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Search results for: THIN FILM DEPOSITION
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Bioactive core material for porous load-bearing implants
PublicationSo far state of knowledge on biodegradable materials is reviewed. Among a variety of investigated materials, those composed of polymers and ceramics may be considered as only candidates for a core material in porous titanium alloy. The collagen and chitosan among natural polymers, polyhydroxy acids among synthetic polymers, and hydroxyapatite and tricalcium phosphate among ceramics are proposed for further research. Three essential...
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Development of Microstructured Carbon Coatings by Substrate-Catalytic CVD
PublicationCarbon nanostructured films were synthesized by chemical vapor deposition (CVD) on H18 stainless steel (AISI 440C) sheets with an H2/CH4/N2 gas mixture at various substrate temperatures. During the synthesis, the iron and chromium oxide layer was formed between the steel and carbonaceous layer. The carbon films exhibited wall-like and spherical morphologies and structures, as characterized by scanning electron microscopy and Raman...
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Improvement of Thrust Bearing Calculation Considering the Convectional Heating within the Space between the Pads
PublicationA modern thrust bearing tool is used to estimate the behavior of tilting pad thrust bearings not only in the oil film between pad and rotating collar, but also in the space between the pads. The oil flow in the space significantly influences the oil film inlet temperature and the heating of pad and collar. For that reason, it is necessary to define an oil mixing model for the space between the pads. In the bearing tool, the solutions...
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Application of the Optimization Methods to the Search of Marine Propulsion Shafting Global Equilibrium in Running Condition
PublicationFull film hydrodynamic lubrication of marine propulsion shafting journal bearings in running condition is discussed. Considerable computational difficulties in non-linear determining the quasi-static equilibrium of the shafting are highlighted. The approach using two optimization methods (the particle swarm method and the interior point method) in combination with the specially developed relaxation technique is proposed to overcome...
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Sensing the onset of epoxy coating degradation with combined Raman spectroscopy/atomic force microscopy/electrochemical impedance spectroscopy
PublicationThe paper presents the results of investigation on epoxy resin durability upon 12-week exposure to UV radiation. The aim was early determination of the onset of epoxy degradation and for this purpose an epoxy film on steel substrate systems were periodically inspected using Raman spectroscopy, atomic force microscopy and electrochemical impedance spectroscopy. The behaviour of examined polymer could be divided into three periods: immunity,...
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Tuning of the finesse coefficient of optoelectronic devices
PublicationOptoelectronic devices attracted considerable attention in many branches of science and technology, which can be attributed to their unique properties. Many of them use optical cavities which parameters can be adopted to specific requirements. This thesis investigates the introduction of diamond structures (nitrogen-doped diamond film, boron-doped diamond film, undoped diamond sheet) to optical cavities to tune their finesse coefficient....
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Hydrogen Damage in Superaustenitic 904L Stainless Steels
Publicationresults on the influence of hydrogen on corrosion resistance and of hydrogen embrittlement of 904L superaustenitic stainless steel were investigated. The cracking behavior was studied by performing a slow strain rate test in synthetic seawater under varying cathodic polarization conditions. The results showed that the steel’s plasticity varied with the applied cathodic current density. Significant reductions in ductility were found,...
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OPERATING CONDITIONS OF SLIDE BEARINGS OF MILLS USED IN KGHM POLSKA MIEDŹ S.A.
PublicationThe paper contains the results from a tec hnical analysis of the conditions of the operation of hydrodynamic bearings supporting the drums of ore processing mills at KGHM Polska Mied ź S.A. A theoretical analysis was performed on the grounds of onsite examination and measurem ents of principal dimensions of the bearings of interest. The computer simulation covered the characteristics of the oil film in the bearings...
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Wide-field magnetometry using nitrogen-vacancy color centers with randomly oriented micro-diamonds
PublicationMagnetometry with nitrogen-vacancy (NV) color centers in diamond has gained significant interest among researchers in recent years. Absolute knowledge of the three-dimensional orientation of the magnetic field is necessary for many applications. Conventional magnetometry measurements are usually performed with NV ensembles in a bulk diamond with a thin NV layer or a scanning probe in the form of a diamond tip, which requires a...
