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Search results for: di-spme
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The Emission and Combustion Characteristics of Marine Diesel Engine with Extreme Throttled of Air or Exhaust Ducts
PublicationPresented paper shows the results of the laboratory tests on the relationship between the extreme throttling of both air intake duct and exhaust gas duct and gaseous emission from the marine engine. The object of research is a laboratory, 4-stroke, DI diesel engine, operated at loads from 50 kW to 250 kW at a constant speed equal to 750 rpm. During the laboratory tests the thermodynamic and exhaust gas emission characteristics...
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Pochodne kwasów ditiokarbaminowych - synteza i budowa
PublicationDitiokarbaminiany - związki powstające w wyniku reakcji amin pierwszo- lub drugorzędowych z disiarczkiem węgla - znalazły zastosowanie m. in. jako ligandy w chemii koordynacyjnej. Ich synteza przebiega według mechanizmu substytucji nukleofilowej SN2, przy czym rolę nukleofila pełni aktywowana przez zasadę amina atakująca centrum elektrofilowe w CS2. Różnorodność połączeń, wynikająca z charakteru grupy >N-CS2-, pozwala na otrzymanie,...
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Pochodne kwasów ditiokarbaminowych - synteza i budowa
PublicationDitiokarbaminiany - związki powstające w wyniku reakcji amin pierwszo- lub drugorzędowych z disiarczkiem węgla - znalazły zastosowanie m. in. jako ligandy w chemii koordynacyjnej. Ich synteza przebiega według mechanizmu substytucji nukleofilowej SN2, przy czym rolę nukleofila pełni aktywowana przez zasadę amina atakująca centrum elektrofilowe w CS2. Różnorodność połączeń, wynikająca z charakteru grupy >N-CS2-, pozwala na otrzymanie,...
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The influence of frequency separation on imaging properties in DFEIT
PublicationW artykule przedstawiono wpływ wyboru składowych częstotliwościowych dla różnicowej tomografii impedancyjnej na wynik i własności obrazowania w dwuczęstotliwościowej różnicowej tomografii impedancyjnej.A Dual Frequency EIT is an extension of a traditional EIT that uses two sinusoidal signals for imaging. Appropriate selection of signals' frequency allows to achieve reasonable contrast of imaged structure. It has already been shown...
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Tuning of photocatalytic activity by creating a tridentate coordination sphere for palladium
PublicationThe synthesis and characterisation of an asymmetric potential bridging ligand bmptpphz (bmptpphz = 2,17-bis(4-methoxyphenyl)tetrapyrido[3,2-a:2’,3’-c:3’’,2’’-h:2’’’,3’’’-j] phenazine) is presented. This ligand contains a 1,10-phenanthroline (phen) and a 2,9-disubstituted phen sphere and possesses a strong absorbance in the visible. Facile coordination of the phen sphere to a Ru(tbbpy)2 core leads to Ru(bmptpphz) ([(tbbpy)2Ru(bmptpphz)](PF6)2;...
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Processing, physico-mechanical and thermal properties of reclaimed GTR and NBR/reclaimed GTR blends as function of various additives
PublicationIn this work, ground tire rubber (GTR) was mechano-chemically reclaimed in the presence of bitumen and various additives. During studies three types of processing and curing additives: (i) peptizer P300; (ii) vulcanization accelerator tetramethylthiuram disulfide (TMTD) and (iii) organic peroxide di(2-tert-butyl-peroxyisopropyl)benzene (BIB1) were applied to enhance reclaiming of GTR. Reclaiming process was evaluated by oscillating...
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Morphology, Thermo-Mechanical Properties and Biodegradibility of PCL/PLA Blends Reactively Compatibilized by Different Organic Peroxides
PublicationReactive blending is a promising approach for the sustainable development of bio-based polymer blends and composites, which currently is gaining more and more attention. In this paper, biodegradable blends based on poly(ε-caprolactone) (PCL) and poly(lactic acid) (PLA) were prepared via reactive blending performed in an internal mixer. The PCL and PLA content varied in a ratio of 70/30 and 55/45. Reactive modification of PCL/PLA...
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Zagospodarowanie ciepła odpadowego z biogazowych agregatów kogeneracyjnych w oczyszczalni ścieków = Waste heat utilisation from cogeneration set in sewage plant
PublicationW pracy opisano koncepcję współpracy biogazowych modułów kogeneracyjnych z niskotemperaturowym obiegiem parowym. Proponowana modernizacja pozwoliłaby na wykorzystanie entalpii fizycznej spalin, tym samym zwiększając sprawność urządzeń wytwarzających ciepło i energię elektryczną. Tego typu rozwiązanie umożliwiłoby częściowe pokrycie zapotrzebowania własnego na energię elektryczną, generując oszczędności w przedsiębiorstwie. W artykule...
