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Smartphone-based digital image colorimetry for the determination of total capsaicinoid content in chili pepper extracts
PublicationA simple smartphone-based digital image colorimetry was proposed for the determination of total capsaicinoid content and the assessment of chili pepper pungency. The biobased solvent D-limonene was used for the first time to isolate analytes. Capsaicinoids were efficiently separated from chili pepper by solid-liquid extraction with D-limonene followed by partitioning of the analytes into the ammonium hydroxide solution to eliminate...
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A novel methodology for the enantiomeric resolution of methamphetamine, its precursors and intermediates by GC-MS
PublicationImpurity profiling and classification of abused drugs using chiral analytical techniques is of particular interest and importance because of the additional information obtained from this approach. When these methods are applied to the synthesis of illicitly used substances, they can supply valuable information about the conditions/chemicals used in the synthesis. In this study, simultaneous chiral separation of methylamphetamine,...
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Analytical Strategies and Applications in Lipidomics
PublicationLipidomics is a field of study aiming at a comprehensive analysis of a set of lipids in biological systems. This includes both quantitative and qualitative characterization of lipid profiles, comparative studies of lipidomes, and analysis of lipid-protein interactions. Lipids are structurally diversified that make their analysis a challenging task. The constant advances in analytical technologies, especially in the field of high-performance...
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Development of chromatographic and mass spectrometry conditions for untargeted lipidomic analysis of human breast milk
PublicationHuman breast milk (HBM) is a complex biofluid containing components which are essential for the proper growth of the newborn (for example nutrients such as carbohydrates, proteins, lipids) and also bioactive substances. According to the literature, most of studies involving HBM nutrients investigations focused essentially on the determination of proteins. The molecular composition of lipids in HBM is not well known as the protein...
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Generalized Savitzky–Golay filters for identification of nonstationary systems
PublicationThe problem of identification of nonstationary systems using noncausal estimation schemes is consid-ered and a new class of identification algorithms, combining the basis functions approach with localestimationtechnique,isdescribed.Unliketheclassicalbasisfunctionestimationschemes,theproposedlocal basis function estimators are not used to obtain interval approximations of the parametertrajectory, but provide a sequence of point...
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Analysis of the parameters of respiration patterns extracted from thermal image sequences
PublicationRemote estimation of vital signs is an important and active area of research. The goal of this work was to analyze the feasibility of estimating respiration parameters from video sequences of faces recorded using a mobile thermal camera. Different estimators were analyzed and experimentally verified. It was demonstrated that the respiration rate, periodicity of respiration, and presence and length of apnea periods could be reliably...
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A Simulative Comparison of Ship Domains and Their Polygonal Approximations
PublicationThe paper investigates the impact of a precise ship domain shape on the size of collision avoidance manoeuvres. The considered collision avoidance manoeuvres include both course and speed alterations. Various ship domains are compared with their polygonal approximations, which vary in the number of points of a domain contour and placement of these points. The best of all considered approximations is determined in the course of...
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Effect of geometric imperfections on aluminium silo capacities
PublicationAn aluminum silo with initial imperfections is analysed. Two types of imperfections are considered. The first one takes the form of local indentations in the shell; their size and range are adopted on the basis of the standard guidelines. The second type is a global imperfection described through the use of its eigenforms and by means of two-dimensional random fields. The calculations are limited to two cases of loading: negative...
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Influence of datasets decreased by applying reduction and generation methods on Digital Terrain Models
PublicationThe number of point clouds provided by LiDAR technology can be sometimes seen as a problem in development and further processing for given purposes (e.g. Digital Terrain Model (DTM) generation). Therefore, there is still a need to reduce the obtained big datasets. Reducing can be done, inter alia, by reducing the size of the set or by generating the set. This paper presents two variants of the reduction of point clouds in order...
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Obliczanie przesunięć osi toru przy modernizacji łuków parabolicznych na liniach kolejowych
PublicationPodstawowym zadaniem modernizacji linii kolejowych jest właściwe zaprojektowanie nowego układu geometrycznego, który będzie spełniał założone kryteria związane z parametrami eksploatacyjnymi danej linii. Dążąc do spełnienia przyjętych warunków nałożonych na projektowany układ, projektant najczęściej koryguje podstawowe parametry geometryczne, tj. przechyłkę, promień łuku kołowego oraz długości krzywych przejściowych. W artykule...
