Publikacje
Filtry
wszystkich: 376
Katalog Publikacji
Rok 2024
-
Expermental investigation on adsorption of methylene blue dye from waste water using corncob cellulose-based hydrogel
PublikacjaHydrogel from corncob cellulose was synthesized in this investigation. The synthesized Hydrogel was characterized by SEM, XRD, and FTIR instruments. As the results indicate the synthesized hydrogel has required and important features, these suggest the suitability of hydrogel for the adsorption of methylene blue dye (MBD). Three important process variables (dosage, contact time, and initial concentration) with three levels were...
-
Study on extraction and characterization of anchote (Coccinia abyssinica) starch and reinforced enset (Ensete ventricosum) fiber for the production of reinforced bioplastic film
PublikacjaPopulation expansion is causing an increase in dependence on plastic materials. The worst aspects of conventional plastics were their inability to biodegrade, their poor capacity to transmit water vapor, and their production of greenhouse gases. Usages of bioplastics are necessary for the advancement of a green economy and environment in order to eradicate these drawbacks of traditional plastics. In this study, reinforced bioplastic...
Rok 2023
-
Hybrid all-cellulose reinforcement in polypropylene matrix biocomposites for injection moulding - influence of particle geometry and volume fraction on hybrid effect
PublikacjaThe presented study is focused on evaluation of influence of reinforcement volume fraction and geometry on the occurrence of positive hybrid effect by the hybridisation of man-made cellulose fibres (rayon viscose) with cellulose microparticle fillers applied in polypropylene matrix. Four volume fractions of reinforcement were used at 1:1 combination of short man-made cellulose fibres with cellulose microfillers of different aspect...
-
M-BDC (M = Co and/ or Fe) MOFs as effective catalysts for hydrogen generation via hydrolysis of sodium borohydride
PublikacjaMono- (Co-BDC, Fe-BDC) and bimetallic FeCo-BDC Metal-Organic Frameworks are successfully synthesized by the solvothermal method in DMF at 150 °C within 15 h and tested as catalysts for sodium borohydride hydrolysis. The materials are characterized by FTIR, PXRD, TGA, ICP-OES, H2-TPR, BET model, and SEM-EDS. The catalytic activity of these materials is studied for dehydrogenation of sodium borohydride in water at various temperatures...
-
Optimization and Modeling of Cr (VI) Removal from Tannery Wastewater onto Activated Carbon Prepared from Coffee Husk and Sulfuric Acid (H2SO4) as Activating Agent by Using Central Composite Design (CCD)
PublikacjaThe primary goal of this research is to lower the hexavalent chromium (Cr (VI)) concentration that has occurred from the growth of the tannery industry. As a result, the potential for heavy metal concentration is increasing day by day. Industrial effluent containing Cr (VI) contributes significantly to water pollution. Chromium hexavalent ion (Cr (VI)) in wastewater is extremely hazardous to the environment. It is critical to address...
-
The influence of magnetic particle incorporation on bisphenol A removal by β-cyclodextrin-derived sorbent
PublikacjaA novel, biomass-derived hybrid sorbent Ban-CD-EPI-Fe was successfully synthesized in a coprecipitation method, in which β-cyclodextrin copolymerized with banana peel extract and epichlorohydrin was grafted onto an iron oxide surface. The composition, presence of functional groups, morphology, thermal stability, and magnetic properties of the obtained material were characterized by Powder X-Ray Diffraction (XRD), X-Ray Photoelectron...
Rok 2022
-
Electrochemical synthesis of 2D copper coordination-polymers: Layer-stacking deviation induced by the solvent and its effect on the adsorptive properties
PublikacjaA 2D Cu-based Metal-Organic Framework (MOF), namely copper-terephthalate (Cu(1,4-BDC)), was successfully synthesized by electrochemical method for effective methylene blue (MB) sorption from aqueous solutions. The composition, morphology, and the presence of functional groups in the obtained material were verified by Fourier Transform Infrared spectroscopy (FTIR), Powder X-Ray Diffraction (PXRD), Thermal (TGA), and Elemental (EA)...
Rok 2021
-
Materiały sorpcyjne wykorzystywane w maskach ochronnych
PublikacjaOd zarania dziejów ludzie starają się chronić przed chorobami zakaźnymi, stosując środki ochrony osobistej, do których należą maski ochronne. Z uwagi na obecnie panującą pandemię wirusa SARS-CoV-2, noszenie masek stało się normą w walce z koronawirusem. Jednak zagrożenia dla górnych dróg oddechowych nie stanowią wyłącznie wirusy, lecz również cząstki stałe zawieszone w powietrzu. Szczególnie w krajach wysoko uprzemysłowionych,...
-
Photoresponsive Amide-Based Derivatives of Azobenzene-4,4′-Dicarboxylic Acid—Experimental and Theoretical Studies
PublikacjaAzobenzene derivatives are one of the most important molecular switches for biological and material science applications. Although these systems represent a well-known group of compounds, there remains a need to identify the factors influencing their photochemical properties in order to design azobenzene-based technologies in a rational way. In this contribution, we describe the synthesis and characterization of two novel amides...
-
β-cyclodextrin-containing polymer based on renewable cellulose resources for effective removal of ionic and non-ionic toxic organic pollutants from water
PublikacjaA novel, bio-derived cyclodextrin-based trifunctional adsorbent has been successfully synthesized for efficient, rapid and simultaneous removal of a broad-spectrum of toxic ionic (anionic and cationic dyes) and non-ionic organic pollutants from water. The composition, morphology and the presence of functional groups in the obtained sorption material were characterized by elemental analysis, XRD, SEM, and FTIR spectroscopy. The...
Rok 2020
-
Ion recognition properties of new pyridine-2,6-dicarboxamide bearing propeller-like pendant residues: multi-spectroscopic approach
PublikacjaThe synthesis and ion binding properties of new amide derived from propeller-like tris(2-pyridyl)amine and 2,6-pyridinedicarboxylic acid chloride were described. Amide binds divalent metal cations: copper(II), nickel(II), zinc(II), and lead(II) in acetonitrile. In acetonitrile:water mixture (9:1 v/v) amide interacts only with copper(II) and nickel(II) cations forming complexes of 1:1 stoichiometry. It was found that the introduction...
