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Search results for: 31P NMR
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A method of predicting the best conditions for large-size workpiece clamping to reduce vibration in the face milling process
PublicationThe paper presents an innovative method of solving the problem of vibration suppression during milling of large-size details. It consists in searching for the best conditions for clamping the workpiece based on a rapid modal identification of the dominant natural frequencies only and requires repetitive changes in the tightening torque of the clamping screws. Then, by estimating the minimum work of the cutting forces acting in...
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ZnO ALD-Coated Microsphere-Based Sensors for Temperature Measurements
PublicationIn this paper, the application of a microsphere-based fiber-optic sensor with a 200 nm zinc oxide (ZnO) coating, deposited by the Atomic Layer Deposition (ALD) method, for temperature measurements between 100 and 300°C, is presented. The main advantage of integrating a fiber-optic microsphere with a sensing device is the possibility of monitoring the integrity of the sensor head in real-time, which allows for higher accuracy during...
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Polarimetric studies of L-arginine-doped potassium dihydrogen phosphate single crystals
PublicationConoscopic interference patterns, channelled spectra and polarimetric techniques have been used for the characterization of pure and doped (with L-arginine amino acid) potassium dihydrogen phosphate (KDP) single crystals. Experimental polarimetric data have been obtained for the frequently used wavelength of 633 nm and for two close wavelengths of 532 and 543 nm in a high-accuracy dual-wavelength polarimeter. The measurement of...
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A mechanistic model for fate and removal of estrogens in biological nutrient removal activated sludge systems
PublicationTwo estrogen fate and transformation models were integrated with a comprehensive activated sludge model (ASM) to predict estrogen removal based on biomass and solids production. Model predictions were evaluated against published full-scale plant data as well as results from a laboratory-scale sequencing batch reactor (SBR) fed synthetic wastewater. The estrogen fate model relating the rate of total estrogen degradation to soluble...
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Manifestation of Intermolecular Interactions in the IR Spectra of 2- and 4-Methylmethcathinones Hydrochlorides: DFT Study and Hirshfeld Surfaces Analysis
PublicationThis paper reports a Hirshfeld surfaces analysis of crystalline 2- and 4-methylmethcathinone (2-MMC and 4-MMC) hydrochlorides to analyze NH∙Cl and CH∙∙∙Cl intermolecular interactions and approve the formation of the NН2+–Cl– salt fragment in both 2-MMC∙HCl and 4-MMC∙HCl crystals. Two isomeric dimers were separated from the corresponding crystal packing to model IR spectra of the crystalline 2-MMC∙HCl...
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Peripheral industrial NUTS 3 sub-regions in the European Union – identification and typology
PublicationA common phenomenon of development is the big difference in its levels, especially between metropolitan and non-metropolitan areas. Non-metropolitan areas are also very different. In some of them, industry plays a big role. European Union’s NUTS 3 non-metropolitan low developed sub-regions, whose gross domestic product per capita in 2011 was below 75% of the EU average, were the subject of research. It is based on the data and...
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Identification of Emotional States Using Phantom Miro M310 Camera
PublicationThe purpose of this paper is to present the possibilities associated with the use of remote sensing methods in identifying human emotional states, and to present the results of the research conducted by the authors in this field. The studies presented involved the use of advanced image analysis to identify areas on the human face that change their activity along with emotional expression. Most of the research carried out in laboratories...
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The Impact of Different Drying Methods on the Metabolomic and Lipidomic Profiles of Arthrospira platensis
PublicationDrying is an inseparable part of industrial microalgae production. In this work, the impacts of eight different drying methods on the metabolome and lipidome of Arthrospira platensis were investigated. The studied drying methods were freeze drying (FD), sun drying (SD), air drying at 40 and 75 °C (AD′ and AD″), infrared drying at 40 and 75 °C (IRD′ and IRD″), and vacuum drying at 40 and 75 °C (VD′ and VD″). Results gathered by...
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Diaryl Sulfide Derivatives as Potential Iron Corrosion Inhibitors: A Computational Study
PublicationThe present work aimed to assess six diaryl sulfide derivatives as potential corrosion inhibitors. These derivatives were compared with dapsone (4,4′-diaminodiphenyl sulfone), a common leprosy antibiotic that has been shown to resist the corrosion of mild steel in acidic media with a corrosion efficiency exceeding 90%. Since all the studied compounds possess a common molecular backbone (diphenyl sulfide), dapsone was taken as the...
