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Search results for: ELASTIC MODULUS DETERMINATION
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Determination of Pesticide Residues in Honey using the GC×GC-TOFMS Technique
PublicationIn this study, a QuEChERS method and gas chromatography coupled with time-of-flight mass spectrometry (GCxGC-TOFMS) was developed for rapid extraction and simultaneous determination of 12 pesticide residues in honey. The GCxGC-TOFMS method was validated according to the SANCO guidance in terms of linearity, selectivity, reproducibility and recovery. Regarding the results, recovery rates ranged between 70-120% with relative standard...
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Determination of Mechanical Properties of P91 Steel by Means of Magnetic Barkhausen Emission
PublicationIn this work, an attempt at determination of mechanical properties by means of a method based on magnetic Barkhausen emission measurements was proposed. The specimens made of P91 steel were subjected to creep or plastic flow which were interrupted after a range of selected time periods in order to achieve specimens with an increasing level of strain. Subsequently, measurements of magnetic Barkhausen emission were carried out, and...
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Comparison of GC–MS and MEKC methods for caffeine determination in preworkout supplements
PublicationIn this study, GC–MS- and MEKC-based methods for determination of caffeine (CAF) in preworkout supplements were developed and validated. The proposed protocols utilized minimal sample preparation (simple dilution and syringe filtration). The developed methods achieved satisfactory validation parameters, i.e. good linearity (R2 0.9988 and R2 0.9985 for GC–MS- and MEKC-based method, respectively), satisfactory intraand interaccuracy...
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Monosaccharides as Potential Chiral Probes for the Determination of the Absolute Configuration of Secondary Alcohols
PublicationHerein, a new method for the elucidation of the absolute configuration of chiral secondary alcohols is proposed. This method is an alternative for a widely used approach reported by Mosher and Dale and similar methods that are based on the 1H NMR shift (δ) changes of protons that are attached to the substituents of the oxymethine carbon atom. The presented method is not based on tracking the chemical shift changes and utilizes...
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Mercury in Living Organisms: Sources and Forms of Occurrence, Bioaccumulation, and Determination Methods
PublicationMercury (Hg) is a heavy metal with well-known and broadly tested toxicity. Since Hg pollution and its impacts on human health are of global concern, it has become necessary to develop analytical methodologies that will provide tools to obtain reliable analytical information about the levels of Hg in samples, which very often have a complex matrix composition. This chapter summarizes key information on Hg and its chemical forms,...
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Multi-Decision Analysis for selection of the best procedure for PAHs determination in smoked food.
PublicationMaking a proper decision in multifacitated situation is very challenging task. Especially, if there are many alternatives and criteria, even contradictory ones. The support tools may be application of MultiCriteria Decision Analysis methods. In this study the application of PROMETHEE...
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The Current State-of-the-Art in the Determination of Pharmaceutical Residues in Environmental Matrices Using Hyphenated Techniques
PublicationSeveral thousand tons of pharmaceuticals and their transformation products (metabolites and degradation products) are introduced into the environment each year. They affect both human health and the environment, therefore, analytical procedures enabling the determination of a wide range of pharmaceuticals at trace levelswithminimal effort, time, and energy are required. Nowadays, hyphenated techniques are commonly applied in pharmaceutical...
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Determination of Local Dye Concentration in Hybrid Porous Silica Thin Films
PublicationThe idea of determination of local dye concentration in a nanoporous matrix is proposed based on donor − acceptor energy transfer. The method was tested for a Rhodamine 110 − Rhodamine 101 system in silica and methylated silica nanolayers. Evaluation of acceptor (Rhodamine 101) local concentration was carried out by comparing the results of Monte Carlo simulation of energy transfer from donor (Rhodamine 110) to acceptor (Rhodamine...
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Determination of Metals Content in Wine Samples by Inductively Coupled Plasma-Mass Spectrometry
PublicationKnowledge about the metal content of wine is very important, for many reasons. Depending on the element, its quantity varies in wine from ng/L to mg/L. Despite the fact that metals are not directly connected to the taste and aroma of the wine, their content should be determined and controlled, because excess is undesirable, and in some cases prohibited, due to potential toxicity. Several analytical procedures for metal determination...
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Elastic and inelastic multi-storey buildings under earthquake excitation with the effect of pounding
PublicationW artykule przeprowadzono analizę różnic w liniowym i nieliniowym zachowaniu się budynków wielokondygnacyjnych podczas trzęsień ziemi z uwzględnieniem efektu zderzeń pomiędzy nimi. Analizę numeryczną przeprowadzono dla różnych wartości ekstremalnych przyspieszeń gruntu. Wyniki pokazują, iż zaimplementowanie nieliniowego modelu zachowania się budowli jest bardzo istotne w celu uzyskania dokładnej odpowiedzi konstrukcji.
