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Search results for: IONIZATION CROSS SECTION
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Determination of Butyltin Species in Sea Water Samples Using Solid Phase Extraction Followed by Liquid Chromatography - Tandem Mass Spectrometry
PublicationReverse phase liquid chromatography (RP-HPLC)-electrospray ionization-tandem mass spectrometry (ESI-MS-MS) was evaluated for the analysis of TBT using solid phase extraction as sample preparation method. TBT was extracted from acidified water samples (spiked with tripropyltin as internal standard) using reversed phase polymeric Strata-X cartridges. Analytes were eluted from cartridges using acetonitrile-water mixture and the volume...
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Structure-rheology relationship of fully bio-based linear polyester polyols for polyurethanes - Synthesis and investigation
PublicationThe synthesis of polyols from renewable substances as an alternative for petrochemical-based polyols play important matter in the polyurethane industry. In this work, the fully bio-based linear polyester polyols with different catalyst amounts were synthesized via two-step polycondensation method. The effect of various catalyst content on the structure and rheological behavior were established. Fourier Transform Infrared Spectroscopy,...
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Chemical composition, antioxidant and anticancer effects of the seeds and leaves and indigo (polygonum tinctorium Ait.) Plant
PublicationSeeds and leaves of indigo (Polygonum tinctorium Ait.) plant were investigated and compared with another medicinal plant named prolipid for their properties such as chemical composition, antioxidant, and anticancer effects by Fourier transform infrared, three-dimensional fluorescence spectroscopy, and electrospray ionization-MS in negative mode. It was found that polyphenols, flavonoids, and flavanols were significantly higher...
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Development of different methods for drugs and psychoactive substances extraction from hair samples and their identification based on HPLC-ESI-QTOF analysis
PublicationOver the past decade, the use of non-controlled designer drugs and drug of abuse has rapidly increased. Hair, as a human matrix, enables detection of drugs incorporated into its structure. Studies of presence and identification of drug metabolites in human hair samples has been performed using liquid chromatography electrospray ionization quadrupole time of flight mass spectrometry (HPLC-ESI-QTOF-MS) with steady alternation of...
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Preparation of Allyl Alcohol Oligomers Using Dipicolinate Oxovanadium(IV) Coordination Compound
PublicationCurrently, new precatalysts for olefin oligomerization are being sought in the group of vanadium(IV) complexes. Thus, the aim of our research was to examine the catalytic activity of the oxovanadium(IV) dipicolinate complex [VO(dipic)(H2O)2] 2 H2O (dipic = pyridine-2,6-dicarboxylate anion) in 2-propen-1-ol oligomerization as well as to characterize oligomerization products using matrix-assisted laser desorption/ionization–time-of-flight...
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Review: synthetic polymer hydrogels for biomedical applications
PublicationSynthetic polymer hydrogels constitute a group of biomaterials, used in numerous biomedical disciplines, and are still developing for new promising applications. The aim of this study is to review information about well known and the newest hydrogels, show the importance of water uptake and cross-linking type and classify them in accordance with their chemical structure.
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Low energy differential elastic electron scattering from trichloromethane
PublicationExperimental differential cross sections for low energy electron scattering from trichloromethane is measured utilizing a crossed electron-molecular beam experiment via the relative flow method, for the incident electron energies in the range of E = 0.5 eV-30 eV and the scattering angles in the range of θ = 10◦ − 130◦ .
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Static electric and magnetic multipole susceptibilities for Dirac one-electron atoms in the ground state
PublicationWe present tabulated data for several families of static electric and magnetic multipole susceptibilities for hydrogenic atoms with nuclear charge numbers from the range $1\leq Z\leq137$. Atomic nuclei are assumed to be point-like and spinless. The susceptibilities considered include the multipole electric polarizabilities $\alpha_{\mathrm{E}L\to\mathrm{E}L}$ and magnetizabilities (magnetic susceptibilities) $\chi_{\mathrm{M}L\to\mathrm{M}L}$...
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Standard and modified falling mass impact tests on preplaced aggregatefibrous concrete and slurry infiltrated fibrous concrete
PublicationAlthough several studies have been conducted to evaluate the impact response of concrete using theAmerican Concrete Institute (ACI) 544-2R falling mass impact test, the variations in test results are themain drawback of this testing method. This study aims to reduce the variations in experimental impacttest results by introducing two simple test setup modifications; (1) using coarse or fine aggregate bed-ding as an alternative...
