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Search results for: SPECTROSCOPIC/ELECTROCHEMICAL MONITORING
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Spectroscopic Study of Plasma Polymerized a-C:H Films Deposited by a Dielectric Barrier Discharge
PublicationPlasma polymerized a-C:H thin films have been deposited on Si (100) and aluminum coated glass substrates by a dielectric barrier discharge (DBD) operated at medium pressure using C2Hm/Ar (m = 2, 4, 6) gas mixtures. The deposited films were characterized by Fourier transform infrared reflection absorption spectroscopy (FT-IRRAS), Raman spectroscopy, and ellipsometry. FT-IRRAS revealed the presence of sp3 and sp2 C–H stretching and...
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Spectroscopic and magnetic studies of highly dispersible superparamagnetic silica coated magnetite nanoparticles
PublicationSuperparamagnetic behavior in aqueously well dispersible magnetite core-shell Fe3O4@SiO2 nanoparticles is presented. The magnetic properties of core-shell nanoparticles were measured with use of the DC, AC magnetometry and EPR spectroscopy. Particles were characterized by HR-TEM and Raman spectroscopy, showing a crystalline magnetic core of 11.5 ± 0.12 nm and an amorphous silica shell of 22 ± 1.5 nm in thickness. The DC, AC magnetic...
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Experimental and theoretical studies of the spectroscopic properties of simple symmetrically substituted diphenylacetylene derivatives
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Spectroscopic Methods in the Evaluation of Modified Vegetable Base Oils from Crambe abyssinica
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Synthesis and Spectroscopic Characterization of Selected Phenothiazines and Phenazines Rationalized Based on DFT Calculation
PublicationTwo unique structures were isolated from the phosphorylation reaction of 10H-phenothiazine.The 5,5-dimethyl-2-(10H-phenothiazin-10-yl)-1,3,2-dioxaphosphinane 2-oxide (2a) illustrates theproduct of N-phosphorylation of phenothiazine. Moreover, a potential product of 2a instability,a thiophosphoric acid 2b, was successfully isolated and structurally characterized. Molecule 2a,similarly to sulfoxide derivative...
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Comprehensive Spectroscopic Characterization of Finasteride Polymorphic Forms. Does the Form X Exist?
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Photoinduced Isomerization of 23-Oxosapogenins: Conformational Analysis and Spectroscopic Characterization of 22-Isosapogenins
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P3HT:PCBM blend films phase diagram on the base of variable-temperature spectroscopic ellipsometry
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Phase diagram of P3HT:PC70BM thin films based on variable-temperature spectroscopic ellipsometry
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Spectroscopic studies of sol-gel derived thin film structures for integrated optics
PublicationPrzedstawiono wyniki badania struktur cienkowarstwowych wykonywanych dla zastosowań w optyce zintegrowanej z polimerów hybrydowych (np. w postaci ścieżek śwaitłowodów planarnych). Jakość i jednorodność stuktur badano za pomocą mikroskopii ramanowskiej, mikroskopii optycznej i profilometrii światła białego. Wykonano porównanie wyników uzyskanych tymi trzema metodami.
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Cadmium tri-tert-butoxysilanethiolates. Structural and spectroscopic models of metal sites in proteins.
PublicationW publikacji opisano syntezy i struktury dla dwóch heteroleptycznych kompleksów kadmu z rdzeniem CdS2NO2 i CdS2N2. Bis(tri-tert-butoksysilanotiolato)(1-metyloimidazol)kadmu(II) oraz bis(tri-tert-butoksysilanotiolato)bis(1-metyloimidazol)kadmu(II) współistnieją w roztworze chloroformu przy różnych stężeniach Bis(tri-tert-butoksysilanotiolanu) kadmu(II) i 1 metyloimidazolu. Rotzwór ten został scharakteryzowany za pomocą analizy spektralnej...