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Elastic electron scattering in krypton in the energy range from 5 to 10 eV
PublicationZmierzono różniczkowe przekroje czynne na rozproszenie sprężyste elektronów w kryptonie dla energii elektronów 5, 7.5 oraz 10 eV, w zakresie kątów rozproszenia od 30 do 180 stopni. Pomiary w zakresie dużych kątów rozproszenia wykonano wykorzystując metodę lokalnego pola magnetycznego.
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Measurements of absolute elastic and vibrational cross sections for electron scattering from tetrahydrofuran
PublicationPrzedstawiono wstępne wyniki pomiaru absolutnych przekrojów czynnych na zderzenie elektronów z drobinami tetrahydrofuranu przy energii 10eV.
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Elastic-plastic properties of metal matrix composites: Validation of mean-field approaches
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Cross section calculations for electron impact ionization and elastic scattering from cisplatin
PublicationCałkowity przekrój czynny na jednokrotną jonizację cisplatyny (H6N2Cl2Pt) w zderzeniach z elektronami został obliczony przy wykorzystaniu modelu BEB (binary-encounter-Bethe) dla energii zderzenia od progu na jonizację do 5 keV. W celu uzyskania danych niezbędnych w modelu BEB, geometryczna i elektronowa struktura cisplatyny została przebadana metodami chemii kwantowej. Obliczono również przekrój czynny na sprężyste rozproszenie...
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Baseline-free debonding detection in reinforced concrete structures by elastic wave propagation
PublicationThe article presents the results of the numerical and experimental analysis concerning wave propagation in reinforced concrete (RC) beams with various extent of debonding between the steel rod and concrete cover. The main aim of the paper was to consider the unsolved research gaps, which considerably limit the application of wave-based methods in practice. The propagation of the flexural wave modes excited and registered on the...
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Relationsship between magnetoriction and the magnetostrictive coupling coefficient for magnetostrctive generation of elastic waves
PublicationPrzedstawiono wyniki doświadczenia z wpływem natężenia stałego pola magnety-cznego na wielkość impulsów magnetostrykcyjnych w rurze stali niskowęglowej.fala akustyczna rejestrowana była także za pomocą układu do emisji akusty-cznej. Wykazano, iż występuje minimum amplitudy impulsów magnetostrykcyjnychoraz emisji akustycznej dla natężenia pola, przy którym magnetostrykcjaosiąga wartość ekstremalną. Wyniki zapisano za pomocą...
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Analysis of non-linear elastic material properties of PVC-coated Panama fabric.
PublicationW pracy omówiono proces identyfikacji parametrów materiałowych dla wybranej tkaniny technicznej typu Panama. Zaproponowano metodę identyfikacji nieliniowo sprężystych właściwości tkaniny Panama. Określono zakres stosowalności nieliniowo sprężystych parametrów, w oparciu o doraźną wytrzymałości tkaniny na rozciąganie (UTS), która poddana redukcji określa tzw. wytrzymałość długoterminową (LTS). Opisano doświadczenia niezbędne do...
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Determination of vertical displacements by using the hydrostatic levelling systems with the variable location of the reference sensor,
PublicationAbstract: In this paper, the author proposed a new method for determination of vertical displacements with the use of hydrostatic levelling systems. The traditional method of hydrostatic levelling uses a rule in which a position of reference sensor is stable. This assumption was not adapted in the proposed method. Regarding the issue mentioned above, the reference sensor is treated in the same way as the others sensors that measure...
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Determination of chlorine concentration using single temperature modulated semiconductor gas sensor
PublicationA periodic temperature modulation using sinusoidal heater voltage was applied to a commercial SnO2 semiconductor gas sensor. Resulting resistance response of the sensor was analyzed using a feature extraction method based on Fast Fourier Transformation (FFT). The amplitudes of the higher harmonics of the FFT from the dynamic nonlinear responses of measured gas were further utilized as an input for Artificial Neural...
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The use of selected analytical techniques for pollutants determination in the environmental samples collected from the Arctic regions
PublicationThe paper concern importance of the use of analytical techniques for pollutants determination in the Arctic based on the example of total organic carbon, phenolsandformaldehyde determinationandmeasurementofpHand electrical conductivity parameters in surfacewater samples collected fromthe Revelva catchment.
