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Search results for: sample preparation techniques
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Thermal Instability of Gold Thin Films
PublicationThe disintegration of a continuous metallic thin film leads to the formation of isolated islands, which can be used for the preparation of plasmonic structures. The transformation mechanism is driven by a thermally accelerated diffusion that leads to the minimalization of surface free energy in the system. In this paper, we report the results of our study on the disintegration of gold thin film and the formation of nanoislands...
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Magnetic superhydrophobic melamine sponges for crude oil removal from water
PublicationThis paper proposes the preparation of a new sorbent material based on melamine sponges (MS) with superhydrophobic, superoleophilic, and magnetic properties. This study involved impregnating the surface of commercially available MS with eco-friendly deep eutectic solvents (DES) and Fe3O4 nanoparticles. The DES selection was based on the screening of 105 eutectic mixtures using COSMO-RS modeling. Other parameters affecting the efficiency...
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Regeneration of marine engine valves using laser surfacing
PublicationThis article presents an analysis of the applicability of laser surfacing of the exhaust valve face of a marine diesel engine using cobalt-based powder. After preparation by machining, the selected valves were subjected to laser surfacing using a high-power ROFIN DL020 laser. The EuTroLoy 16012 powder was used in the surfacing process. One of the valves was cut and subjected to metallographic examination and hardness measurements,...
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Progress, Challenge, and Perspective of Bimetallic TiO2-Based Photocatalysts
PublicationBimetallic TiO2-based photocatalysts have attracted considerable attention in recent years as a class of highly active catalysts and photocatalysts under both UV and Vis light irradiation. Bimetallic noble metal structures deposited on TiO2 possess the ability to absorb visible light, in a wide wavelength range (broad LSPR peak), and therefore reveal the highest level of activity as a result of utilization of a large amount of...
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Steroid Sulfatase Inhibitors Based on Phosphate and Thiophosphate Flavone Analogs
PublicationA series of phosphate and thiophosphate flavone derivatives were synthesized and biologically evaluated in vitro for inhibition of steroid sulfatase (STS) activity. The described synthesis includes the straightforward preparation of 7-hydroxy-2-phenyl-4H-chromen-4-one 3a, 2-(4-fluorophenyl)-7-hydroxy-4H-chromen-4-one 3b, 7-hydroxy-2-(4-(trifluoromethyl)phenyl)-4H-chromen-4-one 3c, 7-hydroxy-2-(p-tolyl)-4H-chromen-4-one 3d modified...
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Temperature influence on tire/road noise evaluated by the drum method
PublicationAmbient air and road surface temperatures substantially affect the road vehicle noise emission. The temperature influence on tire/road noise depends mainly on tire-road combination. It is different for dense and porous pavements, for bituminous and cement ones. It differs also depending on tires. The correction procedures for temperature effect are still under consideration and preparation. Laboratory experiment was prepared to...
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Engineering Au nanoparticle arrays on SiO2 glass by pulsed UV laser irradiation
PublicationWe study semi-regular arrays of Au nanoparticles (NP) obtained via UV laser irradiation of thin Au films on glass substrate. The NP structures are prepared from films of a thickness up to 60 nm produced by discharge sputtering or pulsed laser deposition, and annealed by nanosecond laser pulses at 266 or 308 nm, respectively, at fluencies in the range of 60-410 mJ/cm2. For the rare- and close-packed NP structures, consistent description...
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Biosynthetic and synthetic access to amino sugars.
PublicationAmino sugars are important constituents of a number of biomacromolecules and products of mi crobial secondary metabolism, including antibiotics. For most of them, the amino group is located at the positions C1, C2 or C3 of the hexose or pentose ring. In biological systems, amino sugars are formed due to the catalytic activity of specific aminotransferases or amidotransferases by introducing an amino functionality derived from L-glutamate...
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Analysis of ultimate compressive strength of cracked plates with the use of DOE techniques
PublicationThe objective of this work is to investigate the structural compressive response of plates with locked cracks accounting for all relevant factors and correlation between them. The nonlinear FE model considering both geometric and material nonlinearities is employed herein, and the FE model of the structural response of intact plates is validated with the available experimental data. In the common studies, based on One Factor at...
