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Wyniki wyszukiwania dla: starburst amines
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Self-assembly of secondary aryl amides in cocrystals with perfluoroaryl coformers: structural analysis and synthon preferences
PublikacjaCooperation of aryl⋯perfluoroaryl stacking interactions and hydrogen bonds was utilized in the construction of six novel cocrystals of aromatic cis-amides with pentafluorobenzoic acid (pfba) and pentafluorophenol (pfp). They were obtained by crystallization from solution and structurally characterized. In four instances, the components form heterotetrameric motifs, in which amide:amide homodimer interacts symmetrically on two sides...
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Amides as models to study the hydration of proteins and peptides — spectroscopic and theoretical approach on hydration in various temperatures
PublikacjaInteractions with water are one of the key factors which determine protein stability and activity in aqueous solutions. However, the protein hydration is still insufficiently understood. N-methylacetamide (NMA) is regarded as a minimal part of the peptide backbone and the relative simplicity of its structure makes it a good model for studies on protein–water interactions. In this paper, the influence of NMA and N,N-dimethylacetamide...
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Amine-functionalized magnetite-silica nanoparticles as effective adsorbent for removal of uranium(VI) ions
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Machine Learning Methods in Damage Prediction of Masonry Development Exposed to the Industrial Environment of Mines
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The Synthesis of 3-Amino-pyrazine-2-carbohydrazide and 3-Amino-N'-methylpyrazine-2-carbohydrazide Derivatives
PublikacjaW poszukiwaniu biologicznie aktywnych związków otrzymano szereg pochodnych 3-Amino-pirazyno-2-karbohydrazydu i 3-Amino-N'-metylopirazyno-2-karbohydrazydu w wyniku reakcji hydrazydu aminopirazynoinowegokwasu z izocyjanianami, aldehydami, ketonami, CS2 i kwasem mrówkowym.
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The concentration of geothermal brines with iodine content by membrane distillation
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Mono- and polynuclear Co(II) silanethiolates with aliphatic diamines
PublikacjaFour Co(II) complexes, [Co{SSi(OtBu)3}2(dmpda)] 1, [Co{SSi(OtBu)3}2(bda)2]n2 [Co{SSi(OtBu)3}2(pda)2]n3 and [Co{SSi(OtBu)3}2(hda)2]n4 [dmpda = 3-(dimethylamino)-1-propylamine; bda = 1.4-butanediamine; pda = 1.5-pentanediamine; had = 1.6-hexanediamine] have been synthesized and characterized using X-ray diffraction. Complex 1 is mononuclear and contains Co(II) coordinated by dmpda molecule in chelating mode, whereas compounds 3 and...
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Amino acid formation by electron irradiation
PublikacjaW artykule zaprezentowano procedurę badania reakcji indukowanych przez niskoenergetyczne elektrony w mieszanych warstwach molekularnych CH3COOD:NH3.
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Ruling lines removal in handwritten documents
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Chirality Measures of α-Amino Acids
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Reparatur eines beschdigten Doppelmantel Stahlbehlters.
PublikacjaOmówiono technologię napraw płaszcza wewnętrznego w zbiorniku dwupłaszczowym. Płaszcz został uszkodzony, utracił lokalnie stateczność w wyniku błędu w przeprowadzaniu próby wodnej. Oryginalna metoda naprawy - zastosowanie wtłaczania hydraulicznego - wydatnie uprościło naprawę zmniejszając zakres elementów, które należało wymienić.
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Ferrite coupled slot lines circulator.
PublikacjaW oparciu o metodę rodzajów sprzężonych przeprowadzono analizę macierzy rozproszenia sekcji ferrytowych linii szczelinowych (FLS). W oparciu o uzyskane wyniki opracowano model cyrkulatora zaprojektowany w postaci kaskadowego połączenia sekcji FLS oraz szczelinowego rozgałęzienia typu T. Określono parametry rozproszenia układu, które zweryfikowano eksperymentalnie.
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Modelling of MV and HV Cable Lines
PublikacjaOverhead and cable lines are fundamental elements of power systems. Participation of cable lines is smaller and their percentage decreases as voltage is increased. HV cable lines are often built with the use of cables which are composed of coaxial metallic sheaths. Such cables are also often used in MV networks. The sheath may operate in different confgurations. In the case of Polish MV network the sheaths are earthed at both ends....
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Resonance problems in UHV transmission lines
PublikacjaThe paper presents resonance phenomena observed in 400 kV transmission lines in the Polish power system. Two events are analysed, when shunt reactors used for reactive power compensation, caused overvoltages and overcurrent protection tripping as a result of resonance. An oscillographic fault recordings from protection devices are compared to time domain simulation results. The obtained simulation results match fault recordings,...
