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Search results for: analytical procedures development
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Some problems of slide bearing material fatigue evaluation.
PublicationA slide bearing alloy resistance against fatigue failures have been investigated for three different lubricants, different heat loadings and different stress ratio κ values. The research methods and data handling procedures for determination of particular parameter effects on fatigue strength have been described and analysed for experiments that were set and performed in laboratory tester SKMR-2. Main and interaction effects of...
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Sulfur compounds: Gas chromatography
PublicationSulfur compounds, due to their properties, are responsible for the damage of our environment. For this reason sulfur containing compounds are of constant concern in many fields. Gas chromatography (GC), due to combination of separation capability and sensitive detection is a prime technique for the analysis of thes compounds in various matrices. The chapter rewies general problems of the determination of these compounds by GC and...
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Parameter and delay estimation of linear continuous-time systems
PublicationIn this paper the problem of on-line identification of non-stationary delay systems is considered. Dynamics of supervised industrial processes is usually described by ordinary differential equations. Discrete-time mechanization of their continuous-time representations is based on dedicated finite-horizon integrating filters. Least-squares and instrumental variable procedures implemented in recursive forms are applied for simultaneous...
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Some Optimization Methods for Simulations in Volunteer and Grid Systems
PublicationIn this chapter, some optimization methods have been presented for improving performance of simulations in the volunteer and grid computing system called Comcute. Some issues related to the cloud computing can be solved by presented approaches as well as the Comcute platform can be used to simulate execution of expensive and energy consuming long-term tasks in the cloud environment. In particular, evolutionary algorithms as well...
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On–line Parameter and Delay Estimation of Continuous–Time Dynamic Systems
PublicationThe problem of on-line identification of non-stationary delay systems is considered. The dynamics of supervised industrial processes are usually modeled by ordinary differential equations. Discrete-time mechanizations of continuous-time process models are implemented with the use of dedicated finite-horizon integrating filters. Least-squares and instrumental variable procedures mechanized in recursive forms are applied for simultaneous...
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A scale with ECG measurements capability for home cardiac monitoring
PublicationPresented device -a scale developed for enabling extra measurements, in addition to body weight and composition, the electrical activity of the heart (electrocardiogram - ECG) and the level of oxygen saturation in the blood SaO2. Electrical activity is recorded in the form of six leads, socalled - limb leads. The device allows measurement of all standard limb leads and without the need for additional procedures. ECG, although the...
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Metal-Organic Frameworks in Green Analytical Chemistry
PublicationTaking into consideration the rapid expansion of MOFs applications in the analytical chemistry area, it is important to evaluate the existing and future analytical MOF-based methods according to GAC principles. From this point of view, eco-friendly MOFs-based methods should include features such as: green design and synthesis of MOF, evaluation of toxicity issues of MOFs, and incorporation of MOFs in GAC methods. This Chapter will...
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Analytical studies on the environmental state of the Svalbard archipelago - critical source of information about anthropogenic global impact
PublicationThe Svalbard archipelago differs from other polar regions due to its specific environmental conditions and geographic location which make the area gather pollution from long-range transport. Due to the recent development in analytical techniques it is possible to determine the concentration of pollutants at the level present there. This paper collates and discusses the information from the literature about: pollutants present in...
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Clinical anatomy of the spatial structure of the right ventricular outflow trac
PublicationBackground. The right ventricular outflow tract (RVOT) is located above the supraventricular crest and reaches the level of the pulmonary valve. Detailed knowledge of the RVOT spatial structure and its morphology is extremely important for cardiac invasive therapeutic procedures. Objectives. To examine the spatial structure of the RVOT using virtual models of the right ventricle (RV) interior obtained post mortem. Material and...
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Improved Design Closure of Compact Microwave Circuits by Means of Performance Requirement Adaptation
PublicationNumerical optimization procedures have been widely used in the design of microwave components and systems. Most often, optimization algorithms are applied at the later stages of the design process to tune the geometry and/or material parameter values. To ensure sufficient accuracy, parameter adjustment is realized at the level of full-wave electromagnetic (EM) analysis, which creates perhaps the most important bottleneck due to...
