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Search results for: BIA%C5%81KA%20REKOMBINANTOWE%20TOXOPLASMA%20GONDII
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Preparation of 1-[Ω-(1,4,5,6-Tetrahydropyrimidin-2-yl)alkyl]thymines
PublicationOne-stage prepn. of the hydrochloride salts of 1-[ω-(1,4,5,6-tetrahydropyrimidin-2-yl)alkyl]-thymines, e.g. I, from 1-(ω-cyanoalkyl)thymines and a 1:1-mixt. of 1,3-diaminopropane and ethanol satd. with hydrogen sulfide is described. 1-(2-Cyanoethyl)-thymine gave a facile reversal of the Michael reaction to thymine under the conditions used. The reaction of 1,3-bis(3-cyanobenzyl)thymine with the above reagent produced 1,3-bis[3-(1,4,5,6-tetrahydropyrimidin-2-yl)benzyl]thymine.
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Problemy pracy zabezpieczeń odległościowych linii 400 kV w Polsce północno-wschodniej
PublicationW roku 2015 oddano do użytku połączenie polskiego systemu elektroenergetycznego z systemem elektroenergetycznym Litwy. Połączenie to zrealizowano z wykorzystaniem dwutorowej linii napowietrznej 400 kV Ełk Bis – Alytus oraz łącza back-to-back (BtB). W artykule przeanalizowano wpływ realizacji nowego połączenia, a tym samym zmianę konfiguracji sieci 400 kV, na detekcję zakłóceń przez zabezpieczenia odległościowe linii 400 kV znajdujących...
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Non-linear static stability of bi-layer carbon nanosheets resting on an elastic matrix under various types of in-plane shearing loads in thermo-elasticity using nonlocal continuum
PublicationIn this research, the shear and thermal buckling of bi-layer rectangular orthotropic carbon nanosheets embedded on an elastic matrix using the nonlocal elasticity theory and non-linear strains of Von-Karman was studied. The bi-layer carbon sheets were modeled as a double-layered plate, and van der Waals forces between layers were considered. The governing equations and boundary conditions were obtained using the first order shear...
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Implementation of Hermite-Ritz method and Navier’s Technique for Vibration of Functionally Graded Porous Nanobeam Embedded in Winkler-Pasternak Elastic Foundation Using bi-Helmholtz type of nonlocal elasticity
PublicationPresent study is devoted to investigating the vibration characteristics of Functionally Graded (FG) porous nanobeam embedded in an elastic substrate of Winkler-Pasternak type. Classical beam theory (CBT) or Euler-Bernoulli beam theory (EBT) has been incorporated to address the displacement of the FG nanobeam. Bi-Helmholtz type of nonlocal elasticity is being used to capture the small scale effect of the FG nanobeam. Further, the...
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Head-Space SPME for the Analysis of Organophosphorus Insecticides by Novel Silica IL-Based Fibers in Real Samples
PublicationThis work demonstrates the suitability of a newly developed ionic liquid (IL)-based silica SPME fiber for the determination of seven organophosphorus insecticides in cucumber and grapefruit samples by headspace solid-phase microextraction (HS-SPME) with a gas chromatography–flame ionization detector (FID). The sol-gel method released four different sorbent coatings, which were obtained based on a silica matrix containing ILs immobilized...
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Poly(ε-Caprolactone)/Poly(Lactic Acid) Blends Compatibilized by Peroxide Initiators: Comparison of Two Strategies
PublicationPoly(ε-caprolactone) (PCL) and poly(lactic acid) (PLA) blends were compatibilized by reactive blending and by copolymers formed during reaction in the solution. The reactive blending of PCL/PLA was performed using di-(2-tert-butyl-peroxyisopropyl)benzene (BIB) or dicumyl peroxide (DCP) as radical initiator. PCL-g-PLA copolymers were prepared using 1.0 wt. % of DCP or BIB via reaction in solution, which was investigated through...
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Electrical properties of hybrid planar diode based on palladium phthalocyanine and titanium dioxide
PublicationThis work details experimental studies of a planar diode made of indium tin oxide/titanium dioxide/palladium phthalocyanine/gold. The rectification ratio of current was 105 at 1.5 V. The analysis of the electrical properties of the system was based on small signal complex capacitance spectra measured in the frequency range of 25 Hz-1 MHz at different values of bias. No depletion region at the TiO2/PdPc interface was observed. Forward...
