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Evolution of Ag nanostructures created from thin films: UV–vis absorption and its theoretical predictions
PublikacjaAg-based plasmonic nanostructures were manufactured by thermal annealing of thin metallic films. Structure and morphology were studied using scanning electron microscopy (SEM), transmission electron microscopy (TEM), high-resolution transmission electron microscopy (HR-TEM) and X-ray photoelectron spectroscopy (XPS). SEM images show that the formation of nanostructures is influenced by the initial layer thickness as well as the...
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Obtaining and Characterization of the PLA/Chitosan Foams with Antimicrobial Properties Achieved by the Emulsification Combined with the Dissolution of Chitosan by CO2 Saturation
PublikacjaA new method of obtaining functional foam material has been proposed. The materials were created by mixing the poly lactic acid (PLA) solution in chloroform, chitosan (CS) dissolved in water saturated with CO2 and polyethylene glycol (PEG), and freeze-dried for removal of the solvents. The composite foams were characterized for their structural (SEM, FT-IR, density, porosity), thermal (DSC), functional (hardness, elasticity, swelling...
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Preparation and characterization of TiO2 nanostructures for catalytic CO2 photoconversion
PublikacjaThe titanium dioxide target (99.7%) of 1 cm in dia was ablated in vacuum by laser pulses(6 ns) at 266 nm and at repetition rate of 10 Hz. During deposition the laser fluence between 1 and 3.5 J/cm2 and the O2 pressure from the range of 10-2 - 1 Pa were applied. The thin TiO2 films were deposited on glass substrate (1 × 1 cm2) heated up to 500 °C. The chemical composition of the film and samples produced by annealing were investigated...
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Determination of polybrominated diphenyl ethers (PBDEs) in dust samples collected in air conditioning filters of different usage – method development
PublikacjaThis study presents the results of studies aimed at the development of an analytical procedure for separation, identification, and determination of PBDEs compounds in dust samples collected from automotive cabin air filters and samples collected from filters installed as part of the air purification system in academic facilities. Ultrasound-assisted dispersive solid phase extraction (UA-dSPE) was found to perform better in terms...
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Improved Performance of 1-Ethyl-3-Methylimidazolium Tetrafluoroborate at Steel/HCl Interface by Iodide Ions
PublikacjaThe corrosion and corrosion inhibition of St37 steel in 0.1 M HCl solution by 1-ethyl-3-methylimidazolium tetrafluoroborate (EMITFB) and the effect of addition of KI on the inhibitive performance of EMITFB have been examined by electrochemical [electrochemical impedance spectroscopy, potentiodynamic polarization, and dynamic electrochemical impedance spectroscopy (DEIS)] and surface examination [scanning electron microscope (SEM)...
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Application of headspace-solid phase microextraction followed by gas chromatography-mass spectrometry to determine short-chain alkane monocarboxylic acids in aqueous samples
PublikacjaCelem prowadzonych badań było opracowanie metodyki oznaczania krótkołańcuchowych kwasów alkanomonokarboksylowych (KKA), opartej na ich izolowaniu i wzbogacaniu za pomocą techniki HS-SPME, a następnie oznaczaniu za pomocą chromatografii gazowej sprzężonej ze spektrometrią mas (GC-MS). Do ekstrakcji zastosowano włókno pokryte polarną fazą stacjonarną opartą na glikolu polietylenowym (PEG). Dla celów porównawczych zastosowano również...
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Mikroekstrakcja z wykorzystaniem cieczy jonowych - przygotowanie próbek do chromatograficznego oznaczania krótkołańcuchowych kwasów karboksylowych
PublikacjaPolimerowe ciecze jonowe, ze względu na wyjątkowe właściwości chemiczne i fizyczne mogą znaleźć zastosowanie w wielu technikach analitycznych. Na szczególną uwagę zasługują techniki ekstrakcyjne ograniczające zużycie rozpuszczalników organicznych. Ze względu na możliwości sterowania właściwościami cieczy jonowych poprzez odpowiedni dobór kationu i anionu, można z powodzeniem stosować je jako selektywne pokrycia włókien do SPME,...
