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Search results for: HIGH TEMPERATURE PROTECTIVE COATINGS
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Application of different modes of nanoscale impedance microscopy in materials research
PublicationIn recent years, there is noticeable interest in application of various types of scanning probe microscopy in material science research. One of them is contact atomic force microscopy combined with local impedance measurements, known as nanoscale impedance microscopy. Literature references present its application in investigations of new materials, microelectronics diagnostics, or research of protective coatings performance. In...
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Underwater Electrochemical Offshore Tests of a Paint Coating Applied in Water on the Legs of an Oil Production Platform
PublicationThis paper presents the methodology developed for underwater measurements using electrochemical impedance spectroscopy (EIS) technique, aimed at determining the resistance of an epoxy coating applied in seawater to the legs of an oil production platform. Performing such underwater tests in an offshore environment was technically challenging. The results of measurements obtained on the platform were confronted with comparative results...
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Evaluation of organic coatings condition with AFM-based method
PublicationThe paper presents an atomic force microscopy (AFM)-based approach to evaluation of local protective properties of organic coatings. Apart from topography, it provides local ac and dc characteristics of examined coating. The method consists in application of ac voltage perturbation signal between conductive AFM tip and coated metal substrate. The resulting current is used to determine local impedance characteristics. Both impedance...
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New trifunctional acrylic water-based paint with self-cleaning, biocidal and magnetic properties
PublicationIn the present study, we report the synthesis and application of ZnFe2O4/SiO2-TiO2 nanocomposites with nonstoichiometric content of Fe to Zn used for the first time for the preparation of new generation trifunctional paints with self-cleaning, biocidal and magnetic properties. Currently, there are no compositions on the market for obtaining protective coatings in the form of paint, which simultaneously exhibit biocidal, magnetic...
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Cross-sectional imaging of materials structure using PS-OCT
PublicationOptical low-coherence tomography is a measurement technique for non-contact and non-destructive investigation of materials inner structure. Nowadays, this method is highly applied in medical treatment especially in dermatology and ophthalmology. During our research we have developed an optical low-coherence tomography system with polarization state analysis for structure examination of a broad range of technical materials. In this...
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The changes of crosslink density of polyurethanes synthesised with using recycled component. Chemical structure and mechanical properties investigations.
PublicationThis paper aims at the utilisation of glycerolysate (Gly) obtained in polyurethane recycling process by means of crude glycerine, which has in its structure hydroxyl end groups that allow for further processing. Polyurethanes (PUs) were synthesised using prepolymer method with the mixture of neat polyol and glycerolysate, in different ratios, with 4,4-diphenylmethane diisocyanate (MDI). The prepolymer was subsequently extended...
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HIGH TEMPERATURE
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Influence of Gd deposition on the oxidation behavior and electrical properties of a layered system consisting of Crofer 22 APU and MnCo2O4 spinel
PublicationIn the study, the surface of the Crofer 22APU ferritic steel was modified with gadolinium oxide nanoparticles and a protective-conducting layer consisting of the MnCo2O4 spinel. This system was studied in the context of application in IT-SOFC interconnects. Four types of samples were studied: unmodified steel, steel coated with a manganese-cobalt spinel layer, steel modified with gadolinium oxide nanoparticles, and a system consisting...
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Multivariate analysis of impedance data obtained for coating systems of varying thickness applied on steel
PublicationElectrochemical impedance spectroscopy (EIS) has proven to be a valuable test method for the electrochemical characterization of protective coatings on metals. The common way of analysis in impedance spectroscopy is to model the impedance spectrum by means of an equivalent circuit and to extract the quantity of interest using optimization techniques. A model, corresponding to the behavior of the sample under testing, is important...
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Advanced polarization sensitive analysis in optical coherence tomography
PublicationThe optical coherence tomography (OCT) is an optical imaging method, which is widely applied in variety applications. This technology is used to cross-sectional or surface imaging with high resolution in non-contact and non-destructive way. OCT is very useful in medical applications like ophthalmology, dermatology or dentistry, as well as beyond biomedical fields like stress mapping in polymers or protective coatings defects detection....