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Derivatization of single-walled carbon nanotubes with redox mediator biocatalytic oxygen electrodes
PublicationSingle-walled carbon nanotubes were covalently modyfied with a redox mediator derived from 2,2'-azino-bis-(3-ethylbenzothiazole)-6-sulfonic acid.
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The study on application of biopolyols obtained by cellulose biomass liquefaction performed with crude glycerol for the synthesis of rigid polyurethane foams
PublicationIn this work rigid polyurethane foams (PUR) were obtained by replacement of 0–70 wt% of petrochemical polyol with bio-polyol obtained via cellulose liquefaction in presence of crude glycerol. The foams with different content of a bio-polyol were prepared by single step method for NCO/OH ratio equals 1.5. The prepared materials were analyzed in terms of their morphology, chemical structure, thermal stability and basic physical and...
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Crystal structures of eight- and ten-membered cyclic bisanisylphosphonothioyl disulfanes and comparison with their P-ferrocenyl analogues
PublicationTwo new crystal structures of eight- and ten-membered cyclic bisanisylphosphonothioyl disulfanes, namely 2,5-bis(4-methoxyphenyl)-1,6,3,4,25,55- dioxadithiadiphosphocane-2,5-dithione, C16H18O4P2S4, and 2,5-bis(4-methoxyphenyl)-1,6,3,4,25,55-dioxadithiadiphosphecane-2,5-dithione, C18H22O4P2S4, have been determined and compared to structures of the ferrocenyl analogues. The eight-membered rings have similar conformations (TBC) but...
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Structural, mechanical and thermal behavior assessments of PCL/PHB blends reactively compatibilized with organic peroxides
PublicationThe efficiency of two commercially available organic peroxides, dicumyl peroxide (DCP) and di-(2-tert-butyl-peroxyisopropyl)-benzene (BIB), during reactive processing of poly (ε-caprolactone)/poly (3-hydroxybutyrate) (PCL/PHB) blends was investigated. The changes in chemical structure of PCL/PHB blends, as a function of organic peroxide type (DCP/BIB) and content (in range: 0–1.0 parts by weight - pbw), were characterized by Fourier...
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Asynchronous Charge Carrier Injection in Perovskite Light-Emitting Transistors
PublicationUnbalanced mobility and injection of charge carriers in metal-halide perovskite light-emitting devices pose severe limitations to the efficiency and response time of the electroluminescence. Modulation of gate bias in methylammonium lead iodide light-emitting transistors has proven effective in increasing the brightness of light emission up to MHz frequencies. In this work, a new approach is developed to improve charge carrier...
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Bisphenols (A, S, and F) affect the basic hormonal activity determined for pharmaceuticals – Study of Saccharomyces cerevisiae
PublicationPharmaceuticals and analogs of bisphenol A (BPA) are increasingly threatening environmental pollutants. In this study, mixtures of selected pharmaceuticals (diclofenac sodium salt, chloramphenicol, oxytetracycline hydrochloride, fluoxetine hydrochloride, estrone, ketoprofen, progesterone, gemfibrozil and androstenedione) were prepared with BPA and its two analogs (namely, bisphenols F and S) at such ratios to reflect environmentally...
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Convergence of rational multistep methods of Adams-Padé type
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Convergence of rational multistep methods of of Adams-Padé type
PublicationRational generalizations of multistep schemes, where the linear stiff part of a given problem is treated by an A-stable rational approximation, have been proposed by several authors, but a reasonable convergence analysis for stiff problems has not been provided so far. In this paper we directly relate this approach to exponential multistep methods, a subclass of the increasingly popular class of exponential integrators. This natural,...
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Die Sandgrube „Köplitz“ – ein interessanter geologischer Aufschluss am Nordwestrand der Schmiedeberger Stauchendmoräne
PublicationDie Kiessandgrube Köplitz ermöglicht einen Einblick in die komplizierten, durch glazidynamische Überprägung gekennzeichneten geologischen Lagerungsverhältnisse im Bereich der Schmiedeberger Stauchendmoräne. Anhand neuer Geländedokumentationen wird ein kleiner Eindruck vom komplizierten injektiven „Fließfalten-Schuppenbau“ der Stauchendmoräne vermittelt. Die steil aufgerichteten, aus tertiären (Untermiozän bis Oligozän) und quartären...
