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Search results for: RAPESEED OIL THERMAL DEGRADATION MULTI-DIMENSIONAL GAS CHROMATOGRAPHY PROTON TRANSFER REACTION MASS SPECTROMETRY FOOD CONTROL FOOD QUALITY
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Development of chromatographic and mass spectrometry conditions for untargeted lipidomic analysis of human breast milk
PublicationHuman breast milk (HBM) is a complex biofluid containing components which are essential for the proper growth of the newborn (for example nutrients such as carbohydrates, proteins, lipids) and also bioactive substances. According to the literature, most of studies involving HBM nutrients investigations focused essentially on the determination of proteins. The molecular composition of lipids in HBM is not well known as the protein...
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Application of Thermo-chemical Technologies for Conversion of Associated Gas in Diesel-Gas Turbine Installations for Oil and Gas Floating Units
PublicationThe paper considers the issue of thermo-chemical recovery of engine’s waste heat and its further use for steam conversion of the associated gas for oil and gas floating units. The characteristics of the associated gas are presented, and problems of its application in dual-fuel medium-speed internal combustion engines are discussed. Various variants of combined diesel-gas turbine power plant with thermo-chemical heat recovery are...
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Possibility of thermal imaging use in studies of natural convection heat transfer on the example of an isothermal vertical plate.
PublicationA new method of infrared (IR) camera use in convective heat transfer studies has been presented. Until now, IR cameras were utilized for temperature field visualizations of flat heated surfaces of solid objects only. Because liquids and gasses do not emit radiation in the infrared range of wave lengths, detection of temperature field in the air was conducted with the use of plastic mesh, which, after heating by hot air, emits infrared...
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Analysis of essential oils through comprehensive two-dimensional gas chromatography: General utility
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Chemometric Assessment and Best-Fit Function Modelling of the Toxic Potential of Selected Food Packaging Extracts
PublicationFood packaging materials constitute an ever more threatening environmental pollutant. This study examined options to specifically assess the ecotoxicity of packaged wastes, such as cans, subjected to various experimental treatments (in terms of extraction media, time of exposure, and temperature) that imitate several basic conditions of the process of food production. The extracts were studied for their ecotoxicity with bioluminescent...
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Methods of assaying volatile oxygenated organic compounds in effluent samples by gas chromatography—A review
PublicationThe paper is a review of the procedures for the determination of volatile and semivolatile oxygenated organic compounds (O-VOCs) in effluent samples by gas chromatography. Current trends and outlook for individual steps of the procedure for the determination of O-VOCs in effluents are discussed. The available sample preparation techniques and their limitations are described along with GC capillary columns used for O-VOCs separation...
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Pollutants transfer phenomena
e-Learning CoursesSubject considering fundamentals of the heat and mass transfer in the environment.
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Characterization of volatile compounds, structural, thermal and physico-mechanical properties of cross-linked polyethylene foams degraded thermo-mechanically at variable times
PublicationWaste cross-linked polyethylene foam (wXLPE) was thermo-mechanically degraded at variable time using internal batch mixer. The progress of wXLPE degradation has been investigated by using a simultaneous thermogravimetric/differential scanning calorimetry analyzer coupled with Fourier transform infrared spectroscopy, swelling measurements, tensile tests and scanning electron microscopy. Volatile organic compounds generated during...
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The impact of lipophilicity on environmental processes, drug delivery and bioavailability of food components
PublicationLipophilic properties of the compound allow to predict its fate in living organisms and to propose the models of chemicals transport and accumulation in the ecosystem. Lipophilicity is also useful as the characteristic of chemicals in respect to their optimal attributes for specific biological and non-biological tasks. The lipophilicity descriptors define the potency of endo- and xenobiotics to metabolic transformations and their...
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Polyurethane/Silane-Functionalized ZrO2 Nanocomposite Powder Coatings: Thermal Degradation Kinetics
PublicationA polyurethane (PU)-based powder coating reinforced with vinyltrimethoxysilane (VTMS)-functionalized ZrO2 nanoparticles (V-ZrO2) for thermal stability was developed. Chemical structure, microstructure and thermal degradation kinetics of the prepared coatings were investigated. The peak of aliphatic C–H vibrating bond in the Fourier transform infrared (FTIR) spectrum of V-ZrO2 was a signature of VTMS attachment. Scanning electron...
