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Determination of carbon monoxide, methane and carbon dioxide in refinery hydrogen gases and air by gas chromatography
PublicationW pracy przedstawiono metodę oznaczania śladowych zawartości tlenku węgla, metanu oraz dwutlenku węgla w rafineryjnych gazach wodorowych oraz powietrzu; granica oznaczalności metody wynosi odpowiednio 0,15, 0,15 oraz 0,20 mikro-gram/litr. Zaprezentowano w pracy prostą modyfikację chromatografu gazowego wyposażonego w detektor płomieniowo-jonizacyjny (FID). Zastosowano kolumnę typu PorapakQ, dodatkowo połączono szeregowo z krótką...
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Maritime awareness and emergency management real time system using remotely accessible GIS technology
PublicationPrzedstawiono koncepcję oraz prototyp morskiego GIS do zdalnego monitorowania w czasie rzeczywistym zanieczyszczeń środowiska morskiego. System pozwala na gromadzenie i integrowanie różnych typów danych dotyczących zanieczyszczeń, pozyskiwanych na bieżąco za pomocą wielorakiego rodzaju sensorów, w tym akustycznych (echosondy jednowiązkowe i wielowiązkowe). Zadaniem systemu jest wizualizacja oraz mapowanie zanieczyszczeń, takich...
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A review on Graphene/GNPs/GO modified asphalt
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A Novel Spatio–Temporal Deep Learning Vehicle Turns Detection Scheme Using GPS-Only Data
PublicationWhether the computer is driving your car or you are, advanced driver assistance systems (ADAS) come into play on all levels, from weather monitoring to safety. These modern-day ADASs use various assisting tools for drivers to keep the journey safe; these sophisticated tools provide early signals of numerous events, such as road conditions, emerging traffic scenarios, and weather warnings. Many urban applications, such as car-sharing...
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MoS2-containing composite membranes for separation of environmental energy-relevant liquid and gas mixtures: A comprehensive review
PublicationMolybdenum sulfide (MoS2) materials adapted into membranes have demonstrated potential for different areas dealing with molecular separations. For instance, MoS2-based membranes have been proposed for distinct environmental applications, such as water treatment, seawater desalination, gas separation, and solvent separation. Emergently, such membranes have been ultimately investigated for energy-relevant gas separation mixtures,...
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A novel concept of enhanced direct-contact condensation of vapour- inert gas mixture in a spray ejector condenser
PublicationAn analytical model of direct steam condensation (DCC) in the novel idea of spray ejector condenser (SEC) in the presence of inert gas has been developed. It is based on continuity, momentum and energy equations for the steam-carbon dioxide mixture and direct contact condensation mechanisms due to heat transfer and concentration. Crucial in the process of DCC is atomisation of the motive fluid in the ejector. The effect of atomised...
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A natural deep eutectic solvent - protonated L-proline-xylitol - based stationary phase for gas chromatography
PublicationThe paper presents a new kind of stationary phase for gas chromatography based on deep eutectic solvents (DES) in the form of a mixture of L-proline (protonated with hydrochloric acid) as a hydrogen bond acceptor (HBA) and xylitol as a hydrogen bond donor (HBD) in a molar ratio of HBA:HBD 5:1. DES immobilized on a silanized chromatographic support was tested by gas chromatography (GC) in order to determine its resolving power for...
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Compact High Efficiency and Zero-Emission Gas-Fired Power Plant with Oxy-Combustion and Carbon Capture
PublicationReduction of greenhouse gases emissions is a key challenge for the power generation industry, requiring the implementation of new designs and methods of electricity generation. This article presents a design solution for a novel thermodynamic cycle with two new devices—namely, a wet combustion chamber and a spray-ejector condenser. In the proposed cycle, high temperature occurs in the combustion chamber because of fuel combustion...
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Investigation of Liquid–Gas Flow in a Horizontal Pipeline Using Gamma-Ray Technique and Modified Cross-Correlation
PublicationThis article presents the application of the radioisotope absorption method in the study of two-phase water–air flow in a horizontal pipe. The measurement principle and the test stand are briefly described. The main part of the article presents the signal analysis methods applied to data obtained from scintillation detectors. Because these signals are mostly stochastic waveforms, they were analyzed statistically using the cross-correlation...
