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Search results for: TECHNIKA IMPLICIT SOLVENT
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Dorota Hodyl mgr
PeopleAbsolwentka filologii polskiej ze specjalizacją tekstologiczno-edytorską i przygotowaniem pedagogicznym na Uniwersytecie Mikołaja Kopernika w Toruniu. Ukończyła studia podyplomowe na kierunku bibliotekoznawstwo i informacja naukowa na Uniwersytecie Warmińsko-Mazurskim w Olsztynie. Posiada tytuł technika administracji. Zawodowo związana z bibliotekarstwem, branżą dziennikarską i redaktorską. Pracę w Bibliotece Politechniki...
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Excited-state proton transfer and geminate recombination in the molecular cage of β-cyclodextrin
PublicationExcited-state proton transfer and geminate recombination in aqueous heptakis(2,6-di-O-methyl)-β-cyclodextrin have been compared with those in water by monitoring the photoinduced prototropic tautomerization of 6-hydroxyquinoline, which occurs via forming anionic intermediate. Enol deprotonation decelerates by 18 times whereas its reverse process accelerates slightly with encapsulation. The imine protonation of the intermediate...
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Synthesis and properties of carboxy derivative of Epidian 6 monomethacrylate (in English)
PublicationWe present the synthesis of an oligomer with carboxy and methacrylic groups based on Epidian 6. The effect of the catalyst nature and amount, solvent nature and process temperature on the rate of the reaction between Epidian6 monomethacrylate and adipic acid was examined at 313, 323 and 333 K in the presence of 4-dimethylaminopyridine, 1,4-diazobicyclo[2.2.2]octane, and benzyltriammonium chloride. The synthesized oligomer was characterized...
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Deis assessment of intergranular corrosion process proceeding on AISI 304 stainless steel
PublicationW pracy przedstawiono nowe podejście do badania mechanizmu i intensywności korozji międzykrystalicznej. Badania przeprowadzono przy wykorzystaniu techniki dynamicznej elektrochemicznej spektroskopii impedancyjnej (DEIS), która pozwala na jednoczesne rejestrowanie chwilowych zmian impedancji oraz prądu stałego badanego układu. Tym samym możliwe jest otrzymanie z jednego pomiaru informacji dotyczących zarówno mechanizmu korozji międzykrystalicznej,...
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Chromatografia gazowa z detekcją olfaktometryczną (GC-O) w analizie żywności. Cz. I. Charakterystyka metody
PublicationW ostatnich latach prowadzone są intensywne badania nad aktywnością sensoryczną poszczególnych składników zapachów żywności, a także napojów alkoholowych i nad zależnościami pomiędzy zapachem, a składem chemicznym lotnej frakcji tych produktów. Z oczywistych powodów największe zastosowanie w oznaczaniu lotnych substancji zapachowych znajduje chromatografia gazowa z różnymi wariantami detekcji. Większość osiągnięć w tej dziedzinie...
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Zastosowanie techniki dozymetrii pasywnej do oceny jakości powietrza wewnętrznego. Application of passive sampling technique for assessment of indoor air quality
PublicationJakość powietrza wewnętrznego jest istotnym parametrem wpływającym na dobre samopoczucie i zdrowie człowieka. Kluczowego znaczenia nabiera więc jego nieustanna kontrola i oznaczanie zawartości zanieczyszczeń, które występują w nim na bardzo niskich poziomach stężeń. Do pomiarów jakości powietrza wewnętrznego często wykorzystywana jest (znana od ponad pół wieku) technika dozymetrii pasywnej. W literaturze nadal pojawiają się doniesienia...
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Model symulacyjny i badania sieci MPLS.
PublicationMultiprotocol Label Switching (MPLS) to obiecująca technika, umożliwiająca wsparcie jakości usług w sieciach szkieletowych opartych na protokole IP. Aby skorzystać z jej potencjalnych zalet, należy opracować skuteczne procedury i metody gwarantujące realizację jakości usług. Jednym z kluczowych zagadnień w tym obszarze badań jest kierowanie ruchem (ruting), a niezbędnym narzędziem odpowiedni program symulacyjny do modelowania zjawisk...
