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Search results for: molybdenum carbide
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Studies on the utilization of post-distillation liquid from Solvay process to carbon dioxide capture and storage
PublicationIn this work, a method of precipitated calcium carbonate production from the post-distillation liquid created in the Solvay process and waste carbon dioxide was proposed and investigated. Precipitation was carried out in a model solution of calcium chloride containing ammonia at various molar ratios in relation to Ca2+ ions, while gaseous carbon dioxide was supplied to the reactor as a pure gas or as a mixture with air. It was...
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Experimental examination and modification of chip suction system in circular sawing machine
PublicationThe article presents the results of experimental examination of the wood chip suction system in the existing sliding table saw before and after its modifi cation. The studies focused on the extraction hood of the mentioned system. The methodical experimental research of the pressure distribution inside the hood during wood chip removal for the selected rotational speed of saw blades of 3500 and 6000 min-1 with a diameter of 300...
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The application of Monod equation to denitrification kinetics description in the moving bed biofilm reactor (MBBR)
PublicationIn this paper, the kinetic constants Vmax and KCOD occurring in the Monod equation, which describe the denitrification process in the moving bed, are determined. For this purpose, a laboratory moving bed biofilm reactor (MBBR) was used. The filling of the reactor consisted of EvU Perl carriers. The experiment was carried out with an excess of nitrate, and denitrification rate was dependent on the concentration of external organic...
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Application of the Optimum Dataset Method in Archeological Studies on Barrows
PublicationLight Detection and Ranging (LiDAR) became one of the technologies used in archaeological research. It allows for relatively easy detection of archaeological sites that have their own field form, e.g.: barrows, fortresses, tracts, ancient fields [1]. As a result of the scanning, the so-called point cloud is obtained, often consisting of millions of points. Such large measurement datasets are very time-consuming and labor-intensive...
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Precipitation of Spherical Vaterite Particles via Carbonation Route in the Bubble Column and the Gas-Lift Reactor
PublicationSpherical vaterite particles were produced by carbonation of calcium chloride solution with addition of ammonia to facilitate CO2 absorption. Synthesis of calcium carbonate was carried out in a bubble column or gas-lift reactor. The course of the reaction was monitored by pH measurements. Precipitated solids were analyzed by Fourier-transformed infrared spectroscopy, x-ray powder diffraction and scanning electron microscopy, and...
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Classification of Urban Regeneration Participants as a Basis for Identification of Construction Investment's Risk Sources
PublicationOn the basis of the conducted research it can be concluded that the majority of the existing urban regeneration problems are revealed by the lack of an in-depth analysis of sources and risk factors. For the above reasons, the subject of this study is classification of urban regeneration's participants as a basis for identification of construction investment's risk sources. The research methodology is based on an in-depth analysis...
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Smart Services supporting Drivers in Effective Cars Parking
PublicationThe paper shows how to design and implement intelligent, service oriented systems for management of free places in distributed car parks. The idea of SOA technology is widely used. It is assumed that a state of every car park is automatically determined by a special electronic infrastructure including IoT solutions. The information received from such an infrastructure is sent to the main management system, which processes it and,...
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Some geomechanical properties of a biopolymer treated medium sand
PublicationSome geomechanical properties of a biopolymer treated medium sand. This paper presents a laboratory assessment of geomechanical properties of sandy soil improved by biopolymer application. Additives (biosubstance) consist of polysaccharides and water. Biosubstance used in the project was xanthan gum, which comes from bacteria Xanthomonas campestris. Triaxial shear compression tests and unconfi ned compression tests were carried...
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“Dilute & Shoot” approach for rapid determination of trace amounts of nicotine in zero-level e-liquids by reversed phase liquid chromatography and hydrophilic interactions liquid chromatography coupled with tandem mass spectrometry-electrospray ionization
PublicationTwo analytical procedures are proposed where HILIC and RPLC techniques are coupled with tandem mass spectrometry detection for rapid determination of trace amounts of nicotine in zero-level liquids for electronic cigarettes. Samples are prepared on the basis of the approach “dilute & shoot” which makes this important step quick and not complicated. The chromatographic separation was carried out on a Zorbax XDB column (RPLC method)...
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Numerical analysis of the container vessel's self-propulsion at different rudder deflection angles
PublicationNowadays, CFD becomes one of the most commonly used research method in ship hydrodynamics, limited to the analyses of hull resistance in calm water. With continuously improving computing power and increasingly more accurate numerical methods it is possible to simulate more complex cases. State of the art CFD tools also enable development of new ways of assessing ship maneuvering performance. This paper presents an attempt on...
