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Wyniki wyszukiwania dla: BPA ANALOGUES
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Lignin-based carbon fibers for renewable and multifunctional lithium-ion battery electrodes
PublikacjaLignin-based carbon fibers (LCFs) from the renewable resource softwood kraft lignin were synthesized via oxidative thermostabilization of pure melt-spun lignin and carbonization at different temperatures from 1000°C to 1700°C. The resulting LCFs were characterized by tensile testing, scanning electron microscopy (SEM), X-ray diffraction (XRD) and confocal Raman spectroscopy. The microstructure is mainly amorphous carbon with some...
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Dual-Setting Bone Cement Based On Magnesium Phosphate Modified with Glycol Methacrylate Designed for Biomedical Applications
PublikacjaMagnesium phosphate cement (MPC) is a suitable alternative for the currently used calcium phosphates, owing to beneficial properties like favorable resorption rate, fast hardening, and higher compressive strength. However, due to insufficient mechanical properties and high brittleness, further improvement is still expected. In this paper, we reported the preparation of a novel type of dual-setting cement based on MPC with poly(2-hydroxyethyl...
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Optimization of Hydrogen - Evolving Photochemical Molecular Devices
PublikacjaA molecular photocatalyst consisting of a RuII photocenter, a tetrapyridophenazine bridging ligand, and a PtX2 (X=Cl or I) moiety as the catalytic center functions as a stable system for light-driven hydrogen production. The catalytic activity of this photochemical molecular device (PMD) is significantly enhanced by exchanging the terminal chlorides at the Pt center for iodide ligands. Ultrafast transient absorption spectroscopy...
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The synthesis and structure of a potential immunosuppressant: N-mycophenoyl malonic acid dimethyl ester
PublikacjaThe synthesis of a potential immunosuppressant, i.e. dimethyl ester of N-mycophenoyl malonic acid was optimized in the reaction of mycophenolic acid (MPA) with amino malonic dimethyl ester in the presence of propanephosphonic anhydride (T3P) as a coupling reagent. The structural properties of the obtained MPA derivative were investigated by NMR, MS and single crystal X-ray diffraction methods. Theoretical considerations of conformational...
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Influence of the boron doping level on the electrochemical oxidation of raw landfill leachates: advanced pre-treatment prior to the biological nitrogen removal
PublikacjaThe electrochemical oxidative treatment of landfill leachates (LLs) containing high amounts of ammonia nitrogen and organic matter was used as a promising method, prior to biological processes, to achieve the final effluent quality that would be acceptable by current regulations. The deposited boron-doped diamond electrodes (BDDs) with different boron doping concentrations (10000, 5000 and 500 ppm of B) were applied as anodes....
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Application of vibrational spectroscopy, thermal analyses and X-Ray diffraction in the rapid evaluation of the stability in solid-state of ranitidine, famotidine and cimetidine
PublikacjaThis paper reports the study on applicability of Fourier transform infrared (FTIR), near-infrared (NIR) and Raman spectroscopy, differential scanning calorimetry (DSC) and X-ray diffraction (XRD) for the estimation of the chemical stability and photostability of histamine H2-receptor antagonist substances. Ranitidine hydrochloride (RAN), famotidine (FAM) and cimetidine (CIM) were tested and differences in sensitivity were measured...
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Decision-Making Models of the Human-Operator as an Element of the Socio-Technical Systems
PublikacjaThe authors of the chapter proved that the fundamental intellectual processes, which lie on the basis of decision-making behavior of the human-operator, could be identified on the bases on the analogies with the devices (elements). The basic intellectual processes of the Rational decision-making models can be adequately identified by the transient processes of the PID-controller; the intellectual processes of the Bounded Rationality...
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Computing methods for fast and precise body surface area estimation of selected body parts
PublikacjaCurrently used body surface area (BSA) formulas give satisfactory results only for individuals with typical physique, while for elderly, obese or anorectic people accurate results cannot be expected. Particularly noteworthy are the results for individuals with severe obesity (body-mass index greater than 35 kg/m2), for which BSA estimation errors reached 80%. The main goal of our study is the development of precise BSA models for...