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Zagospodarowanie ciepła odpadowego z biogazowych agregatów kogeneracyjnych w oczyszczalni ścieków
PublicationW pracy opisano koncepcję współpracy biogazowych modułów kogeneracyjnych z niskotemperaturowym obiegiem parowym. Proponowana modernizacja pozwoliłaby na wykorzystanie entalpii fizycznej spalin, tym samym zwiększając sprawność urządzeń wytwarzających ciepło i energię elektryczną. Tego typu rozwiązanie umożliwiłoby częściowe pokrycie zapotrzebowania własnego na energię elektryczną, generując oszczędności w przedsiębiorstwie. W artykule...
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Chemical characterization of wild populations of Brassica oleracea complex species (n=9) for the content of their bioactive compounds
PublicationThe wild species belonging to Brassica oleracea complex species (n=9) are widespread in the Mediterranean basin and represent the relative species of several vegetable crops, such as broccoli, cauliflower, kale, cabbage. They are characterized by the high level of bioactive compounds, such as glucosinolates (GLSs), known for their benefits for human health. Four accessions were evaluated: B. macrocarpa (BM) from Favignana (Trapani),...
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Weak forms of shadowing in topological dynamics
PublicationWe consider continuous maps of compact metric spaces. It is proved that every pseudotrajectory with sufficiently small errors contains a subsequence of positive density that is point-wise close to a subsequence of an exact trajectory with the same indices. Also, we study homeomor- phisms such that any pseudotrajectory can be shadowed by a finite number of exact orbits. In terms of numerical methods this property (we call it multishadowing)...
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Entrepreneurship nests in a polish edge city
PublicationThe last two decades in Poland have been a period of both a dynamic development of the small and medium-sized enterprise sector and a transformation of the city surrounding territories. This development began during the economy transformation after 1989. Population migration and movement of economic entities away from central cities resulted in development of territorial structures within some Polish suburban areas, defined as...
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Silica-Based Ionogels: Nanoconfined Ionic Liquid-Rich Fibers for Headspace Solid-Phase Microextraction Coupled with Gas Chromatography–Barrier Discharge Ionization Detection
PublicationIn this work, hybrid silica-based materials with immobilized ionic liquids (ILs) were prepared by sol–gel technology and evaluated as solid-phase microextraction (SPME) fiber coatings. High loadings of the IL 1-methyl-3-butylimidazolium bis(trifluoromethylsulfonyl)imide ([C4MIM][TFSI]) were confined within the hybrid network. Coatings composition and morphology were evaluated using scanning electron microscopy and energy dispersive...
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Comparison of pavement noise properties on selected road sections using different CPX measuring systems: self-powered vehicle and special test trailer
PublicationThe recently published ISO standard intended to measure the noise properties of road surfaces in a standardized method (ISO 11819-2:2017) precisely defines measurement procedure of the influence of road surface on traffic noise. According to it, two types of test vehicles may be utilized: a self-powered vehicle fitted with one or more test tyres and a trailer towed by a separate vehicle with one or more test tyres mounted on the...
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Heat transfer intensification by enlarged surface roughness in the plate heat exchanger
PublicationIn the paper an experimental analysis of passive heat transfer intensification technique employed in the case of the plate heat exchanger is presented. The passive intensification was obtained by a modification of the heat transfer surface. The roughness of surface was increased by a use of glass micro-beads. Single-phase convective heat transfer in the water-water system was studied. The experiment was accomplished in two stages....
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The EU Tyre Noise Label: The problem with measuring the noise level of only a few of all tyre variants
PublicationThe STEER project, described in another Inter-Noise 2022 paper, has evaluated the performance of the noise label of the European tyre label. The major finding was that uncertainties of the tyre/road noise measurements were higher than should be accepted. One of the worst uncertainty sources was found to be the common practice to measure only some tyres of all sizes or variants within a tyre line, to save money. Generally, only...
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Determination of antifreeze substances in the airport runoff waters by solid-phase microextraction and gas chromatography–mass spectrometry method
PublicationA new method has been developed for the determination of antifreeze agents such as ethylene glycol (EG), propylene glycol (PG), and diethylene glycol (DEG) in the samples of airport runoff water. The method is based on headspace solid–phase microextraction (HS–SPME) of target analytes, which is coupled with gas chromatography–mass spectrometry (GC–MS). Until now, there was a lack of appropriate methodology for collecting reliable...