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Fungal co-culture improves the biodegradation of hydrophobic VOCs gas mixtures in conventional biofilters and biotrickling filters
PublicationThe present study systematically evaluated the potential of Candida subhashii, Fusarium solani and their consortium for the abatement of n-hexane, trichloroethylene (TCE), toluene and α-pinene in biofilters (BFs) and biotrickling filters (BTFs). Three 3.2 L BFs packed with polyurethane foam and operated at a gas residence time of 77 s with an air mixture of hydrophobic volatile organic compounds (VOCs) were inoculated with C. subhashii,...
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Application analysis of a hybrid solid oxide fuel cell-gas turbine system for marine power plants
PublicationThe results of theoretical studies of the possibilities of using hybrid solid oxide fuel cell–gas turbine (SOFC-GT) systems for marine power plants are presented. A 500 kW auxiliary marine power plant scheme using stacks of SOFCs in combination with a regenerative gas turbine operating with over-expansion based on our recent patent application is proposed. The results of mathematical modelling showed the opportunity to obtain a...
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EVALUATION OF LIQUID-GAS FLOW IN PIPELINE USING GAMMA-RAY ABSORPTION TECHNIQUE AND ADVANCED SIGNAL PROCESSING
PublicationLiquid-gas flows in pipelines appear in many industrial processes, e.g. in the nuclear, mining, and oil industry. The gamma-absorption technique is one of the methods that can be successfully applied to study such flows. This paper presents the use of thegamma-absorption method to determine the water-air flow parameters in a horizontal pipeline. Three flow types were studied in this work: plug, transitional plug-bubble,...
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Using the MultiRAEPro Gas Detector to Monitor Odour Emissions from Biogas Plants Processing Municipal Waste
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Research on the separation properties of empty-column gas chromatography (EC-GC) and conditions for simulated distillation (SIMDIS)
PublicationThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Spatial and Temporal Variability of Moisture Condition in Soil-Plant Environmet using Spectral Data and GIS Tools
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Ammonia in Fly Ashes from Flue Gas Denitrification Process and its Impact on the Properties of Cement Composites
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Application of Web-GIS and Geovisual Analytics to Monitoring of Seabed Evolution in South Baltic Sea Coastal Areas
PublicationRegular surveys of coastal zone seabed deliver important information about geomorphologic processes such as silting of waterways. The recent introduction of the Sentinel series of sensors has allowed for the use of satellite sensing for shallow bathymetry morphology monitoring. In this context, this article presents a dedicated Geographic Information System for Baltic Sea shallow water depth monitoring on the basis of Sentinel-2...
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Zastosowanie głębokiego uczenia do określania warunków LOS/NLOS w ultraszerokopasmowych radiowych sieciach WBAN
PublicationW niniejszym artykule przedstawiono zastosowanie głębokiego uczenia do określania warunków bezpośredniej widoczności LOS/NLOS w ultraszerokopasmowych radiowych sieciach WBAN. Zaproponowano głęboką, jednokierunkową sieć neuronową, której efektywność działania sprawdzono na podstawie danych pomiarowych w rzeczywistym wewnątrzbudynkowym środowisku propagacyjnym. Uzyskane wyniki jednoznacznie udowadniają zasadność stosowania zaproponowanej...
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Assessment of Failure Occurrence Rate for Concrete Machine Foundations Used in Gas and Oil Industry by Machine Learning
PublicationConcrete machine foundations are structures that transfer loads from machines in operation to the ground. The design of such foundations requires a careful analysis of the static and dynamic effects caused by machine exploitation. There are also other substantial differences between ordinary concrete foundations and machine foundations, of which the main one is that machine foundations are separated from the building structure....
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Rapid assessment of the authenticity of limequat fruit using the electronic nose and gas chromatography coupled with mass spectrometry
PublicationCitrus fruits are very popular food products. There are many species and varieties of them. There are also documented cases of some citrus fruits causing a severe allergic reaction. Some species of the citrus fruits, especially hybrid ones show a reduced allergenic effect due to the lack of seeds. There is a need for rapid methods for evaluation of citrus’ botanical origin. During research, the headspace of three citrus fruits...