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THE EFFECT OF ALTERNATIVE CUTTER PATHS ON FLATNESS DEVIATIONS IN THE FACE MILLING OF ALUMINUM PLATE PARTS
PublicationIn this paper the relationships between the alternative machining paths and flatness deviations of the aluminum plate part, were presented. The flatness tolerance of the main surface of the plate part has crucial meaning due to the assembly requirement of piezoelectric elements on the radiator. The aluminum bodies under investigation are the base part of the radiators with crimped feathers for the train industry. The surface of...
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Modal analysis of railway current collectors using Autodesk Inventor
PublicationThe paper presents the results of modal analysis of railway current collector type 160EC. In the first place, the analysis was carried out analytically for a simplified two lumped mass pantograph model. Then numerical analysis was conducted in the Autodesk Inventor (AI) on the prepared multibody model using the AI modal analysis algorithm, which is based on the finite element method (FEM). Model elements which are most relevant...
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Mobile wireless measurement system for potatoes storage management
PublicationThe paper discusses the idea and the design of a remote control system for a storage management of agricultural products which temperature may rise in a result of biological processes during the storage. Exemplary potatoes storehouse is discussed as an application of the automation system. Because of existing buildings and infrastructure in the farm, wireless data transfer system has been proposed for both sensors to data acquisition...
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Synthesis of amides under microwave irradiation
PublicationAmides belong to the most important carboxylic acid derivatives. They are constituents of natural compounds like peptides and proteins. They found applications in many branches of science and industry, especially in pharmaceutical and polymer science. Conventional procedures for amide preparation involve reaction between amine and carboxylic acid or their more active derivatives such as acid chlorides, acid anhydrides or esters....
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Application and optimization of headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography - flame-ionization detector (GC-FID) to determine products of the petroleum industry in aqueous samples
PublicationA simple and solvent-free analytical method has been optimized for the determination of hydrocarbons (C6 - C20) from products of the petroleum industry in aqueous samples. Extraction and analysis was carried out using headspace solid-phase microextraction (HS-SPME) and gas chromatography coupled with flame-ionization detector (GC-FID). A ZB-5 capillary column (30 m × 0.25 mm inner diameter, 0.25 µm film thickness) was used for...
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GPU-Accelerated Finite-Element Matrix Generation for Lossless, Lossy, and Tensor Media [EM Programmer's Notebook]
PublicationThis paper presents an optimization approach for limiting memory requirements and enhancing the performance of GPU-accelerated finite-element matrix generation applied in the implementation of the higher-order finite-element method (FEM). It emphasizes the details of the implementation of the matrix-generation algorithm for the simulation of electromagnetic wave propagation in lossless, lossy, and tensor media. Moreover, the impact...
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Evolutionary Planning of Safe Ship Tracks in Restricted Visibility
PublicationThe paper presents the continuation of the author's research on ship track planning by means of Evolutionary Algorithms (EA). The presented method uses EA to search for an optimal set of safe tracks for all ships involved in an encounter. Until now the method assumed good visibility – compliance with standard rules of the Convention on the International Regulations for Preventing Collisions at Sea (COLREGS, 1972). However, in restricted...
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Low-Cost EM-Simulation-Driven Multi-Objective Optimization of Antennas
PublicationA surrogate-based method for efficient multi-objective antenna optimization is presented. Our technique exploits response surface approximation (RSA) model constructed from sampled low-fidelity antenna model (here, obtained through coarse-discretization EM simulation). The RSA model enables fast determination of the best available trade-offs between conflicting design goals. A low-cost RSA model construction is possible through...
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Mono- and polynuclear Co(II) silanethiolates with aliphatic diamines
PublicationFour Co(II) complexes, [Co{SSi(OtBu)3}2(dmpda)] 1, [Co{SSi(OtBu)3}2(bda)2]n2 [Co{SSi(OtBu)3}2(pda)2]n3 and [Co{SSi(OtBu)3}2(hda)2]n4 [dmpda = 3-(dimethylamino)-1-propylamine; bda = 1.4-butanediamine; pda = 1.5-pentanediamine; had = 1.6-hexanediamine] have been synthesized and characterized using X-ray diffraction. Complex 1 is mononuclear and contains Co(II) coordinated by dmpda molecule in chelating mode, whereas compounds 3 and...