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Loop-mediated isothermal amplification (LAMP) as a diagnostic tool in detection of infectious diseases
PublikacjaLoop-mediated isothermal amplification (LAMP) is a gene amplification method which amplifies DNA with high specificity and efficiency under isothermal conditions. Because of its rapidity and simplicity, it is a valuable diagnostic tool in the early detection and identification of infectious diseases. LAMP method is based on the use of a set of four to six specially designed primers spanning six to eight distinct sequences on the...
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Epoxy Composites Filled with Natural Calcium Carbonate. 1. Epoxy Composites Obtained in the Presence of Monoperoxy Derivative of Epidian-6 Epoxy Resin
PublikacjaPhysico-mechanical properties of the products based on filled epoxy-oligomeric mixtures composed of Epidian-5 epoxy resin, oligoesteracrylate TGM-3 and monoperoxide derivative of Epidian-6 epoxy resin (PO) have been investigated. CaCO3 was used as a filler and polyethylene polyamine was a curing agent. The effect of PO and CaCO3 on the gel-fraction content and physico-mechanical properties was examined. Using a scanning electron...
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Synteza ustaleń ''Planu ochrony Zaborskiego Parku Krajobrazowego. W: [Pracazbiorowa] Materiały do monografii przyrodniczej regionu gdańskiego. Gdańsk: Marpress**2003 s. 217-240. Tom 9 Zaborski Park Krajobrazowy. Problemy trójochrony i współistnienia z Parkiem Narodowym ''Bory Tucholskie''. Zaborski Landscape Park. Problems of Landscape Park. Problems of the triprotection and coexistence with the ''Bo- ry Tucholskie'' National Park. Praca zbiorowa pod redakcją M. Przewoźniaka.
PublikacjaArtykuł przedstawia syntezę ustaleń ''Planu ochrony ZPK''wynikających ze spe-cjalistycznych operatów problemowych, jak: operat ochrony litosfery, hydro- logiczny, ochrony roślinności i fauny, sozologiczny, ochrony dziedzictwa kulturowego i krajobrazu oraz operat ochrony walorów rekreacyjnych i zago- spodarowania przestrzennego. Uwzględnione są też zasady rozwoju gospodarki oraz zadania badawcze, edukacyjne i monitorowania...
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Train the trainer course
PublikacjaThis chapter presents the concept, evaluation and evaluation results for the train the trainer. This concept of train the trainers is prepared within Workpackage 5 of EU-funded project: MASTER BSR (Erasmus+ Strategic Partnership Programme). Due to the nature of adult learning the content is designed for the use of participatory methods (involved, active). This method uses various techniques of active learning e.g. group work,...
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‘Green’ multi - residue methods for the determination of high importance currently used pesticides in environmental samples
PublikacjaThe purpose of the research has been to develop and apply ‘green’ analytical methodologies to control and monitor the level of currently used pesticides from different chemical groups in aqueous samples. For extraction of analytes solid - phase microextraction (SPME) and dispersive liquid - liquid microextraction (DLLME) have been applied and compared. For SPME, commonly used materials for coating fibers include: polydimethylsiloxane...
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Metoda opracowania uniwersalnej osnowy na bazie krzemionki do unieruchomienia cieczy jonowych jako materiałów sorpcyjnych w technice mikroekstrakcji do fazy stacjonarnej
PublikacjaRozprawa doktorska stanowi opis badań prowadzonych w trakcie czterech lat (2018-2022) studiów doktoranckich. Rezultaty prac badawczych zostały opublikowane w postaci pięciu oryginalnych artykułów, stanowiących podstawę tej rozprawy. Tematyka badań dotyczy wykorzystania cieczy jonowych w technice mikroekstrakcji do fazy stacjonarnej (ang. SPME). Głównym celem prowadzonych prac badawczych było: (a) otrzymanie nowej, porowatej sorpcyjnej...