-
Photochemical Rearrangement of a 19-Membered Azoxybenzocrown: Products and their Properties
PublikacjaThe preparation and characterization of products of the chemical and photochemical rearrangements of a 19-membered o,o'-azoxybenzocrown were presented. In photochemical rearrangement, besides expected product i.e. 19-membered o-hydroxy-o,o'-azobenzocrown (19-o-OH), obtained under defined conditions with 75% yield, also other macrocyclic products were isolated and identified, namely: 19-membered p-hydroxy-o,o'-azobenzocrown (19-p-OH),...
-
Photoresponsive, amide-based derivative of embonic acid for anion recognition
PublikacjaThe synthesis and ion-binding properties of amide-based derivative of embonic acid andp-aminoazobenzenewere described. The new compound was characterized by X-ray structural analysis and spectroscopic methods.Ligand interacts in acetonitrile with Y-shaped anions (benzoates and acetates) and dihydrogen phosphatesforming complexes of 1:1 stoichiometry. In more polar DMSO the complexes stoichiometry changes to 2:1(L:anion). Light-inducedtranstocisisomerization...
Rok 2019
-
Czujniki optyczne jako narzędzia analityczne do wykrywania i oznaczania jonów
PublikacjaPrawidłowe funkcjonowanie organizmu ludzkiego w dużej mierze opiera się na odpowiedniej równowadze jonowej. Jak wykryć i oznaczyć te jony?
Rok 2018
-
A new method for real-time monitoring of volatiles in frying fumes using proton transfer reaction mass spectrometry with time-of-flight analyse
PublikacjaTo safeguard the consumers’ well-being, it is necessary to develop novel methods for determination of carcinogens in food, including volatiles generated during frying. The currently used procedures for analysis of volatile fraction of vegetable oils are not based on real-time measurements and thus do not enable the determination of carcinogenic compounds in frying fumes; instead, only the headspace or liquid fraction is sampled....
-
Application of fuzzy logic to determine the odour intensity of model gas mixtures using electronic nose
PublikacjaThe paper presents the possibility of application of fuzzy logic to determine the odour intensity of model, ternary gas mixtures (α-pinene, toluene and triethylamine) using electronic nose prototype. The results obtained using fuzzy logic algorithms were compared with the values obtained using multiple linear regression (MLR) model and sensory analysis. As the results of the studies, it was found the electronic nose prototype along...
-
Azo group(s) in selected macrocyclic compounds
PublikacjaAzobenzene derivatives due to their photo- and electroactive properties are an important group of compounds finding applications in diverse fields. Due to the possibility of controlling the trans–cis isomerization, azo-bearing structures are ideal building blocks for development of e.g. nanomaterials, smart polymers, molecular containers, photoswitches, and sensors. Important role play also macrocyclic compounds well known for...
-
Correction to: Azo group(s) in selected macrocyclic compounds
PublikacjaIn the original publication of the article, a part of Scheme 12 was missed. The correct version of Scheme 12 was provided in this correction article. The original article has also been corrected.
-
Electronic Noses for Indoor Air Quality Assessment
PublikacjaThis chapter presents a proposal of the use of electronic noses in the monitoring of indoor air quality. The main focus is put on the detailed characteristics of today’s indoor air quality control methods, the types of pollution in the air, and the development of electronic noses for air testing. Currently, scientists seek methodological and structural solutions that would enable real-time online indoor air control. It has been...
-
Elektrorozpylanie - dogodny sposób jonizacji analitów w przypadku stosowania bezpośrednich procedur pomiarowych opartych na wykorzystaniu spektrometrii mas
PublikacjaSpektrometria mas stanowi obecnie jedno z najważniejszych narzędzi analitycznych, stosowanych w celu oznaczania analitów występujących w próbkach o różnym pochodzeniu i składzie (próbki biologiczne, środowiskowe, żywność). Stosowanie tej techniki w sprzężeniu z rozdzielaniem chromatograficznym jest rozwiązaniem powszechnie stosowanym jednak w większości przypadków zachodzi konieczność oczyszczania, izolacji i wzbogacania analitów...
-
Instrumental measurement of odour nuisance in city agglomeration using electronic nose
PublikacjaThe paper describes an operation principle of odour nuisance monitoring network in a city agglomeration. Moreover, it presents the results of investigation on ambient air quality with respect to odour obtained during six-month period. The investigation was carried out using a network comprised of six prototypes of electronic nose and Nasal Ranger field olfactometers employed as a reference method. The monitoring network consisted...
-
Micellar Route of the Synthesis of Alkyl Xylosides: An Unexpected Effect of Amphiphilic Imidazolium Ionic Liquids
PublikacjaThis manuscript presents results from the investigation on the synthesis of alkyl xylosides by the novel, very efficient and promising protocol of the Fischer synthesis from unprotected xylose and aliphatic alcohol. The use of 1-alkyl-3-methylimidazolium hydrogen sulfate ionic liquids as the catalysts with dual functionality (surfactant + acid catalyst) and micellar reaction system are the main novelty of described method. It has...
-
Ocena skuteczności usuwania wybranych związków odorowych z powietrza z wykorzystaniem biofiltra ze złożem zraszanym
PublikacjaW pracy omówiono najczęściej stosowane metody dezodoryzacji powietrza, zwracając uwagę na zróżnicowane właściwości chemiczne różnych grup związków zapachowych. Omówiono techniki biofiltracyjne, wskazując aktualne trendy rozwojowe. Przedstawiono wyniki badań dotyczących jednoczesnego usuwania (a)-pinenu i cykloheksanu, uzyskując wartości stopnia usunięcia wymienionych związków powyżej 80%.
-
Proces konwersji biomasy lignocelulozowej na drodze hydrolizy zasadowej i utleniania
PublikacjaDo najbardziej nowoczesnych i przyszłościowych metod chemicznych obróbki wstępnej masy lignocelulozowej zalicza się wykorzystanie ozonu. Ozon w znacznym stopniu degraduje ligninę, ale nie narusza struktury celulozy i hemicelulozy, która w rezultacie pozostaje dostępna do bezpośredniego kontaktu z enzymami i mikroorganizmami. Ozonoliza to możliwość prowadzenia procesu w warunkach temperatury i ciśnienia otoczenia. Nie ma miejsca...
