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Development and Validation of SPE-HPLC-MS/MS Method for Determining Cyclophosphamide in Surface Waters
PublicationA rapid and selective method for trace amounts determination of cyclophosphamide in surface water samples has been developed. A solid phase extraction SPE method for extraction and clean-up procedure has been optimized for determination by reversed-phase high-performance liquid chromatography with tandem mass spectrometry. The analyses proceed in the positive ion mode by means of the electrospray ionization method (ESI). Clean...
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Complementary use of GCxGC–TOF–MS and statistics for differentiation of variety in biosolid samples
PublicationFormation of biosolid cakes, which are one of the main wastes generated in wastewater treatment plants, is connected with emission of many hazardous chemical compounds, including odoriferous ones. To optimize particular processes of biosolid cake processing, it is necessary to assess chemical composition of the gas mixtures containing the compounds released from the cakes. The paper proposes application of two-dimensional gas chromatography...
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Transcriptomic Effects of Estrogen Starvation and Induction in the MCF7 Cells. The Meta-analysis of Microarray Results
PublicationEstrogen is one of the most important signaling molecules which targets a number of genes. Estrogen levels regulate cell proliferation and a plethora of metabolic processes, which may interfere with a range of medical conditions and drug metabolism. The MCF7 breast cancer cell line, expressing the estrogen receptor α, is a well-studied model of cellular answer to estrogen. The aim of this study was to characterize transcriptomic...
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Electromagnetic Field Associated With Dermoscope Magnets May Affect the Safety of Cardiac Implanted Electronic Devices Patients
PublicationDermoscopy is currently used as an auxiliary tool in general dermatology. Since some commercially available dermoscopes have built-in magnets, electromagnetic interference (EMI) may occur when examining cardiac implantable electronic devices (CIED) patients. The aim of the study was to create maps of electromagnetic fields defining a safe distance in terms of EMI. The study was performed in laboratory conditions using measuring...
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Method for determining of shallow water depths based on data recorded by UAV/USV vehicles and processed using the SVR algorithm
PublicationBathymetric measurements in waters shallower than 1 m are necessary to monitor seafloor relief changes in the coastal zone. This is especially important for ensuring the safety of navigation, navigation efficiency, as well as during the design and monitoring of hydrotechnical structures. Therefore, the aim of this article is to present a method for determining of shallow water depths based on data recorded by Unmanned Aerial Vehicle...
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Quality control of cheese samples for the presence of natamycin preservative – A natural deep eutectic solvent (NADES) based extraction coupled with HPLC
PublicationA new protocol for the determination of natamycin – an antifungal agent used as a food preservative - in cheese samples – is described. This new method is based on a natural deep eutectic solvent (NADES) green extraction procedure. High-performance liquid chromatography (HPLC) was used for detection and quantification. NADESs with different molar ratios were evaluated for efficient and selective extraction. NADES made of thymol...
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5-Thiocyanato-2′-deoxyuridine as a possible radiosensitizer: electron-induced formation of uracil-C5-thiyl radical and its dimerization
PublicationIn this work, we have synthesized 5-thiocyanato-2′-deoxyuridine (SCNdU) along with the C6-deuterated nucleobase 5-thiocyanatouracil (6-D-SCNU) and studied their reactions with radiation-produced electrons. ESR spectra in γ-irradiated nitrogen-saturated frozen homogeneous solutions (7.5 M LiCl in H2O or D2O) of these compounds show that electron-induced S–CN bond cleavage occurs to form a thiyl radical (dU-5-S˙ or 6-D-U-5-S˙) and...
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Nano-engineered diamond-based materials for supercapacitor electrodes: A review
PublicationOwing to the popularity of carbon-based supercapacitors, diamond has also been examined as a potential candidate with unique advantages such as a wide electrochemical potential window and stable capacitive behavior in both aqueous and non-aqueous electrolytes. Moreover, its chemical stability in harsh environments at extreme applied potential and current provides rare opportunities for designing new supercapacitors. Owing to the...
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Designate of CTOD for WM and HAZ, report no: WOiO/II/122/2014
PublicationTypical (normative) testing of materials and/or welded joints do not answer on all questions about material or welded joint properties. In ship building and off-shore sectors, many strucures requires materials and joint with higher than typical fatigue resistance. Imact tests, which are carried out during welding technology qualification, gives answer about ductility, CTOD tests results about material or welded joint ability to...