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Analysis the Parameters of the Adaptive Controller for Quality Control of Dissolved Oxygen Concentration
PublicationThe wastewater treatment plant can be considered a dynamic large scale complex system, in which the most important control parameter is the dissolved oxygen concentration in the aerobic zone. The air is supplied to this zone by the aeration system. In the paper, both the sequencing batch reactor and the aeration system are modelled and used as plant of control performed by the cascade nonlinear adaptive control system extended...
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Extraction pathways and purification strategies towards carminic acid as natural-based food colorant: A comprehensive review
PublicationAs a current trend of fabricating healthier products, food manufacturing companies seek for natural-based food colorant aiming to replace the synthetic ones, which apart from meeting sensorial and organoleptic aspects, they can also act as health promoters offering additional added value. Carminic acid is a natural based food colorant typically found in several insect taxa. However, there are current approaches which pursue the...
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Photoinduced and thermal oxidation of rapeseed and sunflower oils
PublicationCelem prezentowanych badań było porównanie stabilności oksydatywnej olejów rzepakowych i słonecznikowych. Na etapie przyspieszania utleniania zastosowano promieniowanie UV. Po naświetlaniu lotne produkty utlenienia były izolowane z fazy nadpowierzchniowej przy pomocy mikroekstrakcji do fazy stacjonarnej HS-SPME(włókno DVB/CAR/PDMS) i oznaczane z zastosowaniem chromatografii gazowej z detektorem płomieniowo-jonizacyjnym (GC/FID)....
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Process Control and Investigation of Oxidation Kinetics of Postoxidative Effluents Using Gas Chromatography with Pulsed Flame Photometric Detection (GC-PFPD)
PublicationThis article presents the results of investigations on the use of headspace analysis and gas chromatography with pulsed flame photometric detection (HSA-GC-PFPD) to evaluate the effectiveness of oxidation of postoxidative effluents from the production of bitumens. Samples of effluents from the bitumen oxidation unit were used in the experiments. In addition, the kinetics of effluent oxidation was also investigated. The content...
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The impedance of hydrogen oxidation reaction in a proton exchange membrane fuel cell in the presence of carbon monoxide in hydrogen stream
PublicationEvaluation of performance of a proton exchange membrane fuel cell, which is affected by carbon monoxide that pollutes the hydrogen stream, was presented. This influence was studied for carbon monoxide concentration of 125–325 ppb, which are close to values specified in ISO 14687:2019 standard. Performed studies provided crucial information for further development of fuel cell as an energy source for automotive application. Impedance...
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Multidimensional Gas Chromatography in Essential Oil Analysis. Part 2: Application to Characterisation and Identification
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Biological Activity and Antibiofilm Molecular Profile of Citrus aurantium Essential Oil and Its Application in a Food Model
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Rheological properties of food systems
PublicationPrzedstawiono ocenę systemów żywności pod względem ich właściwości reologi-cznych. Dla określonego schematu podziału opisano podstawowe sposoby pomiaruwłaściwości w tych strukturach. Na podstawie przyjętego modelu reologicznegooraz rozpoznanych sił i zależności działających w odpowiednim zestawie skła-dników struktury żywności, określono wpływ zmian reologicznych na cechy sen-soryczne w niektórych systemach żywności.
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Nanotechnology for Enhancement of Food Value
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Plant Biotechnology in Food Security
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New Economy, Food, and Agriculture
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New Economy, Food, and Agriculture
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Simultaneous determination of hydrophobicity and dissociation constant for a large set of compounds by gradient reverse phase high performance liquid chromatography–mass spectrometry technique
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Approach Manoeuvre During Emergency Ship-to-Ship Transfer Operation with Oil Spill
PublicationOne of the major activities during Ship to Ship (STS) transfer operation at sea is to safe approach the Ship to be Lightered (SBL) which moves on a constant heading with slow speed or drifting. In the paper described the manoeuvring problem for approaching during emergency STS transfer operation with oil spill. The approach manoeuvre is considered as a sequence of navigation manoeuvres in specific navigational environment with...