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Failure characterisation of sandwich beams using integrated acoustic emission and digital image correlation techniques
PublicationThe paper presents the experimental study of the failure behaviour of sandwich beams subjected to bending. The samples examined are sandwich beams made of polyethylene terephthalate foam core and glass fibre-reinforced polymer laminate face sheets. In a series of experiments, it has been proposed to integrate diagnostic techniques with acoustic emission and digital image correlation to accurately track the cracking process on the...
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The use of selected analytical techniques for pollutants determination in the environmental samples collected from the Arctic regions
PublicationThe paper concern importance of the use of analytical techniques for pollutants determination in the Arctic based on the example of total organic carbon, phenolsandformaldehyde determinationandmeasurementofpHand electrical conductivity parameters in surfacewater samples collected fromthe Revelva catchment.
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Determination of odour concentration by TD-GC×GC–TOF-MS and field olfactometry techniques
PublicationField olfactometry is one of the sensory techniques used to determine odour concentration, in atmospheric air, directly in emission sources. A two-dimensional gas chromatography with time of flight mass spectrometer (GC×GC–TOF-MS) allows performing the chemical characterization of various groups of chemical compounds, even in complex mixtures. Application of these techniques enabled determination of odour concentration level in...
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Preparation and characterization of Pt–N/TiO2 photocatalysts and their efficiency in degradation of recalcitrant chemicals
PublicationSeries of Pt–N/TiO2 photocatalysts were synthesized using the sol–gel method. The photocatalysts’ characteristics by X-ray diffractometry (XRD), scanning transmission electron microscopy (STEM), diffuse reflectance spectroscopy (DRS), X-ray photoelectron spectroscopy (XPS) showed that sample with the molar ratio Ti:N equal 1:4 and platinum nanoparticles size of about 3 nm had anatase structure, about 94 m2/g specific surface area...
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Investigation of optical properties of Infitec and Active Stereo stereoscopic techniques for CAVE-type virtual reality systems
PublicationIn recent years, many scientific and industrial centres in the world developed virtual reality systems or laboratories. At present, among the most advanced virtual reality systems are CAVE-type (Cave Automatic Virtual Environment) installations. Such systems usually consist of four, five, or six projection screens arranged in the form of a closed or hemi-closed space. The basic task of such systems is to ensure the effect of user...
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High-Power Jamming Attack Mitigation Techniques in Spectrally-Spatially Flexible Optical Networks
PublicationThis work presents efficient connection provisioning techniques mitigating high-power jamming attacks in spectrally-spatially flexible optical networks (SS-FONs) utilizing multicore fibers. High-power jamming attacks are modeled based on their impact on the lightpaths’ quality of transmission (QoT) through inter-core crosstalk. Based on a desired threshold on a lightpath’s QoT, the modulation format used, the length of the path,...
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Preparation and characterization of biopolymeric films with magnetic properties
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Heteropolyanions doped polyimine—Preparation and spectroscopic properties
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Preparation of samples for analysis: the key to analytical success
PublicationW rozdziale przedstawiono informacje literaturowe o nowych rozwiązaniach metodycznych w zakresie:-izolacji i/lub wzbogacania śladowych składników z próbek środowiskowych-mineralizacji próbek.Szczególna uwagę zwrócono na wykorzystanie w procesie przygotowania próbek nowych typów rozpuszczalników i mediów reakcyjnych spełniających wymogi związane z koncepcją zrównoważonego rozwoju.
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Preparation of silver nanoparticles with controlled particle size
PublicationNanocząstki srebra wykazują zdolność absorpcji promieniowania widzialnego, która jest efektem istnienia powierzchniowego plazmonu. W zależności od kształtu i wielkości cząstek obserwuje się różną barwę koloidów srebra. W wyniku przeprowadzonych badań otrzymano nanocząstki srebra metodą chemicznej redukcji. Zaobserwowano wpływ rodzaju reduktora (kwas askorbinowy, borowodorek sodu), stabilizatora (PVP, PVA) oraz prekursora srebra...
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A new preparation method of catalyst for ammonia synthesis
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Preparation of colloidal silver in W/O microemulsion
PublicationStabilne koloidy srebra otrzymano poprzez redukcję azotanu srebra w mikroemulsji dodekan-woda-AOT. Otrzymane zawiesiny nanocząstek srebra w dodekanie wykazywały stabilność w czasie, tj. nie zmieniały właściwości przez kilka miesięcy. Stwierdzono, że stabilność otrzymanych roztworów koloidalnych nie zależy od stężenia srebra w zakresie od 60 do 1000 mg/dm3, natomiast silnie zależy od stężenia surfaktanta. Niska toksyczność dodekanu,...