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Structure and performance properties of environmentally-friendly biocomposites based on poly(ɛ-caprolactone) modified with copper slag and shale drill cuttings wastes
PublicationThe potential application of two types of industrial wastes, drill cuttings (DC) and copper slag (CS), as silica-rich modifiers of poly(ɛ-caprolactone) (PCL) was investigated. Chemical structure and physical properties of DC and CS fillers were characterized using X-ray diffractometer, X-ray fluorescence spectroscopy, particle size and density measurements. PCL/DC and PCL/CS composites with a variable content of filler (5 to 50...
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Visualizing Carotid Bodies With Doppler Ultrasound Versus CT Angiography: Preliminary Study
PublicationOBJECTIVE. The purpose of this article is to evaluate the utility of ultrasound in identifying carotid bodies (CBs) in patients with drug-resistant arterial hypertension. SUBJECTS AND METHODS. We enrolled 13 patients with drug-resistant hypertension into a trial for surgical CB excision. CT angiography (CTA) and Doppler ultrasound (DUS) of the cervical arteries were performed before surgery. CBs were identified in a blind manner...
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Optimization of Polycrystalline CVD Diamond Seeding with the Use of sp³/sp² Raman Band Ratio
PublicationThe influence of various nanodiamond colloids used for seeding nondiamond substrates in microwave plasma enhanced chemical vapour deposition diamond process was investigated. Colloids based on deionized water, isopropanol alcohol and dimethyl sulfoxide (DMSO) were used with different grain size dispersion: 150, 400 and 35 nm, respectively. The influence of growth time was also taken into consideration and bias enhanced nucleation....
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Shielded HMSIW-based frequency-tunable self-quadruplexing antenna using different solid/liquid dielectrics
PublicationThis article proposes a frequency-tunable self-quadruplexing antenna based on a shielded half-mode substrate integrated waveguide (S-HMSIW). In order to reduce the size of the HMSIW cavity resonator and to obtain quad-band characteristics, a modied E-shaped slot is engraved on the top of the metal. The experimental validation is carried out after analyzing the data using a circuit model. Flexibility of each resonant frequency is...
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Design of a Shape-Memory-Alloy-Based Carangiform Robotic Fishtail with Improved Forward Thrust
PublicationShape memory alloys (SMAs) have become the most common choice for the development of mini- and micro-type soft bio-inspired robots due to their high power-to-weight ratio, ability to be installed and operated in limited space, silent and vibration-free operation, biocompatibility, and corrosion resistance properties. Moreover, SMA spring-type actuators are used for developing different continuum robots, exhibiting high degrees...
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Efficient Surrogate Modeling and Design Optimization of Compact Integrated On-Chip Inductors Based on Multi-Fidelity EM Simulation Models
PublicationHigh-performance and small-size on-chip inductors play a critical role in contemporary radio-frequency integrated circuits. This work presents a reliable surrogate modeling technique combining low-fidelity EM simulation models, response surface approximations based on kriging interpolation, and space mapping technology. The reported method is useful for the development of broadband and highly accurate data-driven models of integrated...
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Highly Miniaturized Self-Diplexed U-Shaped Slot Antenna Based on Shielded QMSIW
PublicationThis article presents an efficient yet simple design approach to highly miniaturized cavity-backed self-diplexing antenna (SDA) with high-isolation. The structure employs a shielded quarter-mode substrate integrated waveguide (QMSIW). Two U-shaped slots are engraved on the top conducting plane, which realize two frequency bands and significant size reduction. The slots are excited by two independent 50Ω orthogonal feed-lines to...
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Overview of Metamaterials-Integrated Antennas for Beam Manipulation Applications: The Two Decades of Progress
PublicationMetamaterials (MMs) are synthetic composite structures with superior properties not found in naturally occurring materials. MMs have gained massive attention over the last two decades because of their extraordinary properties, such as negative permittivity and permeability. These materials enable many applications in communication subsystems, especially in the field of antenna design, to enhance gain, bandwidth, and efficiency,...
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Chemical fingerprint ofPotentillaspecies by using HPTLC method
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Study of the chromatographic behavior of selected steroid hormones on aluminum oxide plates based on quantitative structure-retention relationships
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Highly crystalline colloidal nickel oxide hole transport layer for low-temperature processable perovskite solar cell
PublicationHighly crystalline NiOX usually requires high annealing temperature (>300 °C) which is incompatible with flexible substrate and might consume high amount of energy. Herein, we demonstrate a facile emulsion process to synthesize highly crystalline, low temperature deposition (<150 °C) and solution processable NiOx nanoparticles (NPs) as a hole transport layer for the perovskite solar cells (PVSCs)....