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4-(Cyclic-amidino)phenols. Preparation and Use in a Diamidine Synthesis
PublicationThe Pinner synthesis was applied to the prepn. of phenols 4-substituted with cyclic amidines in high yields from readily available 4-HOC6H4C(OMe):NH.HCl and aliph. diamines. An alternative attempt was made to convert 4-HOC6H4CSNH2 to 4-(1,4,5,6-tetrahydro-5-hydroxy-2-pyrimidinyl)phenol. A procedure for the prepn. of 3,6-bis(4-hydroxyphenyl)-1,2,4,5-tetrazine is reported. The syntheses of 2,4-bis[4-(4,5-dihydro-1H-imidazol-2-yl)phenoxy]pyrimidine...
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Metoda wektorowa pomiaru impedancji pętli zwarciowej w obecności załóceń.** 2002, 116 s. 44 rys. 3 tab. bibliogr. 122 poz. maszyn. Rozprawa doktorska (2002.05.07), Wydz. EiA, P. Gdań. Promotor: dr hab. inż. R. Roskosz, prof. nadzw. PG.
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Zanieczyszczenie obecne w próbkach śniegu pobranego z warstw jako źródło informacji o stanie środowiska w dużej aglomeracji miejskiej = Pollutants present in snow samples collected from various layers of snow cover as a source of information about the state of environment in a big urban agglomeration
PublicationPróbki śniegu pobierano przez okres około miesiąca z 12 miejsc zlokalizowanych na terenie Trójmiasta. Sześć z nich znajdowało się w pobliżu dróg komunikacyjnych o różnym natężeniu ruchu. Każde z nich miało swój punkt odniesienia oddalony od niego o około 200 m. W próbkach śniegu oznaczano pH, przewodność, zawartość wybranych anionów i kationów. Wartości pH wyznaczono przy użyciu elektrody szklanej połączonej z pH/tlenomierzem mikrokomputerowym,...
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Mechanism of Isomerization and Acid-Induced Transformations of 3-Hydroxy-4,4'-dimethoxy-3'-methyl-3-oxo-7,7'-bis(piperidino-carbonyloxy)-2,2'-spirobi-[2H,2'H,3H,3'H-benzo[b]thiophene]. Unusual Equilibrium between the Spiro and 3-Hydroxy-benzothiophene Systems.
PublicationStwierdzono, że 3'-hydroksy-4,4'-dimetoksy-3'-metylo-3-okso-7,7'-bis(piperydynokarbonyloksy)-2,2'-spirobi[2H,2'H,3H,3'H-benzo[b]tiofen] występuje w roztworach postaci mieszaniny dwóch diastereoizomerów pozostających w dynamicznej równowadze. Mechanizm tej równowagi oparty jest na odwracalnym otwarciu pierścienia z 1,5 przeniesieniem protonu i utworzeniu przjściowej formy 3-hydroksybenzotiofenu.
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Mine counter vehicles for Baltic navy. W: [CD-ROM] Conference proceedings. UDT EUROPE 2002. Undersea Defence Technology Conference and Exhibition. La Spezia, Italy, 18-20 June 2002. Classified Conference, La Spezia, Italy, 21 June 2002 [B.m.w.]**2002 [6 s. 3 rys.]. Pojazdy przeciwminowe dla marynarki dzialającej na Bałtyku.
PublicationW opracowaniu omówiono przeciwminowe systemy opracowane przez PolitechnikęGdańską dla potrzeb Marynarki Wojennej RP. Przedstawiono podstawowe wymaga-nia rozwiązań konstrukcyjnych i zasady użycia.
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Bezpośrednie inwestycje zagraniczne w Polsce według kryterium czynnika wytwórczego
PublicationW artykule przeanalizowana została struktura bezpośrednich inwestycji zagranicznych (BIZ) w Polsce zgodnie z kryterium czynnika wytwórczego. Okres badań obejmuje lata 1992-2002.
