Wyniki wyszukiwania dla: KISSINGER’S METHOD - MOST Wiedzy

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Wyniki wyszukiwania dla: KISSINGER’S METHOD

  • Efficient Method for the Synthesis of Functionalized Basic Maleimides

    A three-step procedure involving Diels-Alder condensation of maleic anhydride with furane, formation of N-substituted imide upon reaction with appropriate diamine and a final retro Diels-Alder regeneration of the maleic carbon-carbon double bond is proposed for an unequivocal synthesis of N-substituted basic maleimides. The novel method is characterized by mild reaction conditions, easy work-up, high yields and no need for additional...

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  • Using A Particular Sampling Method for Impedance Measurement

    The paper presents an impedance measurement method using a particular sampling method which is an alternative to DFT calculation. The method uses a sine excitation signal and sampling response signals proportional to current flowing through and voltage across the measured impedance. The object impedance is calculated without using Fourier transform. The method was first evaluated in MATLAB by means of simulation. The method was...

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  • Usefulness of the voltamperometric method for assessment of the purity of soil

    This paper presents a voltammetric analysis of soil. It shows that the voltammetry is a useful method for the assessment of soil contaminated with heavy metal ions. There are two major problems with voltammetry analysis: the diffusion coefficient and the measurement system. The paper contains a short literature study of mathematical equations and a study of differences between soil and water measurements. Suggestions of the solution...

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  • Method of determining the residual fluxes in transformer core

    Publikacja

    - Rok 2017

    The article presents the method of calculating the residual induction in transformer columns. The method is based on measurement of the magnetic induction in selected points around the transformer core. The values of residual induction are calculated as linear combination of the results of measurement.

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  • Fabrication of Bi6Fe2Ti3O18 Ceramics by Mixed Oxide Method

    In the present study Bi6Fe2Ti3O18 (BFTO) ceramics has been fabricated by solid state reaction from the mixture of simple oxides viz. Bi2O3, TiO2 and Fe2O3. Stoichiometric mixture of the powders was thermally analyzed so parameters of the thermal treatment were determined. The EDS measurements have shown conservation of the chemical composition of the ceramic powder after calcination. Hot-pressing method was used for final densification...

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  • Detection of the Oocyte Orientation for the ICSI Method Automation

    Automation or even computer assistance of the popular infertility treatment method: ICSI (Intracytoplasmic Sperm Injection) would speed up the whole process and improve the control of the results. This paper introduces a preliminary research for automatic spermatozoon injection into the oocyte cytoplasm. Here, the method for detection a correct orientation of the polar body of the oocyte is presented. Proposed method uses deep...

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  • Newton’s Method for the McKendrick-von Foerster Equation

    Publikacja

    - Rok 2020

    In the paper we study an age-structured model which describes the dynamics of one population with growth, reproduction and mortality rates. We apply Newton’smethod to the McKendrick-von Foerster equation in the semigroup setting. We prove its first- and second-order convergence.

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  • Hyperbolic Asynchronous Method of a Radio Navigation Technique

    Humans have always wanted to determine position in an unknown environment. At the beginning methods were simple. They were based on the observation of characteristic points, in the case of shipping additional observations of the coastline. Then came navigation based on astronomical methods (astronavigation). At the beginning of the XX-century a new way of determining the current location was developed. It has used radiowave signals....

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  • Engineering method of tire rolling resistance evaluation

    Publikacja

    Tire rolling resistance is one of the most difficult tire parameters to measure. The reason is that for modern tires the force of rolling resistance corresponds to 0.5–1% of tire load, thus measurements of very small forces must be performed in a heavily loaded system. This constitutes great problems, especially in road conditions. Laboratory measurements are easier to perform, as the environment may be better controlled, but roadwheel...

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  • Validity of MRI brain perfusion imaging method

    Publikacja

    W artykule zaprezentowano zbiór analiz dotyczących walidacji metody DSC-MRI. Zbadano wpływ rozmycia, opóźnienia, niskiego SNR bolusa oraz innych możliwych źródeł zakłócających wartość parametru perfuzji. Różne metody uzyskiwania parametrów perfuzji zostały zaprezentowane i porównane.