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Surface Treatment of Rubber Waste
PublicationThis chapter deals with the study of different approaches to improve the compatibility of waste rubber with polymeric matrixes of high density polyethylene (HDPE) by using surface treatments to increase adhesion. Different surface treatments such as etching with sulphuric and nitric acids, the use of a silane as a coupling agent and chlorination with trichloroisocyanuric acid (TCI) have been applied. The modification of waste rubber...
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The effect of nanoparticles size on photocatalytic and antimicrobial properties of Ag-Pt/TiO2 photocatalysts
PublicationAg-Pt-modified TiO2 nanocomposites were synthesized using the sol–gel method. Bimetallic modified TiO2 nanoparticles exhibited improved photocatalytic activity under visible-light irradiation, better than monometallic Ag/TiO2 and Pt/TiO2 nanoparticles (NPs). All modified powders showed localized surface plasmon resonance (LSPR) in visible region. The photocatalysts’ characteristics by X-ray diffractometry (XRD), scanning transmission...
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Thermal and physical properties of ZrO2–AlO(OH) nanopowders synthesised by microwave hydrothermal method
PublicationIndustrially relevant nanopowder was synthesised by microwave hydrothermal synthesis to obtain well-controlled composition (ZrO2–AlO(OH) system) which was found to determine a number of physical and thermal characteristics. This study reports variation of particle size, density, specific surface area (SSABET), as well as thermal behaviour of nanopowder mixtures of ZrO2–AlO(OH) in the whole range of compositions. It was found that...
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STUDY ON THE RELATIONSHIP BETWEEN VEHICLE MAINTENANCE AND FUEL CONSUMPTION
PublicationA contemporary road vehicle (RV) is a rather complex system, consisting of a large number of subsystems, assemblies, units, and elements (parts). While operating, an RV interacts with the environment, and its elements interact with each other. Consequently, the properties (parameters) of these elements change in the process - hardness, roughness, size, relative position, gapping, etc. A partial solution to the presented problems...
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N-doped carbon nanospheres as selective fluorescent probes for mercury detection in contaminated aqueous media: chemistry, fluorescence probing, cell line patterning, and liver tissue interaction
PublicationA precise nano-scale biosensor was developed here to detect Hg2+ in aqueous media. Nitrogen-doped carbon nanospheres (NCS) created from the pyrolysis of melamine–formaldehyde resin were characterized by FESEM, XRD, Raman spectra, EDS, PL, UV–vis spectra, and N2 adsorption–desorption, and were used as a highly selective and sensitive probe for detecting Hg2+ in aqueous media. The sensitivity of NCS to Hg2+ was evaluated by photoluminescence...
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Nanodiamonds Doped with Manganese for Applications in Magnetic Resonance Imaging
PublicationNanodiamonds (NDs) are emerging with great potential in biomedical applications like biomarking through fluorescence and magnetic resonance imaging (MRI), targeted drug delivery, and cancer therapy. The magnetic and optical properties of NDs could be tuned by selective doping. Therefore, we report multifunctional manganese-incorporated NDs (Mn-NDs) fabricated by Mn ion implantation. The fluorescent properties of Mn-NDs were tuned...
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What defines excellent lighting design for humans and animals?
PublicationWhat defines excellent lighting design for humans and animals? The answer to the above question is more than complex. It is not enough nowadays to design a project to make it aesthetically pleasing. Nor is it sufficient to create nicely lit environments, or simply to achieve the light levels required by the lighting norms or standards. With the new scientific research of the last few decades that relates directly or indirectly...
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Ellipticity in couple-stress elasticity
PublicationWe discuss ellipticity property within the linear couple-stress elasticity. In this theory, there exists a deformation energy density introduced as a function of strains and gradient of macrorotations, where the latter are expressed through displacements. So the couple-stress theory could be treated as a particular class of strain gradient elasticity. Within the micropolar elasticity, the model is called Cosserat pseudocontinuum...