-
Zastosowanie niskokosztowych czujników PM10 do monitoringu jakości powietrza atmosferycznego
PublikacjaW pracy przedstawiono wyniki testu terenowego przeprowadzonego na terenie Gdańska w okresie od 7 do 24 lutego 2018 w celu wykazania wiarygodności uzyskiwanych wyników za pomocą komercyjnych czujników PM10 działających na zasadzie laserowego licznika cząstek w stosunku do metody odniesienia.
Rok 2017
-
1,3,4-Thiadiazole-based diamides: Synthesis and complexation properties
PublikacjaAromatic diamides, derivative of 2,6-pyridinedicarboxylic acid and isophthalic acid, bearing 1,3,4-thiadiazole residue were prepared with satisfactory yields in conventional procedures and microwave stimulated reactions. X-ray structure of N,N-bis (1,3,4-thiadiazol-2-yl)-2,6-pyridinedicarboxamide (2) DMSO solvate (2DMSO) was described. Selective zinc(II), lanthanum(III), terbium(III) and L-tyrosine recognition was found for N,N-bis(1,3,4-thiadiazol-2-yl)-2,6-pyridinedicarboxamide...
-
Analiza składu fazy gazowej wytwarzanej podczas fermentacji ciemnej
PublikacjaFermentacja ciemna umożliwia otrzymywanie bio-wodoru z substratów pochodzenia biologicznego, np. z biomasy ligno-celulozowej. Kontrola i właściwe sterowanie przebiegiem procesu fermentacji ciemnej wymaga bieżącego monitoringu składu powstającej fazy gazowej. W niniejszej pracy przedstawiono metodykę analizy składu fazy gazowej z wykorzystaniem techniki GC-TCD-FID. Zaproponowana metodyka umożliwia oznaczenie następujących gazów...
-
Analiza wielokryterialna wariantów systemu zaopatrzenia w wodę zespołu padów
PublikacjaJednym z istotnych problemów decyzyjnych na etapie potencjalnej eksploatacji gazu z formacji łupkowych jest wybór sposobu zaopatrzenia w wodę kopalni gazu łupkowego. Z uwagi na duże zapotrzebowanie na wodę do procesu szczelinowania kolejno przekazywanych do eksploatacji odwiertów wydobywczych, należy poszukiwać systemu zaopatrzenia w wodę, który zagwarantuje wymaganą jej ilość, a jednocześnie nie będzie zbyt dużym obciążeniem dla...
-
Analysis of odor interactions in ternary gas mixtures using electronic nose
PublikacjaIn recent years there has been a noticeable increase in interest in the use of electronic noses in analytical chemistry. These devices perform a holistic analysis of the gas mixtures composition, without the separation and identification of its individual components. For this reason e-noses are increasingly replacing the conventional olfactometers, due to the significantly shorter analysis time and possible automation. In the work...
-
Anion binding by p-aminoazobenzene-derived aromatic amides: spectroscopic and electrochemical studies
PublikacjaThe synthesis and complexing properties of p-aminoazobenzene-derived mono-, bis-, and trisamides were described. Ligands 3 and 4 bind anions, including fluorides, chlorides, bromides, acetates, benzoates, dihydrogen phosphates, hydrogen sulfates, and p-toluenesulfonates, in chloroform forming 1 : 1 complexes. The highest value of stability constant was evaluated for the 4-F− complex (log K = 5.63 ± 0.21). On the basis of 1H NMR,...
-
Bioelectronic nose: Current status and perspectives
PublikacjaA characteristic feature of human and animal organs of smell is the ability to identify hundreds of thousands of odours. It is accompanied by particular smell sensations, which are a basic source of information about odour mixture. The main structural elements of biological smell systems are the olfactory receptors. Small differences in a structure of odorous molecules (odorants) can lead to significant change of odour, which is...
-
Cation sensing by diphenyl-azobenzocrowns
PublikacjaMetal cations complexation and proton binding by 13- and 16-membered diphenyl-azobenzocrowns and diphenyl-hydroxyazobenzocrowns were studied in acetonitrile using spectroscopic methods: UV–vis spectroscopy, spectrofluorimetry, and 1H NMR spectroscopy. Phenyl moieties in benzene rings were found to affect binding strength alkali and alkaline earth metal cations and hydrogen ion, and affect tautomeric equilibrium of hydroxyazobenzocrowns....
-
Currently Commercially Available Chemical Sensors Employed for Detection of Volatile Organic Compounds in Outdoor and Indoor Air
PublikacjaThe paper presents principle of operation and design of the most popular chemical sensors for measurement of volatile organic compounds (VOCs) in outdoor and indoor air. It describes the sensors for evaluation of explosion risk including pellistors and IR-absorption sensors as well as the sensors for detection of toxic compounds such as electrochemical (amperometric), photoionization and semiconductor with solid electrolyte ones....
-
Design and Application of Magnetic Photocatalysts for Water Treatment. The Effect of Particle Charge on Surface
PublikacjaCore-interlayer-shell Fe3O4/SiO2/TiO2, CoFe2O4/SiO2/TiO2 and BaFe12O19/SiO2/TiO2 magnetic photocatalysts were obtained. A water-in-oil microemulsion system with suitable surfactants was used for functionalization of the magnetic core with silica interlayer and TiO2-based photocatalyst. Uncoated and coated particles were characterized by electrophoretic meaurements, X-ray diffractometry (XRD), scanning electron microscopy (SEM),...
-
Determination of odour concentration by TD-GC×GC–TOF-MS and field olfactometry techniques
PublikacjaField olfactometry is one of the sensory techniques used to determine odour concentration, in atmospheric air, directly in emission sources. A two-dimensional gas chromatography with time of flight mass spectrometer (GC×GC–TOF-MS) allows performing the chemical characterization of various groups of chemical compounds, even in complex mixtures. Application of these techniques enabled determination of odour concentration level in...
-
Determination of Odour Interactions of Three-Component Gas Mixtures Using an Electronic Nose
PublikacjaThe paper presents an application of an electronic nose prototype comprised of six TGS-type sensors and one PID-type sensor to identify odour interaction phenomena in odorous three-component mixtures. The investigation encompassed eight odorous mixtures—toluene-acetone-triethylamine and formaldehyde-butyric acid-pinene — characterized by different odour intensity and hedonic tone. A principal component regression (PCR) calibration...
