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Search results for: HODOWLA RYB
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Analysis of the influence of polystyrene microplastics and their derivatives on the DNA of human colon epithelial cells HT29 with the comet assay
PublicationWe have been using plastic for almost a century and nowadays a lot of them circulates as pollutants in the environment and still defragmenting to micro and nanoscale. The exposition through the food chain and its precise impact on human health is still not clear. In our study, we tested real food packaging after contact with food products and real thermoinsulation and environmental samples of polystyrene in different model liquids,...
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The optimization of enzyme immobilization at Au-Ti nanotextured platform and its impact onto the response towards glucose in neutral media
PublicationThe market of non-invasive glucose sensors is drastically growing due to increasing number of people suffering from diabetes. Therefore, there is a significant need for any improvement in the field of biosensors that can be used for monitoring glucose level in human body. In recent years the emphasis is put onto the modification of electrode material with enzymes possessing recognition centre specific towards particular molecules....
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Synthesis, thermal, structural and electrical properties of vanadium-doped lithium-manganese-borate glass and nanocomposites
PublicationA glassy sample with a nominal formula LiMn1−3x/2VxBO3 (where x = 0.05) was synthesised using the melt-quenching method. Material was characterised by differential thermal analysis (DTA), X-ray diffactometry (XRD) at room temperature and as a function of temperature (HT-XRD), X-ray photoelectron spectroscopy (XPS), impedance spectroscopy (IS) and scanning electron microscopy (SEM). Dependences of glass transition and crystallisation...
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Correlation between partial inhibition of hydrogen evolution using thiourea and catalytic activity of AB5-type hydrogen storage alloy towards borohydride electrooxidation
PublicationDirect borohydride fuel cells (DBFCs) are devices which directly convert the chemical energy stored in the borohydride ion and oxidant into electrical energy as a result of redox reactions. Unfortunately, a significant amount of fuel is lost as a result of the undesirable hydrolysis reaction. The selection of an efficient borohydride hydrolysis inhibitor requires detailed knowledge regarding the interaction mechanism between the...
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Ultrastructural analysis of the submandibular sialoliths: Raman spectroscopy and electron back-scatter studies
PublicationThe aim of work was the epidemiological analysis of the occurrence of sialolithiasis of the submandibular gland in adults and the evaluation of the ultrastructure of salivary stones. The study sample consisted of 44 sialoliths. Analysis of the structure and chemical composition of sialoliths was performed using a Scanning Electron Microscope and Raman Spectroscopy. Comparing our results with the literature we can say that the epidemiology...
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Thermally tuneable optical and electrochemical properties of Au-Cu nanomosaic formed over the host titanium dimples
PublicationAu-Cu nanostructures offer unique optical and catalytic properties unlike the monometallic ones resulting from the specific interaction. Among others, they have the ability to exhibit surface plasmon resonance, electrochemical activity towards the oxygen and hydrogen evolution reaction (OER, HER) as well as improved photoresponse in relation to monometalic but those properties depend highly on the substrate where bimetallic structures...
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Multifrequency Nanoscale Impedance Microscopy (m-NIM): A novel approach towards detection of selective and subtle modifications on the surface of polycrystalline boron-doped diamond electrodes
PublicationIn this paper, we describe the modification of Nanoscale Impedance Microscopy (NIM), namely, a combination of contact-mode atomic force microscopy with local impedance measurements. The postulated approach is based on the application of multifrequency voltage perturbation instead of standard frequency-by-frequency analysis, which among others offers more time-efficient and accurate determination of the resultant impedance spectra...
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Studies on Aminoanthraquinone-Modified Glassy Carbon Electrode: Synthesis and Electrochemical Performance toward Oxygen Reduction
PublicationIn this paper, 9,10-anthraquinone (AQ) derivative-modified glassy carbon (GC) electrodes were studied towards the electrochemical reduction of oxygen in aqueous and non-aqueous solutions. The reaction of 1-chloro-9,10-anthraquinone with aliphatic diamines was applied for the synthesis of amino-9,10-anthraquinone derivatives. The obtained AQ derivatives were grafted onto the surface of glassy carbon electrodes by electropolymerisation...