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Geomatyka B 2021
e-Learning CoursesZapoznanie studentów z zagadnieniami pozyskiwania, analizowania, interpretowania i praktycznego stosowania geoinformacji poprzez wzajemne powiązanie aspektów geometrycznych i fizycznych przechodzących od zagadnień globalnych do regionalnych.
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Saint-Venant torsion based on strain gradient theory
PublicationIn this study, the Saint-Venant torsion problem based on strain gradient theory is developed. A total form of Mindlin's strain gradient theory is used to acquire a general Saint-Venant torsion problem of micro-bars formulation. A new Finite Element formulation based on strain gradient elasticity theory is presented to solve the Saint-Venant torsion problem of micro-bars. Moreover, the problem is solved for both micro and macro...
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Interactions of fish gelatin and chitosan in uncrosslinked and crosslinked with EDC films: FT-IR study
PublicationFilms based on fish gelatin, chitosan and blend of fish gelatin and chitosan before and after cross-linking with EDC have been characterized by FT-IR spectroscopy. The FT-IR spectrum of fish gelatin film showed the characteristic amide I, amide II and amide III bands, and the FT-IR spectrum of chitosan film confirmed that the polymer was only a partially deacetylated product, and included CH3-C=O and NH2 groups, the latter both...
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JMATRIX - a package for relativistic J-matrix calculations in elastic scattering of electrons from model potentials
PublicationWe present a software package JMATRIX, consisting of two computer codes written in FORTRAN 95 and parallelized with OpenMP, implementing the so-called J-matrix method, applied to elastic scattering of electrons on the radial potential, vanishing faster than Coulomb one. In the J-matrix method, physical scattering problem is replaced by using well-defined model, which is solved analytically. Presented software implements both non-relativistic...
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An isogeometric finite element formulation for frictionless contact of Cosserat rods with unconstrained directors
PublicationThis paper presents an isogeometric finite element formulation for nonlinear beams with impenetrability constraints, based on the kinematics of Cosserat rods with unconstrained directors. The beam cross-sectional deformation is represented by director vectors of an arbitrary order. For the frictionless lateral beam-to-beam contact, a surface-to-surface contact algorithm combined with an active set strategy and a penalty method...
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Induced Sheath Voltages In 110 Kv Power Cables – Case Study
PublicationThe paper considers shock hazard due to induced sheath voltages in 110 kV power cables. Various configurations of the metallic sheaths bonding and earthing (single-point bonding, both-ends bonding, cross-bonding) are analysed. Taking into account shock hazard and ability of the system to power transfer an optimal configuration is proposed.
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Performance evaluation of GPS anti-spoofing system based on antenna array processing
PublicationThis article concerns the problem of detection and mitigation of spoofing attacks in Global Navigation Satellite Systems. First, background information about spoofing and its possible countermeasures is provided. Next, concept of a novel GPS anti-spoofing system based on antenna array processing is presented and implementation of prototype of this system is described. The third section outlines the performance evaluation of proposed...
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The validation process of truss model with joint eccentricities
PublicationNowadays, due to the technological reasons in modern lightweight steel trusses, fabricated from cold-formed sections, positive eccentricities appear in the truss nodes, to induce additional forces truss chords. In order to account for the real load-carrying capacity of truss node area the steel structure research was conducted in scale 1:1. As a result of experimental research, the forms of deformation and strains of the walls...
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Space-mapping-based design flow of miniaturized broadband matching transformer with perforated metallization
PublicationA fast design procedure of unconventional passive components has been presented and experimentally validated on the basis of a wideband microstrip four-section matching transformer (50:6 OHm). A classic impedance matching circuit has been miniaturized by means of compact microstrip resonant cells (CMRCs) leading to a considerable length reduction (34%) together with minor degradation in its performance. The spacemapping-based design...
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Processing of Marine Satellite Data in WEB-BASED GIS
PublicationGIS systems are important modern word. They allow to quickly analyse and corelate various data bound to their geographical context. The paper describes Web-base GIS with ability to integrate and analyse data from many sources such as: satellite imagery, threat simulation models, marine vessels Automatic Identification System, raster and vector topographic charts. Some details of system architecture and implementation are presented...
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Sensorless five-phase induction motor drive with third harmonic injection and inverter output filter
PublicationThe paper presents a sensorless control approach for a five-phase induction motor drive with third harmonic injection and inverter output filter. In the case of the third harmonic injection being utilised in the control, the physical machine has to be divided into two virtual machines that are controlled separately and independently. The control system structure is presented in conjunction with speed and rotor flux observers that...