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The effect of exogenous application of methyl jasmonate on the lipid and carbohydrate content and composition of winter triticale (Triticosecale Wittm.) grain and the severity of fungal infections in triticale plants and grain
PublikacjaKernels of winter triticale (Triticosecale Wittm. cv. Dinaro) were analyzed. In the autumn of 2015, the effect of methyl jasmonate (MJ) on the germination of triticale kernels and the development of triticale seedlings was analyzed in a laboratory before kernels were sown in experimental plots. Kernels harvested from plots in August 2016 were analyzed to determine their lipid and carbohydrate content and composition and the severity...
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Fabrication and structural properties of Y and Fe co-doped SrTiO3 nanoceramics for SOFC
PublikacjaYttria and iron co-doped strontium titanate perovskites, (Y0,07Sr0,93Ti1-xFexO3-δx=0,1; 0,2) samples were fabricated by two methods: solid-state synthesis (SS) and the Pechinisol-gel modified method. The morphology of samples were measured by SEM and X-raydiffraction. Results were compared and discussed. The strong relationship between fabricationprocedure and microstructure has been proven. It was also observed, that the nanoceramicsobtained...
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Liquid-solid interaction during formation of nanocomposite systems
PublikacjaW pracy zaprezentowano wyniki badań nad zmianami strukturalnymi w układach ciekłego Bi i małych cząsteczek Ni lub Cu w zakresie temperatur od 615 do 1145K. Zaobserwowano (SEM) mikrostruktury kompozytowe i przeanalizowano dla różnych temperaturach i różnych czasów mieszania. Strukturę układów Bi-Ni oraz Bi-Cu, zarówno w stanie stałym i ciekłym, zbadano za pomocą dyfrakcji rentgenowskich.
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Discrete random variables in reliability calculations of a reticulated shell
PublikacjaImplementation of the Point Estimation Method (PEM) in the reliability analysis of a three-dimensional truss structure is presented in the paper. The influence of geometric and material random parameters on the truss load-carrying capacity was investigated. The analysis was performed for different combinations of basic variables. Symmetric and asymmetric cases of snow load were taken to assess the structural reliability. Sensitivity...
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Review of hydrogen production technologies for automotive sector – thermodynamic analysis of energy and exergy losses
PublikacjaFew recent years has shown that hydrogen technology has a good chance to replace petroleum technology in automotive sector. However, hydrogen in pure form practically does not occur on Earth. That is why H2 form is used only as an energy carrier and it must be produced using another source of energy form water or hydrocarbon fuels. In this paper short overview of hydrogen production technology has been presented, with energy and...
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Massive Open Online Courses: strategies and research areas
PublikacjaThe latest education revolution, the massive open online courses (MOOCs), is gaining momentum, accolades, and participation across industry and academia. These learning laboratory behemoths host and assess tens to hundreds of thousands of students in a single class, for free. Similar to their scope, MOOCs’ short- and long-term educational implications seem massive. Immediate MOOC educational outcomes vary widely from roaring successes...
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Weather Hazard Avoidance in Modeling Safety of Motor-Driven Ship for Multicriteria Weather Routing
PublikacjaWeather routing methods find the most suitable ocean?s route for a vessel, taking into account changeable weather conditions and navigational constraints. In the multicriteria approach based on the evolutionary SPEA algorithm one is able to consider a few constrained criteria simultaneously. The approach applied for a ship with hybrid propulsions has already been presented by one of the authors on previous TransNav?2009. This time...
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The impact of China’s One-Belt One-Road initiative on international trade and global value chains
PublikacjaThis study examines the potential effects of China’s ‘One-Belt One-Road’initiative (OBOR) on trade flows and global value chain (GVC) connections.The empirical analysis is based on the augmented trade gravity model, which comprises 186 economies and 199 of their partners from 2000 to 2018. We also estimate the gravity model for involvement in GVC (domestic value added in intermediate exports, foreign value added in exports, and...