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Journal of Protective Coatings and Linings
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Analysis of the Surface Stereometry of Alloyed Austenitic Steel after Fibre Laser Cutting using Confocal Microscopy
PublicationThe paper extends the concept of cut edge quality and examines the fibre laser cutting process. A Prima Power Platino Fiber Evo device with a reference speed (RS) of 3500 mm/min was used for laser cutting. In order to analyse the influence of the laser cutting speed on the cut edge quality of X5CrNi18-10 stainless steel sheets, macroscopic studies were conducted on a stereoscopic microscope and surface stereometry on a confocal...
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HIGH TEMPERATURE MATERIAL PROCESSES
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High Temperature Corrosion of Materials
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Cyclic behavior of FeCoCrNiMn high entropy alloy coatings produced through cold spray
PublicationeCoCrNiMn high entropy alloy powders were employed to produce coatings on carbon steel through high pressure cold spray (at 1100 °C and 7 MPa in temperature and pressure respectively). X-ray diffraction of the sprayed material revealed a dense coating with the retention of the original crystallographic structure. Once splatted, particles revealed high flattening ratio with consequent excellent adhesion of the coating to the substrate....
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High voltage protective assembly.
PublicationW referacie opisano zestaw zabezpieczeniowy, składający się z bezpiecznika i ogranicznika przepięć, przeznaczony dla napowietrznych słupowych stacji transformatorowych średnich napięć. Zastosowany warystorowy ogranicznik przepięć spełnia jednocześnie rolę wspornika dla bezpiecznika gazowydmuchowego. W referacie przedstawiono budowę, podstawowe parametry, przykłady zastosowania oraz wyniki badań zwarciowych zestawu.
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Time-frequency analysis in optical coherence tomography for technical objects examination
PublicationOptical coherence tomography (OCT) is one of the most advanced optical measurement techniques for complex structure visualization. The advantages of OCT have been used for surface and subsurface defect detection in composite materials, polymers, ceramics, non-metallic protective coatings, and many more. Our research activity has been focused on timefrequency spectroscopic analysis in OCT. It is based on time resolved spectral analysis...
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HIGH TEMPERATURE HEAT PUMPS – PERSPECTIVE HEATING SYSTEMS?
PublicationIn the paper presented are authors own concepts of high temperature compressor heat pumps for the utilisation of medium and low temperature sources of heat. Working fluids for use in high temperature heat pumps are discussed, as well as the criteria for their selection. Analyses are presented for the production of in the upper steam source at 130 °C. One-stage systems and cascade systems were analyzed. An analysis of the coefficient...
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Influence of High Temperature Oxidation on Hydrogen Absorption and Degradation of Zircaloy-2 and Zr 700 Alloys
PublicationThe present research was aimed at determining the effects of the oxide layers on hydrogen absorption, microstructure and mechanical properties of the Zircaloy- 2 and Zr 702 alloys. The oxidation was made at 350 °C, 700 °C and 900 °C for 10 to 30 min in laboratory air, followed by hydrogen cathodic charging for 72 h and annealing at 400 °C for 4 h. The slow strain rate tests were carried out on oxidized, charged and annealed specimens. The...
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High temperature corrosion resistance of porous hastelloy alloy
PublicationTo further understand the suitability of Ni-Cr-base alloy for solid oxide fuel cell (SOFC), a commercial Ni-Cr-Fe-Mo alloy, Hastelloy X was selected and evaluated for oxidation behaviour under high temperature conditions. HastelloyX was chosen due to its unusual resistance to oxidizing, reducing and neutral atmospheres. For long term stability of metal supported fuel cell, the corrosion resistance plays a vital role and must be...
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High-temperature kinetics study of 430L steel powder oxidized in air at 600–850 °C
PublicationThe 430L stainless steel powder with a mean particle size of 95 μm was studied to determine its high-temperature oxidation properties. Continuous thermogravimetric measurements were carried out for 100 h in air at temperatures in the range of 600–850 °C. Even though a considerable amount of Cr (up to ˜5 wt.% Cr) inside the grains was depleted – especially inside small grains – no breakaway oxidation was observed. This indicates...
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The selected effects of high temperature air-steam mixture wood drying
PublicationThe results of properties change of beech wood after drying process are presented. The wood taken to experiments was from northern part of Pomeranian region in Poland. Before the main high temperature drying process using air-steam mixture, wood was initially dried in an open air conditions. The high temperature drying process was conducted at temperature 120oC, humidity 48%, flow rate of drying medium 2.5m/s and atmospheric pressure....