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Effect of GIS parameters on modelling runoff from river basin. The case study of catchment in the Puck District
PublicationThe study was preceded to check the impact of the adopted digital elevation model resolution on the determination of catchment parameters and the further influence of the received information on calculations related to the hydrograph at the closing point of the basin after a synthetic 100-year precipitation episode. The study area are river basins located in the Puck commune convoying water directly to the Puck Bay. These studies...
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Investigations of the Working Process in a Dual-Fuel Low-Emission Combustion Chamber for an FPSO Gas Turbine Engine
PublicationThis investigation is devoted to an analysis of the working process in a dual-fuel low-emission combustion chamber for a floating vessel’s gas turbine. The low-emission gas turbine combustion chamber with partial pre-mixing of fuel and air inside the outer and inner radial-axial swirlers was chosen as the object of research. When modelling processes in a dual-flow low-emission gas turbine combustion chamber, a generalized method...
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Fast Fading Influence on the Deep Learning-Based LOS and NLOS Identificationin Wireless Body Area Networks
PublicationIn the article, the fast fading influence on the proposed DL (Deep Learning) approach for LOS (Line-of-Sight) and NLOS (Non-Line-of-Sight) conditions identification in Wireless Body Area Networks is investigated. The research was conducted on the basis of the off-body communication measurements using the developed mobile measurement stand, in an indoor environment for both static and dynamic scenarios. The measurements involved...
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DESIGN OF THE DUAL CONSTELLATION GPS/GALILEO MOBILE DEVICE FOR IMPROVING NAVIGATION OF THE VISUALLY IMPAIRED IN AN URBAN AREA
PublicationIt is well known by users of Personal Navigation Device (PND) and other GPS-based devices that positioning suffers from (local) significant decreases of accuracy in partially obscured environments like urbanized areas, where buildings (especially high buildings), trees or terrain block large portions of the sky. In such areas, GPS receiver performance is usually deteriorated by the reduced number of currently available satellite...
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The comparison of vodka, whisky and moonshine by using the electronic nose based on the technology of ultra-fast gas chromatography
PublicationVodka andwhisky are produced fromgrain distillates. Formerly these alcohols were very often counterfeited, by the made in home conditions spirit drink called moonshine, which is obtained by distilling a mash from the alcoholic fermentation. This study presents research aimed at checking the usefulness of the electronic nose using ultra-fast gas chromatography for the differentiation of whisky, vodka and moonshine. 12 samples of...
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The comparison of vodka, whisky and moonshine by using the electronic nose based on the technology of ultra-fast gas chromatography
PublicationVodka andwhisky are produced fromgrain distillates. Formerly these alcohols were very often counterfeited, by the made in home conditions spirit drink called moonshine, which is obtained by distilling a mash from the alcoholic fermentation. This study presents research aimed at checking the usefulness of the electronic nose using ultra-fast gas chromatography for the differentiation of whisky, vodka and moonshine. 12 samples of...
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Development of gas chromatography - tandem mass spectrometry procedure for development of pesticide residues in honey and honeybee samples
PublicationA new analytical procedure of determination of multiresidue of pesticides based on application of the modified QuEChERS approach at the step of sample preparation and technique GC-MS/MS has been developed and applied for studies the real honey and honeybee samples. Samples were collected from northern Poland (Pomerania). The proposed procedure enables for the determination of 34 and 30 pesticides residues respectively on honey...
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Headspace solid-phase microextraction and gas chromatography-olfactometry analysis of raw spirits of different organoleptic quality
PublicationCelem pracy było określenie, ktore związki wnoszą wkład w aromat destylatów rolniczych i wskazać te z nich które mogą powodować obniżenie ich właściwości organoleptycznych. W badaniach zastosowano ekstrakcję lotnych analitów z fazy nadpowierzchniowej techniką mikroekstrakcji do fazy nadpowierzchniowej w połączeniu z chromatografia gazową z detekcja olfaktometryczną . Znaleziono 40 zsubstancji, które mogą być markerami jakości organoleptycznej
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Effect of irradiation intensity and initial pollutant concentration on gas phase photocatalytic activity of TiO2 nanotube arrays
PublicationWell-organized TiO2 nanotube arrays were fabricated via one-step anodization process. The as-prepared TiO2 nanotubes were characterized by X-ray powder diffractometry (XRD), X-ray photoelectron spectroscopy (XPS), diffuse reflectance spectroscopy (DRS) and scanning electron microscopy (SEM). Photocatalytic activity of obtained photocatalyst was studied in reaction of toluene degradation in the gas phase using low powered and low...
