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Sulfonamides with hydroxyphenyl moiety: Synthesis, structure, physicochemical properties, and ability to form complexes with Rh(III) ion
PublicationSulfonamides are the first successfully synthesized antimicrobial drugs. The mechanism of sulfonamides’ antimicrobial action involves competitive inhibition of folic acid synthesis and prevention of the growth and reproduction of bacteria. Even though they have been applied in therapy for more than 75 years, sulfonamides are still the drugs of choice for the treatment of various diseases. The aim of this work was to synthesize...
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An Overview of Image Analysis Techniques in Endoscopic Bleeding Detection
PublicationAuthors review the existing bleeding detection methods focusing their attention on the image processing techniques utilised in the algorithms. In the article, 18 methods were analysed and their functional components were identified. The authors proposed six different groups, to which algorithms’ components were assigned: colour techniques, reflecting features of pixels as individual values, texture techniques, considering spatial...
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OECD Guidelines for Micro Statistics on Household Wealth
PublicationThis report reflects the contributions of members of the OECD Expert Group on Micro Statistics on Household Income, Consumption and Wealth. Members of the Expert Group included representatives from National Statistical Offices – Bob McColl (Chair, Australia); Alison Hale (Canada); Andre Bustamante and David Niculcar (Chile); Henrik Sejerbo Soerensen (Denmark); Yafit Alfandari (Israel); Shinji Yoshioka (Japan); Sinho Kim...
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Przegląd wykorzystania wybranych metod inżynierii jakości.
PublicationZamieszczono zestawienie najistotniejszych przypadków wykorzystania analitycznych metod inżynierii jakości ujętych w 15 grup tematycznych. W podsumowaniu dokonano skomentowania zaprezentowanego materiału.
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Impact of Work on the Well-Being of Police Officers and Firefighters
PublicationWork is one of the most important spheres of human functioning and has a significant impact on individual overall well-being. The purpose of this study is to assess the positive and negative impact of the work of police officers and firefighters on their well-being in different spheres of life. In particular, the study examines the relationship between the type of occupation and the elements that generate a feeling of well-being,...
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Robust estimation of deformation from observation differences for free control networks
PublicationDeformation measurements have a repeatable nature. This means that deformation measurements are performed often with the same equipment, methods, geometric conditions and in a similar environment in epochs 1 and 2 (e.g., a fully automated, continuous control measurements). It is, therefore, reasonable to assume that the results of deformation measurements can be distorted by both random errors and by some non-random errors, which...
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Stable and degradable microgels linked with cystine for storing and environmentally triggered release of drugs
PublicationEnvironmentally sensitive, degradable microgels based on poly(N-isopropylacrylamide) (pNIPA) crosslinked with the diacryloyl derivative of cystine (BISS) were synthesized by applying surfactant-free emulsion polymerization. pNIPA contributed the sensitivity to temperature to the microgels and the cross-linker made them degradable and sensitive to pH. The morphology of the microgels was investigated by using scanning and transmission...
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Glucose metabolism disorders in patients with non-functioning adrenal adenomas — single-centre experience
PublicationIntroduction: The presence of glucose metabolism disorders and their possible correlation with degree of cortisol secretion were evaluated in patients with non-functioning adrenal incidentalomas (NFAIs). Material and methods: The study group consisted of 131 patients with hormonally inactive adrenal incidentalomas....
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Bisphenol A analogues and metabolic syndrome in women with polycystic ovary syndrome
PublicationBisphenols (BPs) have become a chemical group of special interest due to their ability to interfere with the endocrine system and their ubiquitous presence in the environment. As some of them possess mild estrogenic and anti-androgenic effects, they might be associated with the diagnosis of polycystic ovary syndrome (PCOS). Acting on multiple tissues, BPs exposure may lead to metabolic derangements characteristic for metabolic...
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Remote Work Support Needs of Employees with Autism Spectrum Disorder in Poland: Perspectives of Individuals with Autism and Their Coworkers
PublicationBackground and Aims: With remote work becoming more common across industries, employees with autism may experience different work support needs from neurotypical peers. However, the specific remote work needs of this group of employees are underexplored in the literature. We aim to propose ways to assess workplace digital adaptation needs for individuals with autism and a framework for communicating these needs to employers. Methods:...