-
Different Ways to Apply a Measurement Instrument of E-Nose Type to Evaluate Ambient Air Quality with Respect to Odour Nuisance in a Vicinity of Municipal Processing Plants
PublikacjaThis review paper presents different ways to apply a measurement instrument of e-nose type to evaluate ambient air with respect to detection of the odorants characterized by unpleasant odour in a vicinity of municipal processing plants. An emphasis was put on the following applications of the electronic nose instruments: monitoring networks, remote controlled robots and drones as well as portable devices. Moreover, this paper presents...
-
Direct Analysis of Samples of Various Origin and Composition Using Specific Types of Mass Spectrometry
PublikacjaOne of the major sources of error that occur during chemical analysis utilizing the more conventional and established analytical techniques is the possibility of losing part of the analytes during the sample preparation stage. Unfortunately, this sample preparation stage is required to improve analytical sensitivity and precision. Direct techniques have helped to shorten or even bypass the sample preparation stage; and in this...
-
Direct measurements of odorous volatile organic compounds present in biosolids cakes by Proton Transfer Reaction – Mass Spectrometry Technique
PublikacjaThis paper show the results of investigation of concentration of odorous chemical compounds emitted upon ageing of anaerobically stabilised biosolids that could contribute to the overall odour character of nuisance emissions. Biosolids samples from wastewater treatment plant were collected in spring time. Concentrations of volatile organic compounds using a US EPA flux hood and Proton Transfer Reaction-Time of Flight-Mass Spectrometry...
-
Dynamic Headspace Sampling as an Initial Step for Sample Preparation in Chromatographic Analysis
PublikacjaThis work represents a brief summary of the use of dynamic headspace (DHS) as a technique for sample preparation in chromatographic analysis. Despite numerous developments in the area of analyte isolation and enrichment, DHS remains one of the fundamental methods used with GC. In our opinion, interest in this technique will not diminish significantly because it conforms to stipulations of green analytical chemistry. Moreover, DHS...
-
Electronic noses: Powerful tools in meat quality assessment
PublikacjaMain factors that are considered by consumers when choosing meat products are colour and aroma, of which the latter is a more reliable indicator of quality. However, a simple sensory evaluation of hedonistic qualities is often not sufficient to determine whether protein is past its shelf life, and consumption of spoiled meat can lead to serious health hazards. Some volatile compounds can be used as spoilage indicators, and so a...
-
Enhanced visible light photocatalytic activity of Pt/I-TiO2 in a slurry system and supported on glass packing
PublikacjaHighly photoactive I/TiO2, Pt/I-TiO2 nanocomposites were obtained using a hydrothermal and wet impregnation method. The incorporation of iodine and modification with 0.05 mol% of platinum leads to enhanced photocatalytic activity as compared to singly doped TiO2 due to the presence of impurity energy level in the structure of TiO2. X-ray diffraction, TEM microscopy, UV–Vis spectroscopy, X-ray photoelectron spectroscopy and BET...
-
Insights Into Hydrodynamics of Spinning Fluids Reactor
PublikacjaSpinning fluids reactor (SFR) is one of the most efficient gas-liquid contacting system with high potential of application in many fields. The unique solution of SFR is the contacting of two spinning fluids which generated centrifugal force. The aim of this study was to investigate the pressure field distribution on the inner surface of reactors dispersing element. Obtained results confirm the high heterogeneity of the field pressure...
-
Investigation of Air Quality beside a Municipal Landfill: The Fate of Malodour Compounds as a Model VOC
PublikacjaThis paper presents the results of an investigation on ambient air odour quality in the vicinity of a municipal landfill. The investigations were carried out during the spring–winter and the spring seasons using two types of the electronic nose instrument. The field olfactometers were employed to determine the mean odour concentration, which was from 2.1 to 32.2 ou/m3 depending on the measurement site and season of the year. In...
-
Kapilarna chromatografia gazowa fazy nad-powierzchniowej – HS-CGC w badaniach składu lotnych produktów hydrolizy biomasy ligno-celulozowej – BMLC
PublikacjaW pracy przedstawiono sposoby obróbki biomasy ligno-celulozowej, których celem jest rozpulchnienie struktury surowca i zwiększenie dostępności struktur dla czynników hydrolizujących. Na podstawie przeglądu literatury wskazano na możliwe do zidentyfikowania związki obecne w hydrolizatach z biomasy ligno-celulozowej. Opracowano metodykę oraz zbadano możliwość oznaczania lotnych produktów hydrolizy chemicznej z wykorzystaniem techniki...
-
Magnetic semiconductor photocatalysts for the degradation of recalcitrant chemicals from flow back water
PublikacjaIn the present study treatability of persistent organic compounds from the flow back water after hydrauling fracturing was investigated. The combination of TiO2 photocatalyst and magnetic oxide nanoparticles enhance the separation and recoverable property of nanosized TiO2 photocatalyst. Fe3O4/ TiO2 and Fe3O4@SiO2/TiO2 nanocomposites were prepared by heteroagglomeration. The photocatalysts’ characteristics by X-ray diffractometry...
-
Method for the determination of carboxylic acids in industrial effluents using dispersive liquid-liquid microextraction with injection port derivatization gas chromatography–mass spectrometry
PublikacjaThe paper presents a new method for the determination of 15 carboxylic acids in samples of postoxidative effluents from the production of petroleum bitumens using ion-pair dispersive liquid-liquid microextraction and gas chromatography coupled to mass spectrometry with injection port derivatization. Several parameters related to the extraction and derivatization efficiency were optimized. Under optimized experimental conditions,the...
-
New procedure for the examination of the degradation of volatile organonitrogen compounds during the treatment of industrial effluents
PublikacjaWe present a new procedure for the determination of 32 volatile organonitrogen compounds in samples of industrial effluents with a complex matrix. The procedure, based on dispersive liquid–liquid microex-traction followed by gas chromatography with nitrogen-phosphorus and mass spectrometric detection, wasoptimized and validated. Optimization of the extraction included the type of extraction and disperser sol-vent, disperser solvent...
-
Photocatalytical degradation of toluene and cyclohexane using LED illumination
PublikacjaA sol-gel process followed by hydrothermal reaction was used to prepare coupled WO3-TiO2 photocatalysts with varying amounts of WO3 in respect to TiO2 (3 mol% and 5 mol% respectively). Additionally, photocatalysts have been subjected to different calcination temperatures of 400ºC and 800ºC, which allowed us to compare how these affect photodegradation efficiency. Photocatalysts were characterized under a scanning electron microscope,...