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Impact of diffusion coefficient averaging on solution accuracy of the 2D nonlinear diffusive wave equation for floodplain inundation
PublicationIn the study, the averaging technique of diffusion coefficients in the two-dimensional nonlinear diffusive wave equation applied to the floodplain inundation is presented. As a method of solution, the splitting technique and the modified finite element method with linear shape functions are used. On the stage of spatial integration, it is often assumed that diffusion coefficient is constant over element and equal to its average...
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Application of atmospheric pressure microwave plasma source for hydrogen production from ethanol
PublicationIn contrast to conventional technologies of hydrogen production like water electrolysis or coal gasification we propose a method based on the atmospheric pressure microwave plasma. In this paper we present results of the experimental investigations of the hydrogen production from ethanol in the atmospheric pressure plasma generated in waveguidesupplied cylindrical type nozzleless microwave (915 MHz and 2.45 GHz) plasma source (MPS)....
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Synchronous generator model taking into account the non-uniform saturation of the pole shoes
PublicationFor the evaluation of modern electric power systems with regard to their behavior, weight, and reliability a novel modeling and simulation tools have been developed. The paper presents circuit model of synchronous generator taking into account both the non-sinusoidal distribution of the stator and rotor winding, and non-uniform saturation of the pole shoes. This model is suitable for simulation of both salient and no-salient pole...
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Risks related to car fire on innovative Poroelastic Road Surfaces-PERS
PublicationTo reduce tyre/road noise, the concept of poroelastic road surfaces (PERS) was invented. PERS is a road surface material that is porous, and at the same time, it is flexible because of the substantial amount of rubber granulate content (from 20% to 85%). The rubber and stone particles are bound by polyurethane resin instead of bitumen. It was feared that in case of fire, because of the high content of rubber and polyurethane, there...
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Application of electrochemical impedance spectroscopy to monitoring discharging process of nickel/metal hydride battery.
PublicationThis paper presents the possibility of applying impedance analysis to cell diagnostics. In order to obtain characteristic curves of both electrodes of a NiMH battery simultaneously, a reference electrode was added into the circuit. The authors analysed the cell under three cases, i.e. when its properties are determined only by the state of the positive electrode, only by the state of the negative electrode, or when both electrodes...
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A novel methodology for the enantiomeric resolution of methamphetamine, its precursors and intermediates by GC-MS
PublicationImpurity profiling and classification of abused drugs using chiral analytical techniques is of particular interest and importance because of the additional information obtained from this approach. When these methods are applied to the synthesis of illicitly used substances, they can supply valuable information about the conditions/chemicals used in the synthesis. In this study, simultaneous chiral separation of methylamphetamine,...
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FURTHER REMARKS ON THE SURFACE VIS IMPRESSA CAUSED BY A FLUID-SOLID CONTACT
PublicationIt is well-known that, nano-mechanics should take into account not only physical phenomena occuring within the bulk but, first of all, the physical phenomena appropriate for a surface of two materials contact. The huge volume density of internal surfaces as well countours lines located within the nanomaterial results in our interest in, apart from classical form of mass, momentum and entropy transport, those modes of transportation...
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Methodology for determination of the selected mechanical properties of wood based on cutting tests
PublicationFrom kiln-dried spruce wood (with steam) as well as in natural conditions were randomly selected 8 samples. After determining the average dimensions, moisture content and density of the samples they have been cut on the frame sawing machine PRW15M for measurement of cutting power. Based on those results from a linear rela-tionship of cutting power versus feed per toot mechanical properties of wood such as facture toughness and...
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Absorption spectroscopy setup for determination of whole human blood and blood–derived materials spectral characteristics
PublicationA dedicated absorption spectroscopy system was set up using tungsten-halogen broadband source, optical fibers, sample holder, and a commercial spectrometer with CCD array. Analysis of noise present in the setup was carried out. Data processing was applied to the absorption spectra to reduce spectral noise, and improve the quality of the spectra and to remove the baseline level. The absorption spectra were measured for whole blood...
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Analysis of electromagnetic disturbances in DC network of grid connected building-integrated photovoltaic system
PublicationThis paper focuses on conducted electromagnetic interference (EMI) emissions and propagation in the DC network of grid connected building integrated photovoltaic (PV) system. The investigated PV system, consists of ten solar panels, cabling and the grid-connected one phase inverter. The EMI simulation model of the real PV system has been developed with the aid of impedance analyzer measurements of solar panels and the DC network...