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Assessment of cytotoxic and endocrine potential of selected xenobiotics commonly present in food products
PublicationMore and more increased intensity of anthropopressure processes can be observed, among other things, in the release of great quantities of synthetic substances into the environment, including the Endocrine Disrupting Compounds (EDC). A vast number of chemical substances is considered to belong to the this group, including substances which occur naturally in the environment, such as mycotoxins and phytoestrogens, and substances...
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Quality of Service in ASON/GMPLS Network with Hierarchical Control Plane Structure
PublicationThe paper presents the problem of quality of service for hierarchical control plane structure of Automatically Switched Optical Network (ASON) utilizing Generalized Multi-Protocol Label Switching (GMPLS). The approach is implemented to control the multidomain network with required quality of service, in a use case of incomplete domain network information. The authors examine different factors, including resource reservation algorithms...
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Higher Absorption of Vitamin C from Food than from Supplements by Breastfeeding Mothers at Early Stages of Lactation
PublicationThe aim of the present study was to determine the effect of vitamin C supply in the diet of lactating women on vitamin C concentra¬tions in human milk (n = 97) sampled at different stages of lactation. Vitamin C levels were measured by liquid chromatography. Dietary intake of vitamin C was determined based on 3-day food dairies kept by breastfeeding mothers. Maternal dietary intakes of vitamin C from natural sources on lactation...
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Food & Function
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Research on the separation properties of empty-column gas chromatography (EC-GC) and conditions for simulated distillation (SIMDIS)
PublicationThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Advances in mass spectrometry for iron speciation in plants
PublicationIron is an important nutrient essential for plants and critical for human health. The state-of-the art of methods for iron speciation in cereal grains and plant fluids is critically reviewed. Particular attention is given to the latest developments in the coupling of HPLC with the parallel ICP MS and electrospray ionization (ESI) MS/MS detection, usually QTOF MS or Q-Orbitrap MS, for the identification and quantification of iron...
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Solvent effects for proton transfer reaction from dimethyl(4-nitrophenyl)malonate to cis 1,2-bis(diethylaminomethyl)cyclohexane
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Sources, properties and suitability of new thermostable enzymes in food processing
PublicationW niniejszym artykule przedstawiono przegląd badań wskazujących na przydatność rekombinantowej alfa-amylazy z Pyrococcus woesei i alfa glukozydazy z Thermus thermohilus do jednoetapowego wytwarzania syropów skrobiowych. Rekombinantowa beta-glikozydaza z Pyrococcus woesei może być natomiast stosowana do produkcji bezlaktozowych produktów z mleka i serwatki. Zachowanie aktywności w szerokim zakre-sie pH od 4,3 do 6,6 oraz duża termostabilność...
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Quality 5.0: A Paradigm Shift Towards Proactive Quality Control in Industry 5.0
PublicationIndustry 5.0, the latest wave of industrial revolution, is redefining the traditional manufacturing and production landscapes by leveraging advanced technologies, promoting sustainability, and fostering a human-centric approach. An inevitable consequence of this progression is Quality 5.0, the next phase of quality control and assurance. Quality 5.0 aims to transcend the limitations of conventional quality control techniques, which...
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FOOD RESEARCH INTERNATIONAL
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Volatile Compound Emissions from Stereolithography Three-Dimensional Printed Cured Resin Models for Biomedical Applications
PublicationStereolithography three-dimensional printing is used increasingly in biomedical applications to create components for use in healthcare and therapy. The exposure of patients to volatile organic compounds (VOCs) emitted from cured resins represents an element of concern in such applications. Here, we investigate the biocompatibility in relation to inhalation exposure of volatile emissions of three different cured commercial resins...
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Heat transfer enhancement of modular thermal energy storage unit for reversible heat pump cooperation
PublicationThe following article presents experimental comparison research on a hexagonal shelland-tube latent thermal energy storage (TES). Such shape of a shell was deliberately chosen instead of a cylindrical one due to its high modularity and with intent for future applications in automobiles (EV and PHEV) air conditioning systems (HVAC). Two geometries of helical coils, acting as tubes, were studied in this article. One was a simple...
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Direct Analysis of Samples of Various Origin and Composition Using Specific Types of Mass Spectrometry
PublicationOne of the major sources of error that occur during chemical analysis utilizing the more conventional and established analytical techniques is the possibility of losing part of the analytes during the sample preparation stage. Unfortunately, this sample preparation stage is required to improve analytical sensitivity and precision. Direct techniques have helped to shorten or even bypass the sample preparation stage; and in this...