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Performance‐driven modeling of compact couplers in restricted domains
PublicationFast surrogate models can play an important role in reducing the cost of EM-driven design closure of miniaturized microwave components. Unfortunately, construction of such models is challenging due to curse of dimensionality and wide range of geometry parameters that need to be included in order to make it practically useful. In this letter, a novel approach to design-oriented modeling of compact couplers is presented. Our method...
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MOOCs in SP4CE - case studies (Strategic Partnership for Creativity and Entrepreneurship)
PublicationSP4CE stands for Strategic Partnership for Creativity and Entrepreneurship project which has been funded with support from the European Commission under the ERASMUS+ Programme in the period 1st September 2014 - 31st August 2017. The main purpose of SP4CE project is to design innovative e-learning tools for collaboration between students, enterprises and teachers. It concentrates on identifying users’ needs and supports the development...
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CTOD designation for WM and HAZ in butt joint made from S460 ML steel, Expertise No. WOiO/II/82/2015
PublicationTypical (normative) testing of materials and/or welded joints do not answer on all questions about material or welded joint properties. In ship building and off-shore sectors, many strucures requires materials and joint with higher than typical fatigue resistance. Imact tests, which are carried out during welding technology qualification, gives answer about ductility, CTOD tests results about material or welded joint ability to...
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Application of data segmentation and segregation in alarm dedicated glass breaks detection method,based on Wavelet Transformatio
PublicationAutor opracowuje nowoczesną, dedykowaną dla systemów alarmowych, metodę bezkontaktowej detekcji zbicia szyby, bazującą na analizie sygnałów akustycznych i transformacji falkowej. Struktura badanego sygnału oraz pierwotne metody mające zastosowanie w fazie badawczej projektu przedstawione zostały we wcześniejszych publikacjach autora [1] i [2]. Ze względu na ich dużą złożoność obliczeniowe i przetwarzanie off-line nie mogły być...
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Ideas of the New European Bauhaus (NEB) in architectural education
PublicationThe New European Bauhaus (NEB) is an interdisciplinary project initiated by the European Commission in 2020 [1], based on three values: sustainability, beauty and community (social inclusion). Its aim is to support the European Green Deal programme [2] by accelerating the transformation of various economic sectors, including construction, to improve the quality of people’s lives and protect the natural environment. Even though...
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Małe i średnie przedsiębiorstwa na rynkach międzynarodowych
PublicationCelem ksiązki jest omówienie zasad funkcjonowania MSP na rynkach międzynarodowych. Książka składa się z 7 rozdziałów ułożonych zgodnie z ligiką od ogółu do szczegółu.Rozdział 1 przybliża rolę, jaką MSP odgrywają w gospodarce, rozdział 2 poświęcono powodom zaangażowania MSP w działania międzynarodowe, rozdział 3 prezentuje najważniejsze modele internacjonalizacji MSP, rozdział 4 omawia szkołę przedsiębiorczości międzynarodowej,...
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Designate CTOD of Weld Metal of butt weld, No WOiO/II/108/2013
PublicationTypical (normative) testing of materials and/or welded joints do not answer on all questions about material or welded joint properties. In ship building and off-shore sectors, many strucures requires materials and joint with higher than typical fatigue resistance. Imact tests, which are carried out during welding technology qualification, gives answer about ductility, CTOD tests results about material or welded joint ability...
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Multibeam Sonar Characterisation of Seafloor in the Context of Visualisation and Dissemination of Marine Data
PublicationThe paper presents the seafloor characterisation method based on multibeam sonar data. it relies on using three types of multibeam seafloor sensing data: 1) the grey-level sonar images (echograms) of seabed, 2) the 3D model of the seabed surface which consists of high resolution bathymetric data, 3) the set of time domain bottom echo envelopes received in the consecutive sonar beams. The classification is performed by utilisation...
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Separation of the effects of notch and macro residual stress on the MFL signal characteristics
PublicationMagnetic flux leakage (MFL) distribution for three configurations of samples has been investigated in order to study the influence of notch and plastic deformation separately as well as together. Samples have been made of S355 steel. The MFL signal measurements were carried out along the longest dimension of the sample over a length of 120 mm. Two components of magnetic field were measured: 1) tangential to the main axis and 2)...