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Cross-Platform Real-Time Nuclear Reactor Basic Principle Simulator
PublicationAbstract—In the paper several approaches to building the real-time basic principle simulators of nuclear reactor processes are presented and their characteristics are analyzed. The characteristics of developed simulators for MATLAB/Simulink including their limitations, and the idea of a cross-platform simulator independent of specific hardware or software are presented. Mathematical models of selected nuclear reactor’s processes...
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SENSITIVITY OF PUBLIC PLACES IN GDAŃSK OSOWA DISTRICT
PublicationThis paper summarises the results of the research carried out at the University of Ljubljana, Faculty of Architecture, Slovenia, during the PhD visiting period of the first author from the Gdansk University of Technology, Poland, in the framework of the PhD course "Sensitive urban places", leaded by the second author. Focusing to the specific problems of the Gdansk Osowa district in Poland, this research develops the idea of sensitivity...
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Localized impedance measurements of AA2024 and AA2024-T3 performed by means of AFM in contact mode
PublicationPurpose: The purpose of this paper is to present the results of an atomic force microscopy (AFM) based approach to local impedance spectroscopy (LIS) measurement performed on AA2024 and AA2024-T3 aluminium alloys. Design/methodology/approach: AFM-LIS measurements were performed ex-situ without the electrolyte environment, so in fact the electrical not electrochemical impedance was obtained. Findings: Relative local impedance values...
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Quality Evaluation of Agricultural Distillates Using an Electronic Nose
PublicationThe paper presents the application of an electronic nose instrument to fast evaluation of agricultural distillates differing in quality. The investigations were carried out using a prototype of electronic nose equipped with a set of six semiconductor sensors by FIGARO Co., an electronic circuit converting signal into digital form and a set of thermostats able to provide gradient temperature characteristics to a gas mixture. A volatile fraction...
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Application of passive sampling technique in monitoring research on quality of atmospheric air in the area of Tczew, Poland.
PublicationThis paper presents the results of atmospheric air quality research in Tczew (adjacent to the Vistula River) on the content of BTEX compounds. Analytical procedure applied during the sampling of the analytes from the air used the passive sampling technique (diffusive passive sampler, Radiello®). For determination of BTEX compounds in atmospheric air, two-stage thermal desorption technique combined with gas chromatography (TD-GC-FID)...
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Elderly persons professional activity - substantive issues and methodical challenges
PublicationPopulation ageing and mass withdrawal of persons around retirement age from the labour market constitutes a serious threat for European Union economy, especially in the so-called new member states. The coming years are expected to bring a considerable increase in public spending on pensions and health care, as well as changes in the structure and size of consumer demand and an increase in the number of socially excluded individuals....
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Hydraulic conductivity of a biopolymer treated sand
PublicationThis paper presents results of laboratory assessment of creating seepage barriers in a sandy soil using biopolymer additives (bio substance), which consist of polysaccharides and water. Polysaccharides strongly interact with water to produce a viscous suspension. The aim of the conducted work was to investigate the influence of a biosubstance employed in a highly permeable sandy soil. The amount of the biopolymer used in a sample...
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Effect of underwater wet welding conditions on the diffusible hydrogen content in deposited metal
PublicationIn the study mercury displacement method was used for determination of diffusible hydrogen amount in deposited metal obtained during underwater wet welding with covered electrodes in laboratory conditions according to a two-level full factorial design for three factors. The factors and their levels were chosen among conditions and parameters of welding in accordance with the results of own preliminary studies. A statistical analysis...
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A new quaternion-based encryption method for DICOM images
PublicationIn this paper, a new quaternion-based lossless encryption technique for digital image and communication on medicine (DICOM) images is proposed. We have scrutinized and slightly modified the concept of the DICOM network to point out the best location for the proposed encryption scheme, which significantly improves speed of DICOM images encryption in comparison with those originally embedded into DICOM advanced encryption standard...
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Influence of metallic porous microlayer on pressure drop and heat transfer of stainless steel plate heat exchanger
PublicationThe experimental analysis of passive heat transfer intensification in the case of plate heat exchanger has been carried out. The metallic porous layer was created on the heat transfer surface of analyzed unit. The experiment was accomplished in two stages. In the first stage the commercial stainless steel gasketed plate heat exchanger was investigated, while in the second one – the identical heat exchanger but with the modified...
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STUDIES ON THE USE OF TERRESTRIAL LASER SCANNING IN THE MAINTENANCE OF BUILDINGS BELONGING TO THE CULTURAL HERITAGE
PublicationWithin the frames of the use of terrestrial laser scanning we find numerous examples of registration of building facilities, including also historical and valuable in their culture. In the case presented in this paper, at the root of the problem there is a preservation of the historic blacksmith’s forge located in Gdansk Orunia. The facility dating from the early nineteenth century was intended to repair involving the complete...