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Load effect impact on the exploitation of concrete machine foundations used in the gas and oil industry
PublicationMachine foundations is a critical topic in the gas and oil industry, which design and exploitation require extensive technical knowledge. Machine foundations are the constructions which are intended for mounting on it a specific type of machine. The foundation has to transfer dynamic and static load from machine to the ground. The primary difference between machine foundations and building foundations is that the machine foundations...
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Ocena wpływu dodatku oliwy z oliwek na degradację termiczną rafinowanego oleju rzepakowego
PublicationTłuszcze jadalne to ważny składnik diety człowieka. Mają one znaczący wpływ na prawidłowe funkcjonowanie ludzkiego organizmu. Podczas smażenia olej podlega przemianom chemicznym, dlatego spożywane tłuszcze powinny charakteryzować się jak największą stabilności oksydacyjnej. Celem prowadzonych badań było określenie jakości olejów rzepakowego, mieszanego oraz rafinowanej oliwy z oliwek, pochodzących z rynku krajowego. Podczas badań...
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Determination of tributyltin (TBT) in marine sediment using pressurised liquid extraction–gas chromatography–isotope dilution mass spectrometry (PLE–GC–IDMS) with a hexane–tropolone mixture
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain monocarboxylic acids in cattle farm wastewater and waste landfill leachates
PublicationZaproponowano metodykę oznaczania krótkołańcuchowych kwasów monokarboksylowych w ściekach z hodowli bydła i odciekach ze składowisk zawierających organiczne odpady, oparta na technice mikroekstrakcji do fazy stacjonarnej z fazy nadpowierzchniowej próbek ciekłych, w połączeniu ze sprzężonym układem GC-MS.
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Determination of tributylotin (TBT) in marine sediment using pressurised liquid extraction-gas chromatography-isotope dilution mass spectrometry (PLE-GC-IDMS) with a hexane-tropolone mixture
PublicationOpracowano metodę oznaczania zawartości tributylocyny w próbkach osadu morskiego. Na etapie izolacji zastosowano technikę przyspieszonej ekstrakcji za pomocą roztworu tropolonu w heksanie.Na etapie oznaczeń końcowych wykorzystano technikę chromatografii gazowej, stosując metodę spektrometrii mas rozcieńczenia izotopowego. Wyznaczono parametry walidacyjne opracowanej metody: granicę wykrywalności, precyzję, poprawność i niepewność.
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OIL GAS-EUROPEAN MAGAZINE
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Improved Oil and Gas Recovery
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Upstream Oil and Gas Technology
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EUROPEAN JOURNAL OF MASS SPECTROMETRY
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JOURNAL OF APPLIED BOTANY AND FOOD QUALITY
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Tomasz Zubowicz dr inż.
PeopleTomasz Zubowicz has received his M.Sc. Eng. degree in Control Engineering from the Faculty of Electrical and Control Engineering at the Gda{\'n}sk University of Technology (GUT) in $2008$. He received his Ph.D. Eng. (Hons.) in the field of Control Engineering from the same faculty in $2019$. In $2012$ he became a permanent staff member at the Department of Intelligent Control and Decision Support Systems at GUT and a member of...
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Karolina Sobieraj mgr inż.
PeopleMSc. Karolina Sobieraj graduated in 2018 in the field of Renewable Energy Sources and Waste Management in the specialization of Waste Management, with a scholarship from the Minister of Science and Higher Education for students for outstanding scientific achievements in the 2017/2018 academic year. From October 2019, she started studies at the UPWr Doctoral School in the discipline of environmental engineering, mining and energy....
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[IMe] Selected problems of heat and mass transfer
e-Learning Courses{mlang pl} Dyscyplina: Inżynieria mechaniczna (PG + IMP PAN) Zajęcia obowiązkowe Prowadzący: prof. dr. hab. inż. Dariusz Mikielewicz Liczba godzin: 20 h Forma zajęć: wykład {mlang} {mlang en} Discipline: mechanical engineering (GUT + IFFM PAS) Obligatory course Academic teacher: prof. dr. hab. inż. Dariusz Mikielewicz Total hours of training: 20 teaching hours Course type: lecture {mlang}