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I protagonisti della grande distribuzione in Europa
PublicationThe chapter outlines the main aspects of the history of some of the most important big European department stores (El Corte Ingles, Auchan, Carrefour, LeClerc, Aldi, Esselunga and the Finiper Group,
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Triplet–Triplet Annihilation Upconverting Liposomes: Mechanistic Insights into the Role of Membranes in Two-Dimensional TTA-UC
PublicationTriplet−triplet annihilation upconversion (TTA-UC) implemented in nanoparticle assemblies is of emerging interest in biomedical applications, including in drug delivery and imaging. As it is a bimolecular process, ensuring sufficient mobility of the sensitizer and annihilator to facilitate effective collision in the nanoparticle is key. Liposomes can provide the benefits of two-dimensional confinement and condensed concentration...
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Data governance: Organizing data for trustworthy Artificial Intelligence
PublicationThe rise of Big, Open and Linked Data (BOLD) enables Big Data Algorithmic Systems (BDAS) which are often based on machine learning, neural networks and other forms of Artificial Intelligence (AI). As such systems are increasingly requested to make decisions that are consequential to individuals, communities and society at large, their failures cannot be tolerated, and they are subject to stringent regulatory and ethical requirements....
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Validated GC–MS method for determination of bisphenol a and its five analogues in dietary and nutritional supplements
PublicationBisphenol A (BPA) and its analogues showing structural and functional similarity to BPA are commonly applied in various industrial applications and thus are becoming ubiquitous in the environment. At the same time there is increasing scientific evidence that exposure to these chemicals may lead to adverse health effects in human and wildlife. In recent years dietary and nutritional supplements dedicated for athletes have become...
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Performance Analysis of the "Intelligent" Kirchhoff- Law - Johnson-Noise Secure Key Exchange
PublicationThe Kirchhoff-law - Johnson-noise (KLJN) secure key distribution system provides a way of exchanging theoretically secure keys by measuring random voltage and current through the wire connecting two different resistors at Alice’s and Bob’s ends. Recently new advanced protocols for the KLJN method have been proposed with enhanced performance. In this paper, we analyze the KLJN system and compare with the „intelligent” KLJN (iKLJN)...
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Stimulated by cyclodextrins high yield synthesis of azocrown analogues comprising pyrrole or imidazole residues
PublicationThe influence of cyclodextrins (CDs) on the formation of azocrown ethers comprising pyrrole, imidazole and substituted imidazole has been studied. Pyrrole, imidazole, 2-methyl-, 4-methyl- and 4-phenylimidazole were coupled with bisdiazonium salts derived from bis-1,5-(2-aminophenoxy)-3-oxapentane or bis-1,8-(2-aminophenoxy)-3,6-dioxaoctane to form macrocyclic compounds with two azo units. The syntheses were performed under standard...
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Harmony Search for Self-configuration of Fault–Tolerant and Intelligent Grids
PublicationIn this paper, harmony search algorithms have been proposed to self-configuration of fault-tolerant grids for big data processing. Self-configuration of computer grids lies in the fact that new computer nodes are automatically configured by software agents and then integrated into the grid. A base node works due to several configuration parameters that define some aspects of data communications and energy power consumption. We...
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Problemy pomiarów mocy i energii w linii elektroenergetycznej Polska-Litwa
PublicationW referacie przedstawiono zagadnienia związane z pomiarem mocy i energii w linii dwutorowej. Rozważania oparto na linii łączącej stacje elektroenergetyczne Ełk Bis i Alytus.
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Power and energy measurement problems in transmission line between Poland-Lithuania
PublicationThe paper discusses problem of power and energy metering in double circuit overhead transmission line. Considerations are based on example of transmission line connecting Polish substation Bis Elk and Lithuanian substation Alytus.
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Współczesne projektowanie mostów
PublicationW artykule zaprezentowano historyczne i współczesne aspekty projektowania mostów. Uwagę zwrócono na wirtualne, architektoniczne i funkcjonalne modele, które aktualnie zintegrowane są w środowisku BIM.