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Kompletna dwuwymiarowa chromatografia gazowa - nowoczesne narzędzie analityczne - cz. III. Zastosowania i kierunki rozwoju
PublicationTechnika GC×GC znajduje szerokie zastosowanie w takich obszarach badawczych jak: przemysł petrochemiczny, ochrona środowiska, przemysł kosmetyczny i perfumeryjny, analiza żywności, analiza kliniczna, badania kosmiczne (np. analiza fragmentów meteorytów), metabolomika (np. badanie ludzkiego oddechu) i proteomika (np. identyfikacja białek w próbkach biologicznych) oraz kryminalistyka. W artykule przedstawiono przykłady zastosowań...
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How to make membrane distillation greener? A review on environmentally friendly and sustainable aspects
PublicationThere is an urgent need for the development of new water resources in order to solve the problem of the world’s growing demand for clean water. Membrane distillation (MD) is a promising alternative to conventional seawater desalination. Although MD itself is often defined as sustainable desalination technology, there are many aspects within the membrane manufacture and process operation that make it far from being green. For instance,...
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Fast, sensitive and reliable multi-residue method for routine determination of 34 pesticides from various chemical groups in water samples by using dispersive liquid – liquid microextraction coupled with gas chromatography – mass spectrometry
PublicationA simple and efficient dispersive liquid-liquid microextraction technique (DLLME) was developed by using a mixture of two solvents: 40 μL of tetrachlorethylene (extraction solvent) and 1.0 mL of methanol (disperser solvent), which was rapidly injected with a syringe into 10mL ofwater sample. Some important parameters affecting the extraction efficiency, such as type and volume of solvents, water sample volume, extraction time,...
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New approach for e-cigarette aerosol collection by an original automatic aerosol generator utilizing melt-blown non-woven fabric
PublicationCurrently, there is lack of standardized conditions for the collection and analysis of e-cigarette (EC) aerosol. Considering the urgent need for the development of these guidelines, a procedure for EC aerosol analysis was developed. A novel automatic e-cigarette aerosol generator was designed. For the first time, melt-blown non-woven fabric was applied for the effective uptake of compounds released from vaporized e-liquid. The...
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A Green Chemistry "environmentally friendly" approach to the synthesis of chloro-intermediates of ephedrine/pseudoephedrine
PublicationMethylamphetamine is an addictive stimulant drug that strongly activates certain systems in the brain. It is closely related chemically to amphetamine, but the central nervous system effects of methamphetamine are greater. There is much interest in methylamphetamine among scientists and therefore the synthesizes of methylamphetamine and its metabolites are carried out on a large scale in chemical laboratories. Globally, ephedrine...
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Development and Validation of SPE-HPLC-MS/MS Method for Determining Cyclophosphamide in Surface Waters
PublicationA rapid and selective method for trace amounts determination of cyclophosphamide in surface water samples has been developed. A solid phase extraction SPE method for extraction and clean-up procedure has been optimized for determination by reversed-phase high-performance liquid chromatography with tandem mass spectrometry. The analyses proceed in the positive ion mode by means of the electrospray ionization method (ESI). Clean...
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Development of thin film SPME sorbents based on deep eutectic solvents and their application for isolation and preconcentration of endocrine-disrupting compounds leaching from diapers to urine
PublicationIn this study, the thin film solid phase microextraction (TF-SPME) based on a novel sorbent composed of deep eutectic solvent (DES) is proposed. Among several synthesized sorbents the most efficient was DES containing trihexyl(tetradecyl)phosphonium chloride and docosanol mixed with polydimethylsiloxane (PDMS) in a molar ratio 1:3:0.25 to achieve a more stable structure. The proposed sorbent was applied on a fiberglass mesh and...
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Solubility enhancement of metronidazole using natural deep eutectic solvents: Physicochemical and thermodynamic studies
PublicationThis research aimed to explore the utility of natural deep eutectic solvents (NADES) as the co-solvents for slightly water-soluble metronidazole (MNZ). After testing 70 wt% (percentage by weight) aqueous mixtures of seven NADESs, it was found that MNZ had the highest solubility in water solutions of NADES composed of choline chloride (ChCl) and citric acid (CA). The solubility of MNZ (expressed as 103 mol fraction) increased with...