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A procedure for the identification of effective mechanical parameters of additively manufactured elements using integrated ultrasonic bulk and guided waves
PublikacjaThe subject of the current work was a simple but robust novel two-stage procedure for the non-destructive determination of effective elastic constants using ultrasonic wave propagation. First, ultrasonic bulk wave velocities measured on cubic samples were used to calculate most of the elements of the stiffness matrix. Secondly, the remaining elements were determined using the dispersion curves of elastic guided waves measured on...
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New conjugates of mycophenolic acid and their antiproliferative activity
PublikacjaThe new conjugates of mycophenolic acid (MPA) were obtained in the reaction of N6-(ω-aminoalkyl)adenosines with MPA in the presence of EDCI as a coupling reagent. New compounds 4a–h were evaluated on leukemia cell line (Jurkat) and PBMC from healthy donors. Length of the linker influenced observed activity. The compound 4b possessing 1,3-diamine spacer exhibited the most promising results and can be considered to further investigations.
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Acoustic Processor of the Mine Countermeasure Sonar
PublikacjaThis paper presents the concept of an acoustic processor of the mine countermeasure sonar. Developed at the Department of Marine Electronics Systems, Gdansk University of Technology, the acoustic processor is an element of the MG-89, an underwater acoustic station. The focus of the article is on the modules of the processor. They are responsible for sampling analogue signals and implementing the algorithms controlling the measurement...
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Molecular Umbrella as A Nanocarrier for Antifungals
PublikacjaA molecular umbrella composed of two O‐sulfated cholic acid residues was applied for the construction of conjugates with cispentacin, containing a “trimethyl lock” (TML) or o‐dithiobenzylcarbamoyl moiety as a cleavable linker. Three out of five conjugates demonstrated antifungal in vitro activity against C. albicans and C. glabrata but not against C. krusei, with MIC90 values in the 0.22–0.99 mM range and were not hemolytic. Antifungal...
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RuAl6—An Endohedral Aluminide Superconductor
PublikacjaSuperconductivity is reported in an endohedral aluminide compound, RuAl6, with Tc = 1.21 K. The normalized heat capacity jump at Tc, ΔC/γTc = 1.58, confirms bulk superconductivity. The Ginzburg–Landau parameter of κ = 9.5 shows that RuAl6 is a type-II superconductor. Electronic structure calculations for RuAl6 are explored in comparison to its structural analogue ReAl6 (Tc = 0.74 K). The stability of the phases is discussed in...
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Ocena sprężysto-plastycznych parametrów współpracy georusztu i gruntu w ba-daniu na wyciąganie.**2002, 196 s. 128 rys. 19 tab. bibliogr. 118 + 5 zał. Rozprawa doktorska /24.05.2002/ Wydz. Bud. Wod. Inż. Środ. Promotor: dr hab. inż. Adam Bolt.
Publikacja.
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Influence of Giant Reed (Arundo Donax L.) Culms Processing Procedure on Physicochemical, Rheological, and Thermomechanical Properties of Polyethylene Composites
PublikacjaGiant reed (Arundo donax L.) is a plant species with a high growth rate and low requirements, which makes it particularly interesting for the production of different bioproducts, including natural fibers. This work assesses the use of fibers obtained from reed culms as reinforcement for a high-density polyethylene (HDPE) matrix. Two different lignocellulosic materials were used: i) shredded culms and ii) fibers obtained by culms...
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Ordered TiO2 nanotubes with improved photoactivity through self-organizing anodization with the addition of an ionic liquid: effects of the preparation conditions
PublikacjaModifying the geometric and surface parameters of oriented TiO2 nanotubes (NTs) is beneficial to the utilization of solar energy for chemical reactions, and this performance may be further improved. Thus, the effects of adding an ionic liquid (IL), 1-butylpiridinium chloride [BPy][Cl], and the effects of the water content and preparation conditions on the surface morphological, physicochemical, photocatalytic and photoelectrochemical...