-
Portable Electronic Nose Based on Electrochemical Sensors for Food Quality Assessment
PublikacjaThe steady increase in global consumption puts a strain on agriculture and might lead to a decrease in food quality. Currently used techniques of food analysis are often labour-intensive and time-consuming and require extensive sample preparation. For that reason, there is a demand for novel methods that could be used for rapid food quality assessment. A technique based on the use of an array of chemical sensors for holistic analysis...
-
Poultry meat freshness evaluation using electronic nose technology and ultra-fast gas chromatography
PublikacjaTo ensure that chicken meat products are safe to consume, it is important to be able to reliably determine its shelf-life. To assess the applicability of ultra-fast gas chromatography and electronic nose technology in evaluation of poultry, an analysis of the headspace of ground chicken meat samples refrigerated over a period of 7 days was performed. Chemometric techniques were used to mine additional information from a multiparametric...
-
Properties and Formation of Mineralized Veins in an Organic-Rich Shale Formation
PublikacjaAn earlier paper defined mineral and organic matter constituents in weak interfaces in shale formations (Ptaszynska, et. al., 2016). The formation studied in the earlier work and here is the Jurassic, early-Cretaceous Vaca Muerta formation in the Neuquen basin in Argentina. In this earlier work, mineralized "veins" were noted to be prevalent and complicated, sometimes being shear weak interfaces while in other cases they were not....
-
Prospects of ionic liquids application in electronic and bioelectronic nose instruments
PublikacjaThis paper addresses the problem of application of ionic liquids to chemical sensors and biosensors being an integral part of the electronic and bioelectronic-type instruments. The design and principle of operation of the electronic and bioelectronic noses are compared. Both the benefits and shortcomings of the application of ionic liquids in these type of instruments are described. The prospects of the development and application...
-
Salicylaldimine-based receptor as a material for iron(III) selective optical sensing
Publikacjaα,α-Bis(salicylimino)-m-xylene (L) was prepared using both conventional and microwave-assisted procedure. The compound exhibits ability to colorimetric recognition of iron(III) ions in aqueous environment, what is shown by significant color change from yellow to purple. In DMSO : water (9:1 v/v) solvent system receptor creates with iron(III) cations complexes of 2:1 stoichiometry (L:Fe3+) with stability constant (log K) 7.54±0.21....
-
Spinning Fluids Reactor: A new design of a gas – liquid contactor
PublikacjaCurrent trends in chemical reactor design are based on adapting these to the requirements of a particular chemical process. Processes involving reactions between the gas and liquid phase in particular require precise adjustment of all parameters. The common denominator for most modern design solutions is enhancement of the mass transfer area and the overall volumetric mass transfer coefficient. Gas – liquid contactors evolved from...
-
Study of Different Advanced Oxidation Processes for Wastewater Treatment from Petroleum Bitumen Production at Basic pH
PublikacjaEffluents from production of petroleum bitumens were submitted to treatment by three different AOPs at basic pH (i.e., O3, H2O2 and the combination of O3 and H2O2, a so-called peroxone). The paper presents studies on the identification and monitoring of the volatile organic compounds (VOCs) degradation present in the effluents and formation of byproducts, COD, BOD5, sulfide ions, biotoxicity, and biodegradability changes during...
-
The effect of microemulsion composition on the morphology of Pd nanoparticles deposited at the surface of TiO2 and photoactivity of Pd-TiO2
PublikacjaA series of microemulsion (ME) system, constituted by different water to surfactant molar ratios (Wo) and oil to surfactant mass ratios (S), have been applied for Pd-TiO2 preparation. The effect of ME properties on the morphology of Pd nanoparticles formed at TiO2 surface and an effect of Pd size and distribution on the surface and photocatalytic properties of Pd-TiO2 were investigated. Microemulsion systems were characterized...
-
The ILs-assisted electrochemical synthesis of TiO2 nanotubes: The effect of ionic liquids on morphology and photoactivity
PublikacjaFacile and environmentally benign one-step titanium anodization method for TiO2 nanotubes (NTs) formation in a presence of ionic liquids (ILs) was proposed. Influence of the IL structure and its content in ethylene glycol electrolyte on morphology, surface properties and photoactivity of the TiO2 NTs was investigated. Possible interactions between IL and TiO2 NTs as well as the mechanism of NTs formation during anodic oxidation...
-
The Use of Sensory Analysis Techniques to Assess the Quality of Indoor Air
PublikacjaThe quality of indoor air is one of the significant elements that influences people's well-being and health inside buildings. Emissions of pollutants, which may cause odor nuisance, are the main reason for people's complaints regarding the quality of indoor air. As a result, it is necessary to perform tests aimed at identifying the sources of odors inside buildings. The article contains basic information on the characteristics...
-
Thermal degradation assessment of canola and olive oil using ultra-fast gas chromatography coupled with chemometrics
PublikacjaOil blending is often used to enhance the properties of vegetable oils. The admixture of a more thermally stable oil makes the resulting blend more suitable for use in frying. A new method of quality assessment of vegetable oils used in frying is presented in this paper. In this method, ultra-fast gas chromatography coupled with flame ionization detector and chemometrics is employed. Principal component analysis was used for data...
-
Visible light photocatalytic activity of ionic liquid-TiO2 spheres: effect of the ionic liquid's anion structure
PublikacjaThe effect of the ionic liquid’s (IL) anion type ([BIMIM][X], where X= [Br], [PF6] or [OctSO4]) and content on the morphology, surface properties and photoactivity of TiO2 obtained by solvothermal method has been systematically investigated. Our results revealed that the presence of [Br], [OctSO4] anions favors formation of anatase phase, while presence of [PF6] anion causes formation of mixture of anatase and Ti(OH)PO4 phases....
-
Wielokryterialne Wspomaganie decyzji środowiskowych przy wydobywaniu węglowodorów z formacji łupkowych
PublikacjaPoszukiwanie i eksploatacja gazu z formacji łupkowych wymaga zidentyfikowania i uwzględnienia wielu czynników i uwarunkowań geologiczno-górniczych, ekonomiczno-finansowych, prawnych oraz szeroko rozumianych aspektów przestrzenno-środowiskowych. Poruszane zagadnienia prowadzą do zidentyfikowania problemów decyzyjnych, które mogą pojawiać się przy eksploatacji gazu z łupków, a które wiążą się z intensywnym korzystaniem z zasobów...