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Ionic liquids for nano- and microstructures preparation. Part 2: Application in synthesis
PublicationIonic liquids (ILs) are widely applied to prepare metal nanoparticles and 3D semiconductor microparticles. Generally, they serve as a structuring agent or reaction medium (solvent), however it was also demonstrated that ILs can also play a role of a co-solvent, metal precursor, reducing as well as surface modifying agent. The crucial role and possible types of interactions between ILs and growing particles have been presented in...
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Massively parallel linear-scaling Hartree–Fock exchange and hybrid exchange–correlation functionals with plane wave basis set accuracy
PublicationWe extend our linear-scaling approach for the calculation of Hartree–Fock exchange energy using localized in situ optimized orbitals [Dziedzic et al., J. Chem. Phys. 139, 214103 (2013)] to leverage massive parallelism. Our approach has been implemented in the ONETEP (Order-N Electronic Total Energy Package) density functional theory framework, which employs a basis of non-orthogonal generalized Wannier functions (NGWFs) to achieve...
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Improved-Efficacy EM-Based Antenna Miniaturization by Multi-Fidelity Simulations and Objective Function Adaptation
PublicationThe growing demands for integration of surface mount design (SMD) antennas into miniatur-ized electronic devices have been continuously imposing limitations on the structure dimen-sions. Examples include embedded antennas in applications such as on-board devices, picosatel-lites, 5G communications, or implantable and wearable devices. The demands for size reduction while ensuring a satisfactory level of the electrical and field...
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Knowledge management and factors influencing its implementation in small KIBS firms – evidence from Poland
PublicationPurpose – Even if the notion of knowledge management (KM) has been introduced more than three decades ago, the application of this concept in the context of small firms has still not been sufficiently explored. The relatively few contributions, however, agree on the fact that small companies do not manage knowledge the same way as their larger counterparts. In order to fill this gap, the present paper aims to the investigate the...
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Społeczne uwarunkowania dostępności przestrzeni publicznej
PublicationDziałania projektowe urbanistów i architektów powinny iść w kierunku tworzenia pełnej dostępności przestrzeni publicznej, która spełni oczekiwania wszystkich mieszkańców, bez względu na wiek, stan zdrowia czy ogranicznia mobliności lub percepcji. Powszechna dostępność przestrzeni warunkuje prawidłowy rozwój jednostki i całych wspólnot oraz sprzyja tworzeniu zintegrowanego społeczeństwa obywatelskiego. Dla poprawy bezpieczeństwa...
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Exposure to Bisphenol A Analogs and the Thyroid Function and Volume in Women of Reproductive Age—Cross-Sectional Study
PublicationBisphenols (BPs) are commonly known plastifiers that are widely used in industry. The knowledge about the impact of BPs on thyroid function is scarce. Proper thyroid functioning is especially important for women of reproductive age, as hypothyroidism affects fertility, pregnancy outcomes and the offspring. There are no studies analyzing the influence of BPs on thyroid function and volume in non-pregnant young women. The aim of...
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Multi-objective optimization for assessment of topological modification in UWB antennas
PublicationThis paper addresses an issue of systematic and rigorous assessment of effects of topological modifications on the performance of compact UWB antennas. Application of fast surrogate-assisted multi-objective optimization procedures allows us for obtaining, in a practically acceptable timeframe, a set of designs representing the best possible trade-offs between conflicting objectives (here, antenna size minimization and reduction...
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A quaternion-based modified feistel cipher for multimedia transmission
PublicationIn this paper a quaternion-based modified Feistel Cipher is proposed. The algorithm is based on the scheme proposed by Sastry and Kumar (2012). Our algorithm uses special properties of quaternions to perform rotations of data sequences in 3D space for each of the cipher rounds. The plaintext (image in gray-tone) is divided into two square matrices of equal size which consist of Lipschitz quaternions. A modular arithmetic was implemented...
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Reliable Greedy Multipoint Model-Order Reduction Techniques for Finite-Element Analysis
PublicationA new greedy multipoint model-order reduction algorithm for fast frequency-domain finite-element method simulations of electromagnetic problems is proposed. The location of the expansion points and the size of the projection basis are determined based on a rigorous error estimator. Compared to previous multipoint methods, the quality of the error estimator is significantly improved by ensuring the orthogonality of the projection...
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Series Passive Compensation of Common Mode Voltage in Multilevel Inverter Drives
PublicationThis paper presents an approach to the problem of a magnetic saturation of CM chokes that accompanies the method of passive compensation of a common mode (CM) voltage in an inverter drive system. Measurements have been provided in a drive system including multilevel inverters and the filter having sinusoidal output voltages and zero CM voltage. The theoretical analysis and experimental results show that the problem with magnetic...