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Microwave-Induced Processing of Free-Standing 3D Printouts: An Effortless Route to High-Redox Kinetics in Electroanalysis
Publication3D-printable composites have become an attractive option used for the design and manufacture of electrochemical sensors. However, to ensure proper charge-transfer kinetics at the electrode/electrolyte interface, activation is often required, with this step consisting of polymer removal to reveal the conductive nanofiller. In this work, we present a novel effective method for the activation of composites consisting of poly(lactic...
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Unlocking the electrochemical performance of glassy carbon electrodes by surface engineered, sustainable chitosan membranes
PublicationChitosan coatings, derived from crustacean shell waste, possess inherent biocompatibility and biodegradability, rendering them suitable for various biomedical and environmental applications, including electrochemical biosensing. Its amine and hydroxyl functional groups offer abundant sites for chemical modifications to boost the charge transfer kinetics and provide excellent adhesion, enabling the construction of robust electrode-coating...
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Characterization of Corrosion-Induced Fracture in Reinforced Concrete Beams Using Electrical Potential, Ultrasound and Low-Frequency Vibration
PublicationThe paper deals with the non-destructive experimental testing of the reinforced concrete beams under progressive corrosion. A series of experiments using electrical potential, ultrasound and low-frequency vibrations techniques are reported. Electrical potential and natural frequencies were used to characterise and monitor the corrosion process at its initial state. The P-wave velocity measurements were proved to be effective in...
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Imidazole-Based Lithium Salt LiHDI as a Solid Electrolyte Interphase-Stabilising Additive for Lithium-Conducting Electrolytes
PublicationLithium salt LiHDI (lithium 4,5-dicyano-2-(n-heptafluoropropyl)imidazolide) is proposed as a solid electrolyte interphase-stabilising additive for lithium-ion batteries, which can be added in a smaller amount than fluoroethylene carbonate (FEC) and vinylene carbonate (VC) additives. Electrolytes containing either lithium 4,5-dicyano-2-(trifluoromethyl)imidazolide (LiTDI) or battery-standard LiPF6 were tested with various amounts...
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Laser-Induced Graphitization of Polydopamine on Titania Nanotubes
PublicationSince the discovery of laser-induced graphite/graphene, there has been a notable surge of scientific interest in advancing diverse methodologies for their synthesis and applications. This study focuses on the utilization of a pulsed Nd:YAG laser to achieve graphitization of polydopamine (PDA) deposited on the surface of titania nanotubes. The partial graphitization is corroborated through Raman and XPS spectroscopies and supported...
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Band Gap Engineering toward Semimetallic Character of Quinone-Rich Polydopamine
PublicationSemiconductor|melanin interfaces have received increasingly more attention in the fields of photocatalysis and applied electrochemistry because of their facile synthesis, unique electrical properties, and strong capability toward photosensitization. In this work, we describe the electropolymerization of quinone-rich polydopamine (PDA) on the surface of hydrogenated TiO2 nanotubes with enhanced photoactivity in the visible spectrum....
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Tailoring diamondised nanocarbon-loaded poly(lactic acid) composites for highly electroactive surfaces: extrusion and characterisation of filaments for improved 3D-printed surfaces
PublicationA new 3D-printable composite has been developed dedicated to electroanalytical applications. Two types of diamondised nanocarbons - detonation nanodiamonds (DNDs) and boron-doped carbon nanowalls (BCNWs) - were added as fillers in poly(lactic acid) (PLA)-based composites to extrude 3D filaments. Carbon black served as a primary filler to reach high composite conductivity at low diamondised nanocarbon concentrations (0.01 to 0.2...
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Investigation of the structural and thermal properties of aluminum-rich Ca–Al–Si–O–N glasses
PublicationIn this paper, we investigate the structure and thermal properties of aluminum-rich transparent Ca–Al–Si–O–N glasses. The obtained glasses were prepared by a traditional melt-quenching technique at 1650 °C using AlN as the nitrogen source. The obtained glasses have a nAl/nSi>1 and contain up to 17 eq.% of N. The structure of the glasses was characterized by X-ray diffraction, X-ray photoelectron spectroscopy, infrared, and Raman...