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Analiza dokładności formuł do wyznaczania powierzchni ciała człowieka
PublikacjaPowierzchnia ciała człowieka (body surface area, BSA) jest wskaźnikiem o szerokim spektrum zastosowań w lecznictwie medycznym (m.in. w chemioterapii, transplantologii oraz toksykologii). Każdy z istniejących wzorów do wyznaczania wartości BSA charakteryzuje się pewnym (lepszym bądź gorszym) współczynnikiem zgodności pomiędzy wartością obliczoną, a wartością dokładną – uzyskaną na podstawie pomiaru skanerem 3D. Współczynnik ten...
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Aplikacja wspomagająca procesy obliczania powierzchni ciała człowieka
PublikacjaW materiale przedstawiono strukturę opracowanego i wykonanego systemu komputerowego - BSA Analysis Tool, wspomagającego obliczenia wybranych parametrów organizmu człowieka: BSA, TBSA i BMI. Poza opisem systemu, wskazano na utylitarny charakter przedstawionych rozwiązań, szczególnie w ośrodkach medycznych - jako narzędzie wspomagające procesy leczenia oparzeń i chemioterapii oraz w ośrodkach naukowo-dydaktycznych - jako narzędzie...
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Solid Phase Synthesis and Biological Activity of Tuftsin Conjugates
PublikacjaNew tuftsin/retro-tuftsin conjugates were designed and synthesized using a classical fluorenylmethoxycarbonyl (Fmoc) solid phase procedure. All the peptide conjugates were divided into three series: 1,4-dihydroxyanthraquinone (type A), 1-nitroacridine (type B), and 4-carboxyacridone (type C) derivatives. In type A conjugates, the N-terminal group of the peptide chain is directly connected to the anthraquinone ring at C1 (Scheme...
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The interplay between Disinhibition and Present-Hedonistic time perspective in the relation between Borderline Personality Organization and depressive symptoms
PublikacjaThe purpose of the current study was to examine the moderating effect between borderline personality organization (BPO) and depressive symptoms of factors associated with impulsive behavior – Present-Hedonistic time perspective and Disinhibition. The research sample consisted of 720 adults from Poland (518 females), who participated in a survey through the research panel. In the case of low levels of Disinhibition, the positive...
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Quasistatic and fatigue behavior of an AISI H13 steel obtained by additive manufacturing and conventional method
PublikacjaThis work aims to compare the mechanical behavior of an AISI H13 steel obtained by additive manufacturing with that obtained by conventional manufacturing methods. The average values of the ultimate tensile strength (UTS) and ductility obtained for the specimens produced by the conventional method were equal to 658 MPa and 18%, respectively, which compares with 503 MPa and 0.75% registered for the selective laser melting (SLM)...
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Empirical Analysis of Forest Penalizing Attribute and Its Enhanced Variations for Android Malware Detection
PublikacjaAs a result of the rapid advancement of mobile and internet technology, a plethora of new mobile security risks has recently emerged. Many techniques have been developed to address the risks associated with Android malware. The most extensively used method for identifying Android malware is signature-based detection. The drawback of this method, however, is that it is unable to detect unknown malware. As a consequence of this problem,...
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Integrating Statistical and Machine‐Learning Approach for Meta‐Analysis of Bisphenol A‐Exposure Datasets Reveals Effects on Mouse Gene Expression within Pathways of Apoptosis and Cell Survival
PublikacjaBisphenols are important environmental pollutants that are extensively studied due to different detrimental effects, while the molecular mechanisms behind these effects are less well understood. Like other environmental pollutants, bisphenols are being tested in various experimental models, creating large expression datasets found in open access storage. The meta‐analysis of such datasets is, however, very complicated for various...
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Texture or Linker? Competitive Patterning of Receptor Assembly toward Ultra-Sensitive Impedimetric Detection of Viral Species at Gold-Nanotextured Titanium Surfaces
PublikacjaIn this work, we study the electrodes with a periodic matrix of gold particles pattered by titanium dimples and modified by 3-mercaptopropionic acid (MPA) followed by CD147 receptor grafting for specific impedimetric detection of SARS-CoV-2 viral spike proteins. The synergistic DFT and MM/MD modeling revealed that MPA adsorption geometries on the Au–Ti surface have preferential and stronger binding patterns through the carboxyl...