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A la recherche d’une coherence perdue – Possible Arguments for the Non-application of EU Law in Member States
PublicationThe European Union (EU) is an international organization which has a broad scope of competences that have been transferred to it by its Member States in the founding Treaties. The object of the article is to identify arguments raised, or that potentially might be raised, by national Constitutional Courts (and in the future possibly by other actors as well) to exclude in certain instances the application of EU law or EU jurisprudence...
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Numerical study of turbulent flow and heat transfer of nanofluids in pipes
PublicationIn this work, Nusselt number and friction factor are calculated numerically for turbulent pipe flow (6 000 < Re < 12 000) with constant heat flux boundary condition using nanofluids. The nanofluid is modelled with the single-phase approach and the simulation results are compared with experimental data of Vajjha et al. [1]. Ethylene glycol and water, 60:40 EG/W mass ratio, as base fluid and SiO2 nanoparticles are used as nanofluid...
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Chronographic Imprint of Age-Induced Alterations in Heart Rate Dynamical Organization
PublicationBeat-to-beat changes in the heart period are transformed into a network of increments between subsequent RR-intervals, which enables graphical descriptions of short-term heart period variability. Three types of such descriptions are considered: (1) network graphs arising from a set of vertices and directed edges, (2) contour plots of adjacency matrices A, representing the networks and transition matrices T, resulting from A, and (3)...
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Analysis of Airport Runoff Waters
PublicationA particularly important facet of airport operation is the impact of the pollution caused byrunoff waters. Runoff waters at an airport may contain relatively high concentrations of differentcontaminants resulting from the various aspects of its operation: de/anti-icing operations,washing and cleaning operations, spills of fuel and lubricants, exhaust fumes, and weed removal.The pollution caused by airport operations affects soil,...
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A structure and design optimization of novel compact microscrip dual-band rat-race coupler with enhanced bandwidth
PublicationIn the letter, a topology of a novel compact wideband dual-band rat-race coupler has been presented along with its computationally efficient design optimization procedure. Reduction of the circuit size has been achieved by meandering transmission lines of the conventional circuit. At the same time, the number of independent geometry parameters has been increased so as to secure sufficient flexibility of the circuit, necessary in...
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Designate CTOD Heat Affected Zone of butt weld, Report No: WOiO/II/76/2013
PublicationTypical (normative) testing of materials and/or welded joints do not answer on all questions about material or welded joint properties. In ship building and off-shore sectors, many strucures requires materials and joint with higher than typical fatigue resistance. Imact tests, which are carried out during welding technology qualification, gives answer about ductility, CTOD tests results about material or welded joint ability...
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Model-based testing for execution algorithms in the simulation of cyber-physical systems
PublicationThe understanding of simulation semantics of a hybrid system is a challenge for computational engineers as it requires expertise in computer science, engineering, numerical methods, and mathematics at once. The testing methods for the execution of a simulation are being researched but not yet applied on the industrial level. Consequently, the semantics of the simulation becomes a critical artifact in the system development process....
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Signature of Hydrodynamic Pressure Field
PublicationW artykule przedstawiono wyniki obliczeń pola hydrodynamicznego ciśnienia wokół okrętu specjalnego jako funkcji przestrzennej, obliczonej metodą brzegową. Obliczone pola ćiśnienia hydrodynamicznego jest porównywane z pomierzonym polem okrętu na morzu, przy czym opis kształtu kadłuba okrętu jest przybliżony. Przedstawione wyniki obliczeń uzyskano stosując warstwę pojedynczą , którą stanowią źródła o rozkładzie ciągłym. Skonstruowany...
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MULTI-OBJECTIVE OPTIMIZATION PROBLEM IN THE OptD-MULTI METHOD
PublicationNew measurement technologies, e.g. Light Detection And Ranging (LiDAR), generate very large datasets. In many cases, it is reasonable to reduce the number of measuring points, but in such a way that the datasets after reduction satisfy specific optimization criteria. For this purpose the Optimum Dataset (OptD) method proposed in [1] and [2] can be applied. The OptD method with the use of several optimization criteria is called...