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Two complementary approaches for the synthesis and isolation of stable phosphanylphosphaalkenes
PublicationPhospha-Wittig (phosphanylphosphinidene titanium(IV) complex) and phospha-Peterson (lithiated diphosphane) reactions were used to obtain phosphanylphosphaalkenes with the general formula XYC=P-PtBu2 (X = alkyl, aryl group or H; Y = alkyl or aryl group). Therefore, two series of reactions with different ketones and aldehydes were performed. An examination revealed that the two methods are complementary. For smaller carbonyl compounds,...
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New Carvone-Based Deep Eutectic Solvents for Siloxanes Capture from Biogas
PublicationDuring biogas combustion, siloxanes form deposits of SiO2 on engine components, thus shortening the lifespan of the installation. Therefore, the development of new methods for the purification of biogas is receiving increasing attention. One of the most effective methods is physical absorption with the use of appropriate solvents. According to the principles of green engineering, solvents should be biodegradable, non-toxic, and...
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Potentiometric Solid-Contact Ion-Selective Electrode for Determination of Thiocyanate in Human Saliva
PublicationA new solid-contact potentiometric ion-selective electrode for the determination of SCN− (SCN-ISE) has been described. Synthesized phosphonium derivative of calix[4]arene was used as a charged ionophore. The research included selection of the ion-selective membrane composition, determination of the ISEs metrological parameters and SCN-ISE application for thiocyanate determination in human saliva. Preparation of the ISEs included...
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Determinanty jakości usług w zakładach opieki zdrowotnej
PublicationNiniejsza publikacja ma na celu zaprezentowanie możliwości prowadzenia analiz dotyczących jakości usług zdrowotnych, poprzez zidentyfikowanie i scharakteryzowanie kluczowych determinant jakości usług. Przedstawione analizy ograniczono do przychodni publicznej opieki zdrowotnej, z uwagi na fakt powszechności korzystania klientów z tego typu zakładów opieki zdrowotnej, a także pewnego niedostatku opracowań związanych z przychodniami,...
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Zagospodarowanie wód opadowych
PublicationOgólne zasady tworzenia rozwiązań alternatywnego zagospodarowania wód opadowych. Generalna klasyfikacja grup urządzeń. Formy zbiorcze, infiltracja - zbiornik retencyjny, funkcja mieszana lub rozdzielcza.
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Nowe problemy posadowienia rurociągów.
PublicationSzczególne warunki współpracy współczesnych konstrukcji rurociągów z nawodnionym podłożem. specyfika wymagań poszczególnych grup materiałowych. Problemy występujące w poszczególnych fazach procesu budowlanego.
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Inhibiting activity of HIV-1: protease, reverse transcriptase and integrase all together by novel compounds using computational approaches (flexible and rigid docking)
PublicationAcquired immunodeficiency syndrome (AIDS), caused by human immunodeficiency virus type 1 (HIV-1) infection, is one of the most challenging diseases in recent decades. Nevertheless the shortcomings of chemical drugs such as toxicity, lack of curative effects, the search for more potent anti-HIV agents have been focused in our study. In current study, novel scaffold was designed having a benzyl and imidazole in it which are very...
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Irregularities in university processes concerning the Lean Management typology: The pilot study results
PublicationPurpose: Identify the attitudes regarding key irregularities in university activities of universities referring to muda, mura, and muri from the perspective of two groups of stakeholders - academic teachers and administration/service personnel. Study design/methodology/approach: A pilot quantitative study with the use of a questionnaire containing 48 statements regarding six categories of irregularities assessed according to the...
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Influence of the grains shape on the mechanical behavior of granular materials
PublicationDiscrete Element Method is a numerical method suitable for modeling geotechnical problems concerning granular media. In most cases simple forms of grains, like discs or spheres, are used. But these shapes are capable of soil behavior modeling up to a certain point only, they cannot reflect all of the features of the medium (large shear resistance and large volumetric change). In order to reflect the complex behavior of the real...
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Applying of Doped Graphene Oxide Coatings for Corrosion Prevention
PublicationINTRODUCTION Graphene is a carbonaceous material characterized by extraordinary properties (high electron mobility, high surface area, high mechanical strength of 1100 GPa, very dense network hindering the passage of even the smallest helium atoms) [1]. Therefore, it found many applications, also as an anti-corrosive layer [2]. Electrophoretic Deposition (EPD) is one of the methods to deposit coatings. However, due to slight solubility...