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Investigation of catalytic layers on anode for solid oxide fuel cells operating with synthetic biogas
PublicationIn this paper solid oxide fuel cells operating with dry synthetic biogas have been examined. In order to increase their stability the layers of CuO-CeO2, Cu1.3Mn1.7O4 and Y0.08Sr0.92Ti0.8Fe0.2O3 -δ have been deposited on the Ni-YSZ anode site. These layers should catalyze the internal biogas reforming and prevent the carbon deposition on the anode site. It has been found that CuO-CeO2 and Cu1.3Mn1.7O4 catalysts led to an increase...
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Spatial characterization of H 2: CH 4 dissociation level in microwave ECR plasma source by fibre-optic OES
PublicationSpatially resolved optical emission spectroscopy (SR-OES) was used to investigate microwave activated H2/Ar/CH4 plasma under conditions of the electron cyclotron resonance (ECR). The chemistry and composition of the gas phase were studied using self-designed fibre-optic system with echelle type spectrometer during CVD deposition of polycrystalline diamond. One-dimensional intensity profiles of the main species were collected along...
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Study of the Influence of Heat Convection Coefficient on Predicted Performance of a Large Tilting-Pad Thrust Bearing
PublicationPart of the heat generated by the shearing of the lubricating film during operation of a hydrodynamic bearing is transferred to the bearing components. In the case of the pad, which is usually fully submerged in the lubricating oil, heat is further transferred at the pad free walls to the oil by convection. This mechanism causes a thermal gradient in a pad and, consequently, its thermal deflection. In large hydrodynamic thrust...
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Conducting Polymer Microelectrodes Anchored to Hydrogel Films
PublicationArtykuł prezentuje wytwarzanie organicznych hydrożeli z mikroelektrodami poli(3,4-ethylenedioxythiophene, PEDOT), które wykazują obniżoną rezystywność 100 Ω/□. Proces przygotowania rozpoczyna się elektroosadzania przewodzącego PEDOT (ok. 20 S/cm) na mikroelektrodach Pt. Elektrolityczne wiąże się film PEDOT z hydrożelem. Tak wytworzona struktura jest odrywana elektrycznie pd podłoża.
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A 3D-FEM mesh technique for fast analysis of waveguide problems containing rotatable tuning elements
PublicationIn this paper a meshing technique for 3D Finite Element Method is presented. It allows for fast analysis and optimization of the waveguide structures, which contain rotatable tuning elements. In the proposed procedure a thin layer of varying cylindrical mesh buffer is introduced in order to reuse unchanged mesh and FEM matrices in the rest of the domain.
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Storing Matter’technique in SIMS depth profile analysis
PublicationSecondary ion mass spectrometry (SIMS) is a very useful technique for the analysis of layered systems. It is based on the primary ion beam sputtering of solids and mass analysis of the emitted secondary ions. A main limitation of this technique results from the direct quantitative analysis, since the ionization efficiency of a given atom is highly influenced by the neighbouring atoms at the surface. This phenomenon is known as...
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Osteoblast and bacterial cell response on RGD peptide‐functionalized chitosan coatings electrophoretically deposited from different suspensions on Ti13Nb13Zr alloy
PublicationMetallic materials for long-term load-bearing implants still do not provide high antimicrobial activity while maintaining strong compatibility with bone cells. This study aimed to modify the surface of Ti13Nb13Zr alloy by electrophoretic deposition of a chitosan coating with a covalently attached Arg-Gly-Asp (RGD) peptide. The suspensions for coating deposition were prepared in two different ways either using hydroxyacetic acid...
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Wideband crossover structure with double ring resonators
PublicationThe structure of a four-port microstrip crossover is presented. The device is composed of two ring resonators, one circular and one built from meander lines, connected by four straight lines. The equivalent circuit model of the crossover is derived. The structure is designed on thin and flexible substrate to allow it to bend. The possibility of applying the device on curved surfaces is tested experimentally.
