Search results for: microsocope
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Wpływ azotowania jarzeniowego i laserowego nadtapiania na odporność kawitacyjną stali X5CrNi18-10
PublicationNierdzewne stale austenityczne charakteryzują się doskonałą odpornością korozyjną, aczkolwiek niskimi właściwościami mechanicznymi. W wielu przypadkach ogranicza to ich eksploatację w warunkach przemysłowych. Ponadto, nierdzewne stale austenityczne są wrażliwe na korozję lokalną w obecności jonów halogenkowych. Technologie materiałowe, które dają potencjalne możliwości otrzymywania korzystnego wpływu na właściwości mechaniczne...
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SEM micrographs and photos of salivary gland stones
Open Research DataThis dataset contains SEM micrographs and high-resolution photographs taken for salivary gland stones (sialolith) extracted during joint studies between Medical University of Gdansk and Gdansk University of Technology.
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SEM image and line EDS of SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C
Open Research DataThis dataset contains image of the SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C with line EDS analysis results. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope (SEM) with an accelerating voltage of 20 kV in a high vacuum mode. The chemical compositions of the investigated powder...
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Luminescence of TeO2:Eu thin films
Open Research DataTellurium dioxide doped by europium thin films were deposited by magnetron sputtering method and simultaneously heated at 200 oC. Presence of Eu ions and their valence states was confirmed by X-ray photoemission spectroscopy measurements. The structure of the films as well as the influence of europium dopant on crystalline structure of the films was...
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Nanomateriały o właściwościach magnetycznych, fotokatalitycznych, biobójczych
PublicationTematyka badawcza pracy doktorskiej obejmuje preparatykę i charakterystykę nanomateriałów o właściwościach magnetycznych, fotokatalitycznych, biobójczych. Celem pracy była preparatyka nanomateriałów na bazie TiO2 oraz ZnFe2O4 oraz zastosowanie nanokompozytów w fotokatalizie heterogenicznej do degradacji ksenobiotyków niepodatnych na rozkład biologiczny i otrzymywania funkcjonalnych materiałów budowlanych. Otrzymane nanokompozyty...
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EXPERIMENTAL AND NUMERICAL INVESTIGATIONS OF CONCRETE BEHAVIOUR AT MESO-LEVEL DURING QUASI-STATIC SPLITTING TENSION
PublicationThe paper describes experimental and numerical results of quasi-static splitting tensile tests on concrete specimens at meso-scale level. The loading strip was made of plywood or steel. Fracture in concrete was detected at the aggregate level by means of three non-destructive methods: 3D x-ray micro-computed tomography, 2D scanning electron microscope and manual 2D digital microscope. The discrete element method was used to directly...
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Effect of hybrid modification by ceramic layer formation in MAO process and laser remelting on the structure of titanium bio-alloy Ti13Nb13Zr
PublicationTo improve the biological properties of titanium alloy Ti13Nb13Zr, hybrid modifications involving micro-arc oxidation (MAO) and Nd: YAG laser remelting were carried out in two combinations. The first consisted of laser modification before the production of the ceramic layer by the micro-arc oxidation process, and the second combination involved Nd: YAG laser modification after the MAO process. The creation of developed surface...
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Impedance evaluation of coatings from biobased material
PublicationThe authors propose a modification of sodium caseinate edible coating for foodstuff protection. The aim was to improve the film’s barrier properties. It was achieved by the addition of propolis, which is a natural, environmentally friendly product known from its intrinsic sealing action. In the next step, propolis-admixed sodium caseinate films were exposed to elevated temperature for 10 min. This approach was meant to improve...
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TEM micrographs of V2O5 nanostructures
Open Research DataThe DataSet contains the TEM images of V2O5 nanostructures obtained by the sol-gel method.
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Synergistic effect of multi walled carbon nanotubes and reduced graphene oxides in natural rubber for sensing application
PublicationUtilizing the electrical properties of polymer nanocomposites is an important strategy to develop high performance solvent sensors. Here we report the synergistic effect of multi walled carbon nanotubes (MWCNTs) and reduced graphene oxide (RGO) in regulating the sensitivity of the naturally occurring elastomer, natural rubber (NR). Composites were fabricated by dispersing CNTs alone and together with exfoliated RGO sheets (thermally...
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Chemical and structural studies of screen-printed carbon electrodes (SPCE) with boron-doped diamond foils
Open Research DataThis dataset contains chemical analyses and structural studies by XPS and Raman spectroscopy, carried out for SPCE containing boron-doped diamond BDD foils done with scanning electron microscope. Different points for XPS analysis mark different electrode spots: A) working electrode, B) reference electrode, C) counter electrode, D) pads.