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Determination of pitting corrosion stage of stainless steel by galvanodynamic impedance spectroscopy
PublicationThis paper investigates the methodology for differentiation of multistep process of pitting corrosion of AISI 304 stainless steel in the environment of iron (III) chloride. Measurements were performed using Galvanodynamic Electrochemical Impedance Spectroscopy (GDEIS). Application of this methodology allowed monitoring of natural corrosion process without external current (IDC = 0A) nor potential perturbation of the system. Applied...
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Fuzzy Multi-Regional Fractional PID controller for Pressurized Water nuclear Reactor
PublicationThe paper presents the methodology for the synthesis of a Fuzzy Multi-Regional Fractional Order PID controller (FMR-FOPID) used to control the average thermal power of a PWR nuclear reactor in the load following mode. The controller utilizes a set of FOPID controllers and the fuzzy logic Takagi-Sugeno reasoning system. The proposed methodology is based on two optimization parts. The first part is devoted to finding the optimal...
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Analiza użytkowa systemów telekomunikacji satelitarnej
PublicationOpisano kierunki rozwoju osobistej telekomunikacji satelitarnej. Omówiono zapotrzebowanie na usługi świadczone przy użyciu techniki satelitarnej. Przeanalizowano doświadczenia wynikające z eksploatacji systemów typu LEO i GEO, z punktu widzenia ich możliwości użytkowych i aktualnego zapotrzebowania rynku na usługi telekomunikacyjne dostarczane poprzez satelitę. Scharakteryzowano przydatność quasi-globalnego podsystemu Inmarsat-GAN...
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Ekspertyza dla Rady Dzielnicy Gdańsk Osowa - w sprawie wniosku do Studium uwarunkowań i kierunków zagospodarowania przestrzennego Miasta Gdańska
PublicationEkspertyza posłużyła jako podstawa do sporządzenia Uchwały Rad Dzielnic do Studium nr XI/24/2015 z dnia 9 grudnia 2015 w sprawie wniosków do Studium uwarunkowań i kierunków zagospodarowania przestrzennego Miasta Gdańska
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Cyfrowy akcelerator wybranych modułów standardu kompresji wideo H.264
PublicationW artykule przedstawiono konfigurowalny cyfrowy akcelerator estymacji ruchu przeznaczony dla enkodera wideo standardu H.264. Akcelerator został zaimplementowany w technologii FPGA oraz w układzie ASIC w technologii UMC 90 nm. Obie implementacje zostały zweryfikowane, a szczegółowe wyniki pomiarów akceleratora ASIC zostały porównane z innymi dostępnymi w literaturze propozycjami. System został zoptymalizowany do współpracy z oprogramowaniem...
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Pial artery and subarachnoid width response to apnoea in normal humans
PublicationBackground: Little is known about intracranial pressure (ICP)-cerebral haemodynamic interplay during repetitive apnoea. A recently developed method based on near-infrared transillumination/backscattering sounding (NIR-T/BSS) noninvasively measures changes in pial artery pulsation (cc-TQ) as well as subarachnoid width (sas-TQ) in humans. Method: We tested the complex response of the pial artery and subarachnoid width to apnoea...
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Anti-cancer effect of Rumex obtusifolius in combination with arginase/nitric oxide synthase inhibitors via downregulation of oxidative stress, inflammation, and polyamine synthesis
PublicationCancer continues to be a leading cause of death worldwide, making the development of new treatment methods crucial in the fight against it. With cancer incidence rates increasing worldwide, ongoing research must focus on identifying new and effective ways to prevent and treat the disease. The combination of herbal extracts with chemotherapeutic agents has gained much interest as a novel strategy to combat cancer. Rumex obtusifolius...
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Wrzenie nanocieczy na poziomych gładkich i chropowatych rurkach
PublicationPrzedstawiono wyniki pomiarów współczynnika przejmowania ciepła podczas wrzenia nanocieczy Al2O3 na rurce ze stali nierdzewnej przy ciśnieniu atmosferycznym, pod- i nadciśnieniu. Koncentracja nanocząstek o średnim wymiarze 47 nm wynosiła 0.01%, 0.1% oraz 1%.
