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Search results for: SILANETHIOLATES, COPPER
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A concerted evolution of supramolecular interactions in a {cation; metal complex; π-acid; solvent} anion-π system
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Fast multi-criterial statistical analysis and design optimization of compact microwave couplers
Publication—A rapid statistical analysis and yield estimation of compact microwave couplers involving multiple performance parameters has been presented. The analysis is realized using a fast surrogate model representing appropriate characteristic points of the coupler response. Because of less nonlinear dependence of the characteristic points on the structure geometry (compared to the original response, i.e., S-parameters vs. frequency),...
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99mTc-Galacto-RGD2: A Novel 99mTc-Labeled Cyclic RGD Peptide Dimer Useful for Tumor Imaging
PublicationThis study sought to evaluate [99mTc(HYNIC-Galacto-RGD2)-(tricine)(TPPTS)] (99mTc-Galacto-RGD2: HYNIC = 6-hydrazinonicotinyl; Galacto-RGD2 = Glu[cyclo[Arg-Gly-Asp-D-Phe-Lys(SAA-PEG2-(1,2,3-triazole)-1-yl-4-ethylamide)]]2 (SAA = 7-amino-L-glycero-L-galacto-2,6-anhydro-7-eoxyheptanamide, and PEG2 = 3,6-dioxaoctanoic acid); and TPPTS = trisodium triphenylphosphine-3,3',3''-trisulfonate) as a new radiotracer for tumor imaging. Galacto-RGD2...
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Local properties of organic coatings close to glass transition temperature
PublicationAcrylic coating applied on copper substrate has been investigated at different temperatures starting from the ambient one up to the level above the glass transition temperature. Its local topographic and electric properties have been examined with the atomic force microscopy (AFM) based approach including dc current mapping and local impedance spectroscopy. The local findings have been compared with the information from global...
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The Influence of Nanometals, Dispersed in the Electrophoretic Nanohydroxyapatite Coatings on the Ti13Zr13Nb Alloy, on Their Morphology and Mechanical Properties
PublicationIn this work, nanohydroxyapatite coatings with nanosilver and nanocopper have been fabricated and studied. The presented results concern coatings with a chemical composition that has never been proposed before. The present research aims to characterize the effects of nanosilver and nanocopper, dispersed in nanohydroxyapatite coatings and deposited on a new, non-toxic Ti13Zr13Nb alloy, on the physical and mechanical properties of...
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A New Approach for the Mitigating of Flow Maldistribution in Parallel Microchannel Heat Sink
PublicationThe problem of flow maldistribution is very critical in microchannel heat sinks (MCHS). It induces temperature nonuniformity, which may ultimately lead to the breakdown of associated system. In the present communication, a novel approach for the mitigation of flow maldistribution problem in parallel MCHS has been proposed using variable width microchannels. Numerical simulation of copper made parallel MCHS consisting of 25 channels...
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Aspects of pollution in Gdansk and gdynia Harbours at the coastal zone of the South Baltic Sea
PublicationOrganotin compounds (OTC), as well as metals, are toxic to many organisms. Even at very low concentrations OTC and metals can have several negative effects. The paper discusses key issues relating to the location of harbours in the coastal zone (including near the river mouths and semi-closed access to the sea) and the pollution of harbour sediments with heavy metals (e.g. zinc, copper, nickel and lead) and organotin derivatives...
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Towards Cognitive and Perceptive Video Systems
PublicationIn this chapter we cover research and development issues related to smart cameras. We discuss challenges, new technologies and algorithms, applications and the evaluation of today’s technologies. We will cover problems related to software, hardware, communication, embedded and distributed systems, multi-modal sensors, privacy and security. We also discuss future trends and market expectations from the customer’s point of view.