  • A method of identification of RTS components in noise signals

    W artykule przedstawiono oryginalną metodę wydzielania szumu RTS (Random Telegraph Signal) - dwupoziomowego lub wielopoziomowego - z sygnału szumowego. Podstawą oceny jakości metody jest założenie, że wartości chwilowe szumu RTS mają rozkład niegaussowski natomiast pozostała część sygnału ma rozkład gaussowski.Algorytm identyfikacji wielopoziomowych szumów RTS w sygnałach szumowych małej częstotliwości oparty został na aproksymacji...

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  • Digital mono-pulse method in cylindrical antena.

    Artykuł prezentuje metodę poprawy dokładności namiaru w wielowiązkowym sonarze z anteną cylindryczną. Metoda oparta jest na metodzie monopulsowej, wykorzystywanej w radarach i sonarach. Metoda zapewnia dobrą dokładność namiaru dla pojedynczego impulsu sondującego. Jedyna modyfikacja w stosunku do metody oryginalnej polega na wytworzeniu dwóch odchylonych wiązek i wykonaniu prostych obliczeń. Symulacja komputerowa dowodzi , że uzyskanie...

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  • Validity of MRI brain perfusion imaging method

    W artykule zaprezentowano zbiór analiz dotyczących walidacji metody DSC-MRI. Zbadano wpływ rozmycia, opóźnienia, niskiego SNR bolusa oraz innych możliwych źródeł zakłócających wartość parametru perfuzji. Różne metody uzyskiwania parametrów perfuzji zostały zaprezentowane i porównane.

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  • An new method of audio-visual correlation analysis

    Publikacja

    - Rok 2009

    This paper presents a new methodology of conducting the audio-visual correlation analysis employing the gaze tracking system. Interaction between two perceptual modalities, seeing and hearing, their interaction and mutual reinforcement in a complex relationship was a subject of many research studies. Earlier stage of the carried out experiments at the Multimedia Systems Department (MSD) showed that there exists a relationship between...

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  • Circular saw blade dynamics - the measurement method

    W pracy przedstawiono przyczyny i efekty zmiany położenia ostrzy piły tarczowej w układzie przecinania. Przedstawiony sposób pomiaru dynamiki piły tarczowej umożliwia określenie przyczyn drgań, co stanowi podstawę skutecznej ich minimalizacji.

  • Method for improving multibeam sonar bearing accuracy

    Przedstawiono prostą metodę poprawy dokładności namiarów w sonarach wielowiązkowych. Zasada zaproponowanej metoda jest zbliżona do metody monopulsowej stosowanej powszechnie w radarach i sonarach. Nie wymaga jednak ręcznego lub automatycznego obracania wiązek, co wydatnie zmniejsza potrzebne nakłady obliczeniowe procesorów sonaru Stosowanie metody daje znaczne zmniejszenie błędów namiarów przy względnie dużym wyjściowym stosunku...

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  • A Method for Optimising the Blade Profile in Kaplan Turbine

    Publikacja

    - Rok 2011

    This paper introduces a method of blade profile optimisation for Kaplan-type turbines, based on modelling the interaction between rotor and stator blades. Rotor and stator blade geometry is described mathematically by means of a midline curve and thickness distribution. Genetic algorithms are then used to find a global optimum that minimises the loss coefficient. This allows for variety of possible blade shapes and configurations....

  • On neutral differential equations and the monotone iterative method

    The application of the monotone iterative method to neutral differential equations with deviating arguments is considered in this paper. We formulate existence results giving sufficient conditions which guarantee that such problems have solutions. This approach is new and to the Authors' knowledge, this is the first paper when the monotone iterative method is applied to neutral first-order differential equations with deviating...

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  • A new and convenient method for the preparation of functionalized phosphorothioates

    Publikacja

    - SYNTHESIS-STUTTGART - Rok 2011

    A new and efficient method for the synthesis of alkyl and aryl phosphorothioates in high yields via the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives with trimethyl phosphite was developed.

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  • A method for evaluating durability of porous slide bearings

    Publikacja

    The article presents the structures of porous bearings bushes and greasy lubricants, and the similarity criterion resulting from this structures. A phisical model is proposed which describes the operation of the porous slide bearing bush taking into account, via analogy, the phenomena taking place in the grease lubricant nodes instead of those observed in the bush structures.Included are the result of experimental tests of three...