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The Synergistic Microbiological Effects of Industrial Produced Packaging Polyethylene Films Incorporated with Zinc Nanoparticles
PublikacjaZinc compounds in polyolefin films regulate the transmission of UV-VIS radiation, affect mechanical properties and antimicrobial activity. According to hypothesis, the use of zinc- containing masterbatches in polyethylene films (PE) with different chemical nature—hydrophilic zinc oxide (ZO) and hydrophobic zinc stearate (ZS)—can cause a synergistic effect, especially due to their antimicrobial properties. PE films obtained on an...
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High temperature oxidation of porous alloys for solid oxide fuel cell applications
PublikacjaW pracy proszki PI600, 317L i 430L stali użyto do przygotowania porowatych metalowych podłoży dla tlenkowych ogniw paliwowych. Po spiekaniu w różnych temperaturach oceniana była ich porowatość i wysokotemperaturową odporność na korozję. Cykliczna analiza termograwimetryczna, dyfraktometria rentgenowska i obrazów SEM były używane do opisu właściwości tych porowatych stopów. Właściwości elektryczne badano dla wybranych próbek. Wpływ...
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Evaluation of cavitation erosion-corrosion degradation of mild steel by means of Dynamic Impedance Spectroscopy in galvanostatic mode
PublikacjaPrzedstawiono wyniki badań degradacji stali węglowych na skutek oddziaływania erozji-korozji kawitacyjnej. Do analizy wykorzystano technikę Dynamicznej Elektrochemicznej Spektroskopii Impedancyjnej w trybie galwanostatycznym, bliżej odwzrorowującym warunki naturalne. Do oceny stopnia degradacji posłużyły również funkcja ubytku masy MDPR oraz obrazy mikroskopowe SEM. Potwierdzono wpływ łączonej degradacji erozyjno-korozyjnej na...
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Wpływ metody wytwarzania na właściwości laminatów poliestrowo/szklanych do budowy małych jednostek pływających
PublikacjaW pracy porównano pod względem mikrostruktury i wybranych wskaźników wytrzymałościowych jakość laminatów poliestowo/szklanych wytworzonych w zakładzie budowy dużych łodzi motorowych za pomocą metod: ręcznej, worka próżniowego i infuzji. Badano jakość struktury pod kątem udziału osnowy żywicznej i liczby pęcherzy za pomocą SEM i analizy obrazu. Porównano własności mechaniczne na podstawie prób: trzypunktowego zginania, ścinania...
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Improvement of electrochemical action of zinc-rich paints by addition of nanoparticulate zinc
PublikacjaThe influence of nanosized particles on electrochemical action of standard zinc-rich paints by means of SEM as well as potential and impedance measurements has been investigated. The motivation for doing this was to obtain additional electrical connection between the spherical microparticles themselves and zinc particles and steel substrate. Overall zinc content was at the level of 92% by weight. Samples with different concentration...
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Electrical conductivity and relaxation processes in V2O5 nanorods prepared by sol–gel method
PublikacjaProperties of high purity V2O5 nanorods prepared by a sol – gel method are presented. The studied materials were characterized by: X-ray diffractometry (XRD), scanning electron microscopy (SEM), and X-ray photoelectron spectroscopy (XPS). The electrical impedance was measured as a function of temperature and frequency. The obtained results show that the electrical conductivity increases with increasing temperature. The d.c. conductivity...
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Instantaneous impedance monitoring of AA 7075 aluminum alloy corrosion in borate buffer with admixed chloride ions
PublikacjaThe study presents a research capabilities of Dynamic Electrochemical Impedance Spectroscopy (DEIS) as a tool used for instantaneous on-line monitoring of corrosion processes on the example of AA 7075 aluminum alloy. A borate buffer with admixed chloride ions in a quantity ranging from 0.05 to 25 mM was used to represent different types of corrosion attack. The surface of samples specimens was evaluated before and after the tests...