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Mucinous cystadenocarcinoma, NOS - Female, 66 - Tissue image [10010729534329421]
Open Research DataThis is the histopathological image of OVARY tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Mucinous cystadenocarcinoma, NOS - Female, 66 - Tissue image [10010729534339721]
Open Research DataThis is the histopathological image of OVARY tissue sample obtained in Medical University Gdańsk and deposited in ZMDL-GUMED. The sample image was taken using: Pannoramic 250 3DHistech slide scanner (20x magnification) and saved to DICOM format.
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Impact of aeration conditions on the removal of low concentrations of nitrogen in a tertiary partially aerated biological filter
PublicationA submerged biological aerated filter (BAF) partially aerated was used to study the removal of low concentrations of ammonia nitrogen (0.3 g N/m3 to 30.5 g N/m3) typically found in nutrient enriched river and lake waters, and treated effluents. Four series of experiments were performed with a synthetic wastewater at ammonia loading rates between 6 g N/m3 d and 903 g N/m3 d and C/N ratios from 2 to 20. The results showed that ammonia...
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Biomechanics of Lumbar Spine Injury in Road Barrier Collision–Finite Element Study
PublicationLiterature and field data from CIREN database have shown that lumbar spine injuries occur during car crashes. There are multiple hypotheses regarding how they occur; however, there is no biomechanical explanation for these injuries during collisions with road safety barriers (RSBs). Therefore, the objective of this study was to investigate the mechanics of vertebral fractures during car collisions with concrete RSBs. The finite...
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Hydraulic analysis of causes of washout of Gdynia-Orłowo seashore during the flood in the Kacza river estuary
PublicationIn July 2016 in the Three-city agglomeration a rainfall episode of over a day duration and 150 mm summary rainfall height, occurred. This situation, extreme as for Polish conditions, caused significant freshets in rivers and streams running into Gdansk Bay, the Baltic Sea, and serving as collectors of rainfall waters for the sea-coast towns. In many areas of the Three-city flood phenomena and overflows took place. The flood also...
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Video traffic data - Interchange Sulno (S1-94), Poland
Open Research DataThe data includes video traffic data registered with 8 video cameras at weaving area (weaving section type A) of the Sulno interchange within S1 expressway in Poland (interchange of expressway S1 and national road 94), located in the Silesian Agglomeration. The data covers the two days: 12.09.2017 (expressway S1) and 13.09.2017 (road 94).
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Optoelectronic system for monitoring of thin diamond layers growth
PublicationDevelopment of the optoelectronic system for monitoring of diamond/DLC (Diamond-Like-Carbon) thin films growth during mu PA ECR CVD (Microwave Plasma Assisted Electron Cyclotron Resonance Chemical Vapour Deposition) process is described. The multi-point Optical Emission Spectroscopy (OES) and Raman spectroscopy were employed as non-invasive optoelectronic tools. Dissociation of H-2 molecules, excitation and ionization of hydrogen...
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An improved scalable method of isolating asphaltenes
PublicationA new, improved and scalable procedure of asphaltene fraction isolation is presented and compared to standard test methods. The new procedure uses 1:40 feedstock to solvent (n-heptane) ratio (g/mL), filtration through a cellulosic thimble and extensive washing in a Soxhlet type extractor. The group type composition and purity of the asphaltene fractions have been examined using thin-layer chromatography with flame-ionization detection....
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Direct-Ultrasonic Assisted Microextraction Coupled with RTL-GC-FID/GC-MS as a Future Standard Procedure for Monitoring 26 potentially Allergenic Fragrances in Water Samples
PublicationThis research topic grew up as a result of awareness of constant anthropogenic and natural input to the environment constituents of personal care products (PCPs) residues. This group of emerging pollutants encompasses a wide range of chemicals, including potentially allergenic fragrance compounds. The aim of the present study was to investigate presence of 26 fragrance allergens in water samples. Simple and rapid methodology based...
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Determination of SCFAs in water using GC-FID. Selection of the separation system
PublicationIn the present study, an analytical procedure was developed for the determination of short-chain fatty acids (SCFAs) in landfill leachate and municipal wastewater employing injection of aqueous samples to gas chromatograph with flame ionization detector (GC-FID). Chromatographic conditions such as a separation system, injection volume, oven temperature program were investigated and selected. With two columns, one with a polar (polyethylene...