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Positive results of serological tests for syphilis in pregnancy – diagnostic and therapeutic problems, report of two cases
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Conditions controlling atmospheric pollutant deposition via snowpack
PublicationSolid precipitation represents a potentially important addition to other measures of deposition. However, an accurate estimate of snowfall amount and pollutant loading is not a trivial matter. There are obvious distinctions between regular precipitation collection and snowpack sampling that represent the cumulative chemistry of bulk deposition. The main goal is to show the most important processes and factors that may influence...
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Ionosphere variability II: Advances in theory and modeling
PublicationThis paper aims to provide an overview on recent advances in ionospheric modeling capabilities, with the emphasis in the efforts relevant to electron density variability. The discussion spans a wide range of model formulations (e.g., from purely empirical to physics-based ones and data-driven approaches) seeking for advances or gaps with regard to present challenges. This discussion is further supported by consideration of the...
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Bandwidth-size design trade-offs for compact spline-parameterised patch couplers by means of electromagnetic-driven multi-objective optimisation
PublicationBroad bandwidth and small size are the key performance figures for contemporary microwave couplers. These requirements are conflicting, i.e. improvement of one generally leads to degradation of the other assuming fixed topology of the circuit at hand. From a designer's perspective, the knowledge about available design trade-offs is indispensable as it permits for tailoring the circuit for particular applications as well as comparing...
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Curing epoxy with ethylenediaminetetraacetic acid (EDTA) surface-functionalized Co Fe3-O4 magnetic nanoparticles
PublicationIn this work, the bulk and surface composition of Fe3O4 supermagnetic nanoparticles were modified for efficient epoxy curing. The bare, ethylenediaminetetraacetic acid (EDTA) capped, and cobalt (Co)-doped EDTA capped Fe3O4 nanoparticles were synthesized electrochemically. The crystalline structure and phase information, surface capping, morphology and magnetization behavior of nanoparticles were studied by X-Ray diffraction (XRD),...
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Honey as an indicator of heavy metals in the environment
PublicationHoney bees collect nectar, pollen and honeydew to produce bee products. One of them is honey, which due to chemical composition and properties is considered by human as a valuable food product. When honey bees collect substrates to produce honey they can bring contaminants to the hive. The presence of xenobiotics in bee products may lower their quality and devalue their properties, and also endanger human health. Many scientists...
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Defective TiO2 Core-Shell Magnetic Photocatalyst Modified with Plasmonic Nanoparticles for Visible Light-Induced Photocatalytic Activity
PublicationIn the presented work, for the first time, the metal-modified defective titanium(IV) oxide nanoparticles with well-defined titanium vacancies, was successfully obtained. Introducing platinum and copper nanoparticles (NPs) as surface modifiers of defective d-TiO2 significantly increased the photocatalytic activity in both UV-Vis and Vis light ranges. Moreover, metal NPs deposition on the magnetic core allowed for the effective separation...
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Mono- and bimetallic (Pt/Cu) titanium(IV) oxide photocatalysts. Physicochemical and photocatalytic data of magnetic nanocomposites’ shell
PublicationSurface modification of titania with noble and semi-noble metals resulted in significant enhancement of photocatalytic activity. Presented data, showing the photocatalytic properties of TiO2-M (where M is Pt and/or Cu) photocatalysts were further used as Fe3O4@SiO2/TiO2-M magnetic nanocomposites shells in "Mono- and bimetallic (Pt/Cu) titanium(IV) oxide core-shell photocatalysts with Vis light activity and magnetic separability"...
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Performance Evaluation of a 650V E-HEMT GaN Power Switch
PublicationGaN power switches have better characteristics compared to the state-of-the-art Si power transistors. These devices offer high operating temperature and current densities, fast switching and low on-resistance. However, currently only a few producers offer technology of high voltage GaN transistors. Immaturity of this technology is the reason why experimental evaluation of GaN parameters must be performed to properly exploit their...
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Phosphoroorganic Metal Complexes in Therapeutics
PublicationThe present mini-review highlights recent developments on antitumor activity of metal-based therapeutics which have been a subject of researches for the last few decades. In 1965, Rosenberg found that during an electrolysis on platinum electrodes a complex of Pt is generated which inhibited to a great extent a binary fission in Escherichia coli bacteria. This discovery started a new chapter in medicinal chemistry and the interesting...