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Green sample preparation techniques for chromatographic determination of small organic compounds
PublicationAccurate monitoring of the state of the environment requires the introduction of additional isolation and/or preconcentration step prior to the chromatographic determination. In this work the information about novel methodological and instrumental solutions in relation to different variants of microextraction techniques are presented. Attention is focused on analytical procedure and suitable analytical tools for extraction of the...
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Oznaczanie tlenu – od metody Winklera do czujników enzymatycznych (Determination of oxygen – from Winkler Method to enzymatic sensor)
PublicationMonitoring of dioxygen levels is of utmost importance from the view-point of life processes, medical diagnostics, nutrition and chemical industries. In all these measurements both low and high levels of this element are important. The common methods for the determination of dioxygen are the Winkler method, Clark electrode and pulsoxymeters. A new, already strong field of research can be now recognized – the development of miniaturized...
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Green, simple analytical method for total biogenic amines content determination in wine using spectrophotometry
PublicationA simple, green and equitable procedure for total biogenic amines (BAs) content determination was developed. The scientific novelty lies in the use of commercially available S 0378 dye, the reaction of which with BAs results in a colour change of the solution. Sample preparation and analysis were simplified to make the method suitable for routine analyses even in resource-scarce settings. The optimization of the method was carried...
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Non-linear static stability of bi-layer carbon nanosheets resting on an elastic matrix under various types of in-plane shearing loads in thermo-elasticity using nonlocal continuum
PublicationIn this research, the shear and thermal buckling of bi-layer rectangular orthotropic carbon nanosheets embedded on an elastic matrix using the nonlocal elasticity theory and non-linear strains of Von-Karman was studied. The bi-layer carbon sheets were modeled as a double-layered plate, and van der Waals forces between layers were considered. The governing equations and boundary conditions were obtained using the first order shear...
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Comparison of High Performance Liquid Chromatography Methods with Different Detectors for Determination of Steroid Hormones in Aqueous Matrices
PublicationThis paper presents the development and comparison of procedures for the qualitative and quantitative determination of five estrogenic compounds (17-a-ethynylestradiol, estrone, estradiol, estriol, and progesterone) in drinking water and wastewater samples. Five extraction columns and two disks were tested for their efficiency. The C18 columns were superior on the basis of cost for solid phase extraction of drinking water or sewage....
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Troubleshooting of the determination of bisphenol A at ultra-trace levels by liquid chromatography and tandem mass spectrometry
PublicationDetermination of trace amounts of bisphenol A (BPA) may cause problems mainly related to the presence of BPA in solvents (even in LC-MS grade), laboratory vessels, and plastic equipment used for sample preparation. Variable and sometimes significant amounts of BPA present in the background cause problems in obtaining good repeatability of measurements at the ultra-trace levels. Such observations (i.e., poor repeatability of results)...
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Determination of 3,4-methylenedioxy-α-pyrrolidinobutiophenone (MDPB) in blood. A case report
PublicationSynthetic drugs, known as ‘‘legal highs’’, are still very popular on black market. The determination of their composition are required in courts of law and also to understand what potential users may be subjected to. The interest of new cathinones, e.g. MDPBP, is in view of psychoactive effects that they cause and that, in many cases, they are not controlled by law. The case outlined here concerns 19 years-old man, who was found...
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Joint experimental and theoretical study on low-energy elastic electron scattering by gaseous alkynes: Differential cross sections, shape resonances, and methylation effects
PublicationA detailed comparison of experimental and theoretical elastic cross sections for low-energy electron scattering by ethyne, taken earlier in our group by Gauf et al. [Phys. Rev. A 87, 012710 (2013)], and some of its methylated derivatives, propyne, and the isomers 1-butyne and 2-butyne, taken here, are presented. The present differential cross sections were measured at incident electron energies ranging from 1 eV to 30 eV and...
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Determination of the minimal critical rotational speeds of the circular saw blades with the quasi-twin resonant frequencies
PublicationTo determine the minimal critical rotational speeds of the circular saw blades is the fundamental aspect of obtaining the range of the rotational operating speeds, by which the circular saw blade can work with required stability. While for the circular saw blades with full-homogeneous bodies the determination of such rotational speeds is the relatively low level of difficulty function, whereas for circular saw blades with more...
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Reference-free determination of debonding length in reinforced concrete beams using guided wave propagation
PublicationThis paper presents theoretical and experimental investigations of guided wave propagation in reinforced concrete beams, with pre-existing debonding between steel rebars and concrete blocks, for the purpose of damage detection. The primary aim of these investigations was a detailed analysis of the possible applications of wave propagation in single and multiple debonding detection in reinforced concrete structures and reference-free...