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Cadmium tri-tert-butoxysilanethiolates: Structural and spectroscopic models of metal sites in proteins
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Spectroscopic properties of bismuth-germanate glasses co-doped with erbium and holmium ions
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The influence of Si4+ co-doping on the spectroscopic properties of β-NaCaPO4:Eu2+/Eu3+
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Crystallographic and spectroscopic studies of 5-arylidene-2-amino-imidazol-4-ones
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Energy shifts of K- and L-lines as spectroscopic diagnostic of Z-pinch plasmas
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Spectroscopic and Spectroelectrochemical Studies on Redox Properties of Zinc Sulfide and Their Consequences on Photocatalytic Activity
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GNSS reference solution for permanent sition stability monitoring and geodynamical investigations - the ASG-EUPOS case study
PublicationThe aim of this paper is to present the strategy of determination of the reference solution for the ASG-EUPOS (ActiveGeodetic Network – European Position Determination System) coordinate monitoring system. ASG-EUPOS is a network of permanent GNSS (Global Navigation Satellite System) stations controlled by the Polish Head Office of Geodesy and Cartography (HOGC), which main role is to realize the ETRS89 (European Terrestrial Reference...
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Aluminum-TiO2 NPs Composites as Non-precious Catalysts for Efficient Electrochemical Generation of Hydrogen
PublicationIn this paper, we demonstrated, for the first time, aluminum titania nanoparticle (Al-TiO2 NP) composites with variable amounts of TiO2 NPs as nonprecious active catalysts for the electrochemical generation of H2. These materials were synthesized by mixing desired amounts of hydrogen titanate nanotubes (TNTs), fabricated here by a cost-effective approach at moderate hydrothermal conditions, with aluminum powder (purity 99.7%; size...
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Geier R., Angelmaier V., Gaubner C.-A., Kohoutek J.: Integrale Brücken. Entwurf, Berechnung, Ausführung, Monitoring
PublicationGeier R., Angelmaier V., Gaubner C.-A., Kohoutek J.: Integrale Brücken. Entwurf, Berechnung, Ausführung, Monitoring. Ernst & Sohn, Berlin 2017.
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Cost-Efficient Measurement Platform and Machine-Learning-Based Sensor Calibration for Precise NO2 Pollution Monitoring
PublicationAir quality significantly impacts human health, the environment, and the economy. Precise real-time monitoring of air pollution is crucial for managing associated risks and developing appropriate short- and long-term measures. Nitrogen dioxide (NO2) stands as a common pollutant, with elevated levels posing risks to the human respiratory tract, exacerbating respiratory infections and asthma, and potentially leading to chronic lung...
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Method of Monitoring of the Grinding Process with Lapping Kinematics Using Audible Sound Analysis
PublicationUtilising microphones as audible sound sensors for monitoring a single-side grinding process with lapping kinematics is presented in the paper. The audible sound generated during grinding depended on the cutting properties of electroplated tools with D107 diamond grains and different thicknesses of the nickel bond. The tool wear affected the obtained technological effects such as material removal rate and the surface roughness...
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Heterogeneous distribution of surface electrochemical activity in polycrystalline highly boron-doped diamond electrodes under deep anodic polarization
PublicationThe surface homogeneity of boron-doped diamond electrodes is variable and depends on anodic polarization conditions. The differentiation factor is the gradual and localized change in surface termination. A series of measurements under different polarization conditions was performed in order to investigate the scale of this effect. Nanoscale impedance microscopy (NIM) revealed large variation of surface resistance in individual...
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Electrochemical performance of Co3O4/CeO2 electrodes in H2S/H2O atmospheres in a proton-conducting ceramic symmetrical cell with BaZr0.7Ce0.2Y0.1O3 solid electrolyte
PublicationThe electrochemical performance of Co3O4/CeO2 mixed oxide materials as electrodes, when exposed to H2S/H2O atmospheres, was examined employing a proton conducting symmetrical cell, with BaZr0.7Ce0.2Y0.1O3 (BZCY72) as the solid electrolyte. The impact of temperature (700–850 °C) and H2S concentration (0–1 v/v%) in steam-rich atmospheres (90 v/v% H2O) on the overall cell performance was thoroughly assessed by means of electrochemical...