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High Temperature Air Combustion and Gasification (HTAC; HTAG)
PublicationCombustion and gasification technology utilizing high-cycle regenerative air/steam preheater has drawn increased attention in many application areas. The process is to be realized at temperature level above ash melting point using highly preheated agent. The use of highly preheated media above 900oC provides additional energy in to conversion processes and results in considerable changes to the design of combustion and gasification...
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High temperature drying of beech with content of tension wood
PublicationThe presented artcle is focused on comparison of tension and normal wood of beech (Fagus sylvatica L.) in a high-temperature drying process. Samples of 26 mm thickness were selected from sapwood zone with different angle of growth rings. The article evaluated properties of tension and normal wood before and after drying process. Properties which are monitored were moisture, moisture gradients, covering tests, colour changes and...
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The Influence of Thin Gold Electrodes on the High-Temperature Impedance of Oxide Glasses
PublicationThe influence of thin gold electrodes on the electrical measurements of glasses at high temperatures was studied using impedance spectroscopy. The impedance was measured several times over a wide frequency range from 10 mHz to 1 MHz and the temperature ranged from 213 to 673 K under air and nitrogen atmospheres. The results showed a drop in the conductivity of more than an order of magnitude at a temperature around 603 K during...
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Field Evaluation of High Modulus Asphalt Concrete Resistance to Low-Temperature Cracking
PublicationHigh-modulus asphalt concrete has numerous advantages in comparison to conventional asphalt concrete, including increased resistance to permanent deformations and increased pavement fatigue life. However, previous studies have shown that the construction of road pavements with High Modulus Asphalt Concrete (HMAC) may significantly increase the risk of low-temperature cracking. Those observations were the motivation for the research...
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High-Temperature Structural and Electrical Properties of BaLnCo2O6 Positrodes
PublicationThe application of double perovskite cobaltites BaLnCo2O6−δ (Ln = lanthanide element) in electrochemical devices for energy conversion requires control of their properties at operating conditions. This work presents a study of a series of BaLnCo2O6−δ (Ln = La, Pr, Nd) with a focus on the evolution of structural and electrical properties with temperature. Symmetry, oxygen non-stoichiometry, and cobalt valence state have been examined...
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Numerical analysis of high temperature minichannels heat exchanger performance
PublicationNowadays, the most difficult technological challenge in energy sector is connected with the gas micro-CHP units, dedicated to the distributed power generation. They are expected to be of high efficiency and at the same time of compact in size. Regarding the first reason, significant increase in microturbine efficiency can only be achieved by increase in the engine operating temperature. Therefore, one of the critical elements in...
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High-temperature properties of titanium-substituted yttrium niobate
Publicationhe defect fluorite titanium-doped yttrium niobate samples Y3Nb1−xTixO7−δ have been synthesized and investigated by the means of high-temperature X-ray diffraction, dilatometry, and thermogravimetry. Thermal expansion coefficients (TECs) as well as chemical expansion coefficients for material with 5, 10, and 15 mol% of titanium were determined. All investigated samples exhibit chemical contraction caused by Ti doping. The values...
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The Use of Cluster Analysis to Assess the Wear Resistance of Cermet Coatings Sprayed by High Velocity Oxy-Fuel on Magnesium Alloy Substrate
PublicationCermet coatings are one of the best surface protection of machine elements against wear. On the other hand, the most universal and economically justified method of applying such coatings is high velocity oxy-fuel (HVOF) spraying. This method makes it possible to produce coatings characterized by compact structure, low porosity and very good adhesion to the substrate. All these fundamental properties contribute to the high wear...
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Electrolytic deposition of reactive element thin films on Crofer 22 APU and evaluation of the resulting high-temperature corrosion protection properties at 700 °C–900 °C
PublicationThis article presents electrolytic deposition of thin Rare Earth (RE) coatings on Crofer 22 APU stainless steel substrates for high temperature applications, such as interconnects in solid oxide cell stacks. The deposition of coatings based on yttrium-, gadolinium-, lanthanum-, and cerium nitrates is discussed. The high temperature corrosion properties of surface-modified steels were examined using thermogravimetry and electrical...