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Emissions of selected monoaromatic hydrocarbons as a factor affecting the removal of single-use polymer barbecue and kitchen utensils from everyday use
PublicationThe main focus of this study is the emission of monoaromatic hydrocarbons because these are the preliminary factors of potential solvent and monomer residues present in single-use plastic barbecue and kitchen utensils comprising polystyrene, polypropylene, natural cellulose, and biodegradable polymers intended for use with hot meal or beverages. Herein, the emissions of monoaromatic hydrocarbons (styrene, benzene, toluene, ethylbenzene,...
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A new approach to a fast and accurate design of microwave circuits with complex topologies
PublicationA robust simulation-driven design methodology of microwave circuits with complex topologies has been presented. The general method elaborated is suitable for a wide class of N-port unconventional microwave circuits constructed as a deviation from classic design solutions. The key idea of the approach proposed lies in an iterative redesign of a conventional circuit by a sequential modification and optimisation of its atomic building...
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Liquefaction of macroalgae Enteromorpha biomass for the preparation of biopolyols by using crude glycerol
PublicationThis article describes the liquefaction process of macroalgae Enteromorpha with the use of crude glycerol as a solvent and a reagent, aimed at obtaining of new bio-polyols, which are characterized with respect to their chemical structure, physical and thermal properties. Six different biopolyols were prepared. In order to optimize the liquefaction of algal biomass for the best bio-polyol properties, two catalysts (sulfuric or orthophosphoric...
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The hydration of selected biologically relevant molecules – the temperature effect on apparent molar volume and compression
PublicationThe densities and sound velocities at T = (288.15, 293.15, 298.15, 303.15 and 308.15) K were measured for aqueous solutions of glycine, trimethylamine-N-oxide, taurine and N-methylacetamide. From these data, the apparent molar volumes, V the apparent molar isentropic compressions, KS,, and the Passynski hydration numbers of solutes were determined. The concentration dependencies of the calculated quantities, their limiting values...
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Preparation, characterization and antimicrobial activity of polyvinyl alcohol/gum arabic/chitosan composite films incorporated with black pepper essential oil and ginger essential oil
PublicationIn this study, biocomposite films based on polyvinyl alcohol (PVA), gum arabic (GA) and chitosan (CS) incorporated with BPEO and GEO were fabricated by solvent casting method. FTIR, XRD, SEM and DSC were performed with mechanical and antimicrobial properties of PVA/GA/CS films with and without BPEO and GEO. The BPEO and GEO incorporated PVA/GA/CS films were significantly inhibited the growth of Bacillus cereus, Staphylococcus aureus,...
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Zaufanie w detalicznych transakcjach internetowych
PublicationAutor wprowadza rozróżnienie pomiędzy zaufaniem w relacji interpersonalnej (RI) i nieinterpersonalnej (RN). Odwołując się do analizy Dylematu Więźnia w teorii gier i przywołując teorię kooperacji B. Williamsa, autor pokazuje, że logiczna struktura zaufania powinna zostać uzupełniona przez nieegoistyczne mikro-motywacje. W detalicznym handlu elektronicznym istnieją dwie przeciwstawne tendencje: człowiek i technika. Technologia powoduje...
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Bezpośrednia analiza próbek z wykorzystaniem techniki spektrometrii mas. Cz. I. Rozwiązania metodyczne w zakresie spektrometrii mas umożliwiające bezpośrednią analizę próbek
PublicationTechnika spektrometrii mas stanowi jedno z najważniejszych narzędzi analitycznych, wykorzystywanych do identyfikacji, określania struktury chemicznej oraz oznaczania stężeń wielu związków chemicznych. Aby zidentyfikować obecne w próbkach rzeczywistych anality, konieczne jest jednak z reguły ich wstępne rozdzielenie, toteż spektrometry mas pełnią najczęściej rolę detektora np. w przypadku technik łączonych, gdy na etapie rozdzielania...
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Fizyczne Metody Badań Materiałów II 2022
e-Learning CoursesFizyczne podstawy Metod Badań Nieniszczących stosowanych w przemyśle. Efekt Barkhausena, prądy wirowe, pole magnetyczne rozproszone, impulsy magnetostrykcyjne, technika ultradźwiękowa, termowizja. Podstawy defektoskopii, nieniszczące techniki badania struktury, wyznaczanie rozkładu naprężenia.