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3D Hierarchical Boron-Doped Diamond-Multilayered Graphene Nanowalls as an Efficient Supercapacitor Electrode
PublicationSynthesis of stable hybrid carbon nanostructure for high-performance supercapacitor electrode with long life-cycle for electronic and energy storage devices is a real challenge. Here, we present a one-step synthesis method to produce conductive boron-doped hybrid carbon nanowalls (HCNWs), where sp2-bonded graphene has been integrated with and over a three-dimensional curved wall-like network of sp3-bonded diamond. The spectroscopic...
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COMPOSITE MATERIAL SELECTION FOR A PATIENT TRANSFER ASSIST DEVICE
PublicationLaminates - layered composites containing at least two elements (matrix and reinforcement) widely used in industry have also found their usage in medicine. Their main feature is the ability to modify the material in order to obtain the required properties. Depending on the needs, we can modify reinforcement, type of resin or the method of bonding substrates. Commonly used fibers are: carbon fiber, glass and aramid fibers; resins...
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Beyond the helium buffer: 12C−2 rotational cooling in cold traps with H2 as a partner gas: interaction forces and quantum dynamics
Publicationabstract = { The scattering cross-sections and corresponding rate coefficients for rotationally inelastic collisions of $^{12}$C$_2$^-$ ($^2 \Sigma_g^+$) with H$_2$ ($^1 \Sigma_g^+$) are presented over a broad range of cold-trap temperatures. They have been calculated using quantum scattering theory that employs a new ab initio potential energy surface. The rate coefficients for the inelastic processes in the anionic partner are...
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Novel Class of Proton Conducting Materials—High Entropy Oxides
PublicationHere, for the first time, we present data on proton conductivity of high-entropy, single-phase perovskites. The BaZr0.2Sn0.2Ti0.2Hf0.2Ce0.2O3−δ, BaZr0.2Sn0.2Ti0.2Hf0.2Y0.2O3−δ, BaZr1/7Sn1/7Ti1/7Hf1/7Ce1/7Nb1/7Y1/7O3−δ, and BaZr0.15Sn0.15Ti0.15Hf0.15Ce0.15Nb0.15Y0.10O3−δ single-phase perovskites were synthesized. Before electrical measurements, materials were characterized using X-ray diffraction (XRD), scanning electron microscopy...
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Badania rozkładu temperatury na grubości płaszcza żelbetowego zbiornika oczyszczalni ścieków w okresie zimowym
PublicationPodczas eksploatacji zbiorników oczyszczalni ścieków na skutek różnicy temperatury ścieków a temperaturą powietrza na zewnątrz, powstają oddziaływania termiczne, które w przypadku nieocieplonej ściany żelbetowego zbiornika na ciecz, mogą przyczynić się do powstania zarysowań [1.] co w konsekwencji może doprowadzić do utraty szczelności. Powstałe na skutek różnic temperatur naprężenia rozciągające sumują się z naprężeniami wnikającymi...
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Visual TreeCmp : Comprehensive Comparison of Phylogenetic Trees on the Web
Publication1. We present Visual TreeCmp—a package of applications for comparing phylogenetic tree sets. 2. Visual TreeCmp includes a graphical web interface allowing the visualization of compared trees and command line application extended by comparison methods recently proposed in the literature. 3. The phylogenetic tree similarity analysis in Visual TreeCmp can be performed using eighteen metrics, of which 11 are dedicated to rooted trees...
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Signature of Hydrodynamic Pressure Field
PublicationW artykule przedstawiono wyniki obliczeń pola hydrodynamicznego ciśnienia wokół statku jako funkcję przestrzenną, obliczoną metodą brzegowego rozkładu osobliwości. Obliczone pole ciśnienia hydrodynamicznego jest porównywane z pomierzonym polem ciśnienia wokół okrętu na akwenie specjalnym, opis kształtu kadłuba jest przybliżony. Przedstawione wyniki obliczeń uzyskano stosując pojedynczą warstwę o ciągłym rozkładzie źródłowości....