Rok 2016
-
Analiza społeczno-ekonomiczna produkcji biogazu z odpadów organicznych
PublikacjaW odniesieniu do obaw społecznych dotyczących systemu zarządzania odpadami można wyróżnić główne kategorie wpływu: życie i zdrowie ludzkie, środowisko oraz zasoby naturalne. Zaostrzenie wymagań prawnych w zakresie ochrony środowiska i wykorzystania odnawialnych źródeł energii wymuszają poszukiwania nowych i rozwoju istniejących już metod zagospodarowania odpadów w sposób pozwalający na zmniejszenie ich niekorzystnego oddziaływania....
-
Application of dispersive liquid-liquid microextraction and gas chromatography with mass spectrometry for the determination of oxygenated volatile organic compounds in effluents from the production of petroleum bitumen
PublikacjaWepresent a new procedure for the determination of oxygenated volatile organic compounds in samples of postoxidative effluents from the production of petroleum bitumens using dispersive liquid–liquid microextraction and gas chromatography with mass spectrometry. The eight extraction parameters were optimized for 43 oxygenated volatile organic compounds. The detection limits obtained ranged from 0.07 to 0.82 g/mL for most of the...
-
Application of dynamic headspace and gas chromatography coupled to mass spectrometry (DHS-GC-MS) for the determination of oxygenated volatile organic compounds in refinery effluents
PublikacjaThe paper presents a new procedure for the determination of oxygenated volatile organic compounds (O-VOCs) in postoxidative effluents from the production of petroleum asphalt using dynamic headspace coupled to gas chromatography-mass spectrometry in the selected ion monitoring (SIM) mode (DHSGC-MS). Among the GC capillary columns tested, a polar SLB-IL111 column with the ionic liquid stationary phase was found to be superior due...
-
Application of electrochemical sensors and sensor matrixes for measurement of odorous chemical compounds
PublikacjaIn this paper describes the principle of operation of the electrochemical sensors and the sensor matrixes comprised of electrochemical sensors intended for measurement of odorous compounds. Critical comparison of these sensors’ advantages and disadvantages has been made. The fields of economy contributing to release of odours and the potential sources of their emission have been identified. Commercially available electrochemical...
-
Application of Ionic Liquids in Amperometric Gas Sensors
PublikacjaThis article presents an analysis of available literature data on metrological parameters of the amperometric gas sensors containing ionic liquids as an electrolyte. Four mechanism types of signal generation in amperometric sensors with ionic liquid are described. Moreover, this article describes the influence of selected physico-chemical properties of the ionic liquids on the metrological parameters of these sensors. Some metrological...
-
Application of ionic liquids in electronic nose instruments
PublikacjaAmong many applications in different fields of science and technology the ionic liquids (ILs) are also utilised in chemical sensors yielding improvement of their operation parameters (Buzzeo, 2004; Wei and Ivaska, 2008; Silvester, 2011; Gebicki et al., 2013). Some of these chemical sensors are the components of the devices, which resemble human sense of smell as far as their operation is concerned. These devices are named electronic...
-
APPLICATION OF ULTRAFAST GAS CHROMATOGRAPHY TO RECOGNIZE ODOR NUISANCE
PublikacjaPotentialities of ultrafast gas chromatography applied to periodical monitoring of odor nuisance originating from a municipal landfill have been examined. The results of investigation on classification of the atmospheric air samples collected in a vicinity of the landfill during winter and summer season have been presented. The investigation was performed using ultrafast gas chromatography of Fast/Flash GC type HERACLES II by Alpha...
-
Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. I. Rozwiązania metodyczne w zakresie spektrometrii mas umożliwiające bezpośrednią analizę próbek
PublikacjaTechnika spektrometrii mas stanowi jedno z najważniejszych narzędzi analitycznych, wykorzystywanych do identyfikacji, określania struktury chemicznej oraz oznaczania stężeń wielu związków chemicznych. Aby zidentyfikować obecne w próbkach rzeczywistych anality, konieczne jest jednak z reguły ich wstępne rozdzielenie, toteż spektrometry mas pełnią najczęściej rolę detektora np. w przypadku technik łączonych, gdy na etapie rozdzielania...
-
Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. II. Technika PTR – MS – ciekawe rozwiązanie metodyczne w zakresie spektrometrii mas
PublikacjaTechnika spektrometrii mas stanowi niezwykle istotne narzędzie badawcze, umożliwiające uzyskanie wielu cennych informacji, dotyczących składu chemicznego wielu próbek rzeczywistych pochodzenia biologicznego, farmaceutycznego i spożywczego. Spektrometr mas zazwyczaj pełni role detektora w przypadku stosowania połączenia z urządzeniami chromatograficznymi (GC, LC). Dzięki zastosowaniu pewnych modyfikacji aparaturowych i metodycznych,...
-
Chapter 11 – Application of Chemical Sensors and Sensor Matrixes to Air Quality Evaluation
PublikacjaIndoor and outdoor air quality is one of the key factors influencing human health. However, air quality evaluation is not easy task. Air is a complex system, which is subjected to changes even within short period of time. Progress in analytical methods and analytical tools provides increasingly more reliable information on the condition and quality of indoor and outdoor air. This progress, however, generates an increase in the...
-
Comparison of Evaluation of Air Odour Quality in Vicinity of Petroleum Plant Using a Prototype of Electronic Nose Instrument and Fast GC Technique
PublikacjaThe paper presents the results of investigation on classification of the ambient air samples collected in a vicinity of the LOTOS Group S.A. petroleum plant with respect to odour. The investigations were carried out with an electronic nose prototype and a commercial electronic nose of Fast GC-type – HERACLES II. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and a photoionization sensor of PID-type....
-
Comparison of the measurement techniques employed for evaluation of ambient air odour quality
PublikacjaThe paper presents the results of investigation on ambient air odour quality in a vicinity of the industrial sewage treatment plant being a part of the crude oil processing plant. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. The field...
-
Comparison of the Measurement Techniques Employed for Evaluation of Ambient Air Odour Quality Influenced by Operation of Industrial Sewage Treatment Plant
PublikacjaThe paper presents the results of investigation on ambient air quality evaluation with respect to concentration of odorants in a vicinity of a sewage treatment plant of the LOTOS Group S.A. petroleum plant. The investigation was performed during winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type...