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Multi-objective optimization of microextraction procedures
PublicationOptimization of extraction process requiresfinding acceptable conditions for many analytes and goodperformance in terms of process time or solvent consumption. These optimization criteria are oftencontradictory to each other, the performance of the system in given conditions is good for some criteriabut poor for others. Therefore, such problems require special assessment tools that allow to combinethese contradictory criteria into...
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Assessing Acute Toxicity and Endocrine Disruption Potential of Selected Packages Internal Layers Extracts
PublicationThe focus of the present study is migration of toxic substances from food contact materials and its actual influence on the health of the final consumer. Two food packagings (metal cans, TetraPack®) and five simulants medias (water, ethanol, acetic acid, DMSO, artificial saliva) were selected for simulation studies. For assessment of acute toxicity and endocrine disruption potential of extract samples, two biotests (Microtox® and...
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Synergistic effect of multi walled carbon nanotubes and reduced graphene oxides in natural rubber for sensing application
PublicationUtilizing the electrical properties of polymer nanocomposites is an important strategy to develop high performance solvent sensors. Here we report the synergistic effect of multi walled carbon nanotubes (MWCNTs) and reduced graphene oxide (RGO) in regulating the sensitivity of the naturally occurring elastomer, natural rubber (NR). Composites were fabricated by dispersing CNTs alone and together with exfoliated RGO sheets (thermally...
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Miniaturized solid-phase extraction techniques
PublicationMore than 80% of analysis time is spent on sample collection and sample preparation, so sample preparation is a critical part of the analytical process. Traditionally, liquid-liquid extraction was developed and employed to screen for general unknowns. However, solid-phase extraction (SPE) is becoming highly popular as an alternative, due to its simplicity and economy in terms of time and solvent. This review summarizes the current...
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Salicylaldimine-based receptor as a material for iron(III) selective optical sensing
Publicationα,α-Bis(salicylimino)-m-xylene (L) was prepared using both conventional and microwave-assisted procedure. The compound exhibits ability to colorimetric recognition of iron(III) ions in aqueous environment, what is shown by significant color change from yellow to purple. In DMSO : water (9:1 v/v) solvent system receptor creates with iron(III) cations complexes of 2:1 stoichiometry (L:Fe3+) with stability constant (log K) 7.54±0.21....
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Coupled nonlinear Schrödinger equations in optic fibers theory
PublicationIn this paper a detailed derivation and numerical solutions of CoupledNonlinear Schr¨odinger Equations for pulses of polarized electromagnetic wavesin cylindrical fibers has been reviewed. Our recent work has been compared withsome previous ones and the advantage of our new approach over other methods hasbeen assessed. The novelty of our approach lies is an attempt to proceed withoutloss of information within the frame of basic...
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Atomistic Surrogate-Based Optimization for Simulation-Driven Design of Computationally Expensive Microwave Circuits with Compact Footprints
PublicationA robust simulation-driven design methodology for computationally expensive microwave circuits with compact footprints has been presented. The general method introduced in this chapter is suitable for a wide class of N-port un-conventional microwave circuits constructed as a deviation from classic design solutions. Conventional electromagnetic (EM) simulation-driven design routines are generally prohibitive when applied to numerically...
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On the relationship between the structural and volumetric properties of solvated metal ions in O-donor solvents using new structural data in amide solvents
PublicationThe structures of the N,N-dimethylformamide (dmf), N,N-dimethylacetamide (dma), and N,N-dimethylpropionamide (dmp) solvated strontium and barium ions have been determined in solution using large angle X-ray scattering and EXAFS spectroscopy. The strontium ion has a mean coordination number (CN) between 6.2 and 6.8, and the barium ion has a mean CN between 7.1 and 7.8 in these amide solvents. The non-integer numbers indicates that...
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DETERMINATION OF SURFACTANTS IN ENVIRONMENTAL SAMPLES - PART I. CATIONIC COMPOUNDS = Oznaczanie Surfaktantów W Próbkach Środowiskowych. Część I. Związki Kationowe
PublicationCompounds from the group of cationic surfactants are widely applied in household, industrial, cleaning, disinfectant, cosmetic and pharmaceutical products as their specific properties (antimicrobial, emulsifying, anticorrosion, softening). After use, cationic surfactants are disposed to wastewater-treatment plants and finally with effluent water to surface waters due to their incomplete degradation. Moreover, they can freely circulate...