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Sample preparation procedure for the determination of polycyclic aromatic hydrocarbons in petroleum vacuum residue and bitumen
PublicationThis paper describes a novel method of samplepreparation for the determination of trace concentrations ofpolycyclic aromatic hydrocarbons (PAHs) in high-boilingpetroleum products. Limits of quantitation of the investigatedPAHs in materials of this type range from tens ofnanograms per kilogram to <20 μg/kg. The studies revealedthat in order to separate most of interferences from theanalytes without a significant loss of PAHs, it...
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Determination of Formaldehyde and Cyanide Ion in Human Nasal Discharge by Using Simple Spectrophotometric Methods
PublicationEnvironmental tobacco smoke (ETS) contains many toxic compounds which include substances classified as aldehydes (e.g. formaldehyde) and inorganic substances such as cyanide ions. The information on the determination of these compounds in water is available, but the monitoring data on the level of these substances in human body fluids are still lacking. In this work the procedure for determining cyanide ions and formaldehyde in...
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Detection, identification and determination of chiral pharmaceutical residues in wastewater: Problems and challenges
PublicationChiral pharmaceuticals (CPs) are widely used in different areas of human life, thus they are frequentlydetected in different ecosystems. However, before CPs reach the environment, wastewater is subjected todifferent treatment processes in order to remove them. Nevertheless, such processes may affect thechirality of CPs, thus it is very important to monitor CP levels during the wastewater treatment.This review addresses the present...
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Simultaneous grouping and ranking with combination of SOM and TOPSIS for selection of preferable analytical procedure for furan determination in food
PublicationNovel methodology for grouping and ranking with application of self-organizing maps and multicriteria decision analysis is presented. The dataset consists of 22 objects that are analytical procedures applied to furan determination in food samples. They are described by 10 variables, referred to their analytical performance, environmental and economic aspects. Multivariate statistics analysis allows to limit the amount of input...
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Determination of molybdenum in biological materials
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Determination of Elements in Fruit Juices
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Tyre dynamic radius determination
PublicationW artykule opisano stanowisko wykorzystywane do badania oporu toczenia opon samochodowych znajdujące się w Katedrze Konstrukcji Maszyn i Pojazdów Wydziału Mechanicznego Politechniki Gdańskiej. Przedstawiono wyniki badań promienia dynamicznego opony Michelin 165/80R13 83T z bieżnikiem CLASSIC przeprowadzone z wykorzystaniem tego stanowiska na nawierzchni Safety Walk 80. Badania przeprowadzono zmieniając: prędkość jazdy, obciążenie...
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Determination of tributyltin in marine sediment.
PublicationPrzedstawiono wyniki badań międzynarodowego porównawczego, międzylaboratoryjnego oznaczania zawartości tributylocyny w osadzie morskim. Badania były organizowane przez Comite Consultatif pour la Quantite de Matiere (CCQM) pilot study P-18 international intercomparison i była to ich pierwsza część - badania pilotażowe. W badaniach uczestniczyło 11 laboratoriów. Uzyskano zadowalająco zgodne wyniki oznaczeń tributylocyny.
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Determination of p-y curves for offshore piles based on in-situ soil investigations
PublicationOffshore piles are subjected to complex loads with considerable lateral component. The pile-soil response to lateral loads can be described with the p-y method. For a given depth the load–deflection relationship is built to simulate the surrounding soil stiffness. This state-of-art paper presents a brief discussion of determination methods for the p-y curves using a standard approach based on the soil parameters derived from laboratory...
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Methodology for determination of the selected mechanical properties of wood based on cutting tests
PublicationFrom kiln-dried spruce wood (with steam) as well as in natural conditions were randomly selected 8 samples. After determining the average dimensions, moisture content and density of the samples they have been cut on the frame sawing machine PRW15M for measurement of cutting power. Based on those results from a linear rela-tionship of cutting power versus feed per toot mechanical properties of wood such as facture toughness and...
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Ionic liquids in extraction techniques: Determination of pesticides in food and environmental samples
PublicationThe intensive use of pesticides in agricultural practices has promoted the appearance of environmentaland public health problems. Due to that, scientists face challenges with developing simple, fast, sensitive,selective, and low-cost methods dedicated to determining pesticide residues in food and environmentalsamples. Following thefifth principle of Green Analytical Chemistry, chemists are searching for greeneralternatives for...