-
Comprehensive two dimensional gas chromatography coupled with mass spectrometry as tool for characterization of the main pollutants present in atmospheric air in Gdansk
PublikacjaNowadays, the technique that is commonly used to identify and quantify the chemical compounds in gas sample is gas chromatography. The separation resolution in gas chromatography can be improved by applying the modulation technique. In this paper present is the most important information regarding the pollutants present in atmospheric air. The areas in which the tests were carried out are one of the largest industrial zones in...
-
Conductivity and viscosity changes of imidazolium ionic liquids induced by H2O and CO2
PublikacjaSeveral solutions of ionic liquids based on 1-ethyl-3-methylimidazolium cation saturated and unsaturated with carbon dioxide were prepared and characterized by electrochemical impedance spectroscopy. The in fluence of ILs saturation on its electrical conductivity was determined. Additionally, the in fluence of the water presence and variations of temperature on electrical properties of ionic liquids were investigated. Changes of...
-
Devices for the production of reference gas mixtures
PublikacjaFor many years there has been growing demand for gaseous reference materials, which is connected with development in many fields of science and technology. As a result, new methodological and instrumental solutions appear that can be used for this purpose. Appropriate quality assurance/quality control (QA/QC) must be used to make sure that measurement data are a reliable source of information. Reference materials are a significant...
-
Dual functionality of amphiphilic 1-alkyl-3-methylimidazolium hydrogen sulfate ionic liquids: surfactants with catalytic function
PublikacjaA series of amphiphilic 1-alkyl-3-methylimidazolium hydrogen sulfate ionic liquids were synthesized. Acidic hydrogen sulfate ionic liquids with the alkyl chains C6–C14 are characterized by good surface properties. Their surface properties (adsorption and micellization parameters, degree of ionization of micelles, Krafft temperatures and thermodynamic parameters) were determined. Synthesized ionic liquids were applied as a co-catalyst...
-
Electricity generation from rapeseed straw hydrolysates using microbial fuel cells
PublikacjaRapeseed straw is an attractive fuel material for microbial fuel cells (MFCs) due to its high content of carbohydrates (more than 60% carbohydrates). This study has demonstrated that reducing sugars can be efficiently extracted from raw rapeseed straw by combination of hydrothermal pretreatment and enzymatic hydrolysis followed by utilization as a fuel in two-chamber MFCs for electrical power generation. The most efficient method...
-
Evaluation of Ambient Air Odour Quality in Vicinity of Municipal Landfill Using Electronic Nose Technique
PublikacjaThe paper presents the results of investigation on ambient air quality evaluation with respect to concentration of odorants in a vicinity of municipal landfill. The investigation was carried out with a prototype of electronic nose and a team of panelists utilizing the Nasal Ranger field olfactometers. The prototype was equipped with a set of six semiconductor sensors by FIGARO Co. and one PID-type sensor. Performed measurements...
-
Identification of aromatic compounds in odours mixture by gas chromatography and field olfactometry techniques
PublikacjaThis paper shows the results of investigation on identification aromatic compounds present in odorous mixture in atmospheric air samples collected in a vicinity of the oil refinery LOTOS S.A., located in Gdansk, during March and April period have be presented. The studies were conducted by the use of comprehensive two-dimensional gas chromatograph equipped with a cryogenic modulator and coupled with a time-of-flight mass spectrometer,...
-
Identification of pollutants at the adjacent areas to the landfill site using two dimensional gas chromatography with mass spectrometry technique
PublikacjaMunicipal landfills are considered one of the main sources of air pollutants. In this article is presented the use of a modern analytical technique: a two dimensional gas chromatography to identify the substances in the atmospheric air near a waste processing plant located in Gdansk. In order to determine the types of substances occurring in different atmospheric conditions, the study was conducted from February to April 2016....
-
Ionic liquids for nano- and microstructures preparation. Part 1: Properties and multifunctional role
PublikacjaIonic liquids (ILs) are a broad group of organic salts of varying structure and properties, used in energy conversion and storage, chemical analysis, separation processes, as well as in the preparation of particles in nano- and microscale. In material engineering, ionic liquids are applied to synthesize mainly metal nanoparticles and 3D semiconductor microparticles. They could generally serve as a structuring agent or as a reaction...
-
Ionic liquids for nano- and microstructures preparation. Part 2: Application in synthesis
PublikacjaIonic liquids (ILs) are widely applied to prepare metal nanoparticles and 3D semiconductor microparticles. Generally, they serve as a structuring agent or reaction medium (solvent), however it was also demonstrated that ILs can also play a role of a co-solvent, metal precursor, reducing as well as surface modifying agent. The crucial role and possible types of interactions between ILs and growing particles have been presented in...
-
Measurement techniques for assessing the olfactory impact of municipal sewage treatment plants
PublikacjaThe study presents information about the measurement techniques used for the assessment of air quality in terms of the olfactory intensity resulting from the operation of municipal sewage treatment plants. Advantages and disadvantages of the measurement techniques used are presented. Sources of malodourous substance emission from sewage treatment plants were described, and the malodourous substances emitted were characterised....
-
Micellar aggregation of Triton X-100 surfactant in imidazolium ionic liquids
PublikacjaIn this work we investigated aggregation behavior of a nonionic surfactant Triton X-100 in eighteen imidazolium ionic liquids (ILs) with two to eight carbon atoms in cations alkyl chain, namely 1-ethyl-3-methylimidazolium, [EMIM], 1-butyl-3-methylimidazolium, [PrMIM], 3-methyl-1-propylimidazolium, [BMIM], 1-hexyl-3-methylimidazolium, [PMIM], 3-methyl-1-pentyl-imidazolium, [HMIM], and 1-octyl-3-methylimidazolium, [OMIM], and with...
-
Mineral and Organic Matter Constituents in Weak Interfaces in Shales
PublikacjaThis paper identifies formation interfaces that would appear to be "weak interfaces", in the Jurassic, Early- Cretaceous Vaca Muerta formation, in the Neuquén Basin, Argentina. Significant distribution of the weak interfaces was observed including contacts between volcanic ash layers of varying thicknesses, calcite-filled veins, and contacts between lithology changes, such as between argillaceous mudstone and mottled carbonates....