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  • Quaternion Encryption Method for Image and Video Transmission

    Quaternions are hyper-complex numbers of rank 4. They are often applied to mechanics in 3D space and are considered to be one of the best ways of representing rotations. In this paper a quaternion encryption method, based on algorithm by Nagase et al. (2004) has been proposed. According to a computer-based simulation the results of the performed research yield a high level of security, which is additionally strengthened by the...

  • Application of the J-matrix method to multichannel scattering

    In this contribution we describe the multichannel extension to the nonrelativistic J-matrix method, and present differential cross sections for scattering of slow electrons from Argon atoms. Nonrelativistic phase shifts, then the S-matrix and the cross sections have been calculated using newly developed Fortran code, JMATRIX-MULTI.We applied the model Hartree-Fock potential as the scattering potential, which was truncated in the...

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  • A method of nonlinearities of transformer no-load characteristic modelling

    Publikacja

    A way in which changes of the no-load characteristic are taken into account in the mathematical model of the transformer is presented. Changes of saturation within core of transformer are presented as a combined non-linear flux curve. Analysis of magnetization of the transformer core and simulation of no-load state for distribution transformer of 30 kVA power rating and 15.75/0.4 kV/kV (especially supplying VLV) transformation...

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  • Doppler estimation method for moving target location

    Publikacja

    Artykuł opisuje nowy algorytm lokalizacji obiektów ruchomych bazujących na analizie odchyłek dopplerowskich sygnałów odebranych z sieci hydrofonów rozmieszczonych równomiernie w obserwowanym akwenie. Źródłem analizowanych sygnałów są fale ciągłe o niskim natężeniu odbite od obiektu ruchomego. W artykule została przedstawiona postać algorytmu oraz wyniki symulacji komputerowych.

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  • The particle method for simulation of self-organization phenomena

    Publikacja

    - Rok 2011

    The aim of the work was to design, implement, and use, in a number of experiments, an abstract software environment (an artificial world)suitable for modelling systems consisting of many moving and interactingobjects distributed in space. The environment, named DigiHive, is directed towards modeling of complex systems manifested by processes of self-organization, self-reproduction and self modifications. The environment is mainly...

  • Soft – Partial Frequency Reuse Method for LTE-A

    Publikacja

    In the paper a novel SPFR frequency reuse method is proposed which can be used for improvement of physical resources utilization efficiency in LTE-A. The proposed method combines both SFR and PFR giving the possibility of more flexible use of frequency band in different regions of a cell. First, a short study on the problem of frequency reuse in cells is discussed including bibliography overview....

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  • Rothe’s method for physiologically structured models with diffusion

    Publikacja

    - Mathematica Slovaca - Rok 2018

    We consider structured population models with diffusion and dynamic boundary conditions. The respective approximation, called Rothe’s method, produces positive and exponentially bounded solutions. Its solutions converge to the exact solution of the original PDE.

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  • Arching of railway turnouts by analytical design method

    The paper involved the issue of arching of the railway turnouts. This is an issue which is given relatively less attention to scientific and research activities. Reference has been made to the book by Wladyslaw Rzepka, under the title „Curved turnouts in plan and profile”, which has been used in Poland for more than 50 years as the main source of information relating to the turnouts on the curve. The book is a compilation of elaborations...

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  • A DISCRETE-CONTINUOUS METHOD OF MECHANICAL SYSTEM MODELLING

    Publikacja

    The paper describes a discrete-continuous method of dynamic system modelling. The presented approach is hybrid in its nature, as it combines the advantages of spatial discretization methods with those of continuous system modelling methods. In the proposed method, a three-dimensional system is discretised in two directions only, with the third direction remaining continuous. The thus obtained discrete-continuous model is described...

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  • METHOD OF ROUTING SHIPS SAILING IN DEDICATED ENVIRONMENT

    Publikacja

    The method for determining the suboptimal route of sailing vessels operating in a restricted area of the sea are proposed in the paper. The dynamics of the environment including weather conditions and speed characteristics of ships sailing are considered. As optimiza-tion criterion, measure sailing time T, and the number of maneuvers performed ω, are taken into account. An heuristic algorithm, and the appropriate application routing...