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ECG-based prediction of ventricular fibrillation by means of the PCA
PublicationA Sudden Cardiac Death (SCD) is a death resulting from cardiac failure with no significant symptoms earlier than one hour before occurrence. It is the cause of for approximately 400000 deaths per year in United States and millions of deaths worldwide. The proposed system, including two-stage algorithm and wearable diagnostic device allows for SCD risk estimation and continuous monitoring of high risk patients. A single channel...
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CSR in Polish SMEs- from perception to infatuation. Examples of socially engaged firms from Pomeranian Region
PublicationDespite the increasing worldwide awareness of the importance of social issues in con-temporary business management, Polish small and medium-sized enterprises seem to re-main in the group of followers, certainly not leaders, of the corporate social responsibility (CSR) movement, and this despite important dissemination efforts by numerous institu-tions. The aim of this paper is to present the bumpy road to the (still incomplete)...
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GENERALISED HERSCHEL MODEL APPLIED TO BLOOD FLOW MODELLING
PublicationThis paper introduces a new rheological model of blood as a certain generalisation of the standard Herschel-Bulkley model. This model is a rheological constitutive equation and belongs to the group of the so-called generalised Newtonian fluids. Experimental data is compared with results, obtained from the new model, to demonstrate that it allows for the best agreement together with Luo-Kuang model. The new model may be easily implemented...
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Multidimensional Scaling Analysis Applied to Music Mood Recognition
PublicationThe paper presents two experiments aimed at categorizing mood associated with music. Two parts of a listening test were designed and carried out with a group of students, most of whom where users of online social music services. The initial experiment was designed to evaluate the extent to which a given label describes the mood of the particular music excerpt. The second subjective test was conducted to collect the similarity data...
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A Novel Multicast Architecture of Programmable Networks
PublicationIn the paper a multicast architecture for programmable networks based on separation of group management and network control tasks is proposed. Thanks to this separation, services which want to make use of multicast communications no longer have to implement low-level network functionalities and their operation is greatly simplified. Abstracting service’s view of the network into a fully connected cloud enables us to transparently...
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Performance evaluation of parallel background subtraction on GPU platforms
PublicationImplementation of the background subtraction algorithm on parallel GPUs is presented. The algorithm processes video streams and extracts foreground pixels. The work focuses on optimizing parallel algorithm implementation by taking into account specific features of the GPU architecture, such as memory access, data transfers and work group organization. The algorithm is implemented in both OpenCL and CUDA. Various optimizations of...
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Removal of sulfur from a solvent extract
PublicationThe presence of sulfur in a solvent extract that is to be analyzed chromatographically impairs and sometimes precludes properinterpretation of the chromatogram, as the sulfur peak masks the peaks of other compounds present in the sample, and sulfur alsodisrupts the operation of the mass detector. This means that discrepancies in the results can lead to erroneous interpretations andfalse assessments of environmental risk. For this...
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A measurement system for children endurance tests
PublicationThere are a lot of ethical problems concerning the use of invasive methods for the measurement of a child's body response to physical exercise and physical training. The alternative is are non-invasive methods like ergospirometry or NIRS. The article presents a measurement system dedicated for children endurance tests, composed of a few non-invasive measurement modules, including a temperature measurement module. Temperature is...
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Determination of the substances potentially allergenic in water
PublicationPersonal care chemicals are continuously released into environment through domestic and industrial wastewater, causing adverse effects on human health. Their presence can be detected in different environmental compartments. A group of chemicals included in most personal care products are the allergen fragrances. In the present work, simple and rapid methodology based on ultrasound-assisted emulsification-microextraction (USAEME)...
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Improvement of Fingerprinting Method based on Hill Cipher by using Frequency Domain
PublicationThe main goal of this paper is to present the advantages of a digital fingerprinting in a frequency domain over a pixel domain, in case of VoD services (Video on Demand). The paper presents basic issues of a multimedia data protection by digital fingerprinting. It also describes threats to embedded fingerprints from both collusion attacks and from a transmission itself. Possible solution was presented on the example of the DCT...