-
Monitoring of odour nuisance in the Tricity Agglomeration
PublikacjaThe paper describes a principle of operation of odour nuisance monitoring network, which is being designed in the Tricity Agglomeration. Moreover, it presents the preliminary results of an investigation on ambient air quality with respect to odour nuisance in a vicinity of the municipal landfill. The investigation was performed during spring-winter season using a prototype of electronic nose and the Nasal Ranger field olfactometers. The...
-
Naphthyl-vs. anthrylpyridine-2,6-dicarboxamides in cation binding studies. Synthesis and spectroscopic properties
PublikacjaPyridine-2,6-carboxamides bearing - or -naphthyl- and - or -anthryl- residues were prepared using simple method from pyridine-2,6-carboxylic acid dichloride and the respective aromatic amines. For the obtained receptors selective binding of lead(II), and copper(II) was found. Ion-receptor interactions were studied using UV-vis spectroscopy, spectrofluorimetry, 1H NMR, and FTIR spectroscopy. The reversible lead(II) and copper(II)...
-
New bis(azobenzocrown)s with dodecylmethylmalonyl linkers as ionophores for sodium selective potentiometric sensors
PublikacjaNovel biscrowns 1 and 2 were synthesized from 13-membered azobenzocrown ethers containing bromoalkylenoxy chains in para position relative to the azo group. The synthesized diester molecules are dodecylmethylmalonic acid derivatives differing by the linker length. The synthesized compounds have the potential of being used as sodium ionophores in ion-selective electrodes. They were characterized and used as ionophores in classic...
-
New procedure for the control of the treatment of industrial effluents to remove volatile organosulfur compounds
PublikacjaWe present a new procedure for the determination of volatile organosulfur compounds in samples of industrial effluents using dispersive liquid–liquid microextraction and gas chromatography with flame photometric detection. Initially, the extraction parameters were optimized. These included: type and volume of extraction solvent, volume of disperser solvent, salting out effect, pH, time and speed of centrifugation as well as extraction...
-
OTRZYMYWANIE I CHARAKTERYSTYKA UKŁADU WĘGIEL - POLIMER SYNTETYCZNY
PublikacjaCelem badań było otrzymanie i pełna charakterystyka trwałych, stabilnych węglowych układów z zastosowaniem biopolimerów, jako materiału wyjściowego do syntezy nanostruktur węglowych, i następnie ich modyfikacja polimerami syntetycznymi. Karbonizaty zostały wytworzone metodą pirolizy biopolimerowego prekursora. Nowatorskie, kompozytowe materiały skomponowane na bazie tradycyjnych polimerów z dodatkiem karbonizatów uzyskały unikalne...
-
Porous carbon derived from rice husks as sustainable bioresources: insights into the role of micro-/mesoporous hierarchy in hosting active species for lithium–sulphur batteries
PublikacjaThe exploration of natural resources as sustainable precursors affords a family of green materials. Exploring highly abundant and available biowaste precursors remaining from food processing throughout a scalable and cost-effective material synthesis path is highly important especially for new materials discovery in emerging energy storage technologies such as lithium–sulphur (Li–S) batteries. Herein, we have produced a series...
-
POWIĄZANIE INTENSYWNOŚCI ZAPACHOWEJ Z SYGNAŁAMI CZUJNIKÓW ELEKTRONICZNEGO NOSA
PublikacjaW ostatnich latach obserwuje się znaczny wzrost zainteresowania tematyką wykorzystania sztucznych zmysłów w analityce chemicznej. Szczególną pozycję zajmuje urządzenie, mające naśladować zmysł węchu - elektroniczny nos. Jest to instrument umożliwiający holistyczną analizę składu mieszaniny gazowej, bez rozdzielania i identyfikacji jej poszczególnych składników. Głównym zadaniem, stawianym tym urządzeniom, jest automatyczne rozróżnianie...
-
Release of selected chemical elements from shale drill cuttings to aqueous solutions of different pH
PublikacjaThe effect of pH changes on leachability of light and heavy metals from shale drill cuttings generated from unconventional shale gas production was investigated. Cuttings, being the primary byproduct generated from drilling operations, belong to the potentially hazardous type of wastes due to presence of heavy and radioactive elements and remains of drilling fluid. In this regard, assessment of potentially dangerous components...
-
STRĄCANIE WĘGLANU WAPNIA Z WYKORZYSTANIEM ODPADOWEGO ROZTWORU CHLORKU WAPNIA
PublikacjaWęglan wapnia strącano z modelowych roztworów chlorku wapnia w reaktorze typu gaz(CO2)-lift za pomocą gazowego dwutlenku węgla w obecności amoniaku. Wydajność strącanego węglanu wapnia wynosiła około 70%. Cząstki CaCO3 charakteryzowały się monomodalnymi rozkładami wielkości, a ich średnia średnica wynosiła od 11,8 do 28 um. Zaproponowana metoda pozwala na wykorzystanie roztworu chlorku wapnia, który jest odpadem w technologii Solvay'a...
-
Substancje złowonne powstające w oczyszczalniach ścieków i metody oceny ich uciążliwości zapachowej
PublikacjaW artykule przedstawiono informacje o źródłach emisji substancji złowonnych z oczyszczalni ścieków do otoczenia. Ponadto opisano jakie substancje odpowiadają za występowanie uciążliwości zapachowej i które z nich mogą stanowić potencjalny marker emisji zapachowej. Scharakteryzowano techniki pomiaru stężeń substancji złowonnych zarówno sensoryczne jak i instrumentalne jednocześnie określając ich użyteczność praktyczną. W pracy przedstawiono...
-
Technologie ochrony środowiska w przemyśle i energetyce
PublikacjaPublikacja prezentuje metody oczyszczania powietrza, wody i gleby skażonych podczas produkcji energii w zakładach energetycznych, przemysłowych oraz gospodarstwach domowych. Przedstawia technologie ochrony środowiska w ujęciu chemicznym, fizycznym, mechanicznym
-
Technologie szczelinowania w eksploatacji gazu z łupków – predykcja składu płynu pozabiegowego
PublikacjaNiniejsza rozprawa składa się z dwóch głównych części: literaturowej i doświadczalnej. W części literaturowej przedstawiono modele literaturowe dotyczące płynu pozabiegowego. Wskazano, że dobrze opisane zostały modele wykorzystujące dane dotyczące płynu pozabiegowego do optymalizacji oczyszczania odwiertu i zwiększania produkcji. Modele nawiązujące do przedmiotu dysertacji są nieliczne, ograniczone do danych na wybranych formacjach....