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Potentiometric sensor containing set of ion selective electrodes with lipid modified membranes for quality assessment of tested non-alcoholic beverages
PublicationPotentiometric sensors may be a good tool for fast quality control of commercial drinks. In this work, such a sensor, containing a set of ion-selective electrodes with lipid-modified membranes (benzylhexadecyldimethylammonium chloride monohydrate, hexadecylamine, 1-dodecanol, elaidic acid, cholesterol) was used for discrimination and quality control of non-alcoholic beverages, mainly composed of sugar and citric acid. It was found...
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Efektywna metoda selenenylowania z użyciem diselenidu O,O-diizopropylofosforotioilowego
PublicationTworzenie wiązania C-Se odbywa się zwykle z wykorzystaniem elektrofilowego bromku fenyloselenenylowego generowanego in situ z diselenidu difenylowego. Fenyloselenenylowanie soli sodowych malonianów, użytych z 10-krotnym nadmiarem, prowadzi do powstawania znaczących ilości di(fenyloselenenylo)malonianów obok głównych produktów mono-selenenylowania. 2-Fenyloselenenylomaloniany wykorzystano m.in. w reakcji rodnikowej addycji do wiązania...
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Poly(ε-Caprolactone)/Poly(Lactic Acid) Blends Compatibilized by Peroxide Initiators: Comparison of Two Strategies
PublicationPoly(ε-caprolactone) (PCL) and poly(lactic acid) (PLA) blends were compatibilized by reactive blending and by copolymers formed during reaction in the solution. The reactive blending of PCL/PLA was performed using di-(2-tert-butyl-peroxyisopropyl)benzene (BIB) or dicumyl peroxide (DCP) as radical initiator. PCL-g-PLA copolymers were prepared using 1.0 wt. % of DCP or BIB via reaction in solution, which was investigated through...
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Metamaterial-Based Series-Fed Antenna with High Gain and Wideband Performance for Millimeter Wave Spectrum Applications
PublicationThis paper presents a high-gain, wideband series-fed antenna designed for 5G millimeter-wave (MMW) applications. The structure employs a substrate-integrated waveguide (SIW)-based power splitter and metamaterials (MMs). The power divider functions effectively at 27.5 GHz, exhibiting an impedance bandwidth from 26.9–28.6 GHz. The series-fed dipole is assembled on the SIW-based power splitter, incorporating four dipoles with varying...
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Entangled Histories vs. the Two-State-Vector Formalism - Towards a Better Understanding of Quantum Temporal Correlations
PublicationThe Two-State-Vector formalism and the Entangled Histories formalism are attempts to betterunderstand quantum correlations in time. Both formalisms share some similarities, but they are notidentical, having subtle differences in their interpretation and manipulation of quantum temporalstructures. However, the main objective of this paper is to prove that, with appropriately definedscalar products, both formalisms can be...
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Automatic sound source localization in disturbing conditions using acoustic vector sensors
PublicationA concept, practical realization and applications of a passive acoustic radar to automatic localization and tracking of sound sources in disturbing conditions were presented in the paper. The device consists of the new kind of multichannel miniature sound intensity sensors and a group of digital signal processing algorithms. The sensitivity of the realized acoustic radar was examined in free sound field. Several kinds of sound...
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Aerodynamic shape optimization by variable-fidelity computational fluid dynamics models: a review of recent progress
PublicationA brief review of some recent variable-fidelity aerodynamic shape optimization methods is presented.We discuss three techniques that—by exploiting information embedded in low-fidelity computationalfluid dynamics (CFD) models—are able to yield a satisfactory design at a low computational cost, usu-ally corresponding to a few evaluations of the original, high-fidelity CFD model to be optimized. Thespecific techniques considered here...
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Relativity of arithmetic as a fundamental symmetry of physics
PublicationArithmetic operations can be defined in various ways, even if one assumes commutativity and associativity of addition and multiplication, and distributivity of multiplication with respect to addition. In consequence, whenever one encounters ‘plus’ or ‘times’ one has certain freedom of interpreting this operation. This leads to some freedom in definitions of derivatives, integrals and, thus, practically all equations occurring in...
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Shaping the New Vistula Spit Channel: Political, Economic, and Environmental Aspects
PublicationIn September 2022, the new shipping channel in Poland was opened for service. It connects the Port of Elbląg and the Gdańsk Bay in Poland, cutting through the Vistula Spit and the Vistula Lagoon. It was intended to enable direct access to the Baltic Sea from the Port of Elbląg without crossing Russian territory. Originally conceptualized decades ago, it has taken its final shape only recently. Its construction was associated with...