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Diagnostyka toksoplazmozy u kobiety ciężarnej, płodu i noworodka — stan obecny i nowe możliwości
PublicationW artykule opisano problem toksoplazmozy, skutki oraz obecną diagnostykę. Przedstawiono metody serologiczne pozwalające wykryć pierwotne zarażenie T. gondii u kobiet ciężarnych oraz szereg technik pośrednich i bezpośrednich wykorzystywanych w celu potwierdzenia bądź wykluczenia toksoplazmozy wrodzonej u noworodka. Ponadto wskazano potencjalne możliwości w diagnostyce toksoplazmozy, jakie niosą za sobą nowe techniki (np. 2D Western-blotting),...
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Nonlinear waves in optical waveguides and soliton theory applications
PublicationRównania teorii solitonów zastosowano do propagacji impulsów światła w falo-wodach dielektrycznych.Wyprowadzono i zbadano rozwiazania równań oddziaływa-nia (z uwzględnieniem tłumienia) trzech fal Maxwella-Blocha.
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Liquefaction of alder wood as the source of renewable and sustainable polyols for preparation of polyurethane resins
PublicationLiquefaction of wood-based biomass gives different polyol properties depending on the reagents used. In this article, alder wood sawdust was liquefied with glycerol and poly(ethylene glycol) solvents. Liquefaction reactions were carried out at temperatures of 120, 150 and 170 °C. The obtained bio-polyols were analyzed in order to establish the process efficiency, hydroxyl number, acid value, viscosity and structural characteristics...
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A New Direct-Sequence Spread Spectrum Signal Detection Method for Underwater Acoustic Communications in Shallow-Water Channel
PublicationDirect-Sequence Spread Spectrum (DSSS) is one of the modulation and coding techniques used in Underwater Acoustic Communication (UAC) systems for reliable data transmision even at low signal levels. However, in a shallow water channel, there is a strong multipath propagation which causes a phase fluctuation of the received signal, affecting the performance of the spread-spectrum system. The article presents a differential method...
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Synteza, właściwości i zastosowanie liniowych polioli poliestrowych otrzymanych z wykorzystaniem surowców pochodzenia roślinnego
PublicationCelem rozprawy doktorskiej było opracowanie nowych liniowych polioli poliestrowych z wykorzystaniem surowców pochodzenia roślinnego, dedykowanych do syntez termoplastycznych elastomerów poliuretanowych. Przed przystąpieniem do prac eksperymentalnych wykonałam szczegółowy przegląd literatury, który stanowił aktualne spojrzenie na różne kierunki rozwoju bio-surowców w syntezie poliuretanów. Na podstawie analizy zebranych informacji...
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Problemy pracy zabezpieczeń odległościowych linii 400 kV w Polsce północno-wschodniej
PublicationPrzedstawiono analizę wpływu połączenia polskiego systemu elektroenergetycznego z systemem Litwy na detekcję zakłóceń przez zabezpieczenia odległościowe linii 400 kV znajdujących się w najbliższym otoczeniu stacji Ełk Bis.
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Projektowanie układów sterowania predykcyjnego obiektami z czasem ciągłym z uwzględnieniem niepewności modelowania.**2002, 166 s. 72 rys. 15 tab. bib- liogr. 79 poz. maszyn. Rozprawa doktorska /16.12.2002/ WETI PG. Promotor: dr hab. inż. Z. Kowalczuk, prof. nadzw. PG.
PublicationPrzedmiotem pracy jest uogólniony algorytm sterowania predykcyjnego w czasieciągłym CGPC, przeznaczony do sterowania obiektami ciągłymi o dowolnym cha-rakterze ze względu na stabilność i minmalnofazowość. Przedstawione jestkompletne wyprowadzenie przepisu na regulator, zaprezentowany jest sposóbstrojenia związany z mechanizmem predykcji i polegający na rozwinięciu po-czątkowego fragmentu odpowiedzi modelu obiektu w szereg...
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Structure and transport properties of proton-conducting BaSn 0.5 In 0.5 O 2.75 and A-site substituted Ba 0.9 Ln 0.1 Sn 0.5 In 0.5 O 2.8 (Ln = La, Gd) oxides
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TASK CLOUD INFRASTRUCTURE IN THE CENTRE OF INFORMATICS – TRICITY ACADEMIC SUPERCOMPUTER & NETWORK
PublicationThe cloud solution called the TASK cloud is described. Its main components and the way of their implementation are described. Examples of deployed environments based on the cloud are also presented. Moreover, the idea of combining the cloud and big data platforms is suggested and discussed.