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K07
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K06
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K04
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - PARAFFIN OIL. Specim. set K08
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: PARAFFIN OIL. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig:...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K02
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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Results of SEM examination of nanohydroxyapatite coatings doped nanoCu particles on Ti13Zr13Nb alloy
Open Research DataThe database contains the images of the microstructure of the coatings observed with the SEM scanning electron microscope. The nanohydroxyapatite (nanoHAp) with the addition of copper nanoparticle (nanoCu) coatings deposited on the Ti13Zr13Nb alloy by an electrophoresis process were tested. Two different fractions of nanoCu (with average particles size...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K05
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K03
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). No lubrication (DRY). Specim. set K01
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DRY. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig: TPZ-1...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - PARAFFIN OIL. Specim. set K09
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: PARAFFIN OIL. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test rig:...
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Optical microsc. images of wear marks on ball (JPG). Reciprocating siding friction tests. Ball-on-flat contact. Sintered alumina ceramics (98%). Lubricant - DISTILLED WATER. Specim. set K06
Open Research DataOptical microscope images of wear zone on the 5mm diam. ceramic ball used in tests as the fixed specimen.Friction and wear tests in ball-on-flat contact. Both specimens made of sintered alumina ceramics (98%) - self-mated contact.Linear reciprocating motion.Lubrication: DISTILLED WATER. Sliding velocity (peak): 0.1 m/s. Load (normal force): 5N. Test...
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Influence of bio-polyols with different molecular weight on properites of PUR-PIR foams
Open Research DataThis work attempts to validate the possibility of replacing petrochemical polyols with previously synthesized bio-polyols and their impact on the structure and properties of rigid polyurethane-polyisocyanurate (PUR-PIR). The influence of bio-polyols addition on foam properties was investigated by mechanical testing, Fourier transform infrared spectroscopy...
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Tin oxide nanoparticles from laser ablation encapsulated in a carbonaceous matrix – a negative electrode in lithium-ion battery applications
PublicationThis report concerns carbonaceous electrodes doped with tin(II) oxide nanoparticles. Tin nanoparticles are obtained by pulsed laser ablation in water. Crystalline nanoparticles have been encapsulated in a carbonaceous matrix formed after pyrolysis of a mixture consisting of tin/tin(IV) oxide nanoparticles and gelatine. The obtained material is characterized by means of X-ray diffraction, selected area diffraction, scanning electron...
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Evolution of Ag nanostructures created from thin films: UV–vis absorption and its theoretical predictions
PublicationAg-based plasmonic nanostructures were manufactured by thermal annealing of thin metallic films. Structure and morphology were studied using scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HR-TEM) and X-ray photoelectron spectroscopy (XPS). SEM images show that the formation of nanostructures is influenced by the initial layer thickness as well as the...
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Preparation of Well-Compatibilized PP/PC Blends and Foams Thereof
PublicationThe performance of polypropylene-poly(ethylene brassylate) block and graft copolymers and a polypropylene-polycaprolactone graft copolymer as compatibilizers for polypropylene-rich polypropylene/bisphenol A polycarbonate (PP/PC, 80/20 wt/wt) blends was elucidated. The copolymers were synthesized either by metal-catalyzed ring-opening polymerization or transesterification of a presynthesized polyester, initiated by hydroxyl-functionalized...
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Nanotubular Oxide Layer Formed on Helix Surfaces of Dental Screw Implants
PublicationSurface modification is used to extend the life of implants. To increase the corrosion resistance and improve the biocompatibility of metal implant materials, oxidation of the Ti-13Nb- 13Zr titanium alloy was used. The samples used for the research had the shape of a helix with a metric thread, with their geometry imitating a dental implant. The oxide layer was produced by a standard electrochemical method in an environment of...
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Discrete element method simulations of fracture in concrete under uniaxial compression based on its real internal structure
PublicationThe paper describes experimental and numerical results of concrete fracture under quasi-static uniaxial compression. Experimental uniaxial compression tests were performed on concrete cubic specimens. Fracture in concrete was detected at the aggregate level by means of three non-destructive methods: three-dimensional X-ray microcomputed tomography, two-dimensional scanning electron microscope and manual two-dimensional digital...
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SEM images of Solid Oxide Fuel Cell interface with La0.6Sr0.4Co0.2Fe0.8O3-δ oxygen electrodes sintered at 1050 °C before and after test
Open Research DataThis dataset contains cross section SEM images of Solid Oxide Fuel Cell interface with La0.6Sr0.4Co0.2Fe0.8O3-δ oxygen electrode sintered at 1050 °C before and after test. The cell was tested using Open Flanges™ test Set-up at 700 °C. During the test, the cell was aged for approximately 120 hours at a load of 0.5 A/cm^2. Images were obtained using...