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Biosynthetic and synthetic access to amino sugars.
PublikacjaAmino sugars are important constituents of a number of biomacromolecules and products of mi crobial secondary metabolism, including antibiotics. For most of them, the amino group is located at the positions C1, C2 or C3 of the hexose or pentose ring. In biological systems, amino sugars are formed due to the catalytic activity of specific aminotransferases or amidotransferases by introducing an amino functionality derived from L-glutamate...
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Mechanical properties of concrete mixes M0-M100 concrete mixes
Dane BadawczeDataset of hardneded properties of concretes containing different amount of magnetite aggregate (M0-M100) mixes.Excel file consists results of:
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Fresh properties of concrete mixes M0-M100 concrete mixes
Dane BadawczeDataset of fresh properties of concretes containing different amount of magnetite aggregate (M0-M100) mixes.*. ODS - open-source spreadsheet file file consists results of:
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Influence of Illite and Its Amine Modifications on the Self-Adhesive Properties of Silicone Pressure-Sensitive Adhesives
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Cubane Like Structure of a Silanethiol Primary Amine Assembly a Novel, Unusual Hydrogen Bond Pattern.
PublikacjaMetodą rentgenowskiej analizy strukturalnej wyznaczono struktury krystaliczne i cząsteczkowe trzech soli amoniowych: (t-BuO)3SiS(-)H3N(+)Bu-t, (i-PrO)3SiS(-)H3N(+)Bu-t i (t-BuO)3SiS(-)H3N(+)(CH2)2CH(CH3)2. Wszystkie trzy związki w ciele stałym tworzą tetramery w których atomy S i N wyznaczają w przybliżeniu naroża sześcianu. Trwałość tych agregatów, oprócz sił elektrostatycznego przyciągania, zapewnia sieć wiązań wodorowych N-H
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An in situ derivatization – dispersive liquid–liquid microextraction combined with gas-chromatography – mass spectrometry for determining biogenic amines in home-made fermented alcoholic drinks
PublikacjaA novel dispersive liquid–liquid microextraction (DLLME) gas chromatography mass-spectrometry(GC–MS) method was developed for the determination of 13 biogenic amines in home-made wine sam-ples. The method allows to simultaneous extraction and derivatization of the amines providing a simpleand fast mode of extract enrichment. During the study, two different procedures were examined. Sta-tistical analysis was performed to choose...
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Amino Acid and Peptide‐Based Antiviral Agents
PublikacjaA significant number of antiviral agents used in clinical practice are amino acids, short peptides, or peptidomimetics. Among them, several HIV protease inhibitors (e. g. lopinavir, atazanavir), HCV protease inhibitors (e. g. grazoprevir, glecaprevir), and HCV NS5A protein inhibitors have contributed to a significant decrease in mortality from AIDS and hepatitis. However, there is an ongoing need for the discovery of new antiviral...
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Treatment of the three strip coplanar lines on the ferrite
PublikacjaW pracy przedstawiono badania koplanarnej linii paskowej złożonej z trzech pasków umieszczonych na podłużnie magnesowanym podłożu ferrytowym. W analizie badanej linii zastosowano metodę spektralną oraz metodę rodzajów sprzężonych. Współczynniki sprzężenia żyromagnetycznego oraz charakterystyki dyspersyjne zostały określone przy użyciu obu metod.
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Applications of Unnatural Amino Acids in Protease Probes
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Isolator using a ferrite-coupled-lines gyrator
PublikacjaPrzedstawiono koncepcję nowego typu gyratora wykonywanego poprzez zwarcie lub rozwarcie ferrytowych linii sprzężonych (FCL). Redukując w taki sposób macierz rozproszenia (S) sekcji FCL określono macierz S gyratora oraz procedurę jego projektowania. Poprzez odpowiednie wprowadzenie warstwy rezystywnej do układu gyratora zaprojektowano nowy układ isolatora typu FCL oraz podano metodykę jego projektowania. Koncepcje proponowanych...
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On the characteristic impedance definition in microstrip and coplanar lines
PublikacjaW niniejszej pracy rozważono definicję impedancji charakterystycznej dla bezstratnych linii mikropaskowych i koplanarnych. Wykazano, że ze względu na znaczne wartości prądu przesunięcia związanego z podłużną składową pola elektrycznego, definicja impedancji staje się niejednoznaczna. W rezultacie może to przyczyniać się do istotnych błędów powstających już na etapie projektowania układów. Pokazano, iż efekt ten jest szczególnie...