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Simulation investigation of perovskite-based solar cells
PublicationThree models of thin-layer lead-halide perovskite solar cells with different electron-transport layers (TiO2,SnO2,ZnO) were investigatedby the simulation method. The perovskite layer thickness was optimized for all the systems. The analysis of the standard photovoltaic cell performanceparameters at various operating temperatures was performed. The best performance was achieved for the system with theSnO2conductive layer.
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THE PROPERTIES OF NANOSILVER – DOPED NANOHYDROXYAPATITE COATING ON THE Ti13Zr13Nb ALLOY
PublicationThe aim of this research was to study the properties of nanohydroxyapatite (nanoHAp) and nanohydroxyapatite, doped with nanosilver (nanoHAp/nanoAg), coatings obtained by an electrophoretic deposition process. The suspensions was prepared by dispersing 0.1 g of HAp nanopowder for nanoHAp coatings and 0.1 g of nanoHAp and 0.025 g nanoAg for nanoHAp/nanoAg coatings. The deposition was carried out for 1 min at 50 V voltage followed...
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Nanocrystalline diamond sheets as protective coatings for fiber-optic measurement head
PublicationFiber-optic sensors find numerous applications in science and industry, but their full potential is limited because of the risk of damaging the measurement head, in particular, due to the vulnerability of unprotected tips of the fiber to mechanical damage and aggressive chemical agents. In this paper, we report the first use of a new nanocrystalline diamond structure in a fiber-optic measurement head as a protective coating of...
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Mono- and bi-metallic plasmonic photocatalysts for degradation of organic compounds under UV and visible light irradiation
PublicationTitania powders were surface modified with gold and/or silver nanoparticles (NPs) by photodeposition method. Gold modified titania exhibited much higher photocatalytic activity during methanol dehydrogenation under UV irradiation than titania modified with monometallic silver and bimetallic Au–Ag NPs. Bimetallic photocatalysts exhibited either enhanced or reduced visible light activity, depending on properties of noble metal NPs,...
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COMPARISON OF HEAT TRANSFER CHARACTERISTICS IN SURFACE COOLING WITH BOILING MICROJETS OF WATER, ETHANOL AND HFE7100
PublicationThe basis of microjet technology is to produce laminar jets which when impinging the surface have a very high kinetic energy at the stagnation point. Boundary layer is not formed in those conditions, while the area of film cooling has a very high turbulence resulting from a very high heat transfer coefficient. Applied technology of jet production can result with the size of jets ranging from 20 to 500μm in breadth and 20 to 100μm...
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Experimental comparison of the transition speed of a hydrodynamic journal bearing lubricated with oil and magnetorheological fluid
PublicationA journal bearing test bench is used to find the transition speed between the hydrodynamic and mixed lubrication regimes for a modified magnetorheological (MR) fluid. It is shown that the transition speed of the bearing can be reduced by applying a local magnetic field near minimum film when it is lubricated with the MR fluid, and that this will only marginally increase friction. The lubricating performance of the MR fluid is compared...
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Nitrogen dioxide sensing properties of PEDOT polymer films
PublicationThis work presents a simple and fully electrochemical route for the polymerization of poly(3,4-ethylenedioxytiophene) (PEDOT) films for fabricating a NO2 gas sensor prepared by electropolymerization of 3,4-Ethylenedioxythiophene (EDOT) monomer in lithium perchlorate/acetonitrile solution. The main aim of this study is to determine the sensing properties of conductive polymer at elevated temperatures. The effects of the humidity,...
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Capacity of Surface Production of Band Sawing in Manufacture of Oak Floor Upper Layers
PublicationThin lamellae, corresponding to the layer components of structural glued members, i.e., 2-ply or 3-ply glued flooring, can be manufactured in re-sawing operations of kiln-dried wood blocks or in wet technologies, which currently seem to be more common because of the shorter drying time. The re-sawing process in wet technology is conducted on dedicated thin-cutting band sawing machines with stellite-tipped band saws. The goal of...