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Secured wired BPL voice transmission system
PublicationDesigning a secured voice transmission system is not a trivial task. Wired media, thanks to their reliability and resistance to mechanical damage, seem an ideal solution. The BPL (Broadband over Power Line) cable is resistant to electricity stoppage and partial damage of phase conductors, ensuring continuity of transmission in case of an emergency. It seems an appropriate tool for delivering critical data, mostly clear and understandable...
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Efficient synthesis and antifungal investigation of nucleosides’ quaternary ammonium salt derivatives
PublicationQuaternary ammonium salts are a group of compounds with diverse biological properties, the most important of which are their antiviral, antibacterial, and antifungal activities. The quaternization reactions of 5'-O-tosyl derivatives of uridine and thymidine with triethylamine, trimethylamine, 4-(N ,N -dimethylamino)pyridine, 2-methylpyridine, and pyridine are described in this article. Two of the synthesized compounds are exceptional...
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Productive aging
PublicationThe term “productive aging” refers to the participation of older adults in different activities that contribute to generating goods and services and develop the capacity to produce goods and services. In that sense, it includes both the economic activity of this group – serving in the paid workforce – and its social productivity, understood as volunteer activities (Bass et al. 1993). In the broader sense, “productive aging” can...
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Dissociation of furan-2-carboxylic acid by low energy electrons
PublicationElectron attachment to molecular target can lead to a variety of negative fragment ions. We experi- mentally probe the main dissociative electron attachment channels in furan-2-carboxylic acid (C3H3O2 − COOH) - a molecular target composed of two important structural units: a furan ring and a carboxylic group. In our studies we utilise nearly mono-energetic electrons at electron energies from 0 eV up to 15 eV. Our detection setup...
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Youth Civic Participation in the South Baltic Region. Example of Lithuania, Poland and Sweden
PublicationThe aim of this study was to show youth civic participation as a social inclusion element in the Southern Baltic region in need of reinforcement, based on the examples of selected municipalities from Lithuania, Poland and Sweden. The authors focused on the diagnosis of key elements of youth civic engagement at local and cross-border level, taking into account the context of national youth policies and the European Union policy....
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Zagrożenia w ruchu drogowym na sieci dróg powiatów ziemskich.
PublicationZróżnicowanie stanu bezpieczeństwa na drogach w powiatach.Charakterystyka zagrożeń na drogach powiatów ziemskich.Identyfikacja problemów i grup ryzyka.Klasyfikacja powiatów ziemskich ze względu na stan brd.
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Categorization of Wikipedia articles with spectral clustering
PublicationAbstract. The article reports application of clustering algorithms for creating hierarchical groups withinWikipedia articles.We evaluate three spectral clustering algorithms based on datasets constructed with usage ofWikipedia categories. Selected algorithm has been implemented in the system that categorize Wikipedia search results in the fly.
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Getting to know the potential of social media in forest education
PublicationThe development of social network sites not only facilitates the acquisition and deepening of knowledge but also provides the possibility of easily contacting foresters, specialists in natural sciences and nature enthusiasts. In addition, for some years...
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Optymizm przedsiębiorców a ich postawy wobec zmian
PublicationArtykuł dotyczy postaw przedsiębiorców wobec wprowadzania zmian w zarządzanych przez nich firmach. Celem podjętych badań była weryfikacja hipotezy, że poziom optymizmu przedsiębiorcy wpływa na akceptację sytuacji zmian w organizacji i otwartość na jej wdrażanie. Badaniom kwestionariuszowym poddano przedsiębiorców działających na terenie Trójmiasta. Wykorzystano Skalę Orientacji Pozytywnej oraz adaptację Skali Postaw Pracowniczych...
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Functionalization of cysteine derivatives by unsymmetrical disulfide bond formation
PublicationOpracowano metodę funkcjonalizacji pochodnych cysteiny przy pomocy tworzenia niesymetrycznego wiązania disulfidowego. Opracowana metoda okazała się bardzo łagodna, wydajna, i niewrażliwa na obecność dodatkowych grup funkcyjnych.
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Interfejs miejskiego systemu informacji dla osób niepełnosprawnych.