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Deposition and Electrical and Structural Properties of La0.6Sr0.4CoO3 Thin Films for Application in High-Temperature Electrochemical Cells
PublicationLow-temperature deposition of electroceramic thin films allows the construction of new devices and their integration with existing large-scale fabrication methods. Developing a suitable low-cost deposition method is important to further advance the development of microdevices. In this work, we deposited a 1-lm-thick La0.6Sr0.4CoO3d (LSC) perovskite with high electrical conductivity on sapphire substrates at 400C and analyzed its...
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Multi-Technique Investigation of Grave Robes from 17th and 18th Century Crypts Using Combined Spectroscopic, Spectrometric Techniques, and New-Generation Sequencing
PublicationThe textile fragments of the funeral clothes found in the 17th and 18th century crypts were subjected to spectroscopic, spectrometric, and microbial investigation. The next-generation sequencing enabled DNA identification of microorganisms at the genus and in five cases to the species level. The soft hydrofluoric acid extraction method was optimized to isolate different classes of dyes from samples that had direct contact with...
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A study on microcrack monitoring in concrete: discrete element method simulations of acoustic emission for non-destructive diagnostics
PublicationThe research is focused on the monitoring of fracture evolution in concrete beams under three-point bending using the acoustic emission technique and the discrete element method. The main objective of the study was to numerically and experimentally investigate the mechanism behind the generation of elastic waves during acoustic emission events and their interaction with micro- and macro-cracking in concrete beams under monotonic...
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Correlation between the Reactivity and Spectroscopic Properties of N-Substituted Secondary Thioamides. New Intramolecular N• •H+• •N Binding Approach and Proton Complexes Based on Thioamide Ligation
PublicationFrom a comparison of chem. shifts and wavenumbers of several secondary thioamides and amides having monocationic substituents attached to thiocarbamoyl or carbamoyl groups by a polymethylene chain, new intramol. unconventional N···H+···N H bonding effects were discovered. It is argued that the CH2-N rotation is hindered and two +H···NHMe nonequiv. protons occur in a proton spectrum of hydrochloride RCH2C(S)NH(CH2)3NHMe-HCl...
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In-service measurement of the small wind turbine test stand for structural health monitoring
PublicationThis paper presents the research activity performed on a Small Wind Turbine (SWT) test stand. Commercially available turbine was modified towards incorporation of the sensors system for condition monitoring. Installed sensors measure angular shaft position, torque applied from the wind loads, vibration accelerations and last but not least rotational speed. All gathered data are then transferred and processed in Test.Lab by means...
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Electrochemical determination of nitroaromatic explosives at boron-doped diamond/graphene nanowall electrodes: 2,4,6-trinitrotoluene and 2,4,6-trinitroanisole in liquid effluents
PublicationThe study is devoted to the electrochemical detection of trace explosives on boron-doped diamond/graphene nanowall electrodes (B:DGNW). The electrodes were fabricated in a one-step growth process using chemical vapour deposition without any additional modifications. The electrochemical investigations were focused on the determination of the important nitroaromatic explosive compounds, 2,4,6-trinitrotoluene (TNT) and 2,4,6-trinitroanisole...
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Underwater Electrochemical Offshore Tests of a Paint Coating Applied in Water on the Legs of an Oil Production Platform
PublicationThis paper presents the methodology developed for underwater measurements using electrochemical impedance spectroscopy (EIS) technique, aimed at determining the resistance of an epoxy coating applied in seawater to the legs of an oil production platform. Performing such underwater tests in an offshore environment was technically challenging. The results of measurements obtained on the platform were confronted with comparative results...