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Nanocrystalline CVD Diamond Coatings on Fused Silica Optical Fibres: Optical Properties Study
Publicationpre-treatment by dip coating in two detonation nanodiamond (DND) seeding media has been studied. The DND suspension in ethyl alcohol and dispersion of DND in dimethyl sulfoxide (DMSO) with polyvinyl alcohol (PVA) were chosen for the seeding purpose. The grain size distribution of nanodiamond particles in both seeding media was kept at the same level (approximately 1050 nm). After the seeding nanocrystalline diamond lms were deposited...
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Studies on optical transmittance of boron-doped nanocrystalline diamond films
PublicationThickness is one of the most important parameters in many applications using thin layers. This article describes thickness determination of a boron-doped nanocrystalline diamond (NCD) grown on fused silica glass. A spectroscopic measurement system has been used. A high refractive index (2.3 at 550nm) was achieved for NCD films. The thickness of NCD samples has been determined from the transmission spectrum.
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Effect of power frequency on the stress state of disc actuator
PublicationThis paper presents the concept of determining the optimum frequency of coil supply in inductive-dynamic drive. As a criterion to obtain the sought frequency, the smallest value of reduced stress in the disc was assumed while maintaining the desired dynamics. The disc stress is determined on the basis of solution of vibrating thin plate equation. Magnetic pressure acting on the disc is obtained from a hybrid circumferentially-field...
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Production of new non-matrix reference material of ethene
PublicationThe main objective of the research is to produce new non-matrix reference materials of ethene. The study are based on thermal decomposition of surface compound chemically bonded with the surface of glass fibers coated with thin layer of aluminum. Positivehomogeneity test, stability test and organization of inter-laboratory comparison are leading to find new non-matrix reference materials which are indispensable tools in the analysis...
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Modeling of Composite Shells in 6-Parameter Nonlinear Theory with Drilling Degree of Freedom
PublicationWithin the framework of a 6-parameter nonlinear shell theory, with strain measures of Cosserat type, constitutive relations are proposed for thin elastic composite shells. The material law is expressed in terms of five engineering constants of classical anisotropic continuum plus an additional parameter accounting for drilling stiffness. The theory allows for unlimited displacements and rotations. A number of examples are presented...
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Wpływ stopowania laserowego z użyciem nanorurek węglowych stopu Ti13Nb13Zr do zastosowań biomedycznych na jego wybrane własności mechaniczne
PublicationDo eksperymentu użyto stopu tytanu Ti13Nb13Zr, który ze względu na swój skład chemiczny i właściwości mechaniczne stanowi materiał do zastosowań w inżynierii medycznej. Celem pracy była ocena wpływu stopowania laserowego stopu Ti13Nb13Zr z powłoką z wielościennych nanorurek węglowych na jego właściwości mechaniczne (chropowatość, nanotwardość, moduł Younga). Do wytworzenia powłoki węglowej wykorzystano metodę osadzania elektroforetycznego (EDP)....
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Investigation of the thermal effects in water-lubricated journal bearings with axial grooves
PublicationWater-lubricated hydrodynamic journal bearings are frequently applied as stern tube bearings due to their advantages over other bearing types. They are environmentally friendly, can operate without sealings and in conditions of low friction losses. The most popular are bearings with open axial grooves, which require, for proper operation, forced axial flow of the lubricating water. Correctly designed and operated stern tube bearings...
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Efektywność skrępowania betonu w grubościennych słupach typu Concrete-Filled Steel Tube o przekroju kołowym
PublicationW słupach typu CFST w stanie granicznym dochodzi do zwiększenia wytrzymałości betonu rdzenia na skutek jego skrępowania. Zaistnienie tego zjawiska zależy od wielu czynników. Jednym z najważniejszych z nich jest sztywność obwodowa płaszcza stalowego. Jej wpływ na efektywność wzrostu wytrzymałości betonu rdzenia przebadano eksperymentalnie na grupie 48 grubościennych słupów CFST. Wykazano, że nadmierne zwiększanie grubości płaszcza...
