrodes: stress monitoring of animals
PublicationUltra-thin nanocrystalline boron-doped diamond electrodes (B:NCD) were used for the electrochemical determination of isatin in dog urine samples using cyclic voltammetry and square wave voltammetry in a phosphate buffer saline, pH = 7.2. No additional modification or pretreatment of the electrode surface was required in this approach, being of high importance for the facile detection procedure. The increase of the peak current...
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Parameters of land reference points in the Gdynia region and the Free-air anomaly grid of the South Baltic
Open Research DataThe data was registered during the campaign to verify the catalog value of the absolute point coordinates [point 5403 (POLREF-GORA DONAS)] of the national gravimetric control network. The data was recorded in two three-hour stationary measurement campaigns at the following points: Rozewie of the EUREF-POL network, Góra Donas POLREF, and mareograph points...
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Reduction of the strontium titanate doped by Ytrium ceramics observed by X-ray photoemission spectroscopy method
Open Research DataYtrium-doped strontium titanate (YSTF) ceramics materials were manufactured by three various methods: 1) standard solid-state reaction method from Y2O3 (Sigma Aldrich, 99,9%), TiO2 (Sigma Aldrich, 99%) and SrCO3 (Sigma Aldrich,98%), 2) Pechini method, 3) wet method.
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FFT spectrum based matching algorithm for activedynamic thermography
PublicationIn Active Dynamic thermography (ADT) sequences of consecutive temperature distributions are analyzed. In biomedical applications of ADT, the problems of a patient's movements in front of a thermal camera should be eliminated before data analysis. Complete mechanical stabilization of the patients is impossible due to natural voluntary and involuntary moves caused by pulse breathing, etc. This paper presents a simple and efficient...
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Detection of illicit chemicals by portable Raman spectrometer
PublicationThe Raman spectrometers can be built as the portable devices and can be used in various places to detect illicit chemicals. This method has become popular due to deficiency of other fast methods that could be applied against terrorist attacks or could help police at their work. The conception of a portable Raman spectrometer has been presented. The description enclosures presentation of the prepared device and its possible applications...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 0,5 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 0,5 sec (2 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Thermographic imaging of electrochemical double layer capacitors during cycling charging - discharging 0 - 3,6 V at 420 mA. Sample 103. Image period: 1 sec.
Open Research DataDataset contains thermal images of prototype electrochemical double layer capacitor taken during cyclic charging - discharging. The sample was charged to 3,6 V and discharged to 10 mV by constant current 420 mA. Sample 103. Pictures were taken with period of 1 sec (1 Hz) in order to examine the fast fluctuations of sample temperature during charging...
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Exploration of optical fibres as a carrier for new benzene and toluene matrix-free reference materials
PublicationTo meet high expectations concerning precision and accuracy of reference materials, preparation of matrixfree reference materials using thermal decomposition-gas chromatography-mass spectrometry (TD-GC-MS) was proposed in this study. In the paper, the results obtained in preparation of the new reference materials for benzene and toluene are presented, based on the thermal decomposition technique of compounds chemically bound to...
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Synergistic Effects of Bitumen Plasticization and Microwave Treatment on Short-Term Devulcanization of Ground Tire Rubber
PublicationGround tire rubber (GTR) was mechano-chemically modified with road bitumen 160/220 and subsequently treated using a microwave radiation. The combined impact of bitumen 160/220 content and microwave treatment on short-term devulcanization of GTR was studied by thermal camera, wavelength dispersive X-ray fluorescence spectrometry (WD-XRF), static headspace, and gas chromatography-mass spectrometry (SHS-GC-MS), thermogravimetric analysis...