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Elastic wave propapagation in diagnostics of self-drilling system of grouted anchors
PublicationThe paper presents an experimental investigation of elastic wave propagation in a self-drilling hollow bar system, which is commonly used in geotechnical industry as the element of grouted ground anchors and soil nails. The single self-drilling hollow bar and self-drilling system of two bars connected by a coupler were considered. Longitudinal waves were excited at one end of the bar and registered at both ends, by means of PZT...
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The study on possibilities of recovery non-magnetic fraction by utilisation the magnetic separation technology in conditions of KGHM Polska Miedz S.A. division of concentrators = Próby odzysku frakcji niemagnetycznej metodą separacji magnetycznej w warunkach KGHM Polska Miedź S.A. Oddział Zakłady Wzbogacania Rud
PublicationW referacie przybliżono wyniki badań prowadzonych w kierunku określenia możliwości odzysku frakcji niemagnetycznej i słabomagnetycznej ze strumieni materiałowych O/ZWR, poprzez wykorzystanie metody separacji magnetycznej. Przeprowadzony cykl badawczy obejmował analizę występowania frakcji magnetycznej i związanej z nią frakcji niemagnetycznej w obiegach technologicznych w Rejonie ZWR Lubin, oraz możliwości ich odzysku. Uzyskane...
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Infinite chromatic games
PublicationIn the paper we introduce a new variant of the graph coloring game and a new graph parameter being the result of the new game. We study their properties and get some lower and upper bounds, exact values for complete multipartite graphs and optimal, often polynomial-time strategies for both players provided that the game is played on a graph with an odd number of vertices. At the end we show that both games, the new and the classic...
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ASSESSING THE POTENTIAL REPLACEMENT OF MINERAL OIL WITH ENVIRONMENTALLY ACCEPTABLE LUBRICANTS IN A STERN TUBE BEARING: AN EXPERIMENTAL ANALYSIS OF BEARING PERFORMANCE
PublicationT his study compares the performance of a plain bearing, with a similar structure to a tail shaft stern bearing, lubricated with either mineral oil or an environmentally acceptable lubricant (EAL). The main characteristic of the bearing is its length/diameter ratio of <1. Measurements are carried out with the bearing operating under loads from 0.5 to 1 MPa and seven speeds ranging from 1 to 11 rev/s. The bearing lubricated...
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Offshore surface waters of Antarctica are free of microplastics, as revealed by a circum-Antarctic study
PublicationIn 2018, during a circum navigation of Antarctica below 62° S by the sailing boat Katharsis II, the presence of plastics was investigated with surface sampling nets at ten evenly spaced locations (every 36° of longitude). Although fibres that appeared to be plastic (particles up to 2 cm) were found in numbers ranging from 1 particle (0.002 particles per m3) to 171 particles (1.366 particles per m3) per station, a Fourier-transform...
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Progressing Pollutant Elution from Snowpack and Evolution of its Physicochemical Properties During Melting Period— a Case Study From the Sudetes, Poland
PublicationMain aim of the work assumed recognition of physicochemical changes in snowpack occurring during the melting period. Properties of snow cover had been identified at two sites in Western Sudetes mountains (860 and 1228 m asl) in SW Poland since the end of January, and monitored until the disappearance of snow in late Spring. Snow pit measurements and sample collection at both sites were made followed by chemical analyses with the...
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Biological and antibacterial properties of chitosan-based coatings with AgNPs and CuNPs obtained on oxidized Ti13Zr13Nb titanium alloy
PublicationDespite numerous studies, the antibacterial efficiency and cytotoxicity of chitosan-based coatings with nanometals need further studies. The purpose of this research was to determine the biological properties of chitosan coatings implemented with either silver nanoparticles (AgNPs) or copper nanoparticles (CuNPs), that were electrophoretically deposited on electrochemically oxidized Ti13Zr13Nb alloy. The SEM tests were used to...