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Nowe techniki instrumentalne na tle tradycyjnych metod analizy stabilności oksydatywnej olejów roślinnych
PublikacjaObiecującą metodą oznaczania stabilnosci oksydatywnej olejów roślinnych może okazać się technika mikroekstrakcji do fazy stacjonarnej połączona z techniką chromatografii gazowej (SPME/GC) z detektorem płomieniowo-jonizacyjnym (FID) lub spektrometrii mas (MS). Przy pomocy wspomnianej metody, na podstawie zależności stosunku stężeń heksanalu do 2-trans-nonenalu w funkcji czasu naświetlania promieniowaniem ultrafioletowym, wyznaczono...
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Performance of a single layer fuel cell based on a mixed proton-electron conducting composite
PublikacjaMany of the challenges in solid oxide fuel cell technology stem from chemical and mechanical incompatibilities between the anode, cathode and electrolyte materials. Numerous attempts have been made to identify compatible materials. Here, these challenges are circumvented by the introduction of a working single layer fuel cell, fabricated from a composite of proton conducting BaCe0.6Zr0.2Y0.2O3-δ and a mixture of semiconducting...
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Limitations of Emotion Recognition in Software User Experience Evaluation Context
PublikacjaThis paper concerns how an affective-behavioural- cognitive approach applies to the evaluation of the software user experience. Although it may seem that affect recognition solutions are accurate in determining the user experience, there are several challenges in practice. This paper aims to explore the limitations of the automatic affect recognition applied in the usability context as well as...
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The Impact of EU Funds on the Development of Business Environment Institutions – Research Results in Pomeranian Voivodeship in Poland
PublikacjaThe paper presents the main findings of the research conducted to assess the impact of EU funds on development of business environment infrastructure in Pomeranian Voivodeship in Poland, and – indirectly – on the growth of the innovation capacity of Pomeranian entrepreneurs. The research shows that support of ROP PV 2007-2013 contributed to the creation of multifunctional business infrastructure throughout the Pomorskie Voivodship,...
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Source-related Wavefields in Fluids and Dielectrics: A new way of Thinking about Medium Dynamics
PublikacjaAcoustic and electromagnetic wave phenomena may seem to have a proper formal representation in field theory dating from the 19th century, founded on the mathematics of complex functions. This paper shows, however, that when replacing the classical spectrum-domain approach related to the assumption of harmonic timeform of signals, with a time-domain approach imposingnorestrictionastotheclassoftimeevolutionofsourceandfieldsignals,...
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Insight into the microstructural and durability characteristics of 3D printed concrete: Cast versus printed specimens
PublikacjaThis study presents the comparison of microstructural and durability characteristics of 3D printed concrete (3DPC) depending on its production method (printing or casting). Printed samples with different numbers of layers, as well as a cast specimen with an identical mix composition, were produced and compared, with their microstructural pore and solid characteristics quantitatively and qualitatively investigated. For this purpose,...
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Autogenous Fiber Laser Welding of 316L Austenitic and 2304 Lean Duplex Stainless Steels
PublikacjaThis study presents results of experimental tests on quality of dissimilar welded joints between 316L austenitic and 2304 lean duplex stainless steels, welded without ceramic backing. Fiber laser welded butt joints at a thickness of 8 mm were subjected to non‐destructive testing (visual and penetrant), destructive testing (static tensile test, bending test, and microhardness measurements) and structure observations (macro‐ and...