PublicationArtykuł przedstawia analizę potrzeb różnych grup osób niepełnosprawnych oraz możliwe rozwiązania implementacyjne w zakresie interfejsu użytkownika, ułatwiające posługiwanie się systemami informacyjnymi na przykładzie systemu GDASKON.
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A detector of sleep disorders for using at home
PublicationObstructive sleep apnea usually requires all-ni ght examination in a specialized clinic, under the supervision of a medical staff. Because of those requirements it is an expensive and a non-widely utilized test. Moving the examination procedure to patients’ home with automatic analysis algorithms involved will decrease the costs and make it available for larger group of patients. The developed device allows all-night recordings...
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Syntheses of N-Substituted Thymine Thioacetamides. A Novel Approach to Site Selective Acylation of Diaminoalkanes
PublicationA new series of N-substituted thiocarbamoyl derivs. contg. histamine, tryptamine, and other moieties having at least one amino group attached to an aliph. chain has been synthesized from (1-thyminyl)thioacetamide in good isolated yields (69-86%). N-[2-(4-Imidazolyl)ethyl](1-thyminyl)thioacetamide was hydrolyzed to its amide on prolonged heating in water. Ammonium sulfide (20-22% soln. in water) has found interesting new applications...
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Structure elucidation of carbamoylo-β-lactam diastereoisomers by ROESY and NOESY experiments
PublicationRecently we have focused in the problem of preparation of carbamoylo-β-lactams as a result of oxidative cyclization of malonyl enamides. In our experiments we obtain mixture of two main β-lactam products: as a result of subsequent elimination and a second as a product of substitution. All of the produced β-lactams have trans configuration what was confirmed by 1H coupling constants. However id should be stressed that in the case...
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Effect of tube bundle arrangement on performance of shell-and-tube latent heat storage system
PublicationThis work presents the results of experimental investigation on charging and discharging of latent heat storage systems (LHSS) in the form of shell-and-tube heat exchangers with a variable arrays of the tube bundles. The tests included two tube arrangements – in-line and triangular (staggered), a variable number of tubes in a bundle, two pitch ratios, and different tube positions in a bundle. Three commercial products (LTP56, RT54HC,...
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Asymptomatic Bacteriuria in Kidney Transplant Recipients—A Narrative Review
PublicationUrinary tract infections (UTIs) are the most prevalent complications in kidney transplant (KTx) recipients. The most frequent finding in this group of patients is asymptomatic bacteriuria (ASB). Here, we provide an overview of the available evidence regarding ASB in KTx recipients, including its etiopathology, clinical impact and management. There is a growing body of evidence from clinical trials that screening for and treating...
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9-(Trichloroacetylimino)acridine monohydrate
PublicationThe title compound, alternatively called N-acridin-9(10H)-ylidene-2,2,2-trichloroacetamide monohydrate, C15H9Cl3N2O·H2O, crystallizes in space group P21/c with Z = 4. The acridine moieties are arranged in layers, tilted at an angle of 15.20 (4)° relative to the ac plane, while adjacent molecules pack in a head-to-tail manner. Acridine and water molecules form columns along the b axis held in place by a network of hydrogen...
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Bioactive Ingredients with Health-Promoting Properties of Strawberry Fruit (Fragaria x ananassa Duchesne)
PublicationStrawberries (Fragaria x ananassa Duchesne) belong to the berry group and are characterized primarily by delightful sensory properties. Due to their chemical composition, these fruits are a rich source of bioactive compounds that can modify the metabolic and physiological functions of the body. The aim of this work is to present the current state of research on bioactive ingredients found in these fruits in the context of their...
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Automated anonymization of sensitive data on production unit
PublicationThe article presents an approach to data anonymization with the use of generally available tools. The focus is put on the practical aspects of using open-source tools in conjunction with programming libraries provided by suppliers of industrial control systems. This universal approach shows the possibilities of using various operating systems as a platform for process data anonymization. An additional advantage of the described...
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Device for spoofing in global positioning system
PublicationThis article describes the device which may be used to generate false GPS signals and emit them into radio communication channel. Such attack is called GPS spoofing. Each GPS receiver which remains in the range of a spoofing device (called spoofer) indicates time and position coordinates which are predetermined by the spoofer’s operator. Spoofing may be used e.g. in order to disable the terrorist group from obtaining correct navigation...