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Cu supported on various oxides as a candidate catalyst for dry methane reforming in DIR-SOFCs systems
PublicationA series of Cu-support systems were tested as potential candidates for DIR-SOFC (Direct Internal Reforming SOFC) catalysts towards a dry reforming of methane (DRM). The various supports (-Al2O3, CeO2, ZrO2, SrTiO3) with comparable specific surface area (SSA), and additionally -Al2O3 with SSA an order of magnitude larger than that of the other supports has been applied. The obtained Cu-support systems were characterized in terms...
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Qualification of brazing procedure for furnace brazing of austenitic steel according to requirements of the ASME BPVC section IX
PublicationThe article presents the procedure for qualifying brazing technology in a vacuum furnace on the example of stainless steel elements joined with copper filler material from the F-No group. 105, in accordance with the ASME Sec. IX, part QB (ASME Boiler and Pressure Vessel Code. Qualification Standard for Welding, Brazing and Fusing; Procedures; Welders; Brazers; and Welding, Brazing and Fusing Operators). The essential variables...
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Application of Maximum Lenght Sequence in Silent Sonar
PublicationSilent sonars are designed to reduce the distance over which their sounding pulses can be detected by intercept sonars. In order to meet this objective, we can use periodical sounding signals that have low power, a very long duration and wide spectrum. If used in the silent sonar's receiver, matched filtration ensures very good detection of motionless or slow moving targets. However, it is more difficult to detect echo signals...
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Fast surrogate-assisted simulation-driven design of compact microwave hybrid couplers
PublicationThis work presents a robust methodology for expedited simulation-driven design optimization of compact microwave hybrid couplers. The technique relies on problem decomposition, and a bot-tom–up design strategy, starting from the level of basic building blocks of the coupler, and finishing with a tuning procedure that exploits a fast surrogate model of the entire structure. The latter is constructed by cascading local response surface...
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Inverse surrogate models for fast geometry scaling of miniaturized dual-band couplers
PublicationRe-design of microwave structures for various sets of performance specifications is a challenging task, particularly for compact components where considerable electromagnetic (EM) cross-couplings make the relationships between geometry parameters and the structure responses complex. Here, we address geometry scaling of miniaturized dual-band couplers by means of inverse surrogate modeling. Our approach allows for fast estimation...
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Restoration and preservation of the reinforced concrete poles of fence at the former Auschwitz concentration and extermination camp
PublicationThe objective of this study was to assess the present state of the reinforced concrete poles of fence at the former Auschwitz I and Auschwitz II-Birkenau concentration and extermination camp. The poles were subjected to renovation about 10 years ago. After this time some deficiencies of applied renovation method were noticed. Cracks appeared between fresh and original part of concrete cover. Analysis of the reasons of these failures...
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Restoration and preservation of the reinforced concrete poles of fence at the former Auschwitz concentration and extermination camp
PublicationThe objective of this study was to assess the present state of the reinforced concrete poles of fence at the former Auschwitz I and Auschwitz II-Birkenau concentration and extermination camp. The poles were subjected to renovation about 10 years ago. After this time some deficiencies of applied renovation method were noticed. Cracks appeared between fresh and original part of concrete cover. Analysis of the reasons of these failures...
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Anti-plane shear waves in an elastic strip rigidly attached to an elastic half-space
PublicationWe consider the anti-plane shear waves in a domain consisting of an infinite layer with a thin coating lying on an elastic half-space. The elastic properties of the coating, layer, and half-space are assumed to be different. On the free upper surface we assume the compatibility condition within the Gurtin–Murdoch surface elasticity, whereas at the plane interface we consider perfect contact. For this problem there exist two possible...