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SEM images of Solid Oxide Fuel Cell interface with Sr0.95Ti0.30Fe0.70O3-d oxygen electrodes sintered at 800 °C before and after test
Open Research DataThis dataset contains cross section SEM images of Solid Oxide Fuel Cell interface with Sr0.95Ti0.30Fe0.70O3-d oxygen electrode sintered at 800 °C before and after test. The cell was tested using Open Flanges™ test Set-up at 700 °C. During the test, the cell was aged for approximately 120 hours at a load of 0.5 A/cm^2. Images were obtained using a FEI...
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Topography studies of multiple times processed poly(lactic acid)-carbon black composites
Open Research DataThis dataset contains topography studies with scanning electron microscope of commercially available ProtoPasta 3D printable filament, composed of poly-lactic acid (PLA) and conductive carbon black (CB) filler. The aim of the study is to observe structural differences and applied properties changes under multiple reprocessing of the composite material...
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XRD patterns of the V2O5 coatings after thermal treatment under reducing atmosphere
Open Research DataThe DataSet contains the XRD patterns of V2O5 coatings on the silicon substrate after thermal treatment under a reducing atmosphere. Thin films were annealed at 500C, 600C, and 700C for 10 under a reducing atmosphere (94% Ar, 6% H2).
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The microstructure of aluminium alloys AA1050 and AA7075 subjected to anodic polarization at 8V in KOH electrolyte
Open Research DataThe dataset contains SEM pictures of the microstructure of aluminum alloy AA1050 and AA7075 exposed in aqueous KOH in the pH range between 14–11. Two sets of samples are presented, revealing the topography of the alloys when exposed to aggressive media under open circuit potential conditions as well as when subjected potentiodynamic polarization ranging...
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Nitrogen-Doped Diamond Film for Optical Investigation of Hemoglobin Concentration
PublicationIn this work we present the fabrication and characterization of a diamond film which can be utilized in the construction of optical sensors for the investigation of biological samples. We produced a nitrogen-doped diamond (NDD) film using a microwave plasma enhanced chemical vapor deposition (MWPECVD) system. The NDD film was investigated with the use of scanning electron microscopy (SEM), atomic force microscopy (AFM) and Raman...
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Structural and mechanical properties of hydroxyapatite coatings formed by ion-beam assisted deposition
PublicationThe ion-beam assisted deposition (IBAD) is an advanced method capable of producing crystalline coatings at low temperatures. We determined the characteristics of hydroxyapatite Ca10(PO4)6(OH)2 target and coatings formed by IBAD using X-ray photoemission spectroscopy (XPS), X-ray diffraction (XRD), scanning electron microscopy (SEM), atomic force microscopy (AFM) and energy dispersive X-ray (EDX). The composition of the coatings'...
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Performance of organic coatings upon cyclic mechanical load
PublicationA number of engineering structures fail due to the fatigue damage resulting from cyclic mechanical stress. However, as far as organic coatings are concerned this degradation factor remains underestimated. In the paper the authors propose a methodology combining global electrochemical impedance spectroscopy and local atomic force microscopy measurements for evaluation of coating resistance to an impact of repetitive mechanical stress. Typical...
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Correlations of structural, thermal and electrical properties of sodium doped complex borophosphosilicate glass
PublicationBorophosphosilicate glasses with varying sodium ion concentrations were investigated for their, structural, thermal, and electrical properties. All the obtained glasses were transparent except the glass with the highest sodium content, which exhibited translucency due to inhomogeneities. Increasing sodium content led to reduced boron and silicon content while maintaining a constant B/Si ratio, indicating progressive depolymerization...
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Nonlinear and linear impedance of bismuth vanadate ceramics and its relation to structural properties
PublicationThe nonlinear and linear electrical properties, topography, and microstructure of bismuth-vanadate ceramics, were studied. The structurewas observed with the use of X-ray diffraction (XRD), scanning electronmicroscopy (SEM), atomic force microscopy (AFM) and confocal microscopy methods. The obtained results showed that ceramic is porous. Two phase transitionswere determinedwith the use of DSC measurements. The linear and nonlinear ac...
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Design and Application of Magnetic Photocatalysts for Water Treatment. The Effect of Particle Charge on Surface
PublicationCore-interlayer-shell Fe3O4/SiO2/TiO2, CoFe2O4/SiO2/TiO2 and BaFe12O19/SiO2/TiO2 magnetic photocatalysts were obtained. A water-in-oil microemulsion system with suitable surfactants was used for functionalization of the magnetic core with silica interlayer and TiO2-based photocatalyst. Uncoated and coated particles were characterized by electrophoretic meaurements, X-ray diffractometry (XRD), scanning electron microscopy (SEM),...