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The field–dependent interface recombination velocity for organic–inorganic heterojunction
PublikacjaWe have derived an analytical formula which describes the field–dependent interface recombination velocity for the boundary of two materials characterized by different permittivities. The interface recombination of charge carriers has been considered in the presence of image force Schottky barrier. We suggest that this effect may play an important role in the loss of current for organic–inorganic hybrid heterojunctions. It has...
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Novel 5.1 Downmix Algorithm with Improved Dialogue Intelligibility
PublikacjaA new algorithm for 5.1 to stereo downmix is introduced, which addresses the problem of dialogue intelligibility. The algorithm utilizes proposed signal processing algorithms to enhance the intelligibility of movie dialogues, especially in difficult listening conditions or in compromised speaker setup. To account for the latter, a playback configuration utilizing a portable device, i.e. an ultrabook, is examined. The experiments...
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Application of 3D Whole Body Scanning in Research on Human Body Surface Area
PublikacjaHuman body surface area (BSA) is one of the major parameters used in several medical fields. Its heterogeneity caused by individual human characteristics sustains a many-decades-long research on the matter. Today’s technology allows to create exact body models in mere seconds. However, an extensive research that includes scanning people with major disfigurements or people suffering from diseases, which often prevent their mobility,...
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Modelowanie losowych imperfekcji geometrycznych przestrzennych konstrukcji metalowych
PublikacjaImperfekcje geometryczne zbiorników, silosów i powłok siatkowych mogą znaczą-co wpłynąć na ich nośność, a więc powinny być one uwzględniane w obliczeniach komputerowych i w procesie projektowania. Wykazano, że przy podstawowych obcią-żeniach, działających na tego typu konstrukcje, tj. podciśnieniu oraz naporu wiatru i śniegu (w przypadku powłok siatkowych), wykazują wyraźne różnice w porównaniu z analogicznymi wynikami dla tych...
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Highly-Miniaturized Dual-Mode Bandpass Filter Based on Quarter-Mode Substrate Integrated Waveguide with Wide Stopband
PublikacjaThis paper presents a novel design of a highly-miniaturized dual-mode bandpass filter (BPF) employing a quarter-mode substrate integrated waveguide (QMSIW). The QMSIW resonator is based on a square cavity with metallic vias along two sides, and open-ended edges at the remaining sides that contain orthogonal feed lines. An open slot is introduced along the two sides of the square cavity with metallic vias to form a magnetic wall....
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Możliwość wykorzystania popiołów z osadów ściekowych w betonie
PublikacjaIlość popiołów lotnych ze spalania osadów ściekowych rośnie na całym świecie. Ich unieszkodliwianie jest poważnym problemem ekologicznym. W pracy przedstawiono ocenę możliwości wykorzystania popiołów lotnych z osadów ściekowych w betonie. Wykonano dwie serie badawcze dla dwóch współczynników (w/s) równych 0,49 oraz 0,55 z udziałem 10% i 20% popiołu lotnego (SSA), jako zamiennika cementu. Skład chemiczny wykazał, że popiół (SSA)...
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Problemy planowania strategii i zagospodarowania przestrzennego w zarządzaniu rozwojem obszarów metropolitalnych
PublikacjaCelem pracy jest rozpoznanie i usystematyzowanie problemów związanych z planowaniem kompleksowej strategii zarządzania rozwojem obszarów metropolitalnych i sporządzaniem planu zagospodarowania przestrzennego tych obszarów. Problemy planowania rozumiane są jako trudności, dylematy i wątpliwości związane z różnymi aspektami procesu planistycznego. Autor nawiązuje do cech obszarów metropolitalnych oraz typowych problemów rozwiązywanych...
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Wysokociśnieniowe uszczelnienia ruchu obrotowego wału hydraulicznych maszyn wyporowych
PublikacjaW artykule przedstawiono wyniki badań mające na celu wytypowanie węzła uszczelniającego wał silnika hydraulicznego zapewniającego najwyższą trwałość przy smarowaniu wodą. Parametry pracy: ciśnienie 2 MPa i minimalna prędkość poślizgu uszczelek 2 m/s. Opisano również nowatorski przyrząd, na którym przeprowadzono pomiary wszystkich parametrów węzła uszczelniającego.