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Inhibitors of amino acids biosynthesis as antifungal agents
PublikacjaFungal microorganisms, including the human pathogenic yeast and filamentous fungi, are able to synthesize all proteinogenic amino acids, including nine that are essential for humans. A number of enzymes catalyzing particular steps of human-essential amino acid biosynthesis are fungi specific. Numerous studies have shown that auxotrophic mutants of human pathogenic fungi impaired in biosynthesis of particular amino acids exhibit...
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Method of lines for physiologically structured models with diffusion
PublikacjaWe deal with a size-structured model with diffusion. Partial differential equations are approximated by a large system of ordinary differential equations. Due to a maximum principle for this approximation method its solutions preserve positivity and boundedness. We formulate theorems on stability of the method of lines and provide suitable numerical experiments.
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Stark effect of atomic helium singlet lines
PublikacjaWe present experimental and theoretical investigations of the He spectral series 2S1−nQ1 (n=3÷9, Q=S,P,D,…,n−1) and 2P1−nQ1 (n=3÷9, Q=S,P,D,…,n−1) in electric fields up to 1635 kV/cm. Apart from the allowed transitions with |ΔL|=1, the transitions with |ΔL|=0,2,3,…-without field strictly forbidden-were observed. Several He patterns become similar to hydrogen patterns, which means they are nearly symmetric and show in higher fields...
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Direct conversion of secondary phosphine oxides and H-phosphinates with [di(acyloxy)iodo]benzenes to phosphinic and phosphonic amides
PublikacjaW publikacji przedstawiono metodę pozwalająca na bezpośrednie otrzymywanie amidów kwasu fosfinowego i fosfonowego w reakcji drugorzędowych tlenków fosfin lub H-fosfinianów z [di(acyloksy)iodo]benzenami w obecności amin pierwszo lub drugorzędowych. Wykorzytując silne acylujące właściwości układu [di(acyloksy)iodo]benzen/R2P(O)H.
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Anticancer Properties of Amino Acid and Peptide Derivatives of Mycophenolic Acid
PublikacjaBackground: Although Mycophenolic Acid (MPA) is applied as prodrugs in clinic as an immunosuppressant, it also possesses anticancer activity. MPA acts as Inosine-5’-Monophosphate Dehydrogenase (IMPDH) inhibitor, where the carboxylic group at the end of the side chain interacts with Ser 276 of the enzyme via hydrogen bonds. Therefore, MPA derivatives with other polar groups indicated high inhibition too. On the other hand, potent...
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Search for new tools to combat Gram-negative resistant bacteria among amine derivatives of 5-arylidenehydantoin
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Green, simple analytical method for biogenic amines determination in fruit juice samples using salting-out assisted liquid-liquid microextraction and gas chromatography-mass spectrometry
PublikacjaSalting-out assisted liquid-liquid microextraction (SALLME) was integrated with the derivatization procedure to establish a one-step sample pre-treatment approach for rapid analysis of 14 biogenic amines (BAs) in fruit juices. The methodology consists of salting-out of analytes, derivatization with ethyl chloroformate (ECF), extraction with ethyl acetate (EtAc), and the analysis of the derivatized BAs using gas chromatography-mass...
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Assessment of the factors influencing on the formation of energy-oriented modes of electric power consumption by water-drainage installations of the mines
PublikacjaPurpose. Performing the analysis to determine energy-efficient modes and assess the characteristics of the main indicators of electric power consumption by mine water-drainage installations based on the developed research mathematical model. Methods. To achieve the purpose set, a methodology is used to develop the multiple multifactor correlation-regression modeling with respect to the modes of electric power consumption by electrical...
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Singlet Exciton Diffusion in Vacuum-Evaporated Films of Amine-Based Materials as Studied by Photocurrent and Photoluminescence Quenching Methods
PublikacjaThe singlet exciton diffusion lengths are determined by the photoconductivity as well as the luminescence surface quenching technique, in vacuum‐evaporated layers of (4,4′,4″‐tris(N‐(3‐methylphenyl)‐N‐phenylylamino) triphenylamine) (m‐MTDATA), 4,4′,4″‐tris[2‐naphthyl(phenyl)amino] triphenylamine (2TNATA), and N,N′‐diphenyl‐N,N′‐bis(3‐methylphenyl)‐[1,1′‐biphenyl]‐4,4′‐diamine (TPD) which are frequently used for fabrication of electroluminescent...
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Search for ABCB1 Modulators Among 2-Amine-5-Arylideneimidazolones as a New Perspective to Overcome Cancer Multidrug Resistance
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Acid-aided epoxy-amine curing reaction as reflected in epoxy/Fe3O4 nanocomposites: Chemistry, mechanism, and fracture behavior
PublikacjaThis work seeks to answer the question whether or not the presence of acid functional groups accelerate epoxyamine curing reaction. Epoxy/Fe3O4 nanocomposite was considered as a case, where discussions are based on chemistry, mechanism behind curing reactions and fracture behavior influenced by acid assistance to crosslinking. Fe3O4 magnetic nanoparticles (MNPs) with nanosilica decorative layer (B-MNP) were synthesized and subsequently...