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Auxetic foams
PublicationThis paper presents a method of producing auxetic polyurethane foams (PUFs) and their unique properties. The experience was based on a synthesis of traditional flexible polyurethane foam and thermal conversion to auxetic foam. The foam specimens were transformed from conventional Poisson's ratio to auxetic (negative Poisson's ratio) [1]. Basic research was performed to determine the mechanical properties and cell structure. Auxetic...
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Seafloor Characterisation Using Underwater Acoustic Devices
PublicationThe problem of seafloor characterisation is important in the context of management as well as investigation and protection of the marine environment. In the first part of the paper, a review of underwater acoustic technology and methodology used in seafloor characterisation is presented. It consists of the techniques based on the use of singlebeam echosounders and seismic sources, along with those developed for the use of sidescan...
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Study on AR Application Efficiency of Selected iOS and Android OS Mobile Devices
PublicationCurrently, the number of scenarios for using AR (Augmented Reality) tools grows every year. Yet, there are still some open performance issues associated with this technology, related with the efficiency of the mobile device itself, including build-in components or the operation system. The purpose of this study was to investigate available augmented reality engines for mobile platforms. First, a review of current graphics and AR...
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Modification of TiO2 nanotubes by graphene–strontium and cobalt molybdate perovskite for efficient hydrogen evolution reaction in acidic medium
PublicationHerein, we demonstrate that modification of TiO2 nanotubes with graphene–strontium and cobalt molybdate perovskite can turn them into active electrocatalysts for hydrogen evolution reaction (HER). For this purpose, a simple method of hydrothermal synthesis of perovskites was developed directly on the TiO2 nanotubes substrate. Moreover, the obtained hybrids were also decorated with graphene oxide (GO) during one-step hydrothermal...
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Antitumor DNA-Damaging C-1748 is a New Inhibitor of Autophagy that Triggers Apoptosis in Human Pancreatic Cancer Cell Lines
PublicationDespite the enormous progress that has been made over the past decades in diagnosis, treatment and prevention of many types of tumors, survival rates in pancreatic cancer still remain poor. Pancreatic cancer is one of the most malignant and chemoresistant tumors and the profound mechanism supporting these phenomena is the constitutively activated prosurvival autophagy. The antitumor 1-nitroacridine derivative C-1748 belongs to...
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Research on the Use of Mobile Devices and Headphones on Pedestrian Crossings—Pilot Case Study from Slovakia
PublicationThe topic of the use of mobile devices and headphones on pedestrian crossings is much less explored in comparison to the use of the mobile phone while driving. Recent years have seen many discussions on this issue, especially in foreign countries. The Slovak Republic, however, has not been giving it enough attention (and it is not mentioned in the National Road Safety Plan for the Slovak Republic from 2011 to 2020). This paper...
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Antitumor 1-nitroacridine derivative C-1748 induces significant apoptosis in pancreatic cancer cells.
PublicationPancreatic cancer is the fifth leading cause of cancer death and has the lowest survival rate of any solid cancer in the industrial countries. The poor prognosis of pancreatic cancer results from its tendency for late presentation, aggressive invasion, early metastasis, and resistance to chemotherapy. Gemcitabine still remains the best chemotherapeutic agent available for the treatment of advanced pancreatic cancer. However, gemcitabine...
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Typing of Scopulariopsis and Microascus fungi by Random Amplified Polymorphic DNA (RAPD)
PublicationOBJECTIVES Scopulariopsis species and their teleomorphs of the genus Microascus are commonly isolated from soil, decaying plant material and indoor environments. Moreover, certain Scopulariopsis and Microascus species are recognised as opportunistic human pathogens. Although most species can be identified by detailed morphological study, phenotypic characters appear to overlap in several cases and morphology seems to be insufficient...
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WPŁYW TRANSFORMACJI DANYCH NA JAKOŚĆ OPRACOWANYCH METOD TOŻSAMOŚCIOWYCH W SPEKTROSKOPII BLISKIEJ PODCZERWIENI
PublicationSpektroskopia bliskiej podczerwieni (NIR) wykorzystuje absorpcję promieniowania elektromagnetycznego w zakresie 12000-4000 cm-1, (780¬-2500 nm). Absorpcja NIR pochodzi od nadtonów i drgań kombinacyjnych wiązań C-H, N-H, O-H. Widmo uzyskane techniką NIR jest unikatowym "odciskiem palca" badanej substancji gdyż zależy zarówno od właściwości fizyko-chemicznych próbki jak i od stanu fazowego oraz postaci krystalicznej jej składników.Zaletami...