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Reduction of parasitic pitch variations in archival musical recordings
PublicationA new method for reducing parasitic pitch variations in archival audio recordings is presented. The method is intended for analyzing movie soundtracks recorded in optical films. It utilizes image processing for calculating and reducing effects of tape shrinkage being one of the main reasons for parasitic pitch variations in audio accompanying moving images. As long as the film tape characteristics are known the new method can be...
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Elctrochemical oxidation and corrosion resistance of the Ti13Nb13Zr alloy
PublicationThis paper presents the results of oxidation and corrosion tests carried out on titanium alloy Ti13Nb13Zr. The oxide film was prepared by electrochemical environment 2M H3PO4 for 30 min and 1 h, at a constant voltage 40V. The tests of corrosion resistance were performed by potentiostatic method in Ringer's solution at different pH values: 7, 5 and 3. The change in an appearance of surface and the increase in corrosion resistance...
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A SEARCH OF AN INDUCER GEOMETRY THAT IS BENEFICIAL FOR LIFTING PARAMETERS OF A LIFTED OBJECT OF A SELECTED SHAPE
PublicationThe literature describes acoustic levitation phenomena with the utilization of air squeeze film between the vibrating inducer and the lifted object. The objective of the study is to determine the shape of the inducer with vibration characteristics that would allow the levitation of an object of the assumed geometry. In this paper, the influence of the dimension ratio of the inducer on the frequency of the first mode of vibration...
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Tuning the Laser-Induced Processing of 3D Porous Graphenic Nanostructures by Boron-Doped Diamond Particles for Flexible Microsupercapacitors
PublicationCarbon (sp3)-on-carbon (sp2) materials have the potential to revolutionize fields such as energy storage and microelectronics. However, the rational engineering and printing of carbon-on-carbon materials on flexible substrates remains a challenge in wearable electronics technology. This study demon-strates the scalable fabrication of flexible laser-induced graphene (LIG)-boron doped diamond nanowall (BDNW) hybrid nanostructures...
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Experimental study on the feasibility of alternative materials for tilting pad thrust bearings operating in transition to mixed friction
PublicationIn hydrodynamic bearings traditional bearing alloys: Babbitts and bronzes are most frequently utilized. Polymer sliding layers are sometimes applied as a valuable alternative. Hard diamond-like carbon (DLC) coatings, which are also considered for certain applications may show some advantages, as well. Although material selection is of secondary importance in a full film lubrication regime it becomes important in mixed friction...
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Polymer based thick films - material quality and interface resistance evaluation
PublicationThe properties of polymer based thick film layers mede using different resistive pastes and dipping silvers have been studied. The composite of carbon and graphite (C/Gr) conducting particles suspended in different polymer vehicles were used for preparation resistive layers. Interface resistance Rc created between dipping silver (DiAg) contact layer and resistive layer was determined from the surface potential distribution measurements...
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Organic-inorganic composites consisted of poly(3,4-ethylenedioxythiophene)and Prussian Blue analogues
PublicationThe organic-inorganic material consisted of poly(3,4-ethylenedioxythiophene) (pEDOT) and copper hexacyanoferrate (Cuhcf) was synthesized. The pEDOT film with Fe(CN)63−/4− as counter-ions potentiodynamically polarized in aqueous CuCl2 electrolyte brings about stable hybrid material (pEDOT/Cuhcf) performing single redox activity of FeII/III at a formal potential Ef = 0.61 V (vs. Ag/AgCl/0.1 M KCl) and less clearly shaped two redox...
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Simultaneous optical and electrochemical label-free biosensing with ITO-coated lossy-mode resonance sensor
PublicationIn this work we discuss a new label-free biosensing device based on indium tin oxide (ITO) overlaid section of a multimode optical fiber fused silica core. The sensor has been used to optical measurements also simultaneously interrogated electrochemically (EC). Due to optimized thickness and optical properties of ITO film, a lossy-mode resonance (LMR) could be observed in the optical domain, where electrical properties of the film...
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Static and dynamic modelling blow- out type trauma of orbital wall
PublicationAuthors of the paper present initial results of finite element analysis of a blow-out type trauma of orbital wall. The research is liked with laboratory tests for the Young’s modulus of bones evaluation. In the finite element analysis the neighbourhood of orbital wall is modelled by triangle thin shell finite elements. In the paper results of nonlinear static and transient dynamic analysis (including damping) are compared. The...