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Amino Acid Based Antimicrobial Agents – Synthesis and Properties
PublikacjaStructures of several dozen of known antibacterial, antifungal or antiprotozoal agents are based on the amino acid scaffold. In most of them, the amino acid skeleton is of a crucial importance for their antimicrobial activity, since very often they are structural analogs of amino acid intermediates of different microbial biosynthetic pathways. Particularly, some aminophosphonate or aminoboronate analogs of protein amino acids are...
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Buenos Aires – Toward Comprehensive Development and Sustainable Mobility
PublikacjaThis paper is introducing Buenos Aires’ achievements and challenges in implementing comprehensive development and integrating efficient and sustainable transport system within its urban structure. There are several important steps in this process starting from urban regeneration of Puerto Madero, the introduction and then implementation of a strategic plan Modelo territorial (2010) and of Buenos Aires' Plan de Movilidad Sustentable...
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Hyperfine Structure Study of Several Lines of207Pb I
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Impulse Measurements of Tower Earthings of Overhead Transmission Lines
PublikacjaPrzepisy wymagają okresowego badania uziemień słupów elektroenergetycznych linii przesyłowych. pomiary takie metodami klasycznymi niskiej częstotliwości wymagają odłączania uziomów od konstrukcji słupa, co wiąże się z wyłączaniem linii. wykorzstanie metody udarowej do oceny uziemień nie wymaga odłączania uziomów i może byc przeprowadzane podczas pracy linii.
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The effectiveness of chemotherapy and electrochemotherapy on ovarian cell lines in vitro
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Current advances in membrane processing of wines: A comprehensive review
PublikacjaBackground Membrane-based operations, especially pressure-driven membrane operations, are today well-established procedures for various applications in the wine industry thanks to their intrinsic properties and undoubted advantages over traditional methods. Emerging membrane processes, such as pervaporation, electrodialysis and osmotic distillation, forward osmosis, membrane contactors, offer new and interesting perspectives to...
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Nonreciprocity of a ferrite coupled microstrip-slot lines junction
PublikacjaW oparciu o wyniki modelowania numerycznego zbadano efekty niewzajemne występujące w strukturze sekcji sprzężonych poprzez warstwę ferrytu linii mikropaskowej i szczelinowej. Wykazano występowanie zjawiska periodycznej transformacji energii rodzaju mikropaskowego w rodzaj szczelinowy i odwrotnie.
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Application of Mazur-Orlicz`s theorem in AMISE calculation
PublikacjaW pracy podano nowe wyprowadzenie formuły asymptotycznej błędu aproksymacji dla operatorów całkowych w przestrzeniach niezmienniczych na przesunięcia. Obliczono asymptotykę błędu średniokwakratowego dla estymatora gęstości.
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The iterative method in search for the state of equilibrium in anchor lines.
PublikacjaPrzedstawiono iteracyjną metodę rozwiązywania równań równowagi lin kotwicznych. Metoda jest szczególnie łatwa do zaprogramowania obliczeń numerycznych, ponieważ w każdym kroku iteracyjnym wymaga jedynie obliczania całek oznaczonych znanych funkcji. Wynikiem obliczeń są wartości sił podłużnych w linie i jej kształt, który na skutek oddziaływania prądu oceanicznego na linę może być krzywą przestrzenną. Przytoczone przykłady...
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Structural Health Monitoring of Overhead Power Transmission Lines
PublikacjaStructural Health Monitoring (SHM) is a novel and continuously developing branch of science and technology that draws attention of scientists all over the world. It creates opportunities to detect, localize and identify structural damage of various types such as: line breakage, permissible sag, bolt loosening, fatigue cracking or insulator contamination. On the other hand the methods used to estimate the remaining operational...
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THE APPLICATION EFFECTS OF CONTINUOUS SATELLITE MEASUREMENTS OF RAILWAY LINES
PublikacjaThe paper presents results of satel lite surveying of the railway's rout es, which have been conducted just after starting in Poland (in 2008) the Active Geodesy Network ASG-EU POS. Afterwards it was possible to effectively utilize the GNSS survey ing results for the inventory of the (exploring) railways in service. Already at the beginning of 2009, the research team from Gdansk University of Technology and Naval Academy in Gdynia,...
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Retention modeling of some saccharides separated on an amino column.