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A new and convenient method for the preparation of functionalized phosphorothioates
PublicationA new and efficient method for the synthesis of alkyl and aryl phosphorothioates in high yields via the reaction of (5,5-dimethyl-2-thioxo-1,3,2-dioxaphosphorin-2-yl)disulfanyl derivatives with trimethyl phosphite was developed.
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Preparation of samples of plant material for chromatographic analysis
PublicationPrzedstawiono informacje literaturowe nt. etapów przygotowania próbek materiału roślinnego do analizy chromatograficznej. Szczególną uwagę zwrócono na techniki izolacji i/lub wzbogacenie analitów przed etapem oznaczeń końcowych, walidację stosowanych procedur, sposoby pobierania próbek celem określenia emisji biogenicznej lotnych związków organicznych.
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Preparation and application of lecithin formulation in liquid detergents
PublicationBadano solubilizację odolejonej lecytyny rzepakowej w wodnych roztworach surfaktantów anionowych, kationowych i niejonowych. Najlepszymi solubilizatorami okazały się surfaktanty anionowe (dodecylosiarczan sodu i sól sodowa oksyetylenowanego siarczanowanego alkoholu tłuszczowego). Otrzymano jednorodne preparaty lecytynowe o zawartości lecytyny do 30% i zawartości surfaktantów anionowych do 20%. Preparat lecytyny i Sulforokanolu...
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LC-MS and LC-NMR as Complementary Techniques for the Determination of Pharmaceuticals in Dosage Formulations
PublicationPharmaceuticals contain not only pharmacologically active compounds but also a range of excipients. The danger exists that impurities may also be present in such drugs, which may adversely affect their efficacy and even endanger patient health and life. Monitoring the composition of pharmaceutical products is therefore essential. The trace amounts of such impurities in pharmaceuticals are often identified and determined with liquid...
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Vietnamese version of the Dual Filial Piety Scale: preliminary validation in a student sample
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Gain Correction for Nearly Optimal Variable Fractional Sample Delay Filter Design
PublicationJedną z najbardziej efektywną numerycznie metodą projektowania filtrów jest metoda okien. Sprawia to, że takie podejście bardzo dobrze nadaje się do implementacji filtrów ułamkowoopóźniających o zmiennym opóźnieniu, gdzie wymagana jest częsta aktualizacja współczynników takiego filtru. Z drugiej strony, jeżeli wymagane są filtry wysokiej jakości wybór okna jest najczęściej problematyczny. Z tego powodu w pracy rozpatrzono użycie...
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Comparative Analysis of Numerical and Experimental Studies of the Airflow Around the Sample of Urban Development
PublicationIn this paper, on the background of a short overview of the recent advances in the field of Environmental Wind Engineering (EWE), a comparison of wind tunnel experiment and numerical simulation for some cases of airflow around an urban layout have been reported. The purpose of the study is quantitative and qualitative comparison of measurements in the wind tunnel as well as numerical simulation using Ansys Fluent software. The...
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Influence of sample thickness non-uniformities on the modulated photocur-rents in amorphous solids
PublicationOtrzymano przybliżone wzory opisujące modulowane fotoprądy dla przypadków próbki kanapkowej o nierównomiernej grubości, reprezentowanej przez układ równolegle połączonych próbek o różnych grubościach. Na ich podstawie obliczono przebieg fotoprądów dla przypadku jednorodnego i gaussowskiego rozkładu grubości próbki oraz dla wykładniczego rozkładu pułapek.
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Photocatalytic decolourization of Rhodamine-B dye by visible light active ZIF-8/BiFeO3 composite
PublicationIn this work, preparation of ZIF-8 supported BiFeO3 photocatalyst by ultrasound cavitation technique was reported. The synthesized materials were characterized using solid UV absorption spectroscopy, Raman Spectroscopy, and SEM. The catalytic function of synthesized photocatalyst under ultraviolet and visible light was examined for the decolourization of Rhodamine-B (Rh-B) dye. To understand the action of the photocatalyst on Rh-B...