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Determination of Surfactants in Environmental Samples. Part III. Non-Ionic Compounds
PublicationNon-ionic surface active agents are a diverse group of chemicals which have an uncharged polar head and a non-polar tail. They have different properties due to amphiphilic structure of their molecules. Commercial available non-ionic surfactants consist of the broadest spectrum of compounds in comparison with other types of such agents. Typically, non-ionic compounds found applications in households and industry during formulation...
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'23/'24 Badanie żywności techniką PCR
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'21/'22 Badanie żywności techniką PCR
e-Learning CoursesCEL: Student identyfikuje i klasyfikuje patogeny oraz grzyby toksynotwórcze w żywności i ocenia ich szkodliwość. Przedstawia podstawowe systemy diagnostyczne, stosowane do wykrywania zafałszowań w żywności. Wyjaśnia zasady działania techniki PCR.
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TOiS-w (TOiS: Metody Numeryczne i Narzędzia OiS - wykład ) 2024
e-Learning Courses1. "Technika obliczeniowa i symulacyjna" - wykład (Metody Numeryczne) dla EiT, sem. 2, na studiach I stopnia Wykładowca: dr inż. B. Stawarz-Graczyk 2. "Technika obliczeniowa i symulacyjna" - wykład (z zagadnień dotyczących PSpice'a i Matlaba) dla EiT, sem. 2, na studiach I stopnia Wykładowcy: dr inż. Jan Schmidt (PSpice, Matlab) Osoba odpowiedzialna za przedmiot: dr inż. Jan Schmidt KSON WETI PG
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Genotyping and characterization of virulence factors in Escherichia coli strains isolated from patients from Polish hospital
PublicationZakażenia układu moczowego (UTIs - ang. urinary track infections) są jedną z najczęstszy infekcji, za które w 85% przypadków odpowiedzialne są bakterie Escherichia coli. Infekcje układu moczowego mogą prowadzić do groźnych powikłań m. in. odmiedniczkowego zapalenia nerek. Śmiertelność wśród tej grupy pacjentów wynosi 1-3%. Zakażenia układu moczowego występują również u ok. 7% kobiet ciężarnych. W pracy przebadano 82 szczepy E....
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Maximum transportation growth in energy and solute particles in Prandtl martial across a vertical 3D-heated surface: Simulations achieved using by finite element approach
PublicationThe goal of this study is to determine the maximum energy and solute particles' transportation growth in a 3D-heated region of Prandtl martial through a dynamic magnetic field. The effects of this field on the properties of solvent molecules and heat conduction are studied. A correctly stated functional method and a finite element approach are comparable to a certain type of differential equations. In order demonstrate the effects...
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Polyurethanes for Coating, Adhesives, and Other Applications
PublicationAn interesting group of polyurethane (PU) materials are coatings, adhesives, sealants, and thickeners. A wide base of raw materials and various methods of PU synthesis allows production of materials with a wide range of properties that can be commonly used in many industries. This chapter describes the main types of PU coatings and adhesives and special application PUs and the methods of their production. The materials described...
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Visualizing spatially decomposed intermolecular correlations in the infrared spectra of aprotic liquids
PublicationInfrared (IR) spectroscopy is commonly used to study intermolecular interactions in the liquid phase, including solvation phenomena. On the other hand, ab initio molecular dynamics (AIMD) simulations offer the possibility to obtain IR spectra from first principles. Surpassing the experiment, AIMD simulations can deliver additional information on the spatial intermolecular correlations underlying the IR spectrum of the liquid. Although...
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Występ Ireneusza Krosnego
EventsWszystkich studentów i pracowników Politechniki Gdańskiej zapraszamy do Akademickigo Klubu Politechniki Gdańskiej "Kwadratowa" na darmowy występ Ireneusza Krosnego – Teatr Jednego Mima.
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Identification of continuous systems - Practical issues of insensitivity to perturbations
PublicationIn this paper the issue of continuous systems estimation, insensitive to certain perturbations, is discussed. Such an approach has rational advantages, especially when robust schemes are used to assist a target system responsible for industrial diagnostics. This requires that estimated model parameters are generated on-line, and their values are reliable and to a great extent accurate. Practical hints are suggested to challenge...