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Flavones in cocoa defence against Phytophthora megakarya
PublikacjaCross-pollination of suitable genotypes and earlier selection of elite offspring using adequate plants-associated defence markers in plantlets leaves are decisive for development of T. cacao genotypes tolerant to black pods disease (BPD). T. cacao plantlets from manual cross-pollination of ♀SNK64 × ♂UPA143 were analyzed for their susceptibility to BPD using leaf disc test. Subsequently, leaves (healthy, wounded and wound+infected)...
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Acoustic Processor of the MCM Sonar
PublikacjaThis paper presents the concept of an acoustic processor of the mine countermeasure sonar. Developed at the Department of Marine Electronics Systems, Gdansk University of Technology, the acoustic processor is an element of the MG-89, a modernised underwater acoustic station. The focus of the article is on the modules of the processor. They are responsible for sampling analogue signals and implementing the algorithms controlling...
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RESOURCE ALLOCATION IN DAB+ BROADCASTING SYSTEM
PublikacjaWith over two billion receivers operating worldwide, radio transmission is by far the most accessible medium. It has been a part of our lives since the 1920’s and has become one of the most trusted and friendly mass media. Today, its popularity is still strong, despite the outcome of many electronic media. In order to transform the radio into a viable medium of the 21st century, it will have to migrate from analogue to digital...
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Alternative treatment approaches of urinary tract infections caused by uropathogenic Escherichia coli strains
PublikacjaUrinary tract infections (UTIs) are the most widespread and annoying infections affecting millions of people every year annually. The biggest problem of urinary diseases are recurrences, the increasing resistance of uropathogens to commonly used antibiotics, as well as the high health care costs of afflicted persons. Uropathogenic Escherichia coli strains (UPECs) are the most dominant etiologic agent of community-acquired infections...
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‘Acridines’ as New Horizons in Antifungal Treatment
PublikacjaFrequent fungal infections in immunocompromised patients and mortality due to invasive mycosis are important clinical problems. Opportunistic pathogenic Candida species remain one of the leading causes of systemic mycosis worldwide. The repertoire of antifungal chemotherapeutic agents is very limited. Although new antifungal drugs such as lanosterol 14α-demethylase and β-glucan synthase inhibitors have been introduced into clinical...
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Systems, environments, and soliton rate equations: A non-Kolmogorovian framework for population dynamics
PublikacjaSoliton rate equations are based on non-Kolmogorovian models of probability and naturally include autocatalytic processes. The formalism is not widely known but has great unexplored potential for applications to systems interacting with environments. Beginning with links of contextuality to non- Kolmogorovity we introduce the general formalism of soliton rate equations and work out explicit examples of subsystems interacting with...
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THE INFLUENCE OF HOUSING ARRANGEMENT AND INTERFERENCE ON PRELOAD AND THEORETICAL LIFETIME OF A SYSTEM OF TAPER ROLLER BEARINGS OF A HIGH SPEED SHAFT OF A WIND TURBINE GEARBOX
PublikacjaA system of two taper roller bearings can carry loads with a high ratio of axial load to radial load. Such a system was proposed for a wind turbine gearbox following the poor durability of original bearing design with the aim of increasing durability. Because of size limits, a proposed system is composed of two different taper roller bearings. Standard manufacturers’ catalogues do not provide information on recommended preload...
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Discussing daylight simulations in a proposal for online daylighting education.
PublikacjaThere is increasing interest concerning daylighting in the building sector. However, such knowledge is difficult to penetrate the curricula of architects and designers as existing educational programmes often do not provide sufficient training on BPS. This also leads to superficial use of daylight simulations. This paper presents a proposal for a needs-based education package on daylighting design, that mixes modular eLearning...
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Pressure-induced superconductivity in CaFe2As2
PublikacjaNowo odkryty związek CaFe2As2 pod wpływem zewnętrznego ciśnienia 0.69 GPa przechodzi w stan nadprzewodnictwa z temperaturą krytyczną powyżej 10K.