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Silica Gel Impregnated by Deep Eutectic Solvents for Adsorptive Removal of BTEX from Gas Streams
PublicationThe paper presents the preparation of new adsorbents based on silica gel (SiO2) impregnated with deep eutectic solvents (DESs) to increase benzene, toluene, ethylbenzene, and p-xylene (BTEX) adsorption efficiency from gas streams. The DESs were synthesized by means of choline chloride, tetrapropylammonium bromide, levulinic acid, lactic acid, and phenol. The physico-chemical properties of new sorbent materials, including surface...
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The Physicochemical and Antibacterial Properties of Chitosan-Based Materials Modified with Phenolic Acids Irradiated by UVC Light
PublicationThis paper concerns the physicochemical properties of chitosan/phenolic acid thin films irradiated by ultraviolet radiation with wavelengths between 200 and 290 nm (UVC) light. We investigated the preparation and characterization of thin films based on chitosan (CTS) with tannic (TA), caffeic (CA) and ferulic acid (FA) addition as potential food‐packaging materials. Such materials were then exposed to the UVC light (254 nm) for...
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Self-compacting grout to produce two-stage concrete
PublicationTraditional concrete (TC) is primarily composed of a mixture of cement, fine and coarse aggregates, and water. TC is made by mixing together all the components before placing them. Using non-traditional concrete (two-stage concrete) to solve and to eliminate the problem of the aggregate segregation which appears in TC and in the self-compacting concrete. Two-stage concrete (TSC) consists of two main components, namely the grout...
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Photoelectrochemically Active N‐Adsorbing Ultrathin TiO2 Layers for Water‐Splitting Applications Prepared by Pyrolysis of Oleic Acid on Iron Oxide Nanoparticle Surfaces under Nitrogen Environment
PublicationHighly performing photocatalytic surfaces are nowadays highly desirable in energy fields, mainly due to their applicability as photo water‐splitting electrodes. One of the current challenges in this field is the production of highly controllable and efficient photoactive surfaces on many substrates. Atomic layer deposition has allowed the deposition of photoactive TiO2 layers over wide range of materials and surfaces. However,...
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Aggregation properties of some zirconium phosphate loaded with dirhenium(III) complexes
PublicationOne of the important areas of modern science is the selection of the right forms of drug delivery. Layered inorganic nanoparticles, such as zirconium phosphate, have proven themselves well in this area. The study of the properties of these systems and methods of their preparation makes it possible to determine a rational technology of their manufacture, storage conditions as well as suggest a possible mechanism of therapeutic action....
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Comparison of traditional district heating with low temperature district heating systems featuring organic Rankine cycle and heat pump
PublicationPaper presents a comparison between a traditional district heating system with conventional boilers as a source of heat and electricity purchases from power utilities and a low temperature DH system incorporating the CHP with organic Rankine Cycle providing electricity and local heat pump raising the temperature of the DH fluid to the required temperature in the dwelling, meaning that both heat and electricity are produced within...
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Manufacture and research of TPS/PE biocomposites properties
PublicationIn this paper the process of native starch preparing for modification by extrusion and manufacture of biocomposites is presented. The first aim of this study was to determine the mixing and granulating condition of native starch to obtain granulated native starch. For mixing and granulation of native starch Intensive Mixer manufactured by Maschinenfabrik Gustav Eirich was used. Mixing and granulation in a single process is a new...
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An investigation of selected monoaromatic hydrocarbons released from the surface of polystyrene lids used in coffee-to-go cups
PublicationA consumer trend towards the fast preparation of beverages has increased the popularity of hot beverages (especially coffee and tea) available in disposable containers called coffee-to-go cups with fitted polystyrene lids. Lids in contact with hot beverages may release low molecular weight organic compounds into the gaseous phase causing direct exposure of consumers to these compounds during drinking. The paper describes in detail...
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Synthesis and biological evaluation of thiophosphate tricyclic coumarin derivatives as steroid sulfatase inhibitors
PublicationSteroid sulfatase (STS) enzyme inhibition is an important approach to the management of hormone-dependent breast cancer. In this paper, we report convenient methods for the synthesis and biological evaluation of thiophosphate tricyclic coumarin analogs exhibiting STS activity. The described methods are based on the straightforward preparation of 7-hydroxy-2,3-dihydro-1H-cyclopenta[c]chromen-2-one, 3-hydroxy- 7,8,9,10-tetrahydro-6H-benzo[c]chromen-6-one,...