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Evaluation of adhesive forces and the specific surface energy of zirconia stabilized by yttria with alumina additions ceramic by AFM method
PublicationThe adhesive forces and the specific surface energy of ceramic material surfaces are very important for further tribological and biomedical applications of ceramics. Partially stabilized zirconia (zirconium oxide) is popular for manufacturing various medical products. ZrO2 stabilized by Y2O3 with additions of 5 wt% alumina was produced by slip casting method with a subsequent sintering. Structure and chemical composition of ceramic...
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Influence of electropolymerization conditions on the morphological and electrical properties of PEDOT film
PublicationIn this work the effects of electropolymerization conditions on the morphological properties and conductivity of poly(3,4-ethylenedioxythiophene) (PEDOT) film have been studied. PEDOT films were electrochemically synthesized in a one step process from acetonitrile solution containing 3,4-ethylenedioxythiophene (EDOT) and lithium perchlorate. Based on atomic force microscopy, scanning electron microscopy, cyclic voltammetry and...
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Fibrillar aggregates in powdered milk
PublicationThis research paper addresses the hypothesis that powdered milk may contain amyloid fibrils. Amyloids are fibrillar aggregates of proteins. Up to this time, research on the presence of amyloids in food products are scarce. To check the hypothesis we performed thioflavin T fluorescence assay, X-ray powder diffraction, atomic force microscopy and fluorescence microscopy imaging. Our preliminary results show that commercially available...
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Images revealing the effect of local femtosecond laser ablation of conductive poly(lactic acid) 3D printed electrodes
Open Research DataThe dataset reveals the images of the femtosecond laser (FSL) ablation at the surface of commercially available carbon black-filled poly(lactic acid) 3D printed electrode. The process is used for the increase of the charge transfer of this electrode in electrochemical studies.
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High-Temperature Tensile Behaviour of GTAW Joints of P92 Steel and Alloy 617 for Two Different Fillers
PublicationThis study explores the high-temperature (HT) tensile rupture characteristics of a dissimilar gas-tungsten-arc-welded (GTAW) joint between P92 steel and Alloy 617, fabricated using ER62SB9 and ERNiCrCoMo-1 fillers. The high-temperature tensile tests were performed at elevated temperatures of 550 ◦C and 650 ◦C. An optical microscope (OM) and a field emission scanning electron microscope (FESEM) were utilized to characterize the...
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Validation of polyurethane-wood composites properties
Open Research DataThis study focuses on the development of the PU-WC manufacturing method, the determination of properties of this type of composite, and the indication of its potential application. The mechanical properties of PU-WC were characterized by flexural tests. To determine the thermal properties, dynamic mechanical analysis (DMA) and thermogravimetric analysis...
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Phytoplankton in the Kashubian Lakes – microscopic photo archive
Open Research DataPhytoplankton is a group of microscopic plant organisms passively floating in water. The organisms included in the phytoplankton of lakes include the following main taxonomic groups: cyanobacteria (Cyanobacteria), green algae (Chlorophyta), dinoflagellates (Dinophyta), diatoms (Bacillariophyceae), cryptophytes (Cryptophyta), chrysophytes (Chrysophyceae)...
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SEM image and EDS map of SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C
Open Research DataThis dataset contains image of the SrTi0.50Fe0.50O3-d porous electrode sintered at 800 °C with EDS map analysis results. This study were performed for better understanding the chemical composition of flat like structures that occurs in electrode. Images were obtained using a PhenomXL (Thermo Fisher Scientific, the Netherlands) scanning electron microscope...
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Results of SEM examination of chitosan/Eudragit E 100 coatings electrophoretically deposited on the Ti grade 2 substrate
Open Research DataThe database contains the images of the microstructure of the coatings observed with the SEM scanning electron microscope. The chitosan/Eudragit E 100 coatings deposited on the Ti grade 2 substrate by an electrophoresis process were tested. Different process parameters like Eudragit E 100 concentration (0.25 g and 0.5 g in 100 mL of 1% (v/v) acetic...
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Structure and optical measurements of Eu doped tellurium oxide thin films
Open Research DataThin films were deposited by magnetron sputtering method and simultaneously heated at 200 oC. Presence of Eu ions and their valence states was confirmed by X-ray photoemission spectroscopy measurements. The structure of the films as well as the influence of europium dopant on crystalline structure of the films was examined by X-ray diffraction method. ...
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Determination of Local Corrosion Current from Individual Harmonic Components
PublicationHarmonic analysis has been used in corrosion measurements for several decades. During this period the method has been refined and developed. Nevertheless, the technique has not been applied to properties determination in local scale yet. This paper is focused on local corrosion current measurements based on harmonic analysis. For this purpose, a non-linear nature of electrode processes is used and measured in local scale applying...