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Identification of Continuous Systems - Practical Issues of Insensitivity to Perturbations
PublicationIn this paper the issue of continuous systems estimation, insensitive to certain perturbations, is discussed. Such an approach has rational advantages, especially when robust schemes are used to assist a target system responsible for industrial diagnostics. This requires that estimated model parameters are generated on-line, and their values are reliable and to a great extent accurate. Practical hints are suggested to challenge...
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Wspomaganie diagnostyki układu oddechowego przez modelowanie parametrów respiracji metodą oscylacji wymuszonych
PublicationCelem pracy jest weryfikacja praktycznej przydatności parametrów modeli procesu respiracji w diagnostyce układu oddechowego. Poddana ocenie została technika oscylacji wymuszonych. Wyniki badań eksperymentalnych zaczerpnięto z literatury. Wykorzystano cztero- i sześcioparametrowy model procesu respiracji. Estymaty parametrów porównano z wynikami badań przeprowadzonymi u osób, u których stwierdzono zaburzenia układu oddechowego....
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Obrazowanie parametryczne w badaniach mózgu metodami MRI/PET
PublicationCelem tej monografii jest przedstawienie technik obrazowania metodami tomografii rezonansu magnetycznego (MRI - Magnetic Resonance Imaging) i pozytonowej tomografii emisyjnej (PET - Positron Emission Tomography) w kontekście badań dynamicznych mózgu, szczególnie w zakresie syntezy obrazów parametrycznych opisujących jakościowo lub ilościowo przepływ mózgowy. Obrazowanie parametryczne określa technikę syntezy obrazów na podstawie...
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PCA application in assessment of fertilizer plant impact on different components of environment
PublicationW pracy podjęto próbę oceny wpływu Gdańskich Zakładów Nawozów Fosforowych "Fosfory" S.A. na najbliższe środowisko. W pracy przedstawiono wyniki świadczące o jakości różnych komponentów środowiska na terenie objętym wpływem zakładu. W pracy przedstawiono wyniki oznaczeń 44 pierwiastków w 46 próbkach gleb i traw pobieranych na terenie fabryki oraz w bezpośrednim sąsiedztwie. 37 z 44 oznaczonych pierwiastków użyto do wykonania analiz...
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Electronic nose as a tool for differentiation of volatile organic compounds = Elektroniczny nos jako instrument do rozróżniania lotnych związków organicznych
PublicationW pracy porównano dwie metody analizy zapachów lotnych związków organicznych: klasyczną analizę opartą na percepcji ludzkiego węchu i technikę elektronicznego nosa. W przeprowadzonych badaniach za pomocą klasycznej analizy brało udział 8 ochotników w okresie 2 tygodni. Do instrumentalnej metody analizy zapachu wykorzystano zaprojektowany przez autorów prototypowy 6-cio czujnikowy elektroniczny nos. Przeprowadzone badania z wykorzystaniem...
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The hydration of the protein stabilizing agents: trimethylamine-N-oxide, glycine and its N-methylderivatives - the volumetric and compressibility studies
PublicationThe densities at T = (288.15, 293.15, 298.15, 303.15, and 308.15) K and sound velocities at T = 298.15 K have been measured for aqueous solutions of trimethylamine-N-oxide, glycine, N-methylglycine (sarcosine), N,N-dimethylglycine, N,N,N-trimethylglycine (betaine). From these data the apparent molar volumes, VΦ, the apparent molar isentropic compressions, KS,Φ, and the solvation numbers of solutes have been determined. The concentration...
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Green sample preparation techniques for chromatographic determination of small organic compounds
PublicationAccurate monitoring of the state of the environment requires the introduction of additional isolation and/or preconcentration step prior to the chromatographic determination. In this work the information about novel methodological and instrumental solutions in relation to different variants of microextraction techniques are presented. Attention is focused on analytical procedure and suitable analytical tools for extraction of the...
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Chemometrics approaches to green analytical chemistry procedure development
PublicationChemometric tools are widely used in analytical chemistry for the reduction of data dimensionality, grouping of variables and processing of analytical signals. They have also the potential to be applied in analytical procedure development with the aim of minimizing the procedure’s environmental impact. The design of experiment gives the possibility to obtain much better information on the system response than in case of “changing...