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ROSANNE Project: New Procedure for Noise Characterisation of Road Surfaces in Europe
PublicationROSANNE is a collaborative project in the 7th EU Framework Programme which aims at harmonising measurement methods for skid resistance, noise emission and rolling resistance of road pavements as a preparation for standardization. The project started in November 2013 and is developing and improving standards in the field of working group CEN/TC 227/WG 5. Regarding the influence of the pavement on the road traffic noise emission,...
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Structural and spectroscopic investigation of new luminescent hybrid materials based on calix[4]arene-tetracarboxylate and Ln 3+ ions (Ln = Gd, Tb or Eu)
PublicationLanthanide-calixarene hybrid materials are of particular interest due to the combination of the interesting properties of the ligand cavity-like structure and the luminescent features of lanthanides. The aim of this study was to synthesize and investigate the photophysical properties of Eu3+, Tb3+ and Gd3+ hybrids based on calix[4]arene-tetracarboxylate. The preparation of two structurally different...
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POLISH PUBLISHERS OPEN ACCESS POLICIES DATABASE - FUNCTIONALITIES AND ROLE IN THE IMPLEMENTATION OF OPENNESS POLICIES
PublicationThe aim of the article is to present a base of Polish Publishers Open Access Policies as a tool supporting the scientific community in the implementation of openness policies. It is the first national platform to gather and analyze a publishing policy in the field of Open Access to Polish scientific journals. For scientists, it is a tool for searching for a Polish journal meeting certain criteria. It enables grant recipients to...
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Preparation, characterization and photocatalytic activity of TiO2 microspheres decorated by bimetallic nanoparticles
PublicationComposite photocatalysts that consist of TiO2and noble metal nanostructures have been considered tobe the promising and pivotal material for accessible enhancement of the efficiency in the photocatalyticprocess carried out in the aqueous and gas phases. In this work we fabricated porous TiO2microspheresthrough a hydrothermal process followed by photochemical reduction of noble metal nanoparticles atthe TiO2surface. The morphology...
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Miniaturized Solid Phase Extraction techniques for different kind of pollutants analysis: State of the art and future perspectives – PART 1
PublicationSolid Phase Extraction (SPE) has been practiced in a modern form for more than half a century. It was constantly developing, driven by the analysts needs. These needs are coming from the importance to select an appropriate analytical method, which should have satisfactory accuracy, precision and sensitivity. In the case of sorbent-based microextraction techniques, the choice of miniaturized variants that meet these requirements...
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Multiuser Stereoscopic Projection Techniques for CAVE-Type Virtual Reality Systems
PublicationDespite the development of increasingly popular head mounted displays, CAVE-type systems may still be considered one of the most immersive virtual reality systems with many advantages. However, a serious limitation of most CAVE-type systems is the generation of a three-dimensional (3-D) image from the perspective of only one person. This problem is significant because in some applications, the participants must cooperate with each...
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Verification of GNSS Measurements of the Railway Track Using Standard Techniques for Determining Coordinates
PublicationThe problem of the reproduction of the railway geometric layout in the global spatial system is currently solved in the form of measurements that use geodetic railway networks and also, in recent years, efficient methods of mobile positioning (mainly satellite and inert). The team of authors from the Gdańsk University of Technology and the Maritime University in Gdynia as part of the research project InnoSatTrack is looking for...
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A Case Study on Implementing Agile Techniques and Practices: Rationale, Benefits, Barriers and Business Implications for Hardware Development
PublicationAgile methodologies, along with the corresponding tools and practices, are claimed to facilitate teams in managing their work more effectively and conducting their work more efficiently while fostering the highest quality product within the constraints of the budget. Therefore, the rate of awareness and adoption of Agile frameworks both within and outside the software industry has increased significantly. Yet, the latest studies...
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Sensor data fusion techniques for environment modelling
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Instrumental techniques used for assessment of food quality
PublicationW artykule scharakteryzowano dwie techniki instrumentalne stosowane w ocenie jakości produktów spożywczych, tj. chromatografię gazową w połączeniu z detekcją olfaktometryczną oraz nos elektroniczny. Opisano zasady działania obu technik oraz typowe procedury analityczne stosowane w ocenie zapachu. Ponadto, podano przykłady praktycznego zastosowania obu technik, włącznie z tymi, które wykorzystano w pracowni autorów.
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Computational Techniques Application in Environmental Exposure Assessment
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