PublikacjaUsing an amino column (Supelcosil LC-NH2) and different mixtures of acetonitrile-water, quantitative structure-retention relationship models are discussed. These models are based on computed molecular descriptors representing numerically structured features of some saccharides. The obtained results are underlining the lipophilicity/hydrophilicity balance, and how this is controlling the separation of the saccharides. The resulting...
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Method of lines for Hamilton-Jacobi functional differential equations.
PublikacjaInitial boundary value problems for nonlinear first order partial functional differential equations are transformed by discretization in space variables into systems of ordinary functional differential equations. A method of quasi linearization is adopted. Suffcient conditions for the convergence of the method of lines and error estimates for approximate solutions are presented. The proof of the stability of the diffrential difference...
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A review of amide bond formation in microwave organic synthesis
PublikacjaMicrowave-Assisted Organic Synthesis (MAOS) is one of the most current trends in organic chemistry. Herein, both the most popular and new approaches in microwave-syntheses of very important linkage in Nature - amide bond - are overviewed and compared with conventional synthetic routes.
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Determination of Selected Metals in Fruit Wines by Spectroscopic Techniques
PublikacjaThe determination of metals in different types of food and beverages samples has drawn significant attention due to several reasons with the most important one being the nutritional and toxic effects of these elements or their compounds. The knowledge of certain elements content in wines/fruit wines is of special interest due to their toxicity in case of excessive intake and also the effect they seem to have on the organoleptic...
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Modernization of tram lines with the use of railway design standards
PublikacjaThe article presents the main differences between the process of upgrading railway and tram routes. Geometrical layout designing is an issue of the interest. Railway designing rules that may be helpful in the design of the modernization are specified.
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Elżbieta Luboch prof. dr hab. inż.
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Aminy w środowisku - niebezpieczeństwo czy jego naturalny element?
PublikacjaA lot of amines and their compounds are used in the industry. First of all they are used for the preparation of medicines, plant protection agents, fertilizers and plastics. Amines are also released into the environment as a result of natural biological processes such as the release of certain species of flowers to lure insects, and also biochemical breakdown of amino acids in the protein during decomposition of organic matter. Unfortunately,...
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Jaroslaw Spychala dr
OsobyOprócz bardzo dobrego wykształcenia osoba posiada również wieloletnie doświadczenie zawodowe, które jest poświadczeniem tego, że potrafi wykorzystać swoją wiedzę teoretyczną w praktycznych działaniach. Doświadczenie zawodowe jest bardzo bogate i rozbudowane. Ze względu na nabyte całkiem nowe umiejętności zwiększa się atrakcyjność doświadczonego pracownika. Są to między innymi kreatywne myślenie, zorientowanie na cel, odporność...
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Manganese(III) Promoted Cyclization of N-alkenyl-N-(2-hydroxyethyl) amides to Iso-Oxacepham Potent β-Lactamase Inhibitors
PublikacjaBackground: β-Lactams are still a subject of interest of organic chemists. The main reason for this interest is due to their application as a chemotherapeutic. β-Lactam antibiotics are still the most commonly used drugs in bacterial infections. Method: Methods using 4-exo-trig radical cyclization leading to β-lactams are an alternative to classical Staudinger`s β-Lactams formation. We prepared N-alkenyl-N-(2-hydroxyethyl)amides...
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Sun shines also in Poland - PV's global market and its future in Poland
PublikacjaNiekorzystne zmiany klimatyczne stanowią wyzwanie do poszukiwania konkurencyjnych ekotechnologii. Fotowoltaika ma szansę stać się ważnym źródłem energii w 21 wieku na całym świecie. Systemy fotowoltaiczne (PV) dostarczają energii elektrycznej w wyniku konwersji energii promieniowania słonecznego i przewiduje się, że wniosą one znaczący wkład w systemy energetyczne dzięki stałemu postępowi technologicznemu w tej dziedzinie i znaczącej...
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The application of polypropylene membranes for production of fresh water from brines by membrane distillation
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Synthesis and ionophoric properties of functionalized p-tert-butyl-calix[4]arenes
PublikacjaProjektowanie struktury związków o właściwościach jonoforowych stanowi ważny element chemii supramolekularnej. W pracy przedstawiono wyniki badań nad funkcjonalizacją makrocyklicznych kaliks[4]arenów prowadzacą do nowych związków o zróżnicowanych właściwościach kompleksujących. Syntezowane przez nas jonofory badane były w membranowych elektrodach jonoselektywnych. Wyznaczono potencjometryczne współczynniki selektywności oraz stałe...