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Evaluation of thermal cracking probability for asphalt concretes with high percentage of RAP
PublicationThe paper presents determination of the probability of thermal cracking of asphalt mixtures with different reclaimed asphalt pavement (RAP) content on the basis of laboratory tests and analytical evaluation using thermal stress development method. Probability was evaluated taking into consideration: the type and gradation of the mixture and the quality and content of RAP. Thermal stresses were determined using two models: elastic and...
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Tuning the Laser-Induced Processing of 3D Porous Graphenic Nanostructures by Boron-Doped Diamond Particles for Flexible Microsupercapacitors
PublicationCarbon (sp3)-on-carbon (sp2) materials have the potential to revolutionize fields such as energy storage and microelectronics. However, the rational engineering and printing of carbon-on-carbon materials on flexible substrates remains a challenge in wearable electronics technology. This study demon-strates the scalable fabrication of flexible laser-induced graphene (LIG)-boron doped diamond nanowall (BDNW) hybrid nanostructures...
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Monitoring Trends of Land Use and Land Cover Changes in Rajang River Basin
PublicationIn this study, the spatiotemporal changes in land use and land cover (LULC) were evaluated from 1992 to 2015 for the Rajang River Basin (RRB) located in the Sarawak State of Malaysia. The changes in water bodies cropped lands, and forests were assessed based on the available remotely sensed satellite data. Supervised classification with the Maximum-Likelihood-Algorithm technique was adopted for monitoring the LULC changes using...
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BP-EVD: Forward Block-Output Propagation for Efficient Video Denoising
PublicationDenoising videos in real-time is critical in many applications, including robotics and medicine, where varying light conditions, miniaturized sensors, and optics can substantially compromise image quality. This work proposes the first video denoising method based on a deep neural network that achieves state-of-the-art performance on dynamic scenes while running in real-time on VGA video resolution with no frame latency. The backbone...
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Correction: Titania nanotubes infiltrated with the conducting polymer PEDOT modified by Prussian blue – a novel type of organic–inorganic heterojunction characterised with enhanced photoactivity
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Nasiona roślin strączkowych jako źródło składników odżywczych w diecie roślinnej
PublicationObecnie coraz więcej osób decyduje się na ograniczenie lub wykluczenie produktów pochodzenia zwierzęcego (Fructuoso i in. 2021). Jednym z najczęściej podawanym powodem jest nietolerancja laktozy, alergie na białka np. mleka oraz choroby układu krwionośnego (Kundu i in. 2018). Oprócz aspektów zdrowotnych należy zwrócić uwagę na przyczynianie się rolnictwa, szczególnie hodowli zwierzęcej, do emisji...
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Izolacja drożdży psychrotolerancyjnych oraz ocena ich zdolności do wykorzystania N-fosfonometyloglicyny jako źródła pierwiastków biogennych
PublicationN-fosfonometyloglicyna (PMG, glifosat) jest substancją aktywną herbicydu Roundup o szerokim spektrum aktywności biologicznej. Mechanizm jego działania opiera się na inhibicji aktywności syntazy 5-enolopirogroniano-szikimowo-3-fosforanowej (EPSP), przez co hamowana jest biosynteza aminokwasów aromatycznych u roślin. Glifosat jest związkiem fosforoorganicznym, w którego budowie wyróżnia się trwałe wiązanie C-P. Szybkość rozkładu...
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Wpływ zmiany parametrów geometrycznych na wydajność i efektywność protezy zastawki aortalnej Human Aortic Bioprosthesis
PublicationW pracy wykazano na podstawie rezultatów badań in vitro, że konstrukcja wykonana z nanocelulozy bakteryjnej, posiada wszelkie cechy protezy zastawki aortalnej możliwe do wykazania na drodze ww. badań oraz że określone cechy geometrii protezy wpływają na jej efektywność i funkcjonalność. W szczególności, w pracy przedstawiono wyniki badań in vitro trzech modeli konstrukcji protezy zastawki aortalnej, oznaczonych M2, M4’ i M4. Badania...
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Przestrzenna analiza zgonów kobiet i mężczyzn w Polsce w przekroju podregionów w 2012 roku
PublicationW 2012 roku oczekiwana długość życia w momencie narodzin wynosiła w Polsce dla kobiet 81 lat, a dla mężczyzn 72,7 roku i od 1990 roku wydłużyła się odpowiednio o 5,8 i 6,5 roku. Wartości te są jednak nadal niższe niż w krajach Europy Zachodniej, gdzie kobiety żyją przeciętnie o 3 lata, a mężczyźni o 8 lat dłużej (Richardson i in., 2013). Wydłużenie oczekiwanej długości życia zostało osiągnięte między innymi dzięki malejącej śmiertelności...