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The geodetic monitoring of the engineering structure – a practical solution of the problem in 3D space
PublicationThe study raises the issues concerning the automatic system designed for the monitoring of movement of controlled points, located on the roof covering of the Forest Opera in Sopot. It presents the calculation algorithm proposed by authors. It takes into account the specific design and location of the test object. High forest stand makes it difficult to use distant reference points. Hence the reference points used to study the stability...
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The Role of Thermal Monitoring in Cardiosurgery Interventions
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Sieciowy monitoring i diagnostyka obiektów
PublicationNowatorskie rozwiązania z dziedzin tj. elektronika czy informatyka w dużym stopniu wpływają na intensywny rozwój nietypowych metod w systemach diagnostyki przemysłowej. Proponowany Sieciowy Monitor Obiektu jest nie tylko autonomicznym systemem sterowania, ale jest również zaawansowaną aplikacją umożliwiającą koordynowanie wielu zadań jednocześnie. Modułowość tego typu systemów sprawia, że stają się one bardziej uniwersalne - zdecydowanie...
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Geodesic monitoring of tower and mast structures
PublicationW artykule przedstawiono obciążenia jakim są poddawane konstrukcje wieżowe i masztowe. Opisano zakres oraz wymagania dotyczące pomiarów geodezyjnych przeprowadzanych w czasie eksploatacji konstrukcji smukłych. Wskazano metody pomiaru oraz zaprezentowano niektóre sposoby pomiaru w praktyce. Zamieszczono wyniki pomiarów przemieszczeń elektrowni wiatrowej o mocy 2 MW i wysokości elementu wsporczego 80 m oraz zaprezentowano pomiary...
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Monitoring and analytics of atmospheric air pollution
PublicationPrzedstawiono podstawowe informacje dotyczące: celów i zadań monitoringu i analityki powietrza atmosferycznego, specyficznych wymogów jakie muszą spełniać monitory zanieczyszczeń, tendencji rozwojowych w zakresie kontroli jakości powietrza atmosferycznego oraz klasyfikacji metod i technik pomiarowych.
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Monitoring odbieraków prądu pojazdów kolejowych
PublicationOpracowano stanowisko monitoringu stanu technicznego odbieraków prądu (MOP) w warunkach eksploatacyjnych – w trakcie przejazdu pociągów przez wybrany punkt linii kolejowej. Działanie systemu opiera się na pomiarze uniesienia przewodów jezdnych sieci trakcyjnej w celu wykrycia odbieraków o niewłaściwej sile nacisku. Przedstawiono metodę pośredniego wyznaczania siły statycznej odbieraka prądu. Opisano strukturę systemu MOP, zainstalowanego...
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Multidimensional Monitoring System of State Machines
PublicationTechnical systems are more complex every day as their electronics and mechanics. Technical advances tend to be autonomous in its performance and perform an auto-diagnosis that allows determining an abnormality existence in a component or subsystem and deciding if the system has to be stopped or not.
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Environmental analytics and monitoring. Problems and challenges
PublicationW pracy przedstawiono: a. cele i zadania monitoringu środowiskowego, b. klasyfikację urządzeń kontrolno-pomiarowych i metodyk analitycznych wykorzystywanych w badaniach środowiska, c.możliwość wykorzystania r.óżnych ypów informacji analitycznych w chemii środowiska.
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Intelligent system for environmental noise monitoring.
PublicationW rozdziale przedstawiono projekt i realizację automatycznej stacji monitorowania hałasu środowiskowego. Stanowi ona jeden z elementów tworzonego w Katedrze Systemów Multimedialnych Politechniki Gdańskiej Multimedialnego Systemu Monitorowania Hałasu. Przedstawiono ogólną budowę stacji pomiarowej oraz omówiono jej podstawową funkcjonalność. Obszerniej opisano dodatkowe możliwości stacji, do których należą: komunikacja z wykorzystaniem...