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Mires and Peat
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Berry fruit juices protect lymphocytes against DNA damage and ROS formation induced with heterocyclic aromatic amine PhIP
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e-Minds: International Journal on Human-Computer Interaction
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LFE-Revista de Lenguas para Fines Especificos
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A new approach to cross-bonding in medium voltage cable lines
PublikacjaThe medium voltage underground cable sheaths are usually bonded and earthed in every substation on the cable route. This results in additional power losses in the sheaths. The paper presents an idea of reducing power losses caused by sheaths cross-bonding. The idea of sheaths cross-connecting only in selected MV/LV substations is given instead of a typical solution, where sheaths cross-bonding requires installing additional joints...
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Molecular targets for antifungals in amino acid and protein biosynthetic pathways
PublikacjaFungi cause death of over 1.5 million people every year, while cutaneous mycoses are among the most common infections in the world. Mycoses vary greatly in severity, there are long-term skin (ringworm), nail or hair infections (tinea capitis), recurrent like vaginal candidiasis or severe, life-threatening systemic, multiorgan infections. In the last few years, increasing importance is attached to the health and economic problems...
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The Reactivity of the Imine Bond within Polynuclear Nickel(II) Complexes
PublikacjaThree novel Ni complexes with the Schiff base ligand 2-methoxy-6-(E-2-pyridyliminomethyl)-phenol (L1) are described. In comparison with the similar 2-(pyridine-2-ylimino-methyl)phenol (pymp), the mode of coordination of L1 is altered due to the presence of methoxy substituent introducing the sterical hindrance. During the synthesis of the complexes, partial hydrolysis of the ligand was observed. Since such immediate hydrolysis...
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Symmetrical and unsymmetrical diphosphanes with diversified alkyl, aryl and amino substituents
PublikacjaWe present the comprehensive study of diphosphanes with diversified substituents regarding their syntheses, structures, and properties. To this end, we have synthesized a series of novel unsymmetrical alkyl, aryl and amino-substituted diphosphanes of the general formula R1R2P-PR3R4 (where R1, R2, R3, R4 = tBu, Ph, Et2N or iPr2N) via salt metathesis reactionof halophosphanes with metal phosphides in high yield. We vastly expanded...
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Simulation of Signal Propagation Along Fractional-Order Transmission Lines
PublikacjaIn this paper, the simulation method of signal propagation along fractional-order (FO) transmission lines is presented. Initially, fractional calculus and the model of FO transmission line are introduced. Then, the algorithm allowing for simulation of the nonmonochromatic wave propagation along FO transmission lines is presented. It employs computations in the frequency domain, i.e., an analytical excitation is transformed to the...
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Investigation of hyperfine structure of several major lines in PbI and PbII
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Synthesis and biological activity of mycophenolic acid-amino acid derivatives
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The Relationship between the Structure and Properties of Amino Acid Ionic Liquids
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Atropoisomerism in Mono- and Diaryl-Substituted 4-Amino-2,6-lutidines
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Investigation of multilayer three-strip coplanar lines with the ferrite material
PublikacjaW artykule opisano wyniki badań przeprowadzonych nad wielowarstwową linią koplanarną zawierającą trzy paski umieszczone na podłużnie magnesowanym ferrycie. Analiza opiera się o metodę rodzajów sprzężonych. Uzyskane rezultaty zostały zweryfikowane eksperymentalnie.
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α-Amino Acids In Water: A Review Of VCD And ROA Spectra
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Nonreciprocal components using junction of a ferrite coupled microstrip lines
PublikacjaW oparciu o wyniki modelowania numerycznego zbadano efekty niewzajemne występujące w złączach ferrytowych linii sprzężonych. Opracowano metodyki projektowania złączy w technice linii mikropaskowej dla realizacji ferrytowych układów niewzajemnych. Przeprowadzono symulację parametrów transmisyjnych szeregu układów niewzajemnych wykonanych techniką zintegrowaną.
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Calix[4]arene phosphonates - recognition of amino alcohols in water.
PublikacjaOpracowano syntezę nowych rozpuszczalnych w wodzie pochodnych kaliks[4]arenów posiadających grupy fosfonowe w górnej części pierścieni aromatycznych. Zaprezentowano wyniki kompleksowania tych gospodarzy aminoalkoholi takich jak efedryna, norefedryna i noradrenalina.
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Projekt und Realisierung eines groBen Stahlbehalters fur Erdol.
PublikacjaOmówiono projekt i budowę zbiornika stalowego o pojemności 75 000 m3. Zbiornik jest dwupłaszczowy i ma podwójne dno w celu zabezpieczenia środowiska naturalnego przed skażeniem awaryjnym wyciekami ropy naftowej. Zwrócono uwagę na nowatorskie rozwiązania konstrukcyjne.
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Testing of performance properties of asphalt mixes for thin wearing courses.