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Non-Gaussian Resistance Fluctuations in Gold-Nanoparticle-Based Gas Sensors: An Appraisal of Different Evaluation Techniques
PublicationVolatile organic compounds, such as formaldehyde, can be used as biomarkers in human exhaled breath in order to non-invasively detect various diseases, and the same compounds are of much interest also in the context of environmental monitoring and protection. Here, we report on a recently-developed gas sensor, based on surface-functionalized gold nanoparticles, which is able to generate voltage noise with a distinctly non-Gaussian...
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Investigation of the 16-year and 18-year ZTD Time Series Derived from GPS Data Processing
PublicationThe GPS system can play an important role in activities related to the monitoring of climate. Long time series, coherent strategy, and very high quality of tropospheric parameter Zenith Tropospheric Delay (ZTD) estimated on the basis of GPS data analysis allows to investigate its usefulness for climate research as a direct GPS product. This paper presents results of analysis of 16-year time series derived from EUREF Permanent Network...
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Thermal degradation assessment of canola and olive oil using ultra-fast gas chromatography coupled with chemometrics
PublicationOil blending is often used to enhance the properties of vegetable oils. The admixture of a more thermally stable oil makes the resulting blend more suitable for use in frying. A new method of quality assessment of vegetable oils used in frying is presented in this paper. In this method, ultra-fast gas chromatography coupled with flame ionization detector and chemometrics is employed. Principal component analysis was used for data...
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Time window based features extraction from temperature modulated gas sensors for prediction of ammonia concentration
PublicationElectronic gas recognition systems, in literature commonly referred as electronic noses, enable the recognition of a type and a concentration of various volatile compounds. Typical electronic gas-analyzing device consists of four main elements, namely, gas delivery subsystem, an array of gas sensors, data acquisition and power supply circuits and data analysis software. The commercially available metal-oxide TGS sensors are widely...
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MATCHED FILTER APPROACH FOR MICROSEISMIC SIGNAL PROCESSING OF REAL DATA FROM EAST POMERANIA SHALE GAS
PublicationThe microseismic monitoring is a method of monitoring of fracture propagation during hydraulic fracturing (HF)process. An array of several hundred geophones is placed on the surface to record little ground tremors induced by fracturing process. Filtration and summation of signals from geophones is essential to identify and locate fracturing events from underground. Authors propose a method of matched filtering, that is usually...
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Electroactive polymer/graphene oxide nanostructured composites; evidence for direct chemical interactions between PEDOT and GOx
PublicationThis work concerns electrochemical synthesis of nanocomposites consisting of conducting polymer and reduced graphene oxide (rGOx) as electrode materials for supercapacitors. The electrosynthesis was performed in an aqueous solution of the 3,4-ethylenedioxytiophene (EDOT) monomer and graphene oxide (GOx) without supporting electrolyte. The amount of GOx was optimized to obtain the best electrochemical performance of the nanocomposite...
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Characterizing surface and air temperature in the Baltic Sea coastal area using remote sensing techniques and GIS
PublicationEstimation of surface temperature using multispectral imagery retrieved from satellite sensors constitutes several problems in terms of accuracy, accessibility, quality and evaluation. In order to obtain accurate results, currently utilized methods rely on removing atmospheric fluctuations in separate spectral windows, applying atmospheric corrections or utilizing additional information related to atmosphere or surface characteristics...
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Environmental aspects of using gas chromatography for determination of pharmaceutical residues in samples characterized by different composition of the matrix
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DNA strand breaks induced by nuclear hijacking of neuronal NOS as an anti-cancer effect of 2-methoxyestradiol
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Utilization of thermal decomposition of immobilized compounds for the generation of gaseous standard mixtures used in the calibration of gas analysers
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Study of a method for the preparation of standard gas mixtures based on thermal decomposition of surface compounds. Application to isothiocyanates
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Thermal analysis of macro-encapsulated phase change material coupled with domestic gas heater for building heating
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Results of the application of tropospheric corrections from different troposphere models for precise GPS rapid static positioning
PublicationIn many surveying applications, determination of accurate heights is of significant interest. The delay caused by the neutral atmosphere is one of the main factors limiting the accuracy of GPS positioning and affecting mainly the height coordinate component rather than horizontal ones. Estimation of the zenith total delay is a commonly used technique for accounting for the tropospheric delay in static positioning. However, in the...