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Platform Supporting the Esophageal Impedance Analysis
PublicationThe esophageal pH-impedance examination is one of the most popular diagnostic methods for identifying the upper gastrointestinal tract’s diseases. Inconclusive test evaluation criteria makes it difficult to state the definite diagnosis. In this paper, the computer platform supporting the research and teaching process in the area of pH-impedance analysis is presented. Users, having a variety of mathematical and statistical methods...
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The Hopf type theorem for equivariant gradient local maps
PublicationWe construct a degree-type otopy invariant for equivariant gradient local maps in the case of a real finite-dimensional orthogonal representation of a compact Lie group. We prove that the invariant establishes a bijection between the set of equivariant gradient otopy classes and the direct sum of countably many copies of Z.
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FEM simulations applied to the failure analysis of RC structure under the influence of municipal sewage pressure
PublicationThe paper discusses a failure mechanism of reinforced concrete (RC) structure with steel cover that failed under the influence of municipal sewage pressure. To explain the reasons of failure, in-situ measurements, laboratory experiments and comprehensive Finite Element Method (FEM) computations were performed. Non-destructive in-situ scanning tests were carried out to determine quantity and cover thickness of embedded reinforcement...
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The effective elastic properties of human trabecular bone may be approximated using micro-finite element analyses of embedded volume elements.
PublicationBoundary conditions (BCs) and sample size affect the measured elastic properties of cancellous bone. Samples too small to be representative appear stiffer under kinematic uniform BCs (KUBCs) than under periodicity-compatible mixed uniform BCs (PMUBCs). To avoid those effects, we propose to determine the effective properties of trabecular bone using an embedded configuration. Cubic samples of various sizes (2.63, 5.29, 7.96, 10.58...
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An Application Supporting Gastroesophageal Multichannel Intraluminal Impedance-pH Analysis
PublicationDue to a significant rise in the number of patients diagnosed with diseases of the upper gastrointestinal tract and the high cost of treatment, there is a need to further research on one of the most popular diagnostic tests used in this case – esophageal Multichannel Intraluminal Impedance and pH measurement. This may lead to finding new diagnostically relevant information, used to quicken and improve the diagnostic procedure....
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Experimental Study of Silent Sonar
PublicationStealth is a frequent requirement in military applications and involves the use of devices whose signals are difficult to intercept or identify by the enemy. The silent sonar concept was studied and developed at the Department of Marine Electronic Systems of the Gdansk University of Technology. The work included a detailed theoretical analysis, computer simulations and some experimental research. The results of the theoretical...
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Hydraulic resistance analyses of selected elements of the prototype Stirling engine
PublicationThe paper presents the results of simulation tests of hydraulic resistance and temperature distribution of the prototype Stirling alpha engine supplied with waste heat. The following elements were analyzed: heater, regenerator and cooler. The engine uses compressed air as a working gas. Analyses were carried out for three working pressure values and different engine speeds. The work was carried out in order to optimize the configuration...
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Synthesis of 5-Substituted 1H-Tetrazoles from Nitriles in the Presence of Heterogeneous Catalyst
PublicationTetrazoles are five-membered heterocyclic compounds containing in their rings four nitrogen atoms. They have wide applications as corrosion inhibitors, analytical reagents, high-energy materials and gas generating compositions. Tetrazoles also play important role in coordination chemistry as ligands and in medicinal chemistry as metabolically stable surrogates for carboxylic acids. In recent years, investigation of new method of...
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Evaluating the influence of radiative heat flux on convective heat transfer from a vertical plate in air using an improved heating plate
PublicationThis article examines the influence of radiative heat flux on the accuracy of the results of free convective heat transfer in air. In order to carry out these tests, based on the experience gained during the operation of a plate heated on one side, compensated by a reverse heat loss flux counter-heater, a unique double-sided heating sandwich plate was designed and built, consisting of three thin epoxy resin plates reinforced with...