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  • A method of measuring RLC components for microcontroller systems

    Publikacja

    A new method of measuring RLC components for microcontroller systems dedicated to compact smart impedance sensors based on a direct sensor-microcontroller interface is presented. In the method this direct interface composed of a reference resistor connected in series with the tested sensor impedance is stimulated by a square wave generated by the microcontroller, and then its voltage response is sampled by an internal ADC of the...

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  • Parametric method for evaluating optimal ship deadweight

    Publikacja

    The paper presents a method of choosing the optimal value of the cargo ships deadweight. The method may be useful at the stage of establishing the main owners requirements concerning the ship design parameters as well as for choosing a proper ship for a given transportation task. The deadweight is determined on the basis of a selected economic measure of the transport effectiveness of ship – the Required Freight Rate (RFR). The...

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  • A Review: Applications of the Spectral Finite Element Method

    The Spectral Finite Element Technique (SFEM) has Several Applications in the Sciences, Engineering, and Mathematics, which will be Covered in this Review Article. The Spectral Finite Element Method (SFEM) is a Variant of the Traditional Finite Element Method FEM that Makes use of Higher Order Basis Functions (FEM). One of the most Fundamental Numerical Techniques Employed in the Numerical Simulation is the SFEM, which Outperforms...

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  • Method of lines for physiologically structured models with diffusion

    Publikacja

    - APPLIED NUMERICAL MATHEMATICS - Rok 2015

    We deal with a size-structured model with diffusion. Partial differential equations are approximated by a large system of ordinary differential equations. Due to a maximum principle for this approximation method its solutions preserve positivity and boundedness. We formulate theorems on stability of the method of lines and provide suitable numerical experiments.

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  • Bearing capacity of the working platform with kinematic method

    Bearing capacity of the working platform for heavy tracks was analysed using Distinct Layout Optimization (DLO) method. The platform layer constructed from cohesionless soils is resting on weak cohesive subgrade. Different thickness of the platform, its effective angle of internal friction and undrained shear strength of the soft soil were taken into consideration. Kinematic method permits different failure mechanisms to be analyzed....

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  • Asynchronous time difference of arrival (ATDOA) method

    A new method for a location service in the asynchronous wireless sensor networks is outlined. This method, which is called asynchronous time difference of arrival (ATDOA), enables calculation of the position of a mobile node without knowledge of relative time differences (RTDs) between measuring sensors. The ATDOA method is based on the measurement of time difference of arrival between the node and the same sensor at the discrete...

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  • A method of verification diagnostics for functional safety analysis

    Publikacja

    - Rok 2005

    Problemy analizy bezpieczeństwa zostały zapoczątkowane w lotnictwie i energetyce jądrowej, a obecnie wprowadzane są szeroko do różnych gałęzi przemysłu, jak przemysł chemiczny, mechaniczny, etrochemiczny, spożywczy, itp. W analizie bezpieczeństwa funkcjonalnego względem przyjętego poziomu SIL wyznacza się prawdopodobieństwa nie wypełnienia określonej funkcji na żądanie (PDF). Do tego celu stosuje się różne metody analityczne, wykorzystuje...

  • Characterization of porous materials by capillary rise method

    Publikacja

    - Rok 2005

    Badane były kinetyki penetracji ciał porowatych złożonych z cząstek o różnych wymiarach. Na podstawie przeprowadzonych badań okazało się, że kinetyki penetracji i ważność prawa Washburna zależą nie tylko od wielkości cząstek ale także od dystrybucji wielkości porów. Różnica w czasie jaka wynika z przepływu cieczy przez ośrodek porowaty do całkowitego nasycenia cieczą została zaproponowana jako nowy parametr, opisujący rozkład wielkości...

  • Magnetometric method of detection of visually obscured objects

    Publikacja

    - Rok 2005

    W pracy przedstawiono metody detekcji ukrytych w ziemi i w wodzie niebezpiecznych obiektów. Opisano metodę magnetometryczną wykrywania obiektów o właściwościach ferromagnetycznych oraz zaprezentowano wyniki eksperymentalne wykrywania obiektów z zastosowaniem gradiometrów skalarnych.

  • A handwritten signature verification method employing a tablet

    Publikacja

    - Rok 2016

    A signature verification system based on static features and time-domain functions of signals obtained using a tablet has been presented in the paper. The signature verification method, based mainly on dynamic time warping coupled with some signature image features, has been described. The FRR measures reflecting the method's efficiency have been evaluated for verification attempts performed directly after obtaining model signatures...