PublikacjaPrzedstawiono wyniki badań następujących cech mieszanek mineralno asfaltowych: odporność na starzenie, oddziaływanie wody i mrozu, koleinowanie i oddziaływanie niskich temperatur. W badaniach zastosowano 2 typy mieszanek: beton asfaltowy o nieciągłym uziarnieniu i mastyks grysowy SMA. Wykorzystano 4 rodzaje asfaltów: 1 niemodyfikowany i 3 modyfikowane polimerami. Stwierdzono że wszystkie mieszanki są porównywalnie odporne na starzenie,...
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Immunosuppressive properties of amino acid and peptide derivatives of mycophenolic acid
PublikacjaMycophenolic acid (MPA) was coupled with amino acids and biologically active peptides including derivatives of tuftsin to modify its immunosuppressive properties. Both amino acid unit in the case of simple MPA amides and modifications within peptide moiety of MPA - tuftsin conjugates influenced the observed activity. Antiproliferative potential of the obtained conjugates was investigated in vitro and MPA amides with threonine methyl...
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Cross-Bonding of MV Cable Lines for Energy Losses Decrease
PublikacjaCurrently, almost all medium voltage cable lines (MV) operate with the return wires earthed at both ends of the cable. Such a way of operation causes that during normal states of operation as well as during disturbances, e.g. short-circuits, in the return wires induce currents whose values mainly depend on the currents flowing in the phase wires. These currents in normal operating states are a source of additional energy losses...
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Photoresponsive, amide-based derivative of embonic acid for anion recognition
PublikacjaThe synthesis and ion-binding properties of amide-based derivative of embonic acid andp-aminoazobenzenewere described. The new compound was characterized by X-ray structural analysis and spectroscopic methods.Ligand interacts in acetonitrile with Y-shaped anions (benzoates and acetates) and dihydrogen phosphatesforming complexes of 1:1 stoichiometry. In more polar DMSO the complexes stoichiometry changes to 2:1(L:anion). Light-inducedtranstocisisomerization...
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Practical application of in motion charging: Trolleybuses service on bus lines
PublikacjaNight charging and fast charging are currently the two most common systems for charging electric buses. Despite the fact that numerous trial installations were started, neither of these two systems has obtained unqualified approval of the users. The alternative is to charge vehicles in motion (the so-called In Motion Charging), which combines the advantages of trolleybus transport and of electric buses: the main supply source are...
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Classification of Polish wines by application of ultra-fast gas chromatography
PublikacjaThe potential of ultra-fast gas chromatography (GC) combined with chemometric analysis for classification of wine originating from Poland according to the variety of grape used for production was investigated. A total of 44 Polish wine samples differing in the type of grape (and grape growth region) used for the production as well as parameters of the fermentation process, alcohol content, sweetness, and others which characterize...
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Isotope shifts of multipole lines of Pb I and Pb II
PublikacjaStudies of isotope shifts of three multipole lines between levels of the ground configuration 6s26p2 of Pb I, i.e.: 461.9 nm(1S0→3P1), 531.5 nm(1S0→3P2) and 733.2 nm(1D2→3P1), as well as 710.2 nm line (6s26p2P3∕2→6s26p2P1∕2) of Pb II are presented. We determined the isotope shifts between four stable isotopes: 204, 206, 207, 208. By the use of King plot analysis we were able to separate the mass and the field shifts. We found that...
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The Issues of Reactive Power Compensation in High-voltage Transmission Lines
PublikacjaThis paper discusses the selection of compensation shunt reactors for a double-circuit 400 kV transmission line using the example of the newly built Elk Bis – Alytus transmission line. The analysis takes into account various conditions of the power system. The published results relate to voltage levels in steady states and during switching processes and short circuits.
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Hydration of amino acids: FTIR spectra and molecular dynamics studies
PublikacjaThe hydration of selected amino acids, alanine, glycine, proline, valine, isoleucine and phenylalanine, has been studied in aqueous solutions by means of FTIR spectra of HDO isotopically diluted in H2O. The difference spectra procedure and the chemometric method have been applied to remove the contribution of bulk water and thus to separate the spectra of solute-affected HDO. To support interpretation of obtained spectral results,...
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Nonreciprocal Devices Utilizing Longitudinally Magnetized Ferrite Coupled Lines
PublikacjaThis chapter presents authors’ recent research on the nonreciprocal devices utilizing longitudinally magnetized ferrite coupled line (FCL) junction. The principle of operation of FCL junction is explained and the hybrid techniques of analysis are shown. Numerical and experimental results concerning the nonreciprocal devices utilizing the different configurations of FCL junctions are presented and discussed.