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Variational Method of Finding Streamlines in Ring Cascades for Creeping Flows
PublicationThis paper presents a new, analytical method of finding streamlinesfor creeping flows inside a ring cascade which is composed of an infinite number of infinitely thin blades. An analytical solution has been obtained through minimisation of a dissipation functional by means of variational calculus method. The necessary condition for optimum of a functional gives the Stokes equation if some additional assumptions are introduced....
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Analysis of degaussing process of ferromagnetic objects
PublicationResults of the analytical and numerical analysis of the degaussing process phenomena of ferromagnetic objects were presented in this paper. The screening effectiveness of the electromagnetic field of magnetic screens in most cases depends on thickness, conductivity, magnetic permeability of the screen and angular frequency of degaussing currents. The magnetic field inside thin-layer ferromagnetic object was presented in this paper....
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Postprodukcja nagrania wideo z dzwiekiem dookolnym
PublicationOne of the aims of this paper is to present issues related to audio-video correlation. This is presented on the basis of a short film realization employing surround microphone techniques. First, some related works in the domain of sound and vision correlation are presented. Then assumptions concerning scene creation related to both audio and video are shortly described. Another objective is to discuss results of subjective tests...
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Synergic Effect of Naphthylated Carbon Nanotubes and Gold Nanoparticles on Catalytic Performance of Hybrid Films Containing Bilirubin Oxidase for the Dioxygen Reduction
PublicationTo improve the direct electron transfer from a multicopper oxidase MvBOd to the glassy carbon electrode surface the naphthylated multiwall carbon nanotubes (Napht-MWCNTs) are ombined with gold nanoparticles (AuNPs) to form a conductive network at the electrode and to increase its working surface. Such approach allowed to eliminate the necessity of employing mediators to reach elevated current values. The enzyme stability was improved...
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Tailoring the electrochemical degradation of iron protected with polypyrrole films for biodegradable cardiovascular stents
PublicationThe degradation of polypyrrole (PPy) coated iron is studied in phosphate buffer saline solution at 37 °C by odd random phase multisine electrochemical impedance spectroscopy (ORP-EIS). PPy is electropolymerized with anti-inflammatory salicylates incorporated in the film, as a drug release system. The modelling of EIS over time provides the quantitative description of the corrosion behaviour of the material. Thus, the reliable...
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Search for the most useful geometry of an acoustic journal bearing
PublicationComputer simulations of a number of journal bearing’s geometries utilising acoustic levitation were carried out. The choice of the best geometry depended on the ability of a deformed shape, created by piezo-electric elements, to facilitate squeeze film ultrasonic levitation, and also to create three evenly distributed diverging aerodynamic gaps. Deformations of analysed variants of the bearing’s shape were generated by numerical...
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Fluctuation enhanced gas sensing using UV irradiated Au-nanoparticle-decorated WO3-nanowire films
PublicationWO3 nanowires (WO3-NWs) decorated with gold nanoparticles (AuNPs) were utilized in resistive gas sensor devices to detect ethanol by use of fluctuation enhanced sensing (FES). The experimental system records both DC resistance and fluctuations of the sensing film. Our data verify that the sensitivity and selectivity of the gas sensor are improved by applying FES when the sensor is stimulated with a combination of UV light and heating....
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Ocena możliwości zastosowania obróbki laserowej i implantacji jonowej stopów metali na implant stawu kolanowego
PublicationZagadnieniem podjętym w niniejszym referacie jest zmodyfikowanie warstwy wierzchniej stopu tytanu Ti6Al4V przeznaczonego na implanty. Autor opisuje metody modyfikacji powierzchni w wyniki nakładania warstwy węglowej metodą PA CVD (ang. Plasma Assisted Chemical Vapour Deposition) oraz warstwy hydroksyapatytu metodą zol-żel i elektrochemiczną. Badania zostały przeprowadzone w laboratoriach Zakładu Biomateriałów, Katedry Inżynierii...