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TiO2-based magnetic nanocomposites with core-shell structure
PublicationThe main aim of the doctoral dissertation was preparation and characterization of photocatalysts, with particular emphasis on modified titanium (IV) oxide photocatalysts, which can be applied for the degradation of organic pollutants not susceptible to biodegradation. A particularly important aspect of the work was the development of preparation method of nanocomposites with the magnetic core-shell and photocatalyst shell (TiO2)...
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Young shoots of red cabbage are a better source of selected nutrients and glucosinolates in comparison to the vegetable at full maturity
PublicationCruciferous vegetables are a valuable source of ingredients with health benefits. The most characteristic compounds of cruciferous vegetables with identified anticancer properties are glucosinolates. Young shoots and sprouts of red cabbage are becoming a popular fresh food rich in nutrients and bioactive compounds. The objective of this research was to determine, for the first time in a comprehensive approach, whether young shoots...
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INVESTIGATION OF BOTTOM SEDIMENT STRATIFICATION
PublicationThe main goal of this paper is to find a method to assess remotely the type of sediments on the basis of the signal received using the parametric echosounder. The images of the sea bottom sediments taken by a parametric echosounder show the fine structure of the upper layer of the bottom sediments. The depth of penetration depends on the type of sediment, in fact on the attenuation of acoustic wave. In the paper the method of distinguishing...
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Application in circular sawing machines of the experimental results of investigations of the chip removing system operation
PublicationThe experimental results of the chip removing system operation are presented. The main aim of them was to optimize suction system of the panel saw Fx3 and its follower Fx550. The attention was focused on the upper casing, which was the part of removing system. Within the framework of the work a systematic experimental study of pressure distribution in the casing during operation of the selected rotational speed of saw blade with...
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Ocena stanu technicznego konstrukcji zgarniaczy będących na wyposażeniu osadników wstępnych Grupowej Oczyszczalni Ścieków „DĘBOGÓRZE
PublicationOsadniki wstępne typu DORRA – 4 szt., o pojemności 1830 m3, wyposażone są w elementy mechaniczne do kierunkowego przemieszczania się osadu w kierunku leja centralnego. Celem pracy jest ocena stany technicznego części mechanicznej, a w szczególności: - konstrukcji zespołu zgarniania części pływających oraz osadu. - zespołu napędu i sterowania, - zespołu napędu i jazdy. Pierwsze dwa zespoły będą oceniane również z punktu widzenia...
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STABILITY OF THE INNER SLOPE OF THE POLISH DREDGDIKES RESEARCH DIKE AT STATIONARY FLOW
PublicationFor long duration of the flood the water table can appear on the slope with a problem of out-wash in the case of sand type dike. If the dike corps is covered with less permeable layer some additional push-off forces and shearing can rise in the cover. In both cases the micro stability of the inner slope should be considered at normative high water for homogeneous sand type dike or sand type dike with less permeable covers. The...
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Gas chromatography-olfactometry (GC-O), electronic noses (e-noses) and electronic tongues (e-tongues) for in vivo food flavour measurement
PublicationThe capter revies two types of artificial olfaction instrumentation, i.e. gas-chromatography-olfactometry (GC-O) and chemical sensor technologies (electronic nose and tongue), combined with multivariate data processing methods as promising approaches for rapid analysis of food. The chapter also includes examples of specific applications for the detection of food flavour and volatile components.
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PANTOGRAPH AS AN EXAMPLE OF THE USE OF GEOMETRIC TRANSFORMATIONS IN CONSTRUCTING OF OLD DRAWING INSTRUMENTS = PANTOGRAF JAKO PRZYKŁAD ZASTOSOWANIA PRZEKSZTAŁCEŃ GEOMETRYCZNYCH W KONSTRUOWANIU DAWNYCH PRZYRZĄDÓW KREŚLARSKICH
PublicationThe article describes the pantograph, considered to be the ancestor of today's photocopier. This instrument draws the copies, enlarges or reduces any figure. The author presents its genesis, the scope of application in the past, explains the structure and geometrical transformations used during its action. Based on a specific example, the work illustrates practical application of geometry in the past inventions for designing.