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Comprehensive determination of flavouring additives and nicotine in e-cigarette refill solutions. Part I: Liquid chromatography-tandem mass spectrometry analysis
PublicationLiquid chromatography-tandem mass spectrometry with electrospray ionization (HPLC-ESI–MS/MS) methods were developed for the simultaneous determination of 42 flavouring compounds and nicotine in liquids for e-cigarettes. The chromatographic separation was performed using an Ace® Ultracore™ SuperC18™ (100 × 2.1 mm, 2.5 μm) column in both acidic and alkaline pH conditions to separate all the compounds. A simple “dilute & shoot” approach...
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Organic semiconductor rubrene thin films deposited by pulsed laser evaporation of solidified solutions
PublicationOrganic semiconductor rubrene (C42H28) belongs to most preferred spintronic materials because of the high charge carrier mobility up to 40 cm2(V·s)-1. However, the fabrication of a defect-free, polycrystalline rubrene for spintronic applications represents a difficult task. We report preparation and properties of rubrene thin films deposited by pulsed laser evaporation of solidified solutions. Samples of rubrene dissolved in aromatic...
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Application of electronic nose based on fast GC for comparison of aroma profiles of homemade cherry "Nalewka" made with addition of different amount of sugar
PublicationNalewka is a traditional Polish homemade spirit beverage and there are many different recepies for the production of nalewkas. However, it is not knownwhat amount of sugar can have influence of their aroma profiles. There is little information on the comparison of aroma profiles of Polish cherry nalewkas made with addition of different amount of sugar. For this purpose electronic nose based on fast GC has been used. Electronic...
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Application of electronic nose based on fast GC for comparison of aroma profiles of homemade cherry "Nalewka" made with addition of different amount of sugar
PublicationNalewka is a traditional Polish homemade spirit beverage and there are many different recepies for the production of nalewkas. However, it is not knownwhat amount of sugar can have influence of their aroma profiles. There is little information on the comparison of aroma profiles of Polish cherry nalewkas made with addition of different amount of sugar. For this purpose electronic nose based on fast GC has been used. Electronic...
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Application of normal-phase high-performance liquid chromatography followed by gas chromatography for analytics of diesel fuel additives
PublicationThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Research on the separation properties of empty-column gas chromatography (EC-GC) and conditions for simulated distillation (SIMDIS)
PublicationThe paper presents the results of investigations on new procedures of determination of selected cleaning additives in diesel fuel. Two procedures: one-step analysis using gas chromatography with flame ionization detection (GC-FID) or mass spectrometry (GC-MS) and a two-step procedure in which normal-phase high-performance liquid chromatography (NP-HPLC) was used for preliminary separation of the additives, were compared. The additive...
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Basic sensitivity analysis of a telecommunication tower complementing standard reinforcement design process
PublicationThis paper presents straightforward sensitivity assessment of a telecommunication tower. The analysis is set toidentify the elements of the tower which may be reinforced with the greatest structural advantage. As current expertopin ions on structural redesign of similar structures due to a planned addition of extra loads are mainly based ondeterministic computations or engineering intuition,...
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Formation of Protein Networks between Mucins: Molecular Dynamics Study Based on the Interaction Energy of the System
PublicationMolecular dynamics simulations have been performed for a model aqueous solution of mucin. As mucin is a central part of lubricin, a key component of synovial fluid, we investigate its ability to form cross-linked networks. Such network formation could be of major importance for the viscoelastic properties of the soft-matter system and crucial for understanding the lubrication mechanism in articular cartilage. Thus,the inter- and...
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THRIVING AND JOB SATISFACTION IN MULTICULTURAL ENVIRONMENTS OF MNCS
PublicationPurpose of the article The aim of the paper is to analyze the relationship between thriving and job satisfaction in multicultural environments of multinational corporations (MNCs). Methodology/methods The quantitative cross-sectional study was conducted on the sample of 128 individuals from subsidiaries of various MNCs located in Poland involved in intercultural interactions. Scientific aim The aim of this study was to examine...
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Deep convolutional neural network for predicting kidney tumour malignancy
PublicationPurpose: According to the statistics, up to 15-20% of removed solid kidney tumors turn out to be benign in postoperative histopathological examination, despite having been identified as malignant by a radiologist. The aim of the research was to limit the number of unnecessary nephrectomies of benign tumors. Methods or Background: We propose a machine-aided diagnostic system for kidney...