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Rapid method for the determination of organochlorine pesticides and PCBs in fish muscle samples by microwave-assisted extraction and analysis of extracts by GC-ECD
PublikacjaA procedure for the multiresidue determination of organochlorine pesticides and polychlorinated biphenyls in fish muscle samples has been developed. The method is based on the microwave-assisted extraction (MAE) of food samples from an acetonitrile-water (95 + 5, v/v) mixture followed by SPE cleanup of the extracts and analysis by GC with an electron capture detector. MAE operational parameters, such as the extraction solvent,...
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Wykorzystanie techniki chromatografii jonowej w analityce surfaktantów w próbkach wód powierzchniowych
PublikacjaSurfaktanty stanowią grupę związków charakteryzujących się specyficznymi właściwościami fizykochemicznymi i z tego względu są one wykorzystywane w wielu sferach działalności człowieka. Związki powierzchniowo-czynne ulegają różnorodnym przemianom fizykochemicznym, co umożliwia ich migrację między różnymi elementami środowiska i może prowadzić do jego zanieczyszczenia. Dlatego też istnieje konieczność określania losu środowiskowego...
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Solar light driven degradation of textile dye contaminants for wastewater treatment – studies of novel polycationic selenide photocatalyst and process optimization by response surface methodology desirability factor
PublikacjaThe unplanned anthropogenic activities and raced industrial revolution detrimentally causes serious threat to terrestrial and aquatic life. A high discharge of wastewater from industries using dyes affects living organisms and the environment. This paper presents studies on polycationic selenides (PCS) synthesized by hydrothermal methods for photocatalytic degradation of dyes. The synthesized PCS were confirmed by various characterization...
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Ionic liquids-based microextraction techniques
PublikacjaIn recent years, the development of highly efficient analytical techniques is of great importance, however, the direct analysis of complex sample matrix is still impossible in many cases. Therefore, the step of sample preparation is commonly involved in an analytical procedure. Over the years, it has been realized that the major source of inaccuracy and imprecision on general analysis results from the operations associated to sample...
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A multi-analytical approach to the characterization of natural organic dyestuffs and inorganic substrates present in the 19th-century artistic oil paints manufactured by a French art materials supplier Richard Aines
PublikacjaThis paper presents a comprehensive analysis of artistic paints produced in the 19th century by a French art materials supplier Richard Ain`es. Improved mild extraction with hydrofluoric acid enabled the observation of intact organic dyes. Reversed-phase liquid chromatography with diode-array and mass spectrometry detection was utilised for the identification of 35 dyes present in yellow and red paint samples, and in selected plant...
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Zastosowanie nanocząstek materiałów wykazujących właściwości magnetyczne
PublikacjaKonieczność uzyskiwania miarodajnych wyników, które będą stanowiły podstawę do określenia zawartości już śladowych ilości analitów, stała się bez wątpienia siłą napędową rozwoju współcześnie stosowanych technik analitycznych, takich jak ekstrakcja do fazy stałej (SPE). W ostatnich latach ogromne zainteresowanie wzbudziło wykorzystanie w technice SPE nanocząstek materiałów o właściwościach magnetycznych (magnetic nanoparticles –...
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Effect of kenaf fibre modification on morphology and mechanical properties of thermoplastic polyurethane materials
PublikacjaThe presented study examined the morphology and mechanical properties of biocomposites obtained from kenaf natural fibre and thermoplastic polyurethane. Kenaf was modified using various methods, namely: acetylation, blocked isocyanate, maleic anhydride and permanganate treatment. Those methods and ways of carrying out of surface modifications were not studied before on kenaf/thermoplastic polyurethane composites. Different fibre...
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Fabrication of the cross-linked PVA/TiO2/C nanocomposite membrane for alkaline direct methanol fuel cells
PublikacjaA crosslinked Poly(vinyl alcohol) based composite membrane was developed through a phase inversion process for use in alkaline direct methanol fuel cells (ADMFCs). The titanium dioxide (TiO2) and carbon nanoparticles (NPs) have been incorporated into the PVA polymer matrix to improve the mechanical and thermal properties. The membrane samples were further modified with maleic acid, a carboxylic acid acting as the cross-linker,...