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Laser patterned platform with PEDOT–graphene composite film for NO2 sensing
PublicationThis work presents a simple and fully electrochemical route used for fabricating of a NO2 gas sensor made of reduced-graphene-oxide-poly(3,4-ethylenedioxythiophene) composite film. The sensing platform was fabricated from alumina substrate and equipped with gold interdigitated electrodes and built-in heater.The temperature distribution on the surface of interdigitated electrodes was investigated by a thermalimaging camera and compared...
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Studies on the use of terrestrial laser scanning in the maintenance of buildings belonging to the cultural heritage
PublicationWithin the frames of the use of terrestrial laser scanning we find numerous examples of registration of building facilities, including also historical and valuable in their culture. In the case presented in this paper, at the root of the problem there is a preservation of the historic blacksmith's forge located in Gdansk Orunia. The facility dating from the early nineteenth century was intended to repair involving the complete...
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Improvement of opipramol base solubility by complexation with β-cyclodextrin
PublicationOpipramol (OPI), a tricyclic antidepressant and anxiolytic compound, is administered orally in the form of a dihydrochloride. Salt form of the drug has a higher solubility in water and hence bioavailability and stability. A similar effect can be achieved by closing the hydrophobic part of the drug molecule in the cyclodextrin cavity. The paper presents opipramol inclusion complexes with beta-cyclodextrin (β-CD) in 1:1 molar ratio....
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Problems and challenges associated with estimating the emissions of organic compounds from indoor materials
PublicationFor several years intensive research has been carried out with the aim of developing a database of the types and amounts of pollutants released from indoor materials to the indoor environment. The paper discusses in detail basic problems and challenges encountered when estimating the emissions of chemical compounds released from of indoor materials. Factors affecting the validity of data obtained by using two different types of...
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Influence of vision measurement system spatial configuration on measurement uncertainty, based on the example of electric traction application
PublicationTechnical diagnostics plays a significant role in ensuring operational reliability of electrified rail transport. The most critical point in the transmission of electric energy to vehicles is the sliding contact of the current collector with the traction network. For this reason, work is currently being carried on new measuring methods, whose appliance allows for more complete diagnostics of the contact line and current collectors,...
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Radio Channel Measurements in 868 MHz Off-Body Communications in a Ferry Environment
PublicationIn this paper, a characterization of the 868 MHz off-body radio channel in BANs is presented. Measurements were carried out in a ferry environment using a specific set-up. A method for path loss using radio distance measurements (RDMs) was developed. It allows to automate the measurements process and make it independent from the variable speed of a moving person. Based on the observed path loss as a function of distance, the obtained...
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Dissociative electron attachment to the radiosensitizing chemotherapeutic agent hydroxyurea
PublicationDissociative electron attachment to hydroxyurea was studied in the gas phase for electron energies ranging from zero to 9 eV in order to probe its radiosensitizing capabilities. The experiments were carried out using a hemispherical electron monochromator coupled with a quadrupole mass spectrometer. Diversified fragmentation of hydroxyurea was observed upon low energy electron attachment and here we highlight the major dissociation...
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Comparison between measured and calculated underwater pressure of merchant ship
PublicationFrom 2012 The Polish Naval Academy take part in an international research project SIRAMIS, carried out in the framework of the European Defence Agency. The objective of this project is to improve the understanding of ship signature interaction with multi influence sensors in relevant and realistic scenario's. This paper describes selected results of the comparison results of sea trials and model calculations of the hydrodynamic...
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Methodology and technology for the polymodal allophonic speech transcription
PublicationA method for automatic audiovisual transcription of speech employing: acoustic and visual speech representations is developed. It adopts a combining of audio and visual modalities, which provide a synergy effect in terms of speech recognition accuracy. To establish a robust solution, basic research concerning the relation between the allophonic variation of speech, i.e. the changes in the articulatory setting of speech organs for...
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Methodology and technology for the polymodal allophonic speech transcription
PublicationA method for automatic audiovisual transcription of speech employing: acoustic, electromagnetical articulography and visual speech representations is developed. It adopts a combining of audio and visual modalities, which provide a synergy effect in terms of speech recognition accuracy. To establish a robust solution, basic research concerning the relation between the allophonic variation of speech, i.e., the changes in the articulatory...