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Tensile and flexural moduli for human orbital wall bones – comparative study
PublicationThe main aims of the current research were: (1) to analyze in detail the tensile modulus and ultimate tensile strength (UTS) of orbital wall bones separately for the left and right orbit of the same cadaver and (2) to compare the obtained results with a flexural modulus of the left and right orbit reported earlier by A. C. van Leeuwen et al. [14]. A set of 54 specimens of orbital superior and/or medial walls harvested from 16 human...
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Safety PL - a support tool for Road Safety Impact Assessment
PublicationPublished on 19 November 2008, the European Union's Directive 2008/96/EC is one of the most important EU documents setting out a road safety orientation, in particular, road infrastructure safety management. It identifies four main areas of activity: road safety impact assessment, road safety audit, ranking of high accident concentration sections and network safety ranking and road infrastructure safety inspection. The Directive...
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Study of Aliphatic Polyurethanes by the Low-Field 1H NMR Relaxometry Method with the Inversion of the Integral Transformation
PublicationIn this paper, the distributions of the 1H nuclear magnetic resonance (NMR) spin–lattice and spin–spin relaxation times are used to characterize the mobility of different sections of macromolecules of aliphatic polyurethanes and the cross-linking density of polymer chains. The NMR relaxometry method with inversion of integral transformation is applied to study the effect of poly (ethylene glycol) and glycerol phosphate calcium...
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Investigation of rotational state-changing collisions of C2N− ions with helium
PublicationThe cross sections for rotational inelastic collisions between atoms and a molecular anion can be very large, if the anion has a dipole moment. This makes molecular anions very efficient in cooling atomic gases. We address rotational inelastic collisions of Helium atoms with the molecular anion C2N–. Here we present preliminary calculations of the potential energy surface.
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Role of methylation in electron scattering on X(CH3)4 (X = C, Si, Ge) molecules
PublicationTotal cross sections (TCS) for low-energy electron scattering from X(CH3)4 (where X = C, Si, Ge) molecules have been measured using linear transmission method. Present results and those obtained previously for XH4 molecules were used to determine how methylation of the target is reflected in TCS energy dependence.
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Estimation of wind pressure acting on the new palm house in Gdansk
PublicationThis paper deals with the problem of numerical simulations of wind loads acting on a Palm House with complex geometry. Flow simulations with aid of computational fluid dynamics procedures have been performed to check if the pressure distributions for the structure are greater than those calculated using the standard design codes with assumption that the Palm House horizontal cross sections are described by smooth cylinders.
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Methods of the privatization process of Polish state-owned enterprises in years 1990‒2015
PublicationThis article presents methods of the privatization process of state-owned enterprises in Poland in the period of years 1990‒2015. The author presents the change of number of state-owned companies over the selected period as well as describes the main methods of ownership transformation used in Poland. First part presents the mechanism of commercialization. Second discusses the indirect privatization and contribution to NFI. Next,...
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Dynamic effect of the vehicle passing under lightweight footbridge.
PublicationThe paper describes a numerical study of dynamic response of cable-stayed steel footbridge for a big lorry passing underneath. The footbridge is an existing object crossing Wolska street in Warsaw. The structural model of footbridge was verified by dynamic test loading. A numerical study of a vehicle passing under footbridge is presented. 2D and 3D incompressible flow fields are modeled using sliding mesh in transient CFD computation....
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Maria Damps dr n.med.
PeopleA specialist in anesthesiology and intensive care, Dr. Maria Damps works every day at the Upper Silesian Children's Health Center in Katowice and as a scientific and research assistant at the Faculty of Medical Sciences at the Medical University of Silesian, Poland. Dr. Damps is a graduate of postgraduate studies in medical law and bioethics at the Jagiellonian University in Kraków. Dr. Damps is also the chairwoman of the Ethics...
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Badania eksperymentalne słupów CFST z betonem zwykłym i ekspansywnym
PublicationPraca przedstawia badania eksperymentalne ponad 40 słupów CFST. Analizie poddano wyniki siły niszczącej słupy w aspekcie grubości stalowego płaszcza, smukłości słupa, rodzaju betonu wypełniającego stalową rurę (zwykły i ekspansywny) i jego wytrzymałości a także sposobu obciążania słupa (przez rdzeń lub przez cały przekrój). Sprawdzono efektywność słupów CFST z użyciem betonu ekspansywnego i zwykłego rozumianą jako stosunek nośności...