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Impedance monitoring of fuel cell stacks
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Monitoring of metal structures with the dynamic methods
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ASG-EUPOS Monitoring with Reference to EPN
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Some advances in environmental analytics and monitoring
PublicationW pracy przedstawiono wkład Katedry Chemii Analitycznej w rozwój analityki środowiskowej i monitoringu, ze szczególnym uwzględnieniem analityki pozostałości leków w próbkach wodnych ( w układzie on-line i off-line), badań nad identyfikacją produktów degradacji organicznych zanieczyszczeń, analizy toksyn w wodach za pomocą techniki HPLC-DAD-MS, wykorzystania dozymetrii pasywnej do izolacji analitów z wody oraz jednoczesnego oznaczania...
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HVRmonitor - data replication monitoring method
PublicationArtykuł ten opisuje system służący monitorowaniu replikacji danych, wytworzony w firmie Lufthansa Systems Poland. W artykule przedstawiono w sposób ogólny wiele istotnych problemów a następnie przedstawiono w sposób bardziej szczegółowy ich rozwiązanie. Artykuł opisuje również architekturę wytworzonego systemu, jego funkcjonalność i interfejs, omawia w sposób zwięzły zasady jego działania i wskazuje jak wdrożone rozwiązania mogą...
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Adhesive Monitoring with Instrumented Wedge Test
PublicationThe wedge test (sometimes called the Boeing wedge test) is amongst the most readily exploitable techniques for assessment of the rate-dependent fracture energy of adhesive materials when used to bond relatively rigid substrates. With its siblings: the double cantilever beam (DCB), and the tapered double cantilever beam (TDCB), a force is applied, essentially in cleavage, to provoke substrate separation perpendicularly to the bondline...
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EI measurements for OP-CABG monitoring.
PublicationCelem pracy jest analiza możliwości zastosowania pomiarów elektroimpedanycjnych do śródoperacyjnego monitoringu w kardiochirurgii. Omówiono pomiary przeprowadzone in vivo na świniach podczas operacji z użyciem holdera stosowanego w OP-CABG. Holder ten został przystosowany do prowadzenia pomiarów z wykorzystaniem spektroskopii elektroimpedancyjnej podczas operacji. Wykonana na świniach seria operacji obejmujących eksperymentalny...
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Optical properties of the chemotherapy drugs used in the central nervous system lymphoma therapy: monitoring drug delivery
PublicationOur aim is to optically monitor the delivery of the chemotherapy drugs for brain tumours, particularly used in the central nervous system (CNS) lymphoma therapy. In vivo monitoring would help to optimize the treatment and avoiding unnecessary medications. Moreover, it would be beneficial to be able to measure which of the multi-regimen drugs actually do penetrate and how well into the brain tissue. There exist several potential...
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A Surrogate-Assisted Measurement Correction Method for Accurate and Low-Cost Monitoring of Particulate Matter Pollutants
PublicationAir pollution involves multiple health and economic challenges. Its accurate and low-cost monitoring is important for developing services dedicated to reduce the exposure of living beings to the pollution. Particulate matter (PM) measurement sensors belong to the key components that support operation of these systems. In this work, a modular, mobile Internet of Things sensor for PM measurements has been proposed. Due to a limited...
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Nowoczesne systemy bezpieczeństwa: monitoring, biometryka i Internet Rzeczy
PublicationNowoczesne technologie, takie jak systemy monitoringu, biometryka i Internet Rzeczy (IoT), odgrywają coraz większą rolę w ochronie osób i mienia. W dobie rosnących zagrożeń i dynamicznych zmian technologicznych, wdrażanie tych rozwiązań staje się kluczowe dla zapewnienia skuteczności systemów bezpieczeństwa. Monitoring pozwala na ciągłe śledzenie zdarzeń w czasie rzeczywistym, co umożliwia szybką reakcję na potencjalne...