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Multilevel Converters
PublicationThe newest Special Section is intended to focus on recent research and trends in application of multilevel converters. Multilevel converters have been extensively developed over the last two decades and show several important advantages of power electronic circuits, such as: operation at high voltages, harmonics reduction, higher efficiency, modularity, smaller size and lower cost. Also, thanks to increasing interest in renewable...
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Strength parameters of masonry walls in modelling historic constructions
PublicationThe paper presents the determination of the basic material properties of a historic brickwork. Experimental studies were used to identify the basic material properties of bricks. The mechanical properties of the masonry, as an orthotropic homogenized material, were calculated. Then, numerical simulations using the Finite Element Method (FEM) were performed to verify the experimental outcomes. Macromodels with element sizes of 40,...
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Existence and uniqueness of solutions for single-population McKendrick-von Foerster models with renewal
PublicationWe study a McKendrick-von Foerster type equation with renewal. This model is represented by a single equation which describes one species which produces young individuals. The renewal condition is linear but takes into account some history of the population. This model addresses nonlocal interactions between individuals structured by age. The vast majority of size-structured models are also treatable. Our model generalizes a number...
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Optimization of the System for Determining the Volume of Tissue Needed for Breast Reconstruction
PublicationThis article presents techniques for reconstructing surfaces and volume calculations using a point cloud generated from 3D imaging. The main objective of this article was to optimize the voxel size for the most accurate representation of the surface of the female breast. We experimented with different methods for determining volume using images from the Intel D435i camera. In addition, we designed application and measurement station...
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Analysis of possibility and purposefulness of application of waste-heat boilers to trailing suction hopper dredgers
PublicationThis paper presents an analysis of possibility and purposefulness of application of waste-heat boilers to trailing suction hopper dredgers. Using results of own operational research on dredgers this author determined thermal power demand for six hypothetical trailing suction hopper dredgers of various size, at accounting for a type of power system and kind of fuel combusted by dredger's power plant. By means of basic indices of...
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Novel Structure and EM-Driven Design of Small UWB Monopole Antenna
PublicationA novel structure of a small UWB monopole antenna is presented. In our approach, a compact size is achieved by means of a meander line for current path enlargement as well as the two parameterized slits that introduce additional degrees of freedom helping to ensure good impedance matching. The antenna design is carried out using surrogate-based optimization involving variable-fidelity EM simulations. This allows us to simultaneously...
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A Concept and Design Optimization of Compact Planar UWB Monopole Antenna
PublicationA novel structure concept of a compact UWB monopole antenna is introduced together with a low-cost design optimization procedure. Reduced footprint is achieved by introduction of a protruded ground plane for current path increase and a matching transformer to ensure wideband impedance matching. All geometrical parameters of the structure are optimized simultaneously by means of surrogate based optimization involving variable-fidelity...
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ANALYSIS OF THE PUNCHING FAILURE MECHANISM IN WORKING PLATFORMS
PublicationPaper presents an analysis of the shear failure mechanism which occurs from the punching of a working platform layer in relation to its thickness, grain size arrangement and mechanical properties, taking into consideration the interaction with soft subgrade. The study is based on the observations of performance of natural scale structures (Streefkerk) and the results of model investigations numerically represented with the use...
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Reliability assessment of truss towers using Monte Carlo Method, PEM and RSM
PublicationThe paper discusses reliability assessment of simple random truss structures using three different probabilistic methodologies: the Monte Carlo Method (MCM), the Point Estimate Method (PEM) and the Response Surface Method (RSM). A benchmark truss structure and a simplified full–size engineering tower are both analyzed. A set of ultimate load numerical calculations is performed and the results are taken as the basis of advanced...
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PROBLEMS OF EXPERIMENTAL DETERMINATION OF COEFFICIENTS OF THE WEAR OF SHIP PIPING SYSTEMS
PublicationThe article presents series of considerations relating to experimental evaluation of the reliability of ship piping systems. The aim of this study is to attempt to answer the following questions: What should be the tested element? How to choose the diameter of the tested item? What should be the result of measurements and calculations? How to measure? How to choose the duration of the test? How to choose the sample size and elaborate...
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The Effect of University Campuses on the Modal Split of Polish Cities
PublicationThe article considers the effect Polish public universities have on the characteristics of urban traffic. The article describes how the public university community has changed over 25 years and its share in the urban population. The characteristics of the modal split in Polish university towns is given based on selected cases. The relation between the share of transport modes in the modal split and the size of towns or university...