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Rewitalizacja posadzek betonowych typu lastrico w obiektach zabytkowych. Część 2
PublicationW artykule przedstawiono zagadnienia materiałowe i technologiczne dotyczące posadzek typu lastrico w aspekcie oceny ich stanu technicznego oraz sposobów naprawy i rewitalizacji. Tekst stanowi kontynuacje artykułu zamieszczonego w Builder Science3 nr 9/2021
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The low coherence Fabry-Pérot interferometer with diamond and ZnO layers
PublicationThe authors present a fiber-optic Fabry-Pérot interferometer built with the application of diamond and zinc oxide (ZnO) thin layers. Thin ZnO films were deposited on the tip of a standard telecommunication single-mode optical fiber (SMF- 28) while the diamond layer was grown on the plate of silicon substrate. Investigated ZnO layers were fabricated by atomic layer deposition (ALD) and the diamond films were deposited using Microwave...
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Measurements of fundamental properties of homogeneous tissue phantoms
PublicationWe present the optical measurement techniques used in human skin phantom studies. Their accuracy and the sources of errors in microscopic parameters’ estimation of the produced phantoms are described. We have produced optical phantoms for the purpose of simulating human skin tissue at the wavelength of 930 nm. Optical coherence tomography was used to measure the thickness and surface roughness and to detect the internal inhomogeneities....
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Ag/Pt-modified TiO2 nanoparticles for toluene photooxidation in the gas phase
PublicationAg/Pt-modified TiO2nanocomposites were synthesized using the sol–gel method. The effect of metal typeand amount as well as synthesis route on the photocatalytic activity in reaction of toluene removal, usedas a model volatile organic compound, was investigated. Toluene, at the concentration of about 200 ppm,was irradiated over modified TiO2using light-emitting diodes (LEDs, max= 415 nm). The results showedthat toluene could be...
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Portable Raman spectrometer - design rules and applications
PublicationRaman spectroscopy has become more popular due to its new prospective field applications in forensic sciences, war against terrorism, environment protection and other field chemical analysis. Raman spectrometers can be miniaturised to portable devices and their price is decreasing due to development of optoelectronics components. Unfortunately, this technology has still numerous limitations that influence their design and limit...
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Singlet Exciton Diffusion in Vacuum-Evaporated Films of Amine-Based Materials as Studied by Photocurrent and Photoluminescence Quenching Methods
PublicationThe singlet exciton diffusion lengths are determined by the photoconductivity as well as the luminescence surface quenching technique, in vacuum‐evaporated layers of (4,4′,4″‐tris(N‐(3‐methylphenyl)‐N‐phenylylamino) triphenylamine) (m‐MTDATA), 4,4′,4″‐tris[2‐naphthyl(phenyl)amino] triphenylamine (2TNATA), and N,N′‐diphenyl‐N,N′‐bis(3‐methylphenyl)‐[1,1′‐biphenyl]‐4,4′‐diamine (TPD) which are frequently used for fabrication of electroluminescent...
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Implementation of SiN thin film in fiber-optic sensor working in telecommunication range of wavelengths
PublicationMirrors are used in optical sensors and measurement setups. This creates a demand for mirrors made of new materials and having various properties tailored to specific applications. In this work, we propose silicon covered with a thin silicon nitride layer as a mirror for near-infrared measurements. SiN layer was deposited on a standard silicon wafer with a Low-Pressure Chemical Vapor Deposition furnace. Then, the created layer...
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FIBRE-OPTIC SENSOR FOR SIMULTANEOUS MEASUREMENT OF THICKNESSAND REFRACTIVE INDEX OF LIQUID LAYERS
PublicationIn this paper, we present a fibre-optic sensor for simultaneous measurement of refractive index and thickness of liquid layers. We designed an experimental low-coherence setup with two broadband light sources and an extrinsic fibre-optic Fabry–Pérot interferometer acting as the sensing head. We examined how the refractive index of a liquid film and its thickness affect spectrum at the output of a fibre-optic interferometer. We...
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Identyfikacja wad powierzchni tocznej szyn za pomocą sygnału wibroakustycznego
PublicationW artykule przedstawiono koncepcję metody identyfikacji najczęściej występujących wad powierzchni tocznej szyn za pomocą sygnałów wibroakustycznych. Opisano badane wady szyn take, jak: squat, head checking oraz wybuksowanie. Przedstawiono metodykę prowadzonych badań oraz wyniki analiz zarejestrowanych sygnałów dla warunków techniczno-eksploatacyjnych panujących na liniach kolejowych nr 213 Reda – Hel oraz nr 131 Chorzów Batory...