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Analytical progress on emerging pollutants in the environment: An overview of the topics
PublicationThis overview discusses the ideas behind a collection of articles by invited authors on a diverse range of complex chemical mixtures and analytical methods which represent some of the most relevant and interesting issues on emerging contaminants of environmental health concerns. These chemicals, including those in high volume production, are released on an ongoing basis as a result of various human activities. Moreover, these emerging contaminants...
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Green Analytical Chemistry Approaches in Sample Preparation
PublicationThis chapter presents environmentally friendly solutions for sample preparation. Attention is focused on extraction techniques and the minimization of organic solvent consumption, as the large quantitiesused in analytical laboratories are a pressing environmental problem. Solventless sample preparation techniques, alternative solvents, mediated extractions are discussed. The principle of each technique isbriefly described, together...
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Teaching of Analytical Chemistry in Polisch Universities
PublicationChemia Analityczna zajmuje się poszukiwaniem i opracowywaniem optymalnych strategii (metod i urządzeń) pozwalających na uzyskiwanie miarodajnych informacji dotyczących chemicznej natury różnych obiektów znajdujących się w naszym otoczeniu i przebiegających w nich procesach. Wykorzystanie informacji analitycznej jest bardzo szerokie. Otrzymany wynik jest towarem, tym droższym im jest bardziej miarodajny. Chemik analityk odpowiada...
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Expedited Yield Optimization of Narrow- and Multi-Band Antennas Using Performance-Driven Surrogates
PublicationUncertainty quantification is an important aspect of engineering design, also pertaining to the development and performance evaluation of antenna systems. Manufacturing tolerances as well as other types of uncertainties, related to material parameters (e.g., substrate permittivity) or operating conditions (e.g., bending) may affect the antenna characteristics. In the case of narrow- or multi-band antennas, this usually leads to...
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On the influence of the acceleration recording time on the calculation of impact severity indexes
PublicationThe paper concerns with the analysis of normative requirements pertaining to experimental setup of a crash test and its numerical modelling. An overview of parameters describing the collision of a vehicle with a road restraining system is presented. A short description of a concrete road safety barrier is presented. A brief description of numerical modelling procedures for crash tests is given as well. The parametric influence...
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Report of the ISMIS 2011 Contest : Music Information Retrieval
PublicationThis report presents an overview of the data mining contestorganized in conjunction with the 19th International Symposiumon Methodologies for Intelligent Systems (ISMIS 2011), in days betweenJan 10 and Mar 21, 2011, on TunedIT competition platform. The contestconsisted of two independent tasks, both related to music information retrieval:recognition of music genres and recognition of instruments, for agiven music sample represented...
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Laboratory Stand for Wideband Analysis Radiocommunication Signals
PublicationA laboratory stand for wideband analysis radiocommunication signals is presented in the paper. The stand is designed for signals acquisition in wide spectrum and research a field of digital signal processing. Procedures used for simultaneous acquiring many frequency channels in selected wide band are described. The method of detection of direct sequence spread spectrum signals (DS SS) which power spectral density is lower than...
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Laboratory stand for wideband analysis radiocommunication signals
PublicationA laboratory stand for wideband analysis radiocommunication signals is presented in the paper. The stand is designed for signals acquisition in wide spectrum and research a field of digital signal processing. Procedures used for simultaneous acquiring many frequency channels in selected wide band are described. The method of detection of direct sequence spread spectrum signals (DS SS) which power spectral density is lower than...
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Numerical Studies on Propellers in Open Water and behind Hulls aiming to support the Evaluation of Propulsion Tests
PublicationA RANS based numerical analysis of propellers can contribute considerably to our understanding of propeller/hull interaction. It may also allow for a review of scaling procedures on results from experimental fluid dynamics (EFD). Using various RANS codes (Fluent, CFX, STAR-CCM+ and FreSCo+) on common test cases the authors first focused on propeller open water (POW) calculations. Next we simulated the propeller hull interaction...