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Lower Rim Substituted p-tert-Butyl Calix[4]arenes(V). Synthesis of New 5,11,17,22-tetrakis-p-tert-Butyl-25-27-bis(dialkoxyphosphorylmethoxy)calix[4] arenes and Cation Complexation Studies in Ion Selective Membrane Electrodes.
PublicationZaprezentowano syntezę i właściwości trzech nowych związków (2-4), bis podstawionych na dolnym obrzeżu grupami z resztą fosforylową. Związki te były badane jako jonofory w membranowych elektrodach jonoselektywnych (ISE) wykazując selektywność na kationy Rb+,K+ oraz duży i płaski kation guanidyniowyG+). Badano korelację pomiędzy stereo-strukturą związków a ich selektywnością w ISE. Stałe trwałości kompleksów z kationami metali...
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Zarządzanie Wiedzą (ćw - zaoczne_FK)
e-Learning Coursesimię i nazwisko prowadzącego - FRANCISZEK KUTRZEBA nazwa przedmiotu lub kursu - Zarządzanie Wiedzą (ćw - zaoczne) tryb studiów - Niestacjonarne stopień studiów - II stopnia kierunek studiów lub nazwa studiów podyplomowych - Zarządzanie
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Coastal cliff erosion as a source of toxic, essential and nonessential metals in the marine environment
PublicationDue to the rising environmental awareness, emissions and releases of pollutants, including metals, have been considerably reduced in the last decades. Therefore, the remobiliza-tion of natural and anthropogenic contaminants is gaining importance in their biogeochemical cycle. In the marine coastal zone, this process occurs during the erosion of a shore, especially the most vulnerable cliffs. The research was conducted in the...
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Regulated Control of the Assembly and Diversity of LPS by Noncoding sRNAs
PublicationThe outer membrane (OM) of Gram-negative bacteria is asymmetric due to the presence of lipopolysaccharide (LPS) facing the outer leaflet of the OM and phospholipids facing the periplasmic side. LPS is essential for bacterial viability, since it provides a permeability barrier and is a major virulence determinant in pathogenic bacteria. In Escherichia coli, several steps of LPS biosynthesis and assembly are regulated by the RpoE...
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In situ soil mixing.
PublicationOpracowanie stanowi 9-ty rozdział w książce ''Ground Improvement'' (Wzmacnianie gruntu).W podrozdziałach 9.1 i 9.2 przedstawiono rys historyczny oraz aktualny stan zaawansowania technologii mieszania gruntu na sucho i na mokro. Wprowadzono także klasyfikację metod wdrożonych na świecie przez firmy specjalistyczne. W podrozdziale 9.3 opisano sprzęt i technologię i przebieg mieszania, z podziałem na urządzenia do mieszania głębokiego...
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Family Tree for Aqueous Organic Redox Couples for Redox Flow Battery Electrolytes: A Conceptual Review
PublicationRedox flow batteries (RFBs) are an increasingly attractive option for renewable energy storage, thus providing flexibility for the supply of electrical energy. In recent years, research in this type of battery storage has been shifted from metal-ion based electrolytes to soluble organic redox-active compounds. Aqueous-based organic electrolytes are considered as more promising electrolytes to achieve “green”, safe, and low-cost...
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Morphology Regulation Mechanism and Enhancement of Photocatalytic Performance of BiOX (X = Cl, Br, I) via Mannitol-Assisted Synthesis
PublicationBiOX (X = Cl, Br, I) photocatalysts with dominant (110) facets were synthesized via a mannitol-assisted solvothermal method. This is the first report on the exposed (110) facets-, size-, and defects-controlled synthesis of BiOX achieved by solvothermal synthesis with mannitol. This polyol alcohol acted simultaneously as a solvent, capping agent, and/or soft template. The mannitol concentration on the new photocatalysts morphology...