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Design, Synthesis, and Enzymatic Evaluation of Novel ZnO Quantum Dot-Based Assay for Detection of Proteinase 3 Activity
PublicationHerein, the synthesis and application of functionalized quantum dot-based protease probes is described. Such probes are composed of nontoxic ZnO nanocrystals decorated by amino groups followed by linker and labeled peptide attachment. Spherical NH2-terminated ZnO quantum dots (QDs) with the average size ranging from 4 to 8 nm and strong emission centered at 530 nm were prepared using the sol−gel method. The fluorescence of ZnO...
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Enhancement of fiber-optic low-coherence Fabry-Pérot interferometer with ZnO ALD films
PublicationIn this paper investigation of the enhanced fiber-optic low coherence Fabry-Pérot interferometer with zinc oxide (ZnO) film deposited by atomic layer deposition (ALD) was presented. Model of the interferometer, which was constructed of single-mode optical fiber with applied ZnO ALD films, was built. The interferometer was also examined by means of experiment. Measurements were performed for both reflective and transmission modes,...
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RÓWNOWAŻNOŚĆ METOD POMIAROWYCH CIĄGŁYCH I ODNIESIENIA STOSOWANYCH DO OZNACZANIA PM2,5
PublicationW pracy przedstawiono wyniki testu terenowego przeprowadzonego na terenie województwa pomorskiego w okresie od 01-01-2013 do 31-12-2013 w celu wykazania równoważności wyników stężeń pyłu zawieszonego PM2,5 uzyskanych za pomocą analizatora automatycznego BAM 1020 w stosunku do wyników uzyskanych za pomocą wagowej metody odniesienia. Przedstawiono sposób określania równoważności wyników uzyskanych za pomocą analizatora i szacowania...
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Ekspertyza dla Rady Dzielnicy Gdańsk Orunia -Św. Wojciech-Lipce - w sprawie wniosku do sporządzanego Studium Uwarunkowań i Kierunków Zagospodarowania Przestrzennego Miasta Gdańska
PublicationEkspertyza posłużyła jako podstawa do sporządzenia Uchwały Nr IX/25/2015 z dnia 09.12.2015 Rady Dzielnicy Gdańsk Orunia -Św. Wojciech-Lipce - w sprawie wniosku do sporządzanego Studium Uwarunkowań i Kierunków Zagospodarowania Przestrzennego Miasta Gdańska
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Landfill leachate treatment at a pilot plant using hydrophyte systems
PublicationConstructed wetlands can provide an effective and economical solution to landfill leachate treatment. In the article the performance of a CW for leachate treatment, consisting of two horizontal flow constructed wetlands (HF-CW) beds, working at the municipal landfill in Gdansk-Szadolki in the period 2004-2005 is being discussed. The plant has been operating since 2001. Clogging problems and surface flow occurred in the system...
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Studies on the influence of β-cyclodextrin derivatives on the physical stability of famotidine
PublicationThe usage of Fourier transform infrared spectroscopy, near infrared spectroscopy, differential scanning calorimetry and microscopy is presented in this work focused on the exploration of the effect of CD on the physical stability of famotidine (FAM). The most significant information was achieved by analysis of the second derivatives ofnear infrared (NIR) spectra recorded. Changes in the shape of spectra derivatives allow...
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Evidence for solid state electrochemical degradation within a small molecule OLED
PublicationAcridone derivative have been synthesised and used as OLED (Organic Light Emitting Diode) emitters which were found to be electroactive. Electrochemical investigations showed a side reaction takes place inside an active layer which diminished the overall device efficiency. By using a dopant and host active layer architecture, the formation of the by product was removed. The by-product was identified as a σ-dimer formed inside an...
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The effect of a belt position in the spindle driving system on critical rotational speeds
PublicationThe aim of this paper was to examine how the belt pulley position affects critical rotational speeds of the modernized spindle of the sliding table saw Fx3. Methodology of determination of critical rotational speeds of the spindle in a function of the spindle design features and its driving system is presented. Spindles in these kind of machine tools are mainly driven with V-belts, and the pulleys on the spindles might be positioned:...