  • Trust Management Method for Wireless Sensor Networks

    Publikacja

    - Rok 2017

    A Wireless Sensor Network (WSN) is a network of spatially distributed autonomous sensors to monitor physical or environmental conditions, such as temperature, sound, pressure, etc. and to cooperatively pass their data to the main location. The first wireless network that bore any real resemblance to a modern WSN is the Sound Surveillance System (SOSUS), developed by the United States Military in the 1950s to detect and track Soviet...

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  • Non contact multiband method for emissivity measurment.

    Publikacja

    - INFRARED PHYSICS & TECHNOLOGY - Rok 2003

    W pracy omówiona została metoda bezkontaktowego wielopasmowgo pomiaru emisyjności. W oparciu o opracowany algorytm zbadany został wpływ poszczególnych elementów systemu i czynników zakłócających na dokładność wyznaczania emisyjności. Wyniki modelowania umożliwiają także ocenę dokładności całego systemu pomiarowego.

  • A METHOD OF TRUST MANAGEMENT IN WIRELESS SENSOR NETWORKS

    The research problem considered in this paper is how to protect wireless sensor networks (WSN) against cyber-threats by applying trust management and how to strengthen network resilience to attacks targeting the trust management mechanism itself. A new method, called WSN Cooperative Trust Management Method (WCT2M), of distributed trust management in multi-layer wireless sensor networks is proposed and its performance is evaluated....

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  • A random signal generation method for microcontrollers with DACs

    A new method of noise generation based on software implementation of a 7-bit LFSR based on a common polynomial PRBS7 using microcontrollers equipped with internal ADCs and DACs and a microcontroller noise generator structure are proposed in the paper. Two software applications implementing the method: written in ANSI C and based on the LUT technique and written in AVR Assembler are also proposed. In the method the ADC results are...

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  • Extending transition curve in analytical design method

    Publikacja

    The paper presents the problem of extending the transitional curves, using for this purpose an analytical design method. The basis for the analysis of numerical calculations were carried out for a wide set of parameters characterizing the standard geometric system. We considered an importance of the size of radius of the circular arc and return angle of route on the obtained results after the formulation of appropriate theoretical...

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  • Analytical design method for widening the intertrack space

    The paper involved the issue of arching of the railway turnouts. This is an issue which is given relatively less attention to scientific and research activities. Reference has been made to the book by Wladyslaw Rzepka, under the title „Curved turnouts in plan and profile”, which has been used in Poland for more than 50 years as the main source of information relating to the turnouts on the curve. The book is a compilation of elaborations...

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  • Denudation - a convenient method of isolation and enrichment of analytes

    W pracy przedstawiono: podstawy teoretyczne techniki denudacyjnej; rozwiązania konstrukcyjne podstawowych typów urządzeń denudacyjnych; obszar praktycznego wykorzystania technik denudacyjnych.

  • 2D inverse method of turbomachinery stage design

    Publikacja

    - Rok 2003

    1. How 2D model for turbomachinery stages has developed historically. 2. Recent understanding of physical background of 2D model. 3. Curvilinear system of non-orthogonal coordinates in the application to 2D model. 4. Set of basic equations. 5. Closing conditions for the inverse problem. 6. Examples of solutions a)

  • Continuous frequency method of measurement of electrode impedance.

    Przedstawione zostały matematyczne podstawy nowej metody pomiaru impedancji elektrodowej. Metoda wykorzystuje sygnał pobudzenia którego częstotliwość zmienia się liniowo w czasie. Amplituda sinusoidalnego niestacjonarnego pobudzenia jest stała. Zapis i analiza sygnału pobudzenia i odpowiedzi pozwalana wyznaczenie ciągłego widma impedancyjnego. Jednoczesna analiza czasowo częstotliwościowa wykonano została przy użyciu transformacji...

  • Importance of time evaluation in capillary rise method

    Publikacja

    - Rok 2003

    Badano zwilżalność układu porowatego przez wodę i węglowodany, mierząc zmianę masy rurki wypełnionej szklanymi kulkami. Wskazano na różny czas i szybkość penetracji cieczy przez złoże.