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Realizm kapitalistyczny. Czy nie ma alternatywy? / Mark Fisher; przełożył i posłowiem opatrzył Andrzej Karalus
PublicationPraca rozważa, jak neoliberalna hegemonia instalując „ontologię biznesu” we wszystkich sferach rzeczywistości, formatuje niepostrzeżenie nasze pragnienia, aspiracje i nadzieje. Wbrew triumfalistycznej retoryce „efektywności” i „społecznej odpowiedzialności” realizm kapitalistyczny nie przestaje jednak generować systemowych zaburzeń, które w dłuższej perspektywie go destabilizują. Jest nie tylko przyczyną degradacji środowiska naturalnego...
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Garnizon w Gdańsku przykładem kształtowania atrakcyjnych przestrzeni miejskich na terenach powojskowych
PublicationCelem artykułu jest przedstawienie polskiego przykładu działań rewitalizacyjnych na terenach „odzyskiwanych” w mieście. Opisywany proces dotyczy Garnizonu w Gdańsku Wrzeszczu. Tereny te były dawniej zajmowane przez wojsko, obecnie od kilku lat prowadzone są na nich prace budowlane mające na celu stworzenie kompleksowego zespołu mieszkalno-usługowego z bogatą ofertą usług towarzyszących. Rewitalizacja tego obszaru umożliwia włączenie...
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Application of the 3D DEM in the modelling of fractures in pre-flawed marble specimens during uniaxial compression
PublicationPrzedstawiono w tym artykule wyniki modelowania pęknięć w cylindrycznych próbkach marmurowych ze wstępnymi nacięciami w czasie jednoosiowego ściskania . Zastosowano metodę elementów dyskretnych (DEM). Zbadano propagację i koalescencję pęknięć w próbkach marmuru z istniejącymi otwartymi nacięciami pod różnymi kątami do poziomu. Wyniki numerycznych symulacji trójwymiarowych (3D) zostały bezpośrednio porównane z badaniami laboratoryjnymi....
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Predictive current controller for sensorless induction motor drive
PublicationPrzedstawiono układ bezczujnikowego sterowania dla napedu z silnikiem klatkowym przy zastosowaniu predykcyjnego regulatora pradu. Zastosowany obserwator adaptacyjny wykazuje dużą odporność na zmiany parametrów silnika. W obserwatorze obliczane są wartości sił elektromotorycznych wykorzystywane w procesie regulacji predykcyjnej pradu silnika. Pokazano wyniki badań symulacyjnych i eksperymentalnych.
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Enhanced photoelectrochemical and photocatalytic performance of iodine-doped titania nanotube arrays
PublicationThe paper discusses the synthesis and performance of iodine doped titania nanotube arrays exhibited under irradiation. The doping procedure was performed as an additional, electrochemical process carried out after formation of nanotube arrays via anodization of Ti substrate. The optical and structural properties were characterized using Raman, UV-vis, photoluminescence and X-ray photoelectron spectroscopy. The surface morphology...
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Thin layer of ordered boron-doped TiO2 nanotubes fabricated in a novel type of electrolyte and characterized by remarkably improved photoactivity
PublicationThis paper reports a novel method of boron doped titania nanotube arrays preparation by electrochemical anodization in electrolyte containing boron precursor – boron trifluoride diethyl etherate (BF3 C4H10O), simultaneously acting as an anodizing agent. A pure, ordered TiO2 nanotubes array, as a reference sample, was also prepared in solution containing a standard etching compound: ammonium fluoride. The doped and pure titania...
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The Spectral Compositions of Light Changes Physiological Response of Chinese Cabbage to Elevated Ozone Concentration
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Artificial-Neural-Network-Based Sensorless Nonlinear Control of Induction Motors
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Rotor broken bar diagnostics in induction motor drive using Wavelet packet transform and ANFIS classification
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How Chain Transfer Leads to a Uniform Polymer Particle Morphology and Prevents Reactor Fouling
PublicationABSTRACT: The effect of adding diethyl zinc as a chain transfer agent during the polymerization of propylene in heptane performed at 80 °C was studied. Although it was expected that the chain transfer would stop after precipitation of the polymer, the polymer molecular weight continued to increase throughout the whole of the polymerization. The presence of diethyl zinc had an additional effect that the polymerizations were devoid...