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Ultrafast high-temperature sintering (UHS) of cerium oxide-based compound
PublicationUltrafast high-temperature sintering (UHS) is an innovative sintering technique that can densify ceramics in a few seconds, dramatically reducing the carbon footprint and firing costs. In this work, the feasibility of applying UHS in Gd-doped ceria (GDC) and GDC-Er-stabilized bismuth oxide (ESB) composite powders was investigated. At high UHS currents (22-24 A), a fully dense GDC sample with a large grain size was obtained. Nonetheless,...
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Performance of the very high-temperature heat pump with low GWP working fluids
PublicationTraditional heat pumps are a very attractive pro-ecological solutions for a number of applications, including providing of heating or heat recovery from industrial processes. The application range of heat pumps could be greatly enlarged when the operating temperature would be increased to 130-150°C and/or the temperature lift can be increased to 50-100 K. In the paper, the very high temperature vapour-compressor based single stage...
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High-temperature heat pumps – potential technology for heat recovery and production of process heat
PublicationIn the paper, the high temperature vapour compressor based heat pump with a selection of working fluids, both perspective and ecological ones, is considered. Such system is not yet commercially available on the market and in author’s opinion it has significant potential for various applications. In the presented analysis it was assumed that the heat source has a temperature of 50oC and the temperature lift is 60, 80 and 100K respectively....
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Influence of Heat Treatment Temperature on Fatigue Toughness in Medium-Carbon High-Strength Steels
PublicationCurrent research has demonstrated that the tempering temperature affects the martensitic transformation of medium-carbon high-strength steels. This temperature plays an important role in the final microstructure, percentage ratios of martensite to ferrite phases and, consequently, in the mechanical properties and the fatigue response. So far, the relationship between the martensitic tempering temperature and the cyclic deformation...
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Maciej Wierzbowski dr inż.
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Influence of temperature and nitrogen pressure on the test without active gases for high-temperature proton exchange membrane fuel cells
PublicationHigh-Temperature Proton-Exchange Membrane Fuel Cells (HT-PEMFCs) are a candidate for electrical energy supply devices in more and more applications. Most notably in the aeronautic industry. Before any use, an HT-PEMFC is preheated and after that supplied with its active gases. Only at this state, the diagnostics can be performed. A method of testing not requiring a complete start-up would be beneficial for many reasons. This article...
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The abrasive wear resistance of coatings manufactured on high-strength low-alloy (HSLA) offshore steel in wet welding conditions
PublicationSome marine and offshore structure elements exploited in the water cannot be brought to the surface of the water as this will generate high costs, and for this reason, they require in-situ repairs. One of the repair techniques used in underwater pad welding conditions is a wet welding method. This paper presents an investigation of the abrasive wear resistance of coatings made in wet welding conditions with the use of two grades...
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The influence of high temperature wood drying conditions using air-steam mixture on its properties
PublicationThe results of properties change of beech wood after drying process are presented. The wood taken to experiments was from northern part of Pomeranian region in Poland. Before the main high temperature drying process using air-steam mixture, wood was initially dried in an open air conditions. The high temperature drying process was conducted at temperature 120oC, humidity 48%, flow rate of drying medium 2.5m/s and atmospheric pressure....
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High-temperature heat pumps – new devices for heat recovery and production of technological steam
PublicationIn the paper, the original high temperature compressor based heat pump with a dry working fluid, i.e. the one in which the slope of saturated vapour line is positive, was presented. The objective of the paper is to investigate the possibility of preparation of technological steam with tempperature 120 C from the waste heat resource at temperature of 50 C. Single comppression cycles as well as cascade systems have been considered...
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Deposition and Electrical and Structural Properties of La0.6Sr0.4CoO3 Thin Films for Application in High-Temperature Electrochemical Cells
PublicationLow-temperature deposition of electroceramic thin films allows the construction of new devices and their integration with existing large-scale fabrication methods. Developing a suitable low-cost deposition method is important to further advance the development of microdevices. In this work, we deposited a 1-lm-thick La0.6Sr0.4CoO3d (LSC) perovskite with high electrical conductivity on sapphire substrates at 400C and analyzed its...
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Molecular Strategy for Survival at a Critical High Temperature in Eschierichia coli
PublicationThe molecular mechanism supporting survival at a critical high temperature (CHT) in Escherichia coli was investigated. Genome-wide screening with a single-gene knockout library provided a list of genes indispensable for growth at 47°C, called thermotolerant genes. Genes for which expression was affected by exposure to CHT were identified by DNA chip analysis. Unexpectedly, the former contents did not overlap with the latter except...
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High temperature proton conduction in LaSbO4
PublicationLanthanum orthoantimonate was synthesized using a solid‐state synthesis method. To enhance the possible protonic conductivity, samples with the addition of 1 mol% Ca in La‐site, were also prepared. The structure was studied by the means of X‐ray diffraction, which showed that both specimens were single phase. The materials crystallized in the space group P2 1 /n. Dilatometry revealed that material expands non‐linearly with the...
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High-Temperature Oxidation of Heavy Boron-Doped Diamond Electrodes: Microstructural and Electrochemical Performance Modification
PublicationIn this work, we reveal in detail the effects of high-temperature treatment in air at 600 °C on the microstructure as well as the physico-chemical and electrochemical properties of boron-doped diamond (BDD) electrodes. The thermal treatment of freshly grown BDD electrodes was applied, resulting in permanent structural modifications of surface depending on the exposure time. High temperature affects material corrosion, inducing...
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High Temperature Air/Steam Conversion of Biomass and Wastes Into Fuel Gas for Heat and Electricity Production
PublicationPaper present principle of high temperature air/staem gasification as well as some results of research using this technology for conversion of biomass and wastes into fuel gas.
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The effect of high pressure at subzero temperature on proteins solubility, drip loss and texture of fish (cod and salmon) and mammal’s (pork and beef) meat
PublicationOne of the possibilities of using high pressure technique in inactivation of microorganism is conducting this process at subzero temperature. However, for its practical application in meat preservation the appropriate properties of meat should be kept. Therefore, the aim of this work was to examine the effect of pressure at subzero temperature (without freezing of water) on proteins and texture of mammal’s and cold-adapted fish...
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High temperature corrosion evaluation and lifetime prediction of porous Fe22Cr stainless steel in air in temperature range 700–900 °C
PublicationThis work describes a high temperature corrosion kinetics study of ~30% porous Fe22Cr alloys. The surface area of the alloy (~0.02 m2 g-1) has been determined by tomographic microscopy. The weight gain of the alloys was studied by isothermal thermogravimetry in the air for 100 hours at 700 - 900 °C. Breakaway oxidation was observed after oxidation at 850 °C (~100 hours) and 900 °C (~30 hours). The lifetime prediction shows the...
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Impact of high temperature drying process on beech wood containing tension wood
PublicationThe technology of high temperature drying has a great inuence on dimensional and selected physical changes in tension wood. Article is focused on the measurement properties such as moisture content, color changes and longitudinal warping. The quality of beech wood is determined based on structure and properties of wood, frequency of defects in wood material. The tension wood is considered as an important wood defect causing negative...
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Measurement microsystem for high impedance spectroscopy of anticorrosion coatings
PublicationW artykule przedstawiono mikrosystem do pomiarów bardzo dużych impedancji ukierunkowany na identyfikację parametrów powłok antykorozyjnych metodą spektroskopii impedancyjnej. Do wyznaczania składowych ortogonalnych sygnałów pomiarowych zastosowano w nim technikę cyfrowego przetwarzania sygnałów. Pozwoliła ona na uzyskanie szerokiego zakresu częstotliwości pomiarowych, zwłaszcza bardzo niskich, od ćHz, przy zachowaniu prostej konstrukcji...
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Exchange of radiation in high temperature air combustion furnaces by application of the transfer configuration factors
PublicationW artykule przedstawiono metodę obliczeń pasmowej radiacyjnej wymiany ciepła w układzie otwartym z gazem iztermicznym za pomocą uogólnionych współczynników konfiguracji. Metoda może być użyta do obliczeń wymiany ciepła w piecach z technologią High Temperature Air Combustion gdzie występuje prawie jednorodna temperatura. Podano przykład obliczeniowy.