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Studies on micellar aggregation of nonionic surfactants in imidazolium liquids
PublicationA number of imidazolium ionic liquids, with 2-8 carbon atoms in cation alkyl chains, and tetrafluoroborate, hexafluorophosphate, bis(trifluoromethylsulfony)imide and trifluoromethanesulfonate anions, were characterized for their ability to support micellar aggregation of nonionic surfactants in binary solutions.
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Assestment of the anti-cancer activity of the copper complexes with imidazole and pivalato ligands
PublicationDespite the development of science and technology progress so far there have not been found effective drugs for cancer. Many coordination compounds were investigated due to their antitumor potential. The most known cis-diamminedichloroplatinum(II) is used as anti-cancer therapeutic agent. The copper complexes are the coordination compounds possessing anti-tumour properties. Their capability to kill cancer cells is mainly linked...
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An improvement of body surface area formulas using the 3D scanning technique
PublicationObjectives: Body surface area (BSA) is one of the major parameters used in several medical fields. However, there are concerns raised about its usefulness, mostly due to the ambiguity of its estimation. Material and Methods: Authors have conducted a voluntary study to investigate BSA distribution and estimation in a group of 179 adult people of various sex, age, and physique. Here, there is provided an extended analysis of the...
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Linear and Nonlinear Optical Properties of Azobenzene Derivatives Modified with an (Amino)naphthalene Moiety
PublicationThe design of two-photon absorbing azobenzene (AB) derivatives has received much attention; however, the two-photon absorption (2PA) properties of bis-conjugated azobenzene systems are relatively less explored. Here, we present the synthesis of six azobenzene derivatives and three bisazobenzenes substituted (or not) at para position(s) with one or two amino group(s). Their linear and nonlinear absorption properties are studied...
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LC–MS/MS analysis, antioxidant and anticholinergic properties of galanga (Alpinia officinarum Hance) rhizomes
PublicationGalanga (Alpinia officinarum Hance) is a pungent and aromatic rhizome, which is a member of the ginger family (Zingiberaceae). The rhizomes of this plant have been used as a traditional medicine in far east countries for relieving stomach ache, invigorating the circulatory system, treating colds, and reducing swelling. The aim of this study was to investigate antioxidant and anticholinergic properties of galanga. For this purpose,...
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Synthesis, structure and properties of novel poly(hydroxyurethane)s obtained by non-isocyanate route
PublicationNon-isocyanate polyurethanes (NIPUs) can be synthesized by polyaddition of five-membered bis(cyclic carbonate)s and primary diamines. NIPUs are an alternative for the commonly used (in the form of foams, elastomers, coatings or fibers) in the industry polyurethanes obtained using toxic and moisture sensitive diisocyanates, polyols and low-molecular weight chain extenders. The main aim of this work was to synthesize non-isocyanate...
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Synthesis, physicochemical and theoretical studies on new rhodium and ruthenium dimers. Relationship between structure and cytotoxic activity
PublicationTwo dimeric compounds of the general formulae (Et3NH)2[Rh2(μ2-L)4Cl2] (1) (where L = thiophene-2-carboxylate) and [((η6-p-cymene)Ru)2(μ-Cl)3]PF6 (2) have been synthesized using a new method. The unique anionic complex 1 (space group P bca) has octahedral coordination in which the equatorial positions are occupied by the oxygen atoms of four thiophene-2-carboxylates in a paddle wheel fashion. In complex 2 (space group ), each Ru(II)...
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Investigating the potential of CuSCN as hole transport layer for perovskite solar cells for applications in indoor photovoltaics
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A new division of bacterial UvrA homologues
PublicationThe UvrA protein is a DNA-binding and damage-recognition enzyme which participates in the prokaryotic type nucleotide excision repair (NER) pathway. It has recently been noted that some bacterial genomes comprise additional uvrA genes which encode five distinct types of UvrA homologue. We investigated the sequences of over 2400 bacterial genomes and found 130 examples of bacteria containing uvrA 2 genes. The sequence analyses conducted...