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Approximate Quality Criteria for Difficult Multi-Objective Optimization Problems
PublicationThis paper introduces approximate analytic quality criteria useful in assessing the efficiency of evolutionary multi-objective optimization (EMO) procedures. We present a summary of extensive research into computing. In the performed comparative study we take into account the various approaches of the state-of-the-art, in order to objectively assess the EMO performance in highly dimensional spaces; where some executive criteria,...
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Real and imaginary motion classification based on rough set analysis of EEG signals for multimedia applications
PublicationRough set-based approach to the classification of EEG signals of real and imaginary motion is presented. The pre-processing and signal parametrization procedures are described, the rough set theory is briefly introduced, and several classification scenarios and parameters selection methods are proposed. Classification results are provided and discussed with their potential utilization for multimedia applications controlled by the...
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Approximate Quality Criteria for Difficult Multi-Objective Optimization Problems
PublicationThis paper introduces approximate analytic quality criteria useful in assessing the efficiency of evolutionary multi-objective optimization (EMO) procedures. We present a summary of extensive research into computing. In the performed comparative study we take into account the various approaches of the state-of-the-art, in order to objectively assess the EMO performance in highly dimensional spaces; where some executive criteria,...
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Multi-objective optimization for assessment of topological modification in UWB antennas
PublicationThis paper addresses an issue of systematic and rigorous assessment of effects of topological modifications on the performance of compact UWB antennas. Application of fast surrogate-assisted multi-objective optimization procedures allows us for obtaining, in a practically acceptable timeframe, a set of designs representing the best possible trade-offs between conflicting objectives (here, antenna size minimization and reduction...
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Numerical simulation of asphalt mixtures fracture using continuum models
PublicationThe paper considers numerical models of fracture processes of semi-circular asphalt mixture specimens subjected to three-point bending. Parameter calibration of the asphalt mixture constitutive models requires advanced, complex experimental test procedures. The highly non-homogeneous material is numerically modelled by a quasicontinuum model. The computational parameters are averaged data of the components, i.e. asphalt, aggregate...
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Optimization of the System for Determining the Volume of Tissue Needed for Breast Reconstruction
PublicationThis article presents techniques for reconstructing surfaces and volume calculations using a point cloud generated from 3D imaging. The main objective of this article was to optimize the voxel size for the most accurate representation of the surface of the female breast. We experimented with different methods for determining volume using images from the Intel D435i camera. In addition, we designed application and measurement station...
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Recent advances on spinel-based protective coatings for solid oxide cell metallic interconnects produced by electrophoretic deposition
PublicationThe application of ceramic protective coatings to the metallic interconnects in solid oxide cells (SOCs) is a viable and effective method to limit interconnect degradation issues. This featured letter provides a critical overview of the main outcomes of current research on the use of the electrophoretic deposition (EPD) technique to produce protective coatings for SOC metallic interconnects, specifically focusing on different approaches...
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Novel Analytical Techniques, GT 2022
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Ferrofluids based analytical extractions and evaluation of their greenness
PublicationFerrofluids are stable dispersions of magnetic nanoparticles in a carrier liquid. They have attracted considerable attention in analytical extractions as they combine fluid-like properties with magnetic character, providing magnetic control over the extraction process. The synthesis of ferrofluids is very straightforward, and it generally involves the preparation of magnetic nanoparticles, their coating, and then mixing in a suitable...
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Microextraction by packed sorbent: Uncommon detection techniques, sorbents, samples and analytes
PublicationAmong sample preparation approaches, the most desirable are procedures that ensure high efficiency and reproducibility, that are cheap, fast and simple, that minimize the number of operational steps and that require a small amount of sample and solvent and are thus environmentally friendly. Microextraction by packed sorbent (MEPS) is a miniaturized form of solid-phase extraction, the use of which has been continuously expanding...