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Determination of the Bending Properties of Wire Rope Used in Cable Barrier Systems
PublicationThis paper presents research on the bending properties of 3 × 7 19-mm wire rope commonly used in road cable barriers. A total of 19 experimental tests were conducted. In addition, two nonlinear 3D numerical models of the wire rope using beam and solid finite elements were developed. Based on these models, four numerical simulations were carried out. The numerical results were validated against the experimental ones and a very good...
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Determination of the refractive index and wavelength‐dependent optical properties of few‐layer CrCl3 within the Fresnel formalism
PublicationBased on previous reports on the optical microscopy contrast of mechanically exfoliated few layer CrCl3 transferred on 285 nmand 270 nmSiO2 on Si(100), we focus on the experimental determination of an effective mean complex refractive index via a fitting analysis based on the Fresnel equations formalism. Accordingly, the layer and wavelength-dependent absorbance and reflectance are calculated. Layer and wavelength-dependent optical...
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Amygdalin: Toxicity, Anticancer Activity and Analytical Procedures for Its Determination in Plant Seeds
PublicationAmygdalin (D-Mandelonitrile 6-O--D-glucosido--D-glucoside) is a natural cyanogenic glycoside occurring in the seeds of some edible plants, such as bitter almonds and peaches. It is a medically interesting but controversial compound as it has anticancer activity on one hand and can be toxic via enzymatic degradation and production of hydrogen cyanide on the other hand. Despite numerous contributions on cancer cell lines, the clinical...
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Determination of SCFAs in water using GC-FID. Selection of the separation system
PublicationIn the present study, an analytical procedure was developed for the determination of short-chain fatty acids (SCFAs) in landfill leachate and municipal wastewater employing injection of aqueous samples to gas chromatograph with flame ionization detector (GC-FID). Chromatographic conditions such as a separation system, injection volume, oven temperature program were investigated and selected. With two columns, one with a polar (polyethylene...
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Application of TOPSIS for Selection and Assessment of Analytical Procedures for Ibuprofen Determination in Wastewater
PublicationThis paper describes the possible implementation of the Technique for Order Preference by Similarity to Ideal Solution (TOPSIS) as green analytical chemistry metrics tools. TOPSIS is one of the multi-criteria decision analysis (MCDA) tools that is applied in the selection of the best alternative from many possible. In this case we have applied it to assess the nineteen analytical procedures for ibuprofen determination in wastewater...
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Determination of moisture resistance of covered electrodes according to PN-EN ISO 14372
PublicationMoisture present in the electrode covering is one of the sources of diffusible hydrogen in welded joints. In order to study the diffusible hydrogen content in deposited metal, a stand for moisturizing covered electrodes, in accordance with the PN-EN ISO 14372 standard, was built. After the stand was completed, a test of moisturizing the electrodes was carried out and measurements of the diffusible hydrogen content in deposited...
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DETERMINATION OF SP3 FRACTION IN ta-C COATING USING XPS AND RAMAN SPECTROSCOPY
PublicationThe paper presents results of studies on the structure of tetrahedral amorphous carbon films (ta-C) with a thickness in the range from 20 to 280 nm, deposited using pulsed vacuum arc technique with an electromagnetic Venetian blind plasma filter. The results of the phase structure analysis, obtained using visible Raman spectroscopy and UV Raman spectroscopy methods, showed a strong dependence of the results on the presence, on...
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Comparison of Two Methods for the Determination of Selected Pesticides in Honey and Honeybee Samples
PublicationDeveloped and validated analytical methods for the determination of a wide spectrum of pesticide residues in honey and honeybee samples after the modification of QuEChERS extraction in combination with gas chromatography–tandem quadrupole mass spectrometry (GC-MS/MS) and liquid chromatography–tandem quadrupole mass spectrometry (LC-MS/MS) were discussed and compared. The developed methods were evaluated regarding the utilized equipment...
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Damage tests of the single shell ship fuel tank with additional elastic protective coating
PublicationWejście na mieliznę lub kolizja średniej wielkości np. kontenerowca może doprowadzić do zanieczyszczenia środowiska Morza Bałtyckiego paliwem uwolnionym z rozszczelnionych, jednoposzyciowych zbiorników dennych, a ilość tego paliwa może być znaczna. W związku z tym podjęto prace badawcze zmierzające do opracowania sposobu obniżenia ryzyka rozlewu paliwa w wypadku kolizji poprzez wprowadzenie drugiej bariery ochronnej. Idea pomysłu...