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Underwater Local Cavity Welding of S460N Steel
PublikacjaIn this paper, a comparison of the mechanical properties of high-strength low-alloy S460Nsteel welded joints is presented. The welded joints were made by the gas metal arc welding (GMAW)process in the air environment and water, by the local cavity welding method. Welded joints were testedfollowing the EN ISO 15614-1:2017 standard. After welding, the non-destructive—visual, penetrant,radiographic, and ultrasonic (phased array) tests...
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Modifications of total synthesis of mycophenolic acid
PublikacjaThe total synthesis of mycophenolic acid (MPA), a potent immunosuppressant, was modified. The obtained mycophenolic acid was suitable for further preparation of new prospective immunosuppressants with improved therapeutic properties.
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Karaś P., Kochanowicz K., Pitek M., Domański P., Obuchowski I., Tomiczek B., Liberek K.: Evolution towards simplicity in bacterial small heat shock protein system// eLife -, (2023), s.1-21
PublikacjaEvolution can tinker with multi-protein machines and replace them with simpler single-protein systems performing equivalent functions in an equally efficient manner. It is unclear how, on a molecular level, such simplification can arise. With ancestral reconstruction and biochemical analysis, we have traced the evolution of bacterial small heat shock proteins (sHsp), which help to refold proteins from aggregates using either...
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Evolution towards simplicity in bacterial small heat shock protein system
PublikacjaEvolution can tinker with multi-protein machines and replace them with simpler single-protein systems performing equivalent functions in an equally efficient manner. It is unclear how, on a molecular level, such simplification can arise. With ancestral reconstruction and biochemical analysis, we have traced the evolution of bacterial small heat shock proteins (sHsp), which help to refold proteins from aggregates using either two...
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Pool Boiling of Water–Al2O3 and Water–Cu Nanofluids Outside Porous Coated Tubes
PublikacjaThis paper deals with pool boiling ofwater–Al2O3 and water–Cu nanofluids on porous coated, horizontal tubes. Commercially available stainless-steel tubes having 10 mm outside diameter and 0.6 mm wall thickness were used to fabricate a test heater. Aluminum porous coatings 0.15 mm thick with porosity of about 40% were produced by plasma spraying. A smooth tube served as a reference tube. The experiments were conducted under different...
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Starch-clay nanocomposite films
PublikacjaStarch is a natural polymer which, due to its renewability, biodegrability, availability and a relatively low cost, has a high potential for applications in biodegradable materials. However, because of its hydrophilic nature, the number of commercially available starch-based products is still limited. Recently, starch-based nanocomposites with the addition of clay minerals as nanofillers have given rise to large-scale improvements...
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High-speed memoryless binary/residue converter
PublikacjaW pracy zaprezentowano nowy szybki konwerter z systemu binarnego do systemu resztowego dla liczb o zakresie do 60 bitów. W konwerterze stosowane są wyłącznie układy kombinacyjne. Algorytm konwertera oparty jest na dodawaniu niezerowych cyfr binarnych reprezentacji kolejnych potęg 2 modulo m. Dodawanie jest realizowane przy użyciu wielooperandowego sumatora CSA oraz sumatora CPA. Suma wyjściowa CPA jest redukowana do zakresu 2m-1...
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Effect of high pressure and sub-zero temperature on some gram-negative bacteria.
PublikacjaCelem pracy było określenie przeżywalności wybranych gramujemnych bakterii na działanie wysokiego ciśnienia i ujemnej temperatury. Traktowanie komórek bakterii ciśnieniem 193 MPa w temperaturze -20C przez 24 godziny, powodowało całkowitą inaktywację bakterii E. coli, P. fluorescens i T. thermophilus. Po działaniu ciśnienia przez krótszy czas występowały różnice we wrażliwości między badanymi szczepami. Najmniej odporny na działanie...
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Utilization of oriented crystal growth for screening of aromatic carboxylic acids cocrystallization with urea
PublikacjaThe possibility of molecular complex formation in the solid state of urea with benzoic acid analogues was measured directly on the crystallite films deposited on the glass surface using powder X-ray diffractometry (PXRD). Obtained solid mixtures were also analyzed using Fourier transform infrared spectroscopy (FTIR). The simple droplet evaporation method was found to be efficient, robust, fast and cost-preserving approach for first...