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Wykorzystanie układów kogeneracyjnych małoskalowych i mikroskalowych opartych o silniki spalinowe na gaz ziemny
PublicationArtykuł poświęcony jest zagadnieniu wykorzystania układów kogeneracyjnych małoskalowych i mikroskalowych opartych o silniki spalinowe na gaz ziemny. W artykule znajdują się uwarunkowania prawne związane z kwestiami ulg i dofinansowania "produkcji energii elektrycznej" z wykorzystaniem kogeneracji. Ponadto dokonano przeglądu konstrukcji czołowych producentów silników spalinowych wykorzystujących gaz ziemny oraz zaprezentowano przykłady...
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Cross-linking of sodium caseinate-structured emulsion with transglutaminase alters postprandial metabolic and appetite responses in healthy young individuals
PublicationThe physico-chemical and interfacial properties of fat emulsions influence lipid digestion and may affect postprandial responses. The aim of the present study was to determine the effects of the modification of the interfacial layer of a fat emulsion by cross-linking on postprandial metabolic and appetite responses. A total of fifteen healthy individuals (26·5 (sem 6·9) years and BMI 21·9 (sem 2·0) kg/m2) participated in a cross-over...
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Exploiting multi-interface networks: Connectivity and Cheapest Paths
PublicationLet G = (V,E) be a graph which models a set of wireless devices (nodes V) that can communicate by means of multiple radio interfaces, according to proximity and common interfaces (edges E). The problem of switching on (activating) the minimum cost set of interfaces at the nodes in order to guarantee the coverage of G was recently studied. A connection is covered (activated) when the endpoints of the corresponding edge share at...
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Long-Term Stability of Benzodiazepines and Z-Hypnotic Drugs in Blood Samples Stored at Varying Temperatures
PublicationBenzodiazepines (BZDs) and Z-drugs are among the most commonly prescribed pharmaceuticals in the world and are considered standard care for various mental illnesses and for treatment of sleeping and anxiety disorders, alcohol withdrawal, muscle spasms and epilepsy. Some BZDs are not allowed as pharmaceuticals in many countries, and they are used as "designer benzodiazepines" (DBZDs). All these compounds are typically screened in...
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Sense of safety and opinions about COVID-19 vaccinations in Polish school teachers: The role of conspiracy theories belief and fear of COVID-19
PublicationThe co-occurrence of COVID-19 conspiracy theories (CCT) and fear of the coronavirus (FCV) can be linked to how safe people feel and how much they endorse vaccinations. School teachers were one of the vaccination priority groups in Poland. We conducted three cross-sectional studies (N1 = 1006; N2 = 1689; N3 = 627) to find out the potential interactive effects of CCT belief and FCV in predicting sense of safety (SoS; Studies 1-3),...
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Kolmatacja złóż hydrofitowych z pionowym przepływem ścieków w warunkach niedotlenienia
PublicationNa podstawie uzyskanych wyników badań dotyczących wpływu ograniczonego natlenienia złóż VF-CW na kolmatację sformułowano następujące wnioski:1. Obecność zawiesiny w ściekach miała wpływ na szybkość biodegradacji doprowadzanej substancji organicznej. Ścieki dopływające do Wieszyna ulegały stabilizacji biochemicznej dwukrotnie wolniej niż ścieki pochodzące z Wiklina. Przyczyną niższej szybkości biodegradacji było wyższe stężenie...
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Multiple bifurcation in the solution set of the von Karman equations with S^{1}-symmetries
PublicationRozważmy cienką, sprężystą, kołową płytę, położoną na sprężystym podłożu, poddawaną działaniu sił ściskających koncentrycznie wzdłuż jej brzegu. Formy równowagi takiej płyty są rozwiązaniami równań von Karmana z dwoma parametrami określonych na dysku w R^{2}. Są to równania różniczkowe cząstkowe rzędu czwartego. Można je zapisać jako równanie operatorowe F(x,p)=0 w przestrzeniach Höldera, gdzie zmienna x odpowiada formom równowagi...