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Polityka Rozwoju/Development Policy 2022/23
e-Learning CoursesCourse address the challenges of achieving the 11th goal of the Global Sustainable Development Policy (17 Sustainable Development Goals)_ Make cities and human settlements inclusive, safe, resilient and sustainable Lectures are held in a remote formula in the layout of classes blocked according to an individual plan. Starting point TUE the 28th Feb 2023 8.30 am join here! https://teams.microsoft.com/l/meetup-join/19%3ameeting_NTY2ZWNkMmItMWY1Yi00Y2NjLWEwMTQtNjY5ZjExYmExYjk4%40thread.v2/0?context=%7b%22Tid%22%3a%2286760356-0022-486f-b793-a2d470bba5a5%22%2c%22Oid%22%3a%2247795e6d-82a8-484f-89a6-1d30ab1df5c5%22%7d teacher:...
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Polityka Rozwoju/Development Policy 2023/24
e-Learning CoursesThe course addresses the challenges of achieving Goal 11 of the Global Sustainable Development Policy (17 Sustainable Development Goals) to make cities and human settlements inclusive, safe, resilient and sustainable. teacher: dr Gabriela Rembarz grem@pg.edu.pl Lectures are held remotely (TEAMS) in the arrangement of classes blocked according to an individual schedule. Starting point: Wed February 28, 2024, 8:30 a.m. Join under...
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Equivalent standard manoeuvres for pod-driven ships
PublicationProcedures for carrying out the manoeuvring tests presented in International Maritime Organisation (IMO) resolution MSC.137(76) are based on the capabilities of ships with conventional steering-propulsion systems. Therefore they do not correspond to ships with other steering-propulsion devices, like pod drives. IMO is aware of this shortcoming and for ships with non-conventional steering and propulsion system may permit the use...
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Expedited Variable-Resolution Surrogate Modeling of Miniaturized Microwave Passives in Confined Domains
PublicationDesign of miniaturized microwave components is largely based on computational models, primarily, full-wave electromagnetic (EM) simulations. EM analysis is capable of giving an accurate account for cross-coupling effects, substrate and radiation losses, or interactions with environmental components (e.g., connectors). Unfortunately, direct execution of EM-based design tasks such as parametric optimization or uncertainty quantification,...
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Rapid Multi-Criterial Antenna Optimization by Means of Pareto Front Triangulation and Interpolative Design Predictors
PublicationModern antenna systems are designed to meet stringent performance requirements pertinent to both their electrical and field properties. The objectives typically stay in conflict with each other. As the simultaneous improvement of all performance parameters is rarely possible, compromise solutions have to be sought. The most comprehensive information about available design trade-offs can be obtained through multi-objective optimization...
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Mass Spectrometry-Based Direct Analytical Techniques
PublicationDirect analysis of samples is considered as one of the most environmentally sustainable solutions in analytical chemistry. In the ideal case, such solutions do not require sample preparation and analytes separation steps, therefore do not consumpt harmful substances (or consumpt only minimum amounts of them) and do not generate hazardous waste. Technical solutions for direct analysis also offer miniaturized and field-portable analyzers...
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9. Sustainable Development
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European Economic Development
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Green Analytical Chemistry: Summary of Existing Knowledge and Future Trends
PublicationAnalysis of recent publications in green analytical chemistry shows the current trends and future needs in this area. The main issues are related with search for cheaper, more efficient, more accurate, greener and miniaturized alternatives. Miniaturization is perhaps, the most notable current trend in analytical chemistry. Rapid developments and improvements in instrumentation have led to impressive range of benchtop technology...
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Remarks on use of the term “deep eutectic solvent” in analytical chemistry
PublicationAbout 20 years ago, Abbott and co-workers researched new solvents that were based on mixtures of choline chloride with urea and carboxylic acids and that were liquid at ambient temperature. The term “deep eutectic solvent” (DES) was later adopted for similar mixtures. As DESs have a number of interesting features, they quickly attracted the attention of researchers and found application in various branches of chemical and materials...
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Nanoparticles: Synthesis, characteristics, and applications in analytical and other sciences
PublicationNanoparticles (NPs) are widely employed in different research areas, ranging from analytical chemistry and environmental science to medicine, the agriculture and pharmaceutical industry. This is mainly due to the unique characteristics of NPs and the novelty they introduce in such applications. In analytical chemistry, the role of NPs can differ depending on the nature of the steps involved in analytical process. NPs are probably...