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The Effect of Protrusions on the Initiation of Partial Discharges in XLPE High Voltage Cables
PublicationThis paper is focusing on 3D Finite Elements Analysis (FEA) based modelling of protrusions as defects or imperfections in the XLPE high voltage cable. This study is aiming to examine the impact protrusions have on the initiation of partial discharges. Spherical and ellipsoidal protrusions with different sizes at the conductor screen of the high voltage cable is an essential content of this paper. In addition, a spherical gas-filled...
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Facet effect of TiO2 nanostructures from TiOF2 and their photocatalytic activity
PublicationIn this study, special attention is focused on the design of TiO2 morphology and microstructure in the two-step preparation procedure using TiOF2 as a precursor to study their photodegradation mineralization efficiency. Firstly, TiOF2 was synthesized by a simple solvothermal method using titanium(IV) tetrafluoride, which was further used as a precursor in preparation of anatase 2D nanosheets, octahedral, decahedral, and rectangular prisms...
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Capacitance Enhancement by Incorporation of Functionalised Carbon Nanotubes into Poly(3,4-Ethylenedioxythiophene)/Graphene Oxide Composites
PublicationThis paper reports on the role of oxidised carbon nanotubes (oxMWCNTs) present in poly-3,4-ethylenedioxytiophene (PEDOT)/graphene oxide (GOx) composite. The final ternary composites (pEDOT/GOx/oxMWCNTs) are synthesised by an electrodeposition process from the suspension-containing monomer, oxidised carbon nanotubes and graphene oxide. Dissociated functional groups on the surface of graphene oxide play a role of counter-ions for the...
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Diaryl Sulfide Derivatives as Potential Iron Corrosion Inhibitors: A Computational Study
PublicationThe present work aimed to assess six diaryl sulfide derivatives as potential corrosion inhibitors. These derivatives were compared with dapsone (4,4′-diaminodiphenyl sulfone), a common leprosy antibiotic that has been shown to resist the corrosion of mild steel in acidic media with a corrosion efficiency exceeding 90%. Since all the studied compounds possess a common molecular backbone (diphenyl sulfide), dapsone was taken as the...
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Novel composite of Zn/Ti-layered double hydroxide coupled with MXene for the efficient photocatalytic degradation of pharmaceuticals
PublicationIn the present study, a hybrid photocatalyst of Zn/Ti layered double hydroxide (LDH) coupled with MXene – Ti3C2 was synthesized for the first time and applied in photocatalytic degradation of acetaminophen and ibuprofen, two commonly present in the natural environment and prone to accumulate in the aquatic ecosystem pharmaceuticals. The effect of MXene content (0.5 wt%, 2.5 wt%, and 5 wt%) on the photocatalytic activity of LDH/MXene...
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Defective TiO2 Core-Shell Magnetic Photocatalyst Modified with Plasmonic Nanoparticles for Visible Light-Induced Photocatalytic Activity
PublicationIn the presented work, for the first time, the metal-modified defective titanium(IV) oxide nanoparticles with well-defined titanium vacancies, was successfully obtained. Introducing platinum and copper nanoparticles (NPs) as surface modifiers of defective d-TiO2 significantly increased the photocatalytic activity in both UV-Vis and Vis light ranges. Moreover, metal NPs deposition on the magnetic core allowed for the effective separation...
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Enhanced stability of electrochemical performance of few-layer black phosphorus electrodes by noncovalent adsorption of 1,4-diamine-9,10-anthraquinone
PublicationIn this paper, the novel noncovalent functionalisation strategy of few-layer black phosphorus by 1,4-diamine-9,10-anthraquinone electrode was proposed and studied. The degradation of few-layer black phosphorus under exposure to oxygen and water is a significant obstacle to its use as an electroanalytical electrode. The anthraquinone compound adsorbed at black phosphorus flakes results in improved prevention of the phosphorus surface...
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Pseudo-superparamagnetic behaviour of bariumhexaferrite particles
PublicationThe effect of hexadecyltrimethylammonium bromide (CTAB) addition on the crystal structure, morphology,and magnetic properties of co-precipitated hexagonal barium ferrite was investigated. For afixed amount ofsurfactant, different Fe3+concentrations and Fe3+/Ba2+ratios were used to optimize the formation ofsingle-phase barium ferrite particles. The results indicated that the obtained ferrite particles exhibitedcoercivity changes...