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Instantaneous Heating and Cooling Caused by Periodic or Aperiodic Sound of Any Characteristic Duration in a Gas with Vibrational Relaxation
PublicationThermodynamic relaxation of internal degrees of a molecule's freedom in a gas occurs with some characteristic time. This makes wave processes in a gas behave differently depending on the ratio of characteristic duration of perturbations and the relaxation time. In particular, generation of the secondary non-wave modes by intense sound in a nonlinear flow dependens on frequency. These kinds of interaction are considered in this...
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DETERMINING THE TIME CONSTANT USING TWO METHODS AND DEFINING THE THERMOCOUPLE RESPONSE TO SINE EXCITATION OF GAS TEMPERATURE
PublicationThis paper describes the two methods of determining the time constant of type K thermocouple, for two construction solutions: the exposed weld and the mantle fillet weld. This is an important parameter indicating the response time of the thermocouple on the recorded signal. The first method consists of determining the value of τ in the way of numerical simulation of heat exchange between the thermocouple and the current of gas...
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Standing Waves in One-Dimensional Resonator Contaning an Ideal Isothermal Gas Affected by the Constant Mass Force
PublicationThe study is devoted to standing acoustic waves in one-dimensional planar resonator which containing an ideal gas. A gas is affected by the constant mass force. Two types of physically justified boundary conditions are considered: zero velocity or zero excess pressure at both boundaries. The variety of nodal and antinodal points is determined. The conclusion is that the nodes of pressure and antinodes of velocity do not longer...
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Laboratory station for research of the innovative dry method of exhaust gas desulfurization for an engine powered with residual fuel
PublicationContemporary methods of exhaust gas desulfurization in marine engines are all expensive methods (4-5 million euro). This is, among other reasons, due to the limited market audience, but primarily due to the monop-olized position of manufacturers offering fabrication and assembly of this type of marine ship installations. Proposed as part of a research project financed by the Regional Fund for Environmental Protection and Maritime...
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Direct solid phase microextraction combined with gas chromatography – Mass spectrometry for the determination of biogenic amines in wine
PublicationA direct method based on immersion solid phase microextraction (DI-SPME) gas chromatography mass-spectrometry (GC-MS) was optimized and validated for the determination of 16 biogenic amines in Polish wines. In the analysis two internal standards were used: 1,7-diaminoheptane and bis-3-aminopropylamine. The method allows for simultaneous extraction and derivatization, providing a simple and fast mode of extraction and enrichment....
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Evaluation of flavour profiles in e-cigarette refill solutions using gas chromatography–tandem mass spectrometry
PublicationMany flavour compounds that are present in e-liquids for e-cigarettes are responsible for specific tastes and smoking sensations for users. Data concerning content and specific types of flavours is often limited and unknown to users. The aim of the research was to define and compare flavour profiles of e-liquids with the same group taste from different manufacturers. Gas chromatography coupled with tandem mass spectrometry (GC–MS/MS)...
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New Technique of preparation of standard gas mixtures needed for validation of analytical procedures used in environmental studies
PublicationStandard gas mixtures are indispensable reference materials for ensuring the reliability of analytical work. Paper presents one novel approach in the field of production of gaseous reference materials based on the application of thermal decomposition process of proper surface compound for obtaining the desired gaseous analyte. The main fields of application of reference materials are presented. The field of application of thermal...
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Związki endokrynne w środowisku. Problemy i wyzwania cz. I Emisja i los środowiskowy
PublicationWzrost świadomości dotyczącej niekorzystnego wpływu działalności człowieka na stan środowiska oraz dynamiczny rozwój technik analitycznych spowodował, że w ostatnich latach wzrosło zainteresowanie problematyką związków zakłócających prawidłowe funkcjonowanie układu endokrynnego. W opracowaniu zamieszczono informacje o niektórych związkach z grupy estrogenów, ich losie środowiskowym oraz oddziaływaniu na organizmy żywe.