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APPLYING RANSAC ALGORITHM FOR FITTING SCANNING STRIPS FROM AIRBORNE LASER SCANNING
PublicationDuring the development of the data acquired by airborne laser scanning the important issue is the fitting and georeferencing of ALS point clouds by means of the tie surfaces and the reference planes. The process of scanning strips adjustment is based on mutual integration of point clouds (scanning strips) and their adaptation to the reference planes.In simultaneous adjustment all strips are combined into one geometrically coherent...
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Reactivity of triphosphinoboranes towards H3B·SMe2: access to derivatives of boraphosphacycloalkanes with diverse substituents
PublicationTriphosphinoboranes activated the B–H bond in the BH3 molecule without any catalysts at room temperature. Hydroboration reactions led to boraphosphacyloalkanes with diverse structures. The outcomes of reactions depend on the size of the phosphanyl substituent on the boron atom of the parent triphosphinoborane, where derivatives of boraphosphacyclobutane and boraphosphacyclohexane were obtained. Furthermore, the precursor of triphosphinoboranes,...
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Zróżnicowanie zadłużenia w zależności od wielkości przedsiębiorstwa
PublicationW artykule przedstawiono różnice w sposobie kształtowania wartości wskaźników z obszaru zadłużenia pomiędzy małymi, średnimi i dużymi przedsiębiorstwami. W trakcie przeprowadzonych badań uwzględniono 97 471 sprawozdań finansowych przedsiębiorstw, prowadzących działalność gospodarczą w 12 różnych działach polskiej gospodarki narodowej. Do potwierdzenia zróżnicowania zadłużenia w zależności od wielkości przedsiębiorstwa wykorzystano...
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Wielkogabarytowe hydrodynamiczne łożyska wzdłużne
PublicationW monografii przedstawiono problemy konstrukcyjne i badawcze hydrodynamicznych łożysk wzdłużnych o dużych średnicach. Łożyska takie stanowią istotne i niezwykle odpowiedzialne podzespoły hydrogeneratorów elektrowni wodnych. Z uwagi na rozmiary (średnice przekraczają niekiedy 5 metrów) i złożoność zjawisk łożyska te wymagają specjalnej postaci konstrukcyjnej, a ich dokładna analiza obliczeniowa przysparza wiele problemów. Dodatkowo...
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ZRÓŻNICOWANIE PŁYNNOŚCI FINANSOWEJ W ZALEŻNOŚCI OD WIELKOŚCI PRZEDSIĘBIORSTWA
PublicationW artykule przedstawiono różnice w sposobie kształtowania wartości wskaźników z obszaru płynności finansowej pomiędzy małymi, średnimi i dużymi przedsiębiorstwami. W trakcie przeprowadzonych badań uwzględniono 97 471 sprawozdań finansowych przedsiębiorstw, prowadzących działalność gospodarczą w 12 różnych działach polskiej gospodarki narodowej. Do potwierdzenia zróżnicowania płynności finansowej w zależności od wielkości przedsiębiorstwa...
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Surrogate-assisted EM-driven miniaturization of wideband microwave couplers by means of co-simulation low-fidelity models
PublicationThis article proposes a methodology for rapid design optimization of miniaturized wideband couplers. More specifically, a class of circuits is considered, in which conventional transmission lines are replaced by their abbreviated counterparts referred to as slow-wave compact cells. Our focus is on explicit reduction of the structure size as well as on reducing the CPU cost of the design process. For the sake of computational feasibility,...
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Amperometric sensing of chemical oxygen demand at glassy carbon and silicon electrodes modified with boron-doped diamond
Publication.A boron-doped diamond (BDD) sensor is proposed for effective detection of chemical oxygen demand (COD) by means of amperometric technique. Boron-doped diamond thin films, acting as active sensors, were deposited on both silicon wafer and glassy carbon (GC) substrates by microwave plasma assisted chemical vapour deposition. SEM micrographs showed that BDD–Si displays triangle-faceted crystallites ca. 0.5–3 μm in size, while BDD–GC...
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Thermal and physical properties of ZrO2–AlO(OH) nanopowders synthesised by microwave hydrothermal method
PublicationIndustrially relevant nanopowder was synthesised by microwave hydrothermal synthesis to obtain well-controlled composition (ZrO2–AlO(OH) system) which was found to determine a number of physical and thermal characteristics. This study reports variation of particle size, density, specific surface area (SSABET), as well as thermal behaviour of nanopowder mixtures of ZrO2–AlO(OH) in the whole range of compositions. It was found that...