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Distillery Wastes as External Carbon Sources for Denitrification in Municipal Wastewater Treatment Plants
PublicationW pracy przedstawiono wyniki badań nad zastosowaniem półproduktów oraz produktów odpadowych z gorzelni i destylarni, jako potencjalne źródło zewnętrznego węgla organicznego w celu poprawy denitryfikacji w systemach z biologicznym usuwaniem związków biogennych. W celu porównania efektywności trzech badanych substancji (oleje fuzlowe, odcieki i syrop) wykonano testy na szybkość redukcji azotanów (z ang. NUR) oraz szybkość zużycia...
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Distillery Wastes as External Carbon Sources for Denitrification in Municipal Wastewater Treatment Plants
PublicationW pracy przedstawiono wyniki badań nad zastosowaniem półproduktów oraz produktów odpadowych z gorzelni i destylarni, jako potencjalne źródło zewnętrznego węgla organicznego w celu poprawy denitryfikacji w systemach z biologicznym usuwaniem związków biogennych. W celu porównania efektywności trzech badanych substancji (oleje fuzlowe, odcieki i syrop) wykonano testy na szybkość redukcji azotanów (z ang. NUR) oraz szybkość zużycia...
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Technika satelitarna w telekomunikacji
PublicationScharakteryzowano różne rozwiązania satelitarnych systemów telekomunikacyjnych, głównie pod względem rodzaju zastosowanej orbity, co ma zasadnicze znaczenie użytkowe. Dokonano przeglądu dotychczasowych reprezentatywnych projektów takich systemów, analizując kolejne fazy ich rozwoju oraz występujące bariery technologiczno-ekonomiczne. Przedstawiono stan prac ETSI w zakresie specyfikacji GMR, której praktycznym przykładem są pierwsze...
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Sposoby i skutki fałszowania paliw silnikowych oraz metody wykrywania.Cz. 2
PublicationPrzedstawiono dwie grupy metod kontroli jakości paliwa - metody konwencjonalne i wybrane ''metody przesiewowe'' - w tym zastosowanie spektrofotometrii w bliskiej podczerwieni (NIR), które umożliwiają identyfikację sfałszowanego paliwa. Opisano także metodykę badań prowadzącą do oznaczenia nieznanego parametru użytkowego badanego paliwa, począwszy od utworzenia optymalnych postaci równań korelacyjnych poprzez kontrolę ich poprawności...
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Stability of free floating ship. Part II
PublicationJest to część II artykułu, którego I część ukazała się w PMR 2/2005. Ramiona prostujące są niejednoznaczne dla statku swobodnego, bowiem zależą od sposobu działania momentu przechylającego. Omówiono dwa przypadki, gdy moment przechylający jest równoległy do płaszczyzny symetrii statku oraz gdy wykonuje najmniejszą pracę, czyli gdy jest równoległy do głównej osi bezwładności wodnicy pływania. Pokazano, że przemieszczenia kątowe...
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Krajowy Program Bezpieczeństwa Ruchu Drogowego 2005-2007-2013. GAMBIT 2005
PublicationW artykule przedstawiono syntezę Krajowego Programu Bezpieczeństwa Ruchu Drogowego GAMBIT 2005. Jest to dokument opracowany na zamówienie Krajowej Rady BRD, przyjęty przez Radę Ministrów w dniu 19 kwietnia 2005 jako program dla Polski na lata 2005-2007-2013. Polska wchodząc do Unii Europejskiej w maju 2004 przyjęła cel ustalony w Polityce Transportowej UE ''w ciągu dekady zmniejszyć o połoweę liczbę śmiertelnych ofiar wypadków...
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Polymer based thick films - material quality and interface resistance evaluation
PublicationThe properties of polymer based thick film layers mede using different resistive pastes and dipping silvers have been studied. The composite of carbon and graphite (C/Gr) conducting particles suspended in different polymer vehicles were used for preparation resistive layers. Interface resistance Rc created between dipping silver (DiAg) contact layer and resistive layer was determined from the surface potential distribution measurements...
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Insights into Stoichiometry Adjustments Governing the Performance of Flexible Foamed Polyurethane/Ground Tire Rubber Composites
PublicationPolyurethanes (PU) are widely applied in the industry due to their tunable performance adjusted by changes in the isocyanate index—stoichiometric balance between isocyanate and hydroxyl groups. This balance is affected by the incorporation of modifiers of fillers into the PU matrix and is especially crucial for PU foams due to the additional role of isocyanates—foaming of the material. Despite the awareness of the issue underlined...