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Development of a Formability Prediction Model for Aluminium Sandwich Panels with Polymer Core
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Cover Feature: Electronic Circular Dichroism Imaging (ECD i ) Casts a New Light on the Origin of Solid‐State Chiroptical Properties (Chem. Eur. J. 4/2022)
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Higginsianins D and E, Cytotoxic Diterpenoids Produced by Colletotrichum higginsianum
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Circular Dichroism Imaging: Mapping the Local Supramolecular Order in Thin Films of Chiral Functional Polymers
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Rabenchromenone and Rabenzophenone, Phytotoxic Tetrasubstituted Chromenone and Hexasubstituted Benzophenone Constituents Produced by the Oak-Decline-Associated Fungus Fimetariella rabenhorstii
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Electronic Circular Dichroism Imaging (ECD i ) Casts a New Light on the Origin of Solid‐State Chiroptical Properties
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Properties of an innovative multi-functional finish for the improvement of indoor air quality
PublicationDue to lifestyle changes, people spend most of their time indoors at present; thus, Indoor Air Quality (IAQ) is a matter of utmost importance. Multi-functional and innovative finishes can help to passively improve the IAQ, benefitting the health and comfort of occupants. For this study, reference and pre-mixed commercial mortars are compared to a new multi-functional hydraulic lime mortar for indoor finishes, in which conventional...
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Trends in solventless sample preparation techniques for environmental analysis
PublicationPraca przedstawia najnowsze tendencje w metodach przygotowania próbek do analizy środowiskowej. Najpierw przedstawiono klasyfikację tzw. bezrozpuszczalnikowych technik przygotowania próbek. Następnie, szczegółowo przedstawiono trzy techniki, traktowane priorytetowo, a mianowicie: mikroekstrakcję do fazy stacjonarnej (SPME), ekstrakcję do pojedynczej kropli (SPME)i analizę fazy nadpowierzchniowej (HS), w odniesieniu do ich użyteczności...
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Revising Entrepreneurial Orientation Construct in Social Enterprise
PublicationEntrepreneurial behavior and entrepreneurial orientation (EO) have received significant scholarly attention in entrepreneurship and management research, but mainly in the commercial context. However, some attempts discussing such behavior and EO among non-profit organizations, but limited in the social enterprise context. The literature argues that EO is higher in such contexts (Zahra, Gedajlovic, Neubaum & Shulman, 2009; Lumpkin,...
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On adaptive covariance and spectrum estimation of locally stationary multivariate processes
PublicationWhen estimating the correlation/spectral structure of a locally stationary process, one has to make two important decisions. First, one should choose the so-called estimation bandwidth, inversely proportional to the effective width of the local analysis window, in the way that complies with the degree of signal nonstationarity. Too small bandwidth may result in an excessive estimation bias, while too large bandwidth may cause excessive...
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Museum of the Second World War in Gdansk as an Example of Contemporary Design Trends in Museum Buildings
PublicationAt a time when history gives us one of the last opportunities to confront our knowledge of World War II, with the knowledge of people living in those days, there are buildings created with strong transmission not only architectural, but also of a great emotional load. At the same time, when the political system does not forbid to speak openly about the past period, and the technology allows you to create structures, about which...
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Sample preparation for gas chromatographic determination of halogenated volatile organic compounds in environmental and biological samples
PublicationPodstawowym elementem przygotowania próbek środowiskowych i biologicznych do analizy jest etap izolacji i/lub wzbogacania polegający na przeniesieniu analitów z matrycy pierwotnej charakteryzującej się złożonym i często zmiennym składem (próbka oryginalna) do matrycy wtórnej z równoczesnym usunięciem substancji przeszkadzających (izolacja)i zwiększeniem stężenia analitów do poziomu powyżej granicy oznaczalności stosowanego przyrządu...
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Multivariate Assessment of Procedures for Molecularly Imprinted Polymer Synthesis for Pesticides Determination in Environmental and Agricultural Samples
PublicationIn the case of quantitative and qualitative analysis of pesticides in environmental and food samples, it is required to perform a sample pre-treatment process. It allows to minimalize the impact of interferences on the final results, as well as increase the recovery rate. Nowadays, apart from routinely employed sample preparation techniques such as solid-phase extraction (SPE) or solid-phase microextraction (SPME), the application...
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Analysis of turnouts with non-linear curvature of diverging track for different train running speeds
PublicationThe paper deals with the issue of shaping a variable curvature in the diverging track of the railway turnout. Solution without a circular arc in the central zone, comprising two zones of non-linear curvature, of the same length, having zero curvature values at the end points, was adopted as a model, on the basis of the previously conducted dynamic tests. Optimum type of curvature was selected from the point of view of the kinematic...