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Multi-Technique Investigation of Grave Robes from 17th and 18th Century Crypts Using Combined Spectroscopic, Spectrometric Techniques, and New-Generation Sequencing
PublikacjaThe textile fragments of the funeral clothes found in the 17th and 18th century crypts were subjected to spectroscopic, spectrometric, and microbial investigation. The next-generation sequencing enabled DNA identification of microorganisms at the genus and in five cases to the species level. The soft hydrofluoric acid extraction method was optimized to isolate different classes of dyes from samples that had direct contact with...
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A facile approach to fabricate load-bearing porous polymer scaffolds for bone tissue engineering
PublikacjaBiodegradable porous scaffolds with oriented interconnected pores and high mechanical are load-bearing biomaterials for bone tissue engineering. Herein, we report a simple, non-toxic, and cost-effective method to fabricate high-strength porous biodegradable scaffolds, composed of a polymer matrix of polycaprolactone (PCL) and water-soluble poly (ethylene oxide) (PEO) as a sacrificial material by integrating annealing treatment,...
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GTR/Thermoplastics Blends: How Do Interfacial Interactions Govern Processing and Physico-Mechanical Properties?
PublikacjaIn this work, GTR/thermoplastics blends (in ratio 50/50 and 75/25 wt.%) were prepared by melt-compounding in an internal mixer. During research, trans-polyoctenamer rubber (TOR), ethylene-vinyl acetate copolymer (EVA), ethylene-octene copolymer (EOC), and linear low-density polyethylene (LLDPE), were used in their thermoplastic phase. Microstructure and processing-performance property interrelationships of the studied materials...
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Wytwarzanie i modyfikacja powierzchni porowatych struktur tytanowych przeznaczonych na implanty
PublikacjaCelem pracy było wytworzenie stopu Ti-13Nb-13Zr z wykorzystaniem technologii selektywnego topienia laserowego (SLM) oraz jego biofunkcjonalizacja za pomocą utleniania mikrołukowego (MAO), a następnie określenie wpływu parametrów procesowych na właściwości otrzymanych materiałów pod kątem ich zastosowania na implanty. Oceniono wpływ napięcia, natężenia i czasu procesu MAO przeprowadzanego w elektrolicie zawierającym wapń i fosfor...
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Temperature and potential-dependent structural changes in Pt cathode electrocatalyst viewed by in situ XAFS
PublikacjaW pracy przedstawiono wyniki badań widm absorpcji promieniowania rentgenowskiego nano-platyny używanej jako katalizator w katodach polimerowych ogniw paliwowych (PEM FC). Badania XAFS realizowane były w warunkach pracy ogniwa paliwowego. Wysokiej jakości widma, uzyskane za pomocą specjalnie przygotowanej do pomiarów XAFS in situ komórki FC, umożliwiły przeprowadzenie zaawansowanej analizy obrazującej zmiany w lokalnej strukturze...
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Impedance Studies of Phosphate-iron Glasses Containing Niobium and Titanium
PublikacjaThe ac and dc conductivity in phosphate-iron-niobate glasses with addition of titanium oxide was investigated as a function of temperature and frequency with the use of impedance spectroscopy. The topography and microstructure of glasses were investigated by the means of X-ray diffraction (XRD), scanning electron microscopy (SEM), and confocal microscopy methods. The obtained results show that all samples are amorphous but they...
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Phase Separation and Electrical Properties of Manganese Borosilicate Glasses
PublikacjaThe structure and electrical properties of manganese borosilicate glasses of a composition of xMnO-(0.8-x)SiO2-(0.2)B2O3 (x=0.4, 0.5 and 0.6 in mol) were investigated by impedance spectroscopy, SEM, XRD and confocal microscopy methods. The influence of composition on the glass structure and electrical properties was discussed. A separation of two amorphous phases was observed and it was concluded that one phase is SiO2-rich and...