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Synthesis and biological activity of mycophenolic acid-amino acid derivatives
PublikacjaIn search of new immunosuppressants, mycophenolic acid (MPA) was coupled with amino acid methyl esters followed by hydrolysis to analogs bearing free carboxylic groups. The obtained compunds were tested in vitro as growth inhibitors of lymphoid cell line (Jurkat) and human peripheral blood mononuclear cells (PBMC) from healthy donors. According to obtained results recovering of free carboxylic group increased their activity. Additionally,...
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Projects of noise level on railway lines
Dane BadawczeProjects of acoustic signals from railway lines for further analysis in the BK Connect program.
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projects of noise level on railway lines
Dane BadawczeProjects of acoustic signals from railway lines for further analysis in the BK Connect software.
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Mathematical model to assess energy consumption using water inflow-drainage system of iron-ore mines in terms of a stochastic process
PublikacjaPurpose is to develop a unified mathematical model to assess energy efficiency of a water inflow-drainage process as the real variant of stochastic method for water pumping from underground workings of iron-ore mines. Methods. The research process was based upon the methods of probability theory as well as stochastic modelling methods. The stochastic function integration has been reduced to summation of its ordinates and further...
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Fabrication of high-density nitrogen-vacancy (NV) center-enriched diamond particles through methyl trityl amine (C20H19N) seeding
PublikacjaDiamond particles (DPs) show promise for advanced applications in bioimaging and quantum sensing due to the presence of defect centers. This work reports a unique growth process for diamond particles composed of nitrogen-vacancy centers (NV-DPs) using a methyl trityl amine (C20H19N) diamondoid seed, which acts as a nitrogen source for NV creation. Growth was performed via microwave plasma-assisted chemical vapor deposition in a...
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A Reaction of Thioamides with Zinc Ammoniates Leading to Simple Amidines. Discovery of a New Zwitterionic Monomethylamidine
PublikacjaThe reaction of thioamides with the R1R2N-ZnCl ammoniates leads to N-mono-, N,N'-di-, N,N-disubstituted, and unsubstituted amidines with high concns. of amines in abs. ethanol. The efficient direct formation of the N,N'-dimethylamidine can be explained by a greater reactivity of methylamine compared with dimethylamine. Discovery of a new zwitterion (induced by a carbonyl oxygen) suggests that the stabilization in the thymine...
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Ammine(2-ethylpyridine-κN)bis(tri-tert-butoxysilanethiolato-κS)cobalt(II)
PublikacjaTytułowy związek [Co(C12H27O3SSi)2(C7H9N)(NH3)] został otrzymany w reakcji dimerycznego amoniakalnego tri-tert-butoksysilanotiolanu kobaltu(II) z 2-etylopirydyną. Atom kobaltu w otrzymanym związku jest koordynowany przez dwa atomy siarki, jedną resztę 2-etylopirydyny i jedną cząsteczkę amoniaku. Dzięki specyficznemu przestrzennemu ustawieniu ligandów, dodatkowo tworzy się wiązanie wodorowe wewnątrz cząsteczkowe N-H - S
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Calix[4]Arenes Appended with Thioamide Moieties as Powerful Tool for Heavy Metals Recognition
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Calix[4]arenes appended with thioamide moieties as powerful tool for heavy metals recognition
PublikacjaSelectivity of new thioamide derivatives was assessed using those ligands as sensor materials in ion-selective membrane electrodes and tested towards Pb2+ - selectivity. The influence of the nature of the thioamide function (linear, branched or cyclic substituents) on their ionophoric properties was investigated. Electrodes based on cyclic thioamide moieties are promising analytical tools for monitoring Pb2+ concentration in natural...
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HYDRAULIC CONDUCTIVITY OF COAL MINE TAILINGS
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Acoustic Processor of the Mine Countermeasure Sonar
PublikacjaThis paper presents the concept of an acoustic processor of the mine countermeasure sonar. Developed at the Department of Marine Electronics Systems, Gdansk University of Technology, the acoustic processor is an element of the MG-89, an underwater acoustic station. The focus of the article is on the modules of the processor. They are responsible for sampling analogue signals and implementing the algorithms controlling the measurement...
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One-step formation of n-alkenyl-malonamides and n-alkenyl-thiomalonamides from carbamoyl meldrum's acids.
PublikacjaA one-pot synthesis for the preparation of N-alkenyl-malonamides and N-alkenyl-thiomalonamides was developed. 5-[Hydroxy/mercapto(aryl/alkylamino)methylene]-2,2-dimethyl-1,3-dioxane-4,6-dione act as a source of ketenes that react with the tautomeric form of alkyl-(2-phenyl-propylidene)-amines. A possible [2+2] or [4+2] cycloaddition product of ketene to imines was not observed.
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Hyperfine Structure Study of Several Lines of207Pb I – Part II
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