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Qualia: About Personal Emotions Representing Temporal Form of Impressions - Implementation Hypothesis and Application Example
PublicationThe aim of this article is to present the new extension of the xEmotion system as a computerized emotional system, part of an Intelligent System of Decision making (ISD) that combines the theories of affective psychology and philosophy of mind. At the same time, the authors try to find a practical impulse or evidence for a general reflection on the treatment of emotions as transitional states, which at some point may lead to the...
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Acoustic evaluation of road surfaces using different Close Proximity testing devices
PublicationAccording to the valid standard, Close Proximity (CPX) method intends to evaluate the influence of road surfaces on traffic noise. Measurements may be carried out with the use of a self-powered vehicle or a special test trailer equipped with testing tyre towed by another vehicle. Two different testing devices took part in the research organized in Poland in order to determine the ranking of road surfaces in terms of acoustic parameters....
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CSR and small business from the international and national perspective
PublicationCorporate and social responsibility is nowadays quite a popular topic among large companies but thanks to numerous popularization activities undertaken by national and international institutions, also small entrepreneurs become more and more interested in exploring this fairly new approach. This paper outlines the main differences between the implementation of the CSR approach in large companies and in SMEs, which are not able...
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On the current state of dovetail wall-corner joints in wooden Greek Catholic churches in Polish Subcarpathia with structural and sensitivity analyses
PublicationThis paper describes the current condition of some dovetail joints which form the wall corners of two Greek Catholic churches of wooden construction in Polish Subcarpathia. It also gives the historical background of the sacral architecture of that region. The two structures, which represent the same type of log corner joints are situated in Chotylub and Cewków. The buildings were examined e.g. for damage, wood moisture content,...
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Rotational state-changing collisions of C2H− and C2N− anions with He under interstellar and cold ion trap conditions: A computational comparison
PublicationWe present an extensive range of quantum calculations for the state-changing rotational dynamics involving two simple molecular anions that are expected to play some role in the evolutionary analysis of chemical networks in the interstellar environments, C2H− (X1Σ+) and C2N− (X3Σ−), but for which inelastic rates are only known for C2H−. The same systems are also of direct interest in modeling selective photo-detachment experiments...
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The influence of polymer bearing material and lubricating grooves layout on wear of journal bearings lubricated with contaminated water
PublicationThe goal of the present paper is to investigate wear properties of journal sliding bearing operating in the conditions of contaminated water lubrication. Several bearing materials and bearing sleeve designs (differing in the axial grooves position and their shape) were tested experimentally under typical operating conditions in a dedicated test rig, which was equipped with a lubricating system, enabling lubrication with contaminated...
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The effect of aeration mode (intermittent vs. continuous) on nutrient removal and greenhouse gas emissions in the wastewater treatment plant of Corleone (Italy)
PublicationThe paper reports the results of an experimental study aimed at comparing two configurations of a full-scale wastewater treatment plant (WWTP): conventional activated sludge (CAS) and oxic-settling-anaerobic process (OSA) with intermittent aeration (IA). A comprehensive monitoring campaign was carried out to assess multiple parameters for comparing the two configurations: carbon and nutrient removal, greenhouse gas emissions, respirometric...
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Immunization with an anti-idiotypic antibody against the broadly lipopolysaccharide-reactive antibody WN1 222-5 induces Escherichia coli R3-core-type specific antibodies in rabbits
PublicationThe mouse monoclonal antibody (mAb) WN1 222-5 recognizes a carbohydrate epitope in the inner core region of LPS that is shared by all strains of Escherichia coli and Salmonella enterica and is able to neutralize their endotoxic activity in vitro and in vivo. Immunization of mice with mAb WN1 222-5 yielded several anti-idiotypic mAbs one of which (mAb S81-19) competitively inhibited binding of mAb WN1 222-5 to E. coli and Salmonella...
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Lean Six Sigma in French and Polish Small and Medium-Sized Enterprises - The Pilot Research Results
PublicationThe article presents results of the research conducted in Polish and French small and medium-sized enterprises referring to the context of the implementation and application of the concept of Lean Six Sigma. The research was conducted in the form of case studies, observations and individual interviews. The pilot studies led to the identification of the needs, expectations, concerns and experiences of these companies. At the same...
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How to enhance perception of reassembled but incomplete works of ancient art? Eye-tracking study of virtual anastylosis.
Publicationn 1964 the Venice Charter described anastylosis as the only acceptable method of reassembly of architectural remains. Although the scientific community has agreed with the Charter’s decision, many questions pertaining to the technical and aesthetic aspects of anastylosis remain unanswered. Virtual anastylosis seems one of the most promising digital solutions to finding at least some answers, as it permits testing various solutions...