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Safety PL - a support tool for Road Safety Impact Assessment
PublicationPublished on 19 November 2008, the European Union's Directive 2008/96/EC is one of the most important EU documents setting out a road safety orientation, in particular, road infrastructure safety management. It identifies four main areas of activity: road safety impact assessment, road safety audit, ranking of high accident concentration sections and network safety ranking and road infrastructure safety inspection. The Directive...
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Application of analytical methods for the determination of bioactive compounds in some berries
PublicationFluorometry, ESI-MS, FTIR, and radical scavenging assays were used for characterization of bioactive compounds and the levels of their antioxidant activities. Polyphenols, flavonoids, anthocyanins, and ascorbic acid and the level of antioxidant activity of water extracts of “Murtilla-like” [Myrteola nummularia (Poiret) Berg.], and other widely consumed berries were determined and compared. The contents of bioactive compounds and...
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"3D-Breast System for Determining the Volume of Tissue Needed for Breast Reconstruction"
PublicationThis article presents methods for surface reconstruction and volume determination based on the point cloud created by 3D imaging. Such a system would be used to accurately estimate breast volume in patients classified for breast reconstruction surgery at plastic surgery centers. To develop such a system, various methods of determining volume, based on images from the Intel D435i camera, were tested. In addition, an application...
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Improving flexibility and performance of PVM applications by distributed partial evaluation
PublicationA new framework for developing both flexible and efficient PVM applications is described. We propose Architecture Templates Interface (ATI) that allows to control application granularity and parallelism. To ensure high application efficiency we extend partial evaluation strategy into domain of distributed applications obtaining Distributed Partial Evaluation (DPE). Both ATI and DPE were implemented using a new distributed programming...
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Magnetic instrumentation and other applications of magnets in NOTES
PublicationModern surgery is developing towards a minimally invasive approach. To minimize the trauma the number of ports is either limited as in single incision laparoscopic procedures or ports are introduced through natural orifices as in nat- ural orifice translumenal endoscopic surgery (NOTES). To provide surgeons with appropriate instrumentation novel technologies are employed involving magnets. This article summarizes the theoretical...
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Reversible Video Stream Anonymization for Video Surveillance Systems Based on Pixels Relocation and Watermarking
PublicationA method of reversible video image regions of interest anonymization for applications in video surveillance systems is described. A short introduction to theanonymization procedures is presented together with the explanation of its relation to visual surveillance. A short review of state of the art of sensitive data protection in media is included. An approach to reversible Region of Interest (ROI) hiding in video is presented,...
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Influence of statistical errors on damage detection based on structuralflexibility and mode shape curvature
PublicationDamage detection procedures based on measured natural frequencies and building structure mode shapes are discussed in this paper. Modal curvature and structural flexibility approaches are tested. Attention is paid to the modal identification errors that influence damage detection. This problem is studied using a computer simulation of a simple supported beam. For practical cases, the peak picking methodand its statistical errors...
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Study of the Operation of Synchronous Generator Voltage Regulator During the Creation of Post Blackout Start-up Path
PublicationThis paper presents the influence of automatic voltage regulator (AVR) of synchronous generator on the process of creation of post black-out start-up path. Two elements of AVR have a significant impact on this process: underexcitation limiter (UEL) and load compensation (LC). The authors present a theoretical investigation and simulation results that illustrate how the mentioned elements of AVR affect voltage levels in a power...
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Reference FEM model for SHM system of cable-stayed bridge in Rzeszów
PublicationThe paper presents the references model for structural health monitoring system (SHM) of cable-stayed bridge recently constructed in Rzeszów over Wisłok River. The SHM system is design to provide on-line information on the structure state and facilitate its maintenance procedures. The main feature of the SHM system is permanent observation of the dynamic behavior of the bridge with focus on cable vibrations. The paper discusses...
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Handwritten signature verification system employing wireless biometric pen
PublicationThe handwritten signature verification system being a part of the developed multimodal biometric banking stand is presented. The hardware component of the solution is described with a focus on the signature acquisition and on verification procedures. The signature is acquired employing an accelerometer and a gyroscope built-in the biometric pen plus